Ocean Optics XE-1 User Manual

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XE-1 Xenon
Calibration Light Source
Installation and Operation Instructions
Description
The XE-1 Xenon Calibration Source is a wavelength calibration source for UV-VIS-Shortwave NIR spectrophotometric systems. The XE-1 produces Xenon lines from 916-1984 nm, and is an ideal lamp to use when performing fast, accurate spectrometer wavelength calibrations.
The XE-1 features an SMA 905 Connector for interfacing with our optical fibers. It operates with a 12 VDC power supply (included with the unit) or 9V battery (not included).
The following sections detail the features of the XE-1 Xenon Calibration Light Sources.
XE-1 Xenon Calibration Light Source
Note
The XE-1 is NOT designed to operate as an excitation source in your experiments. Spectral lines above 922 nm are not easily detectable by Ocean Optics spectrometers.
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XE-1-CAL Installation and Operation Instructions
Parts Included
The XE-1 package includes the following items:
XE-1 Xenon Calibration Light Source
12 VDC power supply
WARNING
The beam emerging from the light source contains UV radiation that can cause serious eye injury upon direct contact with the eye. Never look directly into the light source.
The SMA 905 Connector may get extremely hot during operation. After lamp use, allow sufficient time to cool before handling.
Dangerous voltages are present, and there are no user-serviceable parts inside. Never open the XE-1.
Additional Accessories
The following are additional accessories available from Ocean Optics that you may need, depending on your system set-up:
Spectrometer
SMA-terminated optical fiber
Ocean Optics software
Connecting the XE-1
Follow the steps below to set up your XE-1 for use.
Procedure
1. Plug the 12 VDC power supply into a power outlet, then connect the barrel connector of the power supply to the power input on the rear of the XE-1.
or
Alternately, you can use a 9-volt battery (not included) to power the XE-1. Open the battery hatch of the XE-1 and install the 9-volt battery, and then proceed to Step 2.
2. Connect a fiber to the SMA 905 Connector on the XE-1. If your spectrometer does not have an entrance slit, use a 50 reduced optical resolution.
m diameter (or smaller) fiber. Larger fibers and slits result in
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XE-1-CAL Installation and Operation Instructions
Note
If the spectrometer does not have a slit and your experiment requires you to use fibers of varying diameters, you will need to perform a wavelength calibration after changing fibers. You should perform a wavelength calibration each time you unscrew the fiber from the spectrometer and change fiber size.
3. Move the On/Off switch on the XE-1 (next to the SMA 905 Connector) to the On position. The red LED will illuminate to indicate that the XE-1 is powered on.
You have now configured the XE-1 for use.
Calibrating With the Light Source
The information in this section explains how to calibrate your spectrometer’s wavelength using the XE-1 light source.
About the Wavelength Calibration
You are going to be solving the following equation, which shows that the relationship between pixel number and wavelength is a third-order polynomial.
= I + C1 p + C2 p2+ C3p
p
Where = the wavelength of pixel p,
I = the wavelength of pixel 0, C1= the first coefficient (nm/pixel), C2= the second coefficient (nm/pixel2) C3 = the third coefficient (nm/pixel3)
You will be calculating the value for I and the three Cs.
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Calibration Requirements for Ocean Optics Spectrometers
To re-calibrate the wavelength of your Ocean Optics spectrometer using the XE-1, you will need the following items:
XE-1 Xenon Calibration Light Source
Ocean Optics spectrometer and its manual
An optical fiber (for spectrometers without a built-in slit, a 50-m fiber works best)
A spreadsheet program (Excel or Quattro Pro, for example) or a calculator that performs third-
order linear regressions
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XE-1-CAL Installation and Operation Instructions
Note
If you are using Microsoft Excel, choose Tools | Add-Ins and check AnalysisToolPak and AnalysisTookPak-VBA.
Calibration Procedure
Please see the appropriate manual for your model Ocean Optics spectrometer for instructions on how to calibrate it. Ocean Optics manuals are located at
http://www.oceanoptics.com/technical/operatinginstructions.asp.
XE-1 Specifications
The following sections detail the specifications of the XE-1.
Spectral Output
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XE-1-CAL Installation and Operation Instructions
Strong XE Emission Lines by Wavelength (nm)
There are more emission lines shown below than printed on the label on the XE-1 housing. The label is intended as a quick, convenient reference and does not list every XE emission line that exists.
Below is a list of wavelengths for Xenon (as well as Krypton and Neon). Wavelengths listed in blue are the ones listed on the calibration lamp’s label.
Wavelength Lamp Wavelength Lamp Wavelength Lamp Wavelength Lamp
341.790 Ne 503.135 Ne 733.930 Xe 904.545 Xe
342.391 Ne 503.775 Ne 738.600 Xe
344.770 Ne 508.038 Ne 739.379 Xe
345.076 Ne 511.367 Ne 740.040 Xe
345.419 Ne 511.650 Ne
346.052 Ne
346.658 Ne
347.257 Ne
349.806 Ne
350.121 Ne
351.519 Ne
352.047 Ne
359.353 Ne
360.017 Ne
363.366 Ne
368.573 Ne
370.122 Ne
431.958
436.264
437.612
439.997
445.392
446.369
450.235
452.186 Xe
462.420 Xe
466.849 Xe
469.097 Xe
469.804 Xe
473.415 Xe
479.262 Xe
480.702 Xe
482.971 Xe
484.329 Xe
491.651 Xe
492.315 Xe
Kr Kr Kr Kr Kr Kr Kr
540.056
556.222
557.029
576.441
582.015
585.249
587.096
588.189
594.483
597.553
602.000
607.433
609.616
612.884
614.306
616.359
621.728
626.649
630.479
633.442
638.299
640.225
650.653
653.288
659.895
667.828
671.704
692.947
703.241
717.394
724.512
Ne
Kr
Kr Ne Ne 755.979 Xe 1317.741 Kr Ne 758.468 Xe 1363.422 Kr
Kr Ne Ne 764.391 Xe 1442.679 Kr Ne Ne Ne 780.265 Xe 1537.204 Kr Ne Ne 788.132 Xe Ne Ne 796.734 Xe 1689.676 Kr Ne 805.726 Xe 1800.223 Kr Ne Ne 806.134 Xe 2190.851 Kr Ne Ne Ne 823.163 Xe 1620.872* Kr Ne Ne 826.652 Xe Ne Ne 837.761 Ne Ne 849.536 Ne 1785.738* Kr Ne Ne 878.375 Ne Ne 881.941 Xe Ne
743.890
747.244
748.887
753.577
754.404
758.741
760.155
768.525
769.454
785.482
791.343
805.950
810.436
819.006
826.324
829.811
877.675
892.869
Ne Ne 1117.752 Ne Ne 1152.275 Ne Ne 1181.938 Kr Ne 1220.353 Kr
Kr Kr
Kr Kr 1473.444 Kr
Kr
Kr
Kr 1816.733 Kr
Kr Kr 1520.310* Kr
Kr
Kr 1755.350* Kr
Kr
Kr
916.265
979.970
992.319
1083.837
1365.706
1414.244
1473.281
1541.839
1605.328
1672.815
1262.339*
1647.29*
1656.023*
1763.882*
1790.45*
1809.09*
1832.53*
1959.94*
1984.638*
Xe Xe Xe Xe
Xe Xe
Xe
Xe Xe Xe
Xe
Xe Xe
Xe
Xe Xe Xe Xe Xe
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XE-1-CAL Installation and Operation Instructions
Specifications Table
Output Low-pressure gas discharge lines of Xenon
Dimensions (in mm): 125.7 x 70 x 25.8
Power consumption: 250 mA at 12 VDC
Power requirements: 12 VDC wall transformer (included) or 9 VDC battery (optional)
Bulb life: Approx. 3500 hours (at 20 mA)
Internal voltage: 600 volts at 30 kHz
Aperture: 3 mm
Amplitude stabilization: ~ 1 minute
Connector: SMA 905
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