IKA RV 10 basic, RV 10 digital Operating Instructions Manual

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Page 1

36 785 00

IKA®RV 10 basic

IKA®RV 10 digital

042009

Reg.-No. 4343-01

Betriebsanleitung DE 5 Operating instructions EN 17 Mode d’emploi FR 29 Instrucciones de manejo ES 41

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Contents

Page

CE-Declaration of conformity 3 Safety instructions 17 Correct use 18 Unpacking 18 Useful information 18 Setting up 19

Drive RV 10 basic/ digital Heating bath Glassware Hose system

Safety instructions

For your protection

• Read the operating instructions in full before starting up and

follow the safety instructions.

• Keep the operating instructions in a place where they can be accessed by everyone.

• Ensure that only trained staff work with the appliance.

• Follow the safety instructions, guidelines, occupational health and safety and accident prevention regulations. When working

under a vacuum in particular!

•

Wear your personal protective equipment in accordance with the hazard category of the medium to be processed. Otherwise there is a risk of:

- splashing liquids,

- body parts, hair, clothing and jewellery getting caught,

- injury as a result of glass breakage.

• CAUTION! Inhalation of or contact with media such as poisonous liquids, gases, spray mist, vapours, dusts or biological and microbiological materials can be hazardous to user.

• Set up the device in a spacious area on an even, stable, clean, non-slip, dry and fireproof surface.

• Ensure that there is sufficient space above the device as the glass assembly may exceed the height of the device.

• Prior to each use, always check the device, accessories and especially the glass parts for damage. Do not use damaged components.

• Ensure that the glass assembly is tension-free! Danger of cracking as a result of:

- stress due to incorrect assembly,

- external mechanical hazards,

- local temperature peaks. Ensure that the stand

• spectively unbelance.

• Beware of hazards due to:

- flammable materials,

- combustible media with a low boiling temperature,

- glass breakage.

• CAUTION! Only process and heat up media that has a flash point higher than the adjusted safe temperature limit of the heating bath that has been set. The safe temperature limit of the heating bath must always be set to at least 25 °C lower than the fire point of the media used.

•Do not operate the appliance in explosive atmospheres, with ha- zardous substances or under water.

• Only process media that will not react dangerously to the extra energy produced through processing. This also applies to any extra energy produced in other ways, e.g. through light irradiation. Tasks with the device must only be performed when operation

• is monitored.

•

Operation with excess pressure is not permitted (for cooling water pressure see "Technical Data").

• Do not cover the ventilation slots of the device in order to ensure adequate cooling of the drive.

• There may be electrostatic discharges between the medium and the drive which could pose a direct danger.

• The appliance is not suitable for manual operation.

•

Safe operation is only guaranteed with the accessories described in the ”Accessories” chapter.

•

Refer to the operating instructions for the HB 10 basic/ digital heating bath.

•

Refer to the operating instructions for the accessories, e.g. vacuum pump.

•

Position the positive pressure outlet of the vacuum pump under a fume hood.

042009

does not start to move due to vibrations re-

Interfaces and outputs 22 Commissioning 23 Maintenance and cleaning 24 Accessories 25 Error codes 27 Technical data 27 Solvent table (excerpt) 28 Warranty 28

•

Use the HB 10.2 cover or the HB 10.1 spray guard.

• Only use

•

• ATTENTION! Avoid delayed boiling! Never heat the evaporating

•

the device under an all side-closed exhaust, or a compa rable protective device. Adapt the quantity and the type of distilland to the size of the distillation equipment. The cooler must work properly. Monitor the coolant flow rate at the cooler outlet. The glass equipment must always be ventilated when working under normal pressure (e.g. open outlet at cooler) in order to prevent a pressure build-up. Please note that dangerous concentrations of gases, vapours or particulate matter can escape through the outlet at the cooler. Take appropriate action to avoid this risk, for example, downstream cold traps, gas wash bottles or an effective extraction system. Evacuated glass vessels must not be heated on one side; the evaporating flask must rotate during the heating phase. The glassware is designed for operation under a vacuum of up to 10 mbar. (see chapter ”Commissioning”). The equipment must only be aired again after cooling. When carrying out vacuum distillation, uncondensed vapours must be condensed out or safely dissipated. If there is a risk that the distillation residue could disintegrate in the presence of oxygen, only inert gas must be admitted for stress relief. CAUTION! Avoid peroxide formation. Organic peroxides can accumulate in distillation and exhaust residues and explode while decomposing! Keep liquids that tend to form organic peroxides away from light, in particular from UV rays and check them prior to distillation and exhaust for the presence of peroxides. Any existing peroxides must be eliminated. Many organic compounds are prone to the formation of peroxides e.g. dekalin, diethyl ether, dioxane, tetrahydrofuran, as well as unsaturated hydrocarbons, such as tetralin, diene, cumene and aldehydes, ketones and solutions of these substances. DANGER OF BURNING! The heating bath, tempering medium, evaporator piston and glass assembly can become hot during operation and remain so for a long time afterwards! Let the components cool off before continuing work with the device.

flask in the heating bath without switching on the rotary drive!Sudden foaming or exhaust gases indicate that flask content is beginning to decompose. Switch off heating immediately. Use the lifting mechanism to lift the evaporator piston out of the heating bath. Evacuate the danger zone and warn those in the surrounding area! When the device is switched off or the power supply disconnected, the internal safety lift removes the evaporator piston from the heating bath. The maximum load (evaporator piston and contents) is 1.5 kg for a permissible safety lift with no power. CAUTION! Never operate the device when the evaporator piston is rotating and the lift is raised. Always lower the evaporator piston into the heating bath first before starting the rotation drive. Otherwise hot tempering medium may be sprayed out! Set the speed of the drive so no tempering medium is sprayed out as a result of the evaporator piston rotating in the heating bath. If necessary reduce the speed. Do not touch rotating parts during operation. Imbalance may result in uncontrolled resonance behaviour of the device or assembly. Glass apparatus may be damaged or destroyed. In the event of unbalance or unusual noises, switch off the appliance immediately or reduce the speed. The appliance does not start up again automatically following a cut in the power supply.

The

equipment must be evacuated prior to heating

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•

The device is only disconnected from the power supply network if the device power switch is off or the plug is pulled out.

• The socket for the mains cord must be easily accessible.

Correct use

For protection of the equipment

•

The voltage stated on the type plate must correspond to the mains voltage.

•

Socket must be earthed (protective ground contact).

•

Removable parts must be refitted to the appliance to prevent the infiltration of foreign objects, liquids etc.

• Protect the appliance and accessories from bumps and impacts.

• The appliance may only be opened by experts.

• Use



Together with the accessories recommended by IKA, the device is suitable for:

- quick and gentle distillation of liquids

- evaporation of solutions and suspensions

- crystallisation, synthesis or cleaning of fine chemicals

- drying of powder and granulate material

- recycling of solvents

Mode of operation: Tabletop device

• Range of use

- Laboratories - Schools

- Pharmacies - Universities

Unpacking

• Unpacking

- Please unpack the device carefully

- In the case of any damage a fact report must be set immediately (post, rail or forwarder)

• Delivery scope

see table

The safety of the user cannot be guaranteed if the appliance is operated with accessories that are not supplied or recommended by the manufacturer or if the appliance is operated improperly contrary to the manufacturer’s specifications.

Drive RV 10 basic

Drive RV 10 digital

Heating bath HB 10 basic

Heating bath HB 10 digital

Vertical glassware RV 10.1

Vertical glassware RV 10.10,

coated

Diagonal Glassware RV 10.2

Diagonal Glassware RV 10.20,

coated

Woulff bottle

Bracket

Cooler locking device, compl.

RV 10 basic V x x x x x x x RV 10 basic VC x x x x x x x RV 10 basic D x x x x x x x RV 10 basic DC x x x x x x x RV 10 digital V x x x x x x x RV 10 digital VC x x x x x x x RV 10 digital D x x x x x x x RV 10 digital DC x x x x x x x

Operating instructions

Useful information

Distillation is a thermal separating process for liquid compounds based on substance-specific, pressure-dependent boiling points through evaporation and subsequent condensation. The boiling point temperature decreases with decreasing external pressure which means that work is usually done under reduced pressure. In this way the heating bath can be maintained at a constant temperature (e.g. 60 °C). Using the vacuum, the boiling point is set with a steam temperature of approx. 40 °C. The cooling water for the condensation cooler should not be warmer than 20 °C (6040-20 rule).

A chemical resistant membrane pump with a vacuum controller should be used to create the vacuum. The pump is protected from solvent residue by the addition of a Woulff bottle and/or a vacuum separator. Working with a jet pump to create a vacuum can only be recommended to a limited extent as the solvents may contaminate the environment when using these systems

Speed, temperature, piston size and system pressure all affect the evaporator air capacity. The optimum capacity of the flow-through condenser is approx. 60%.

This corresponds to condensation on approx. 2/3 of the cooling coil. With larger capacities there is the risk that the uncondensed solvent vapour will be extracted.

The device is equipped with a piston-operated safety mechanism. The glass apparatus may contain a vacuum following interruption to the power supply; vent the system before switching back on. If the power cuts out, the evaporator piston is automatically lifted out of the heating bath by an integrated gas spring.

CAUTION! The maximum load (evaporator piston and contents) is

1.5 kg for a permissible safety lift with no power for glass apparatus with diagonal or vertical condenser. When using other types of condensers such as dry ice or intensive condensers as well as when using return distillation distributors with slip-on condensers, it may be necessary to reduce the mass of the media to compensate for the mass of this additional glassware. Thus, prior to distillation, check whether the lift goes up without power when laden with the glass and distillation material.

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Setting up

Drive RV 10 basic/digital

☞ Remove the clamping device for the angle setting of the rotation

CAUTION! Loosen transportation lock (fig. 4a)!

☞ Set the drive at an angle of approx. 30° (fig. 7).

Fig. 4a

☞ Hold the lift with your hand on the height position and remove the

thumb screw on the back of the appliance (A).

☞ Once the transportation lock has been removed, the lift moves

slowly to its upper end position. The distance is approx. 140 mm.

☞ Connect the device to the power supply (B) using the supplied

power cord (B).

Adjustable base (Fig. 4b)

☞ Then secure the rotation drive from being accidentally turned by

Heating bath HB 10 basic/digital CAUTION! Refer to the chapter entitled "Commissioning" in the hea-

ting bath instruction manual! ☞ Place the heating bath on the stand of the rotation drive and push

drive on the right side of the lift by rotating the knurled screw counter clockwise (by lightly pressing and turning at the same time, the knurled screw comes out farther).

Fig. 7

tightening the knurled screw in a clockwise direction.

it into the left position (fig. 8).

Fig. 4b

☞ Attach the bracket for the Woulff bottle to the left side of the lift

(fig. 5).

Note: Data is exchanged between the drive unit and the heating bath by means of an infrared link. Please note that reliable communication is only guaranteed when the infrared beam has clear

Fig. 5

☞ Insert the bottle and attach the supplied hose connectors to the

bottle (fig. 6).

line-of-sight to the detector.

Glassware

☞ Open the locking device on the drive head by turning it 60° coun-

Fig. 6

Fig. 8

ter clockwise (D), (fig. 9).

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Fig. 9

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☞ Feed the steam pipe in until it stops. ☞ Then lock the locking device by turning it clockwise by 60°

(fig. 10).

Prior to commissioning - Mounting the seal RV 06.15

☞

Fig. 10

Insert vapour tube (1). Insert seal RV 06.15 (2). Mount the cooler (3a). Tighten the cap nut hand-screwed. Start the device at 120 rpm for 20 minutes. Then tighten the cap nut firmly (3b)

☞ Check the axial locking device on the steam pipe.

Push-off mechanism

The plastic screw nut (E) helps loosen tight-fitting piston ground-in

connections (Fig. 10).

☞ The plastic screw nut (E) helps loosen tight-fitting piston ground-

in connections (Fig. 10).

☞ To do so, hold the tight-fitting evaporator piston and turn the pla-

stic screw nut (E) until the evaporator piston neck.

Note: Prior to commissioning, hand-tighten the plastic screw nut

Assembling the vertical glassware cooler locking device

☞ Assemble the condenser locking device according to the diagram

☞ Mount the plate (A) using the thumb screw (B). ☞ Put the support rod (C) on the plate (B) and attach it with the

☞ Attach the rubber protector (E). ☞ Fasten the Velcro band (F) to the support rod (C). ☞ Secure the vertical glassware with the Velcro band (F).

(E) left-aligned. This will hold the steam pipe locking device (D) firmly in place.

Place the RV 06.15 or RV 06.13 condenser seal in the condenser

☞

receptacle and fit the glassware to the device according to the assembly instructions (Fig. 11 a,b and c).

(fig. 12).

screw nut (D).

Fig. 11c

Fig. 11a

Fig. 12

Fig. 11b

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Removing the condenser

☞ Use the ring spanner provided to loosen union nuts that are tightly

fitted.

☞ Loosen the union nut by turning anticlockwise.

Hose system

☞ Connect the water hoses to the condenser according to the coun-

ter-flow principle (fig. 14).

☞ Install the vacuum connections to the condenser, Woulff bottle,

vacuum controller with valve and vacuum pump.

☞ Always connect the vacuum hose to the condenser at the high-

test point to minimise solvent losses during suctioning.

☞ Use typical laboratory vacuum hoses with an inside diameter of

8 mm and a wall thickness of 5 mm (see accessories).

Fig.13

Description of special condensers

•

RV10.3 Vertical-intensive condenser with manifold

This vertical-intensive condenser features a double jacket design for particularly efficient condensation. Also available with coating (RV10.30)

•

RV10.4 Dry ice condenser

Dry ice condenser for distilling low-boiling solvents. Cooling by dry ice, no cooling water required. Maximum condensation thanks to low temperatures. Also available with coating (RV10.40) Not suitable for use with the RV10 control in automatic mode.

•

RV10.5 Vertical-condenser with manifold and cut-off valve for

reflux distillation

Also available with coating (RV10.50)

•

RV10.6 Vertical-intensive condenser with manifold and cutoff valve for reflux distillation

This vertical-intensive action condenser features a double jacket design for particularly efficient reflux distillation. Also available with coating (RV10.60)

Fig.14

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Interfaces and outputs

Data transfer

HB 10 digital

The heating bath transfers data via IR interfaces. These are located

on the left display side of the heating bath or on the right side of the drive unit. Do not place any objects between the two operating units as otherwise the data transfer may be interrupted (fig. 15)!

RV10 digital

The RS 232 interface at the back of the device is fitted with a 9-pole

SUB-D jack and can be connected to a PC. The pins have serial signals. Using the laboratory device software “labworldsoft”, the device can be operated in “Remote” mode.

Note: Please note the system requirements as well as the operating

instructions and help section included with the software.

Serial interface RS 232 (V24)

Configuration

- The functions of the interface lines between the device and the automation system are a selection from the signals specified in the EIA standard RS232 C, as per DIN 66 020 Part 1.

- For the electrical characteristics of the interface and the allocation of signal status, standard RS 232 C applies in accordance with DIN 66 259 part 1.

- Transmission procedure: asynchronous character transmission in start-stop mode.

- Type of transmission: full duplex.

- Character format: character representation in accordance with data format in DIN 66 022 for start-stop mode. 1 start bit; 7 character bits; 1 parity bit (even); 1 stop bit.

- Transmission speed: 9600 bit/s.

- Data flow control: none

- Access procedure: data transfer from the device to the computer takes place only at the computer’s request.

Command syntax and format The following applies to the command set:

- Commands are generally sent from the computer (Master) to the device (Slave).

- The stirrer machine sends only at the computer’s request. Even fault indications cannot be sent spontaneously from the stirrer machine to the computer (automation system).

- Commands are transmitted in capital letters.

- Commands and parameters including successive parameters are separated by at least one space (Code: hex 0x20).

Fig.15

- Each individual command (incl. parameters and data) and each re-

- The decimal separator in a number is a dot (Code: hex 0x2E).

The above details correspond as far as possible to the recommendations of the NAMUR working party (NAMUR recommendations for the design of electrical plug connections for analogue and digital signal transmission on individual items of laboratory control equipment, rev. 1.1.

The NAMUR commands and the additional specific mands serve only as low level commands for communication between the rotary evaporator and the PC. With a suitable terminal or communications programme these commands can be transmitted directly to the rotary evaporator. The package, labworld rotary evaporator and collecting data under MS Windows, and includes graphical entry features, for motor speed ramps for example.

The following table summarises the (NAMUR) commands understood by the

Abbreviations used X,y = Numbering parameter (integer) m = Variable value, integer n = Variable value, floating-point number X = 4 Speed X = 60 Interval time (1-99 seconds, 1 <= m >=99) X = 61 Timer (1-199 minutes, 1 <= m >=199) X = 62 Direction of lift (m=2-> lift up , m=1-> lift down)

sponse are terminated with Blank CR Blank LF (Code: hex 0x20 hex 0x0d hex 0x20 hex 0x0A) and have a maximum length of 80 characters.

IKA

co m-

IKA

soft

, provides a convenient tool for controlling

IKA

control equipment.

NAMUR Function Commands

IN_NAME Request designation IN_PV_X Read actual value X = 4 IN_SOFTWARE Request software Id-number,

IN_SP_X Read target value input X = 4 OUT_SP_X m Set target value to m X = 1,60,61,62 RESET Switch to normal operation START_X Switch on appliance (remote) function X = 4,60,61,62 STATUS Status output

STOP_X Switch off appliance function. The variable X = 1,60, 61, 62 set with OUT_SP_X remains.

date and version

0:Manual operation without interruption 1:automatic operation Start

(without interruption)

ERROR z (z error number see table)

software

PC 1.1 Cable (Fig. 16)

This cable is required to connect the 9-pin connector to a PC.

Fig. 16

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Commissioning

The unit is ready for service when the mains plug has been plugged in.

On/Off switch

☞ Switch on the device on the right side of the device. ☞ Device functions activated.

Function keys

•

“Power” key (1)

☞ Press the "Power" key once ☞ “Stand-by” mode ☞ Press the "Power" key again ☞ Device functions reactivated

“Software version” display changes to "Parameter” display.

Note: The device must first be switched on at the on/off switch on the right side of the device.

Note: The device is not dead or deenergised until the on/off switch has been switched to off (right side of device)!

•

Lift position key “L“ (2)

☞

When you press the When you release the

☞

that position.

•

Lift position key “M“ (3)

☞

When you press the When you release the

☞

that position.

•

Rotating knob (4)

Setting the speed

☞ Turn the rotating knob ☞ Speed setting accuracy: +

Speed range 20-270 rpm Note: When you select the speed > 100 rpm, smooth start is automatically activated.

Start / Stop Rotation drive

☞ Press the rotating knob ☞ Rotation drive starts ☞ Press the rotating knob again ☞ Rotation drive stops

•

Timer key (5)

☞ Press the “Timer” key. ☞ The timer block appears on the display, the “TIMER” indicator

flashes.

☞ Set the target value “Timer” on the knob by turning (1 to 199 mi-

nutes).

☞ Save the “Timer” target value by pressing the "Timer" key again. ☞ Starting the “Timer” function:

- Automatic when rotation drive is running,

- Start the rotation drive.

Note: Once the timer has run out, there is a beep, the rotation finishes and the lift goes up.

☞ The previously saved value appears on the display. ☞ Deactivate the timer by setting the target value to “0”.

(Fig. 17)

(see page 4)

Fig.17

“L”key, the lift goes up.

“L” key, the lift stops and remains in

“M“key, the lift goes down.

“M“ key, the lift stops and remains in

5 rpm,

☞ Set the target value “Int” on the knob by turning (1 to 60 minu-

☞ Starting the “Int” function

Note: In interval mode the maximum speed is limited to 200 rpm.

☞ Save the “Int” target value by pressing the "Int" key again. ☞ Deactivate the interval by setting the target value to “0”.

Display

• (only for RV 10 digital) Remote control via PC in connection with software “labworldsoft” is active.

• Current target and actual speed indicator in revolutions per minute [rpm]. When the device is switched on the most recently selected target value "speed" appears.

• Rotation drive active.

• Time lapse control active. Indication of remaining distillation time in minutes [min].

Note: With the software "labworldsoft", RV 10 digital can also switch off the heating bath once the timer has run out.

• Interval mode activated.

•

--- not pictured --Error codes, see chapter entitled "Error Codes”.

Setting the lower end stop CAUTION! Depending on the size of the piston, the setting angle of

the rotation drive and the position of the heating bath and lift, the evaporator piston can be in contact with the bottom of the heating bath. CAUTION - glass may break! Limit the lower lift position with the variable end stop.

☞ Press the “M” key until the lift reaches the desired position.

Note: The evaporator piston should be 2/3 immersed in the heating bath.

☞ To adjust the stop element, press the centre button on the front

☞ Move the stop to the desired position (fig. 19). ☞ Press the “L” key until the lift has reached the upper end stop.

Note: The path is limited from 0 – 6 cm.

tes).

- Automatic when rotation drive is running

- Start the rotation drive

(see page 4)

Display “REMOTE” (10)

Display “888 rpm” (20)

Display (30)

Display “TIMER” (40)

Display “INT” (50)

Display “E01” (20)

of the lift (fig. 18).

Fig.18

•

Int key (6)

Interval cycle for right-left running (change of direction) of the evaporator piston in seconds.

☞ Press the “Int” key. ☞ The interval block appears on the display, the “INT” indicator flashes.

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Page 9

Setting up the heating bath Refer also to the operating instructions for the HB 10 basic /di-

gital heating bath!

☞ Move the lift to the bottom position and check the position of the

☞ Fill the heating bath with the tempering medium until the evapo-

☞ Switch on the rotation drive and slowly increase the speed.

Note: Avoid creating waves.

☞ Switch on the heating bath using the main on/off switch.

Note: Avoid stress on the glass due to different evaporator piston

Fig.19

Check that the limit stop is functioning properly:

☞ Lower the lift by holding down the “M” key. ☞ The drive stops automatically when the preset desired lower end

position has been reached.

☞ Move the drive back to the upper position.

Filling the evaporator piston

Prior to filling the evaporator piston, a vacuum controller is used to regulate the glass apparatus to the target pressure.

☞ Now fill the evaporator piston using the backfeed line. ☞ Due to the vacuum present, the solvent is suctioned into the eva-

porator piston. This enables you to keep solvent loss due to suctioning to a minimum.

☞ You can also fill the evaporator piston manually prior to creating

the vacuum. The evaporator piston should not be filled more than half its volume.

Note: CAUTION! The maximum allowed load (evaporator piston and contents) is 3 kg.

and heating bath temperatures when lowering the evaporator piston into the heating bath!

Note: If non-original accessories are used that are not supplied by IKA, then it is possible that the 50 mm travel range provided by the heating bath will not be sufficient. This applies in particular when using 3 L evaporator flasks with foam brake.

Use the IKA RV 10.3000 mounting plate to extend the heating bath travel range by 150 mm.

heating bath in relation to the evaporator piston. When using larger evaporator pistons (2 or 3 litres) or depending on the angle of the rotation drive, you can move the heating bath 50 mm to the right.

rator piston is surrounded by tempering medium to 2/3 of its volume.

Fig. 20

Maintenance and cleaning

The device is maintenance-free. It is subject only to the natural wear and tear of components and their statistical failure rate.

The seal on the glass condenser should be checked at regular intervals and replaced if necessary.

For cleaning disconnect the main plug.

To clean the device use only water with a detergent that contains tensides, or use isopropylalcohol for stubborn soiling.

parts order

Spare When ordering spare parts, please give:

- machine type,

- manufacturing number, see type plate,

- item and designation of the spare part, see www.ika.net, spare

parts diagram and spare parts list.

Repair In case of repair the device has to be cleaned and free from any ma-

terials which may constitute a health hazard. If you require servicing, return the appliance in its original packaging.

Storage packaging is not sufficient. Please also use suitable transport packaging.

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Page 10

Accessories

RV 10.1 NS 29/32 Vertical glassware (1) RV 10.10 NS 29/32 Vertical glassware, coated (1) RV 10.2 NS 29/32 Diagonal glassware (2) RV 10.20 NS 29/32 Diagonal glassware, coated (2)

RV 10.700 NS 29/42 Vertical glassware (1) RV 10.710 NS 29/42 Vertical glassware, coated (1) RV 10.800 NS 29/42 Diagonal glassware (2) RV 10.810 NS 29/42 Diagonal glassware, coated (2)

RV 10.900 NS 24/40 Vertical glassware (1) RV 10.910 NS 24/40 Vertical glassware, coated (1)

RV 10.1000 NS 24/40 Diagonal glassware (2) RV 10.1010 NS 24/40 Diagonal glassware, coated (2)

RV 10.3 Vertical-intensive condenser with manifold RV 10.30 Vertical-intensive condenser with manifold, coated RV 10.4 Dry ice condenser RV 10.40 Dry ice condenser, coated RV 10.5 Vertical-condenser with manifold and cut-off valve

for reflux distillation

RV 10.50 Vertical-condenser with manifold and cut-off valve

for reflux distillation, coated

RV 10.6 Vertical-intensive condenser with manifold and cut-off valve

for reflux distillation

RV 10.60 Vertical-intensive condenser with manifold and cut-off valve

for reflux distillation, coated

HB 10.1 Protection shield (Heating bath HB 10) HB 10.2 Protection cover (Heating bath HB 10)

RV 10.70 NS 29/32 Steam pipe RV 10.71 NS 24/29 Steam pipe RV 10.72 NS 29/42 Steam pipe RV 10.73 NS 24/40 Steam pipe

RV 10.80 NS 29/32 Evaporator piston 50 ml RV 10.81 NS 29/32 Evaporator piston 100 ml RV 10.82 NS 29/32 Evaporator piston 250 ml RV 10.83 NS 29/32 Evaporator piston 500 ml RV 10.84 NS 29/32 Evaporator piston 1000 ml RV 10.85 NS 29/32 Evaporator piston 2000 ml RV 10.86 NS 29/32 Evaporator piston 3000 ml

RV 10.90 NS 24/32 Evaporator piston 50 ml RV 10.91 NS 24/32 Evaporator piston 100 ml RV 10.92 NS 24/32 Evaporator piston 250 ml RV 10.93 NS 24/32 Evaporator piston 500 ml RV 10.94 NS 24/32 Evaporator piston 1000 ml RV 10.95 NS 24/32 Evaporator piston 2000 ml RV 10.96 NS 24/32 Evaporator piston 3000 ml RV 10.97 NS 24/40 Evaporator piston 1000 ml

RV 10.2001 NS 29/42 Evaporator piston 50 ml RV 10.2002 NS 29/42 Evaporator piston 100 ml RV 10.2003 NS 29/42 Evaporator piston 250 ml RV 10.2004 NS 29/42 Evaporator piston 500 ml RV 10.87 NS 29/42 Evaporator piston 1000 ml RV 10.2005 NS 29/42 Evaporator piston 2000 ml RV 10.2006 NS 29/42 Evaporator piston 3000 ml

RV 10.2007 NS 24/40 Evaporator piston 50 ml RV 10.2008 NS 24/40 Evaporator piston 100 ml RV 10.2009 NS 24/40 Evaporator piston 250 ml RV 10.2010 NS 24/40 Evaporator piston 500 ml RV 10.2011 NS 24/40 Evaporator piston 1000 ml RV 10.2012 NS 24/40 Evaporator piston 2000 ml RV 10.2013 NS 24/40 Evaporator piston 3000 ml

RV 10.100 KS 35/20 Receiving flask 100 ml RV 10.101 KS 35/20 Receiving flask 250 ml RV 10.102 KS 35/20 Receiving flask 500 ml RV 10.103 KS 35/20 Receiving flask 1000 ml RV 10.104 KS 35/20 Receiving flask 2000 ml RV 10.105 KS 35/20 Receiving flask 3000 ml

042009

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RV 10.200 KS 35/20 Receiving flask, coated 100 ml RV 10.201 KS 35/20 Receiving flask, coated 250 m RV 10.202 KS 35/20 Receiving flask, coated 500 ml RV 10.203 KS 35/20 Receiving flask, coated 1000 ml RV 10.204 KS 35/20 Receiving flask, coated 2000 ml RV 10.205 KS 35/20 Receiving flask, coated 3000 ml

RV10.300 NS 29/32 Powder piston 500 ml RV10.301 NS 29/32 Powder piston 1000 ml RV10.302 NS 29/32 Powder piston 2000 ml

RV10.303 NS 24/29 Powder piston 500 ml RV10.304 NS 24/29 Powder piston 1000 ml RV10.305 NS 24/29 Powder piston 2000 ml

RV10.2014 NS 29/32 Powder piston 500 ml RV10.2015 NS 29/32 Powder piston 1000 ml RV10.2016 NS 29/32 Powder piston 2000 ml

RV10.217 NS 24/40 Powder piston 500 ml RV10.218 NS 24/40 Powder piston 1000 ml RV10.219 NS 24/40 Powder piston 2000 ml

RV10.400 NS 29/32 Evaporator cylinder 500 ml RV10.401 NS 29/32 Evaporator cylinder 1500 ml

RV10.402 NS 24/29 Evaporator cylinder 500 ml RV10.403 NS 24/29 Evaporator cylinder 1500 ml

RV10.2020 NS 29/42 Evaporator cylinder 500 ml RV10.2021 NS 29/42 Evaporator cylinder 1500 ml

RV10.2022 NS 24/40 Evaporator cylinder 500 ml RV10.2023 NS 24/40 Evaporator cylinder 1500 ml

RV10.500 NS 29/32 Foam brake RV10.501 NS 24/29 Foam brake RV10.2024 NS 29/42 Foam brake RV10.2025 NS 24/40 Foam brake

RV10.600 NS 29/32 Distillation spider with 6 sleeves RV10.601 NS 29/32 Distillation spider with 12 sleeves RV10.602 NS 29/32 Distillation spider with 20 sleeves

RV10.603 NS 24/29 Distillation spider with 6 sleeves RV10.604 NS 24/29 Distillation spider with 12 sleeves RV10.605 NS 24/29 Distillation spider with 20 sleeves

RV10.2026 NS 29/42 Distillation spider with 6 sleeves RV10.2027 NS 29/42 Distillation spider with 12 sleeves RV10.2028 NS 29/42 Distillation spider with 20 sleeves

RV10.2029 NS 24/40 Distillation spider with 6 sleeves RV10.2030 NS 24/40 Distillation spider with 12 sleeves RV10.2031 NS 24/40 Distillation spider with 20 sleeves

RV10.610 Distilling sleeve 20 ml

RV10.606 NS 29/32 Distillation spider with 5 flasks 50 ml RV10.607 NS 29/32 Distillation spider with 5 flasks 100 ml

RV10.608 NS 24/29 Distillation spider with 5 flasks 50 ml RV10.609 NS 24/29 Distillation spider with 5 flasks 100 ml

RV10.2032 NS 29/42 Distillation spider with 5 flasks 50 ml RV10.2033 NS 29/42 Distillation spider with 5 flasks 100 ml

RV10.2034 NS 24/40 Distillation spider with 5 flasks 50 ml RV10.2035 NS 24/40 Distillation spider with 5 flasks 100 ml

RV10.3000 Extension plate

RV06.13 FKM seal with PTFE-coating (1) RV06.15 PTFE seal (2)

PC 1.1 Cable

Labworldsoft

042009

Page 12

Error codes

Any malfunctions during operation will be identified by an error message on the display (only for RV 10 digital). Once a serious error message has been displayed, the lift moves to the top end position and the device can no longer be operated. The lift can be operated again.

Proceed as follows in such cases:

☞ Switch off device using the main switch (A) ☞ Carry out corrective measures ☞ Restart device

Error code Effect Cause Correction

E01 No or too little rotation - Cable break Reduce the volume in the evaporator piston

E02 No communication with the heating bath Interface hidden or dirty Check / clean the interface

If the actions described fail to resolve the fault or another error code is displayed then take one of the following steps:

- Contact the service department,

- Send the device for repair, including a short description of the fault.

- Load too large

- Motor blocked

Technical Data

Operating voltage range Vac 100 - 230 + Rated voltage Vac 100 - 230 Frequence Hz 50 / 60 Power input without heating bath Power input in operation “stand by” Speed rpm 20-270 Speed display digital Dimensions of visible display area (W x H) mm 48 x 35 Display 7 segment display Multiple languages Right and left movement/ interval operation yes Smooth start ja Lift automatic Lifting speed mm/s 50 Stroke mm 140 Setting of lower end stop 60 mm, contactless Head angle adjustable 0° - 45° Timer 1-199 Minuten Interval 1-60 sec Integrated vacuum controller Interface Ramp programming Distillation processes programmable - with accessory labworldsoft Remote control Cooling surface cm Fuse 2xT1, 6A 250V 5x20 Perm. On- time % 100 Perm. ambient temperature °C 5-40 Perm. humidity % 80 Protection acc. to DIN EN 60529 IP 20 Protection class I Overvoltage category II Contamination level 2 Weight (no glassware; no heating bath) Dimensions(W x D x H Operation at a terrestrial altitude m max. 2000 above sea level

)

W75 W 3,3

kg 16,8 17,5

mm 500 x 410 x 430

RV 10 basic RV 10 digital

10%

- RS 232

- with accessory labworldsoft

1200

Subject to technical changes!

042009

Page 13

Solvent table (excerpt)

Solvent Formula Pressure for

Acetic acid C2H4O Acetone C3H6O 556 Acetonitrile C2H3N 226 N-Amylalcohol, C5H12O11 n-Pentanol

n-Butanol C4H tert. Butanol, C4H10O 130 2-Methyl-2-Propanol

Butylacetate C6H12O Chlorobenzene C6H5CI 36 Chloroform CHCI Cyclohexane C6H Dichloromethane, CH2CI Methylenechloride

Diethylether C4H10O atm.press. 1,2,-Dichloroethylene (trans) C2H2CI Diisopropylether C6H14O 375 Dioxane C4H8O Dimethylformamide (DMF) C3H7NO 11 Ethanol C2H6O 175

boiling point 40 °C in mbar

474 235 atm.press.

751

107

Ethylacetate C4H8O Ethylmethylketone C4H8O Heptane C7H Hexane C6H Isopropylalcohol C3H8O 137 Isoamylalcohol, C5H12O14 3-Methyl-1-Butanol

Methanol CH4O 337 Pentane C5H n-Propylalcohol C3H8O67 Pentachloroethane C2HCI 1,1,2,2,-Tetrachloroethane C2H2CI 1,1,1,-Trichloroethane C2H3CI Tetrachloroethylene C2CI Tetrachloromethane CCI Tetrahydrofurane (THF) C4H8O 357 Toluene C7H Trichloroethylene C2HCI Water H2O72 Xylene C8H

Warranty

In accordance with IKA warranty conditions, the warranty period is 24 months. For claims under the warranty please contact your local dealer. You may also send the machine direct to our factory, enclosing the delivery invoice and giving reasons for the claim. You will be liable for freight costs.

The warranty does not cover worn out parts, nor does it apply to faults resulting from improper use, insufficient care or maintenance not carried out in accordance with the instructions in this operating manual.

16 14

4 3

240 243 120 335

atm.press.

13 35 300 53 271

77 183

042009