Hanna Instruments HI 8043 User Manual

Instruction Manual
HI 8043
Portable
Dissolved Oxygen Meter
DO meter
HI 8043
STB
OFF
°C
O
2
ZERO
SLOPE
rum
°C
n
s
This Instrument is in
Compliance with the CE
Directives
1
Dear Customer, Thank you for choosing a Hanna Instruments
Product. Please read this instruction manual carefully
before using the instrument. This manual will provide you with all the neces-
sary information for the correct use of the instrument, as well as a more precise idea of its versatility in a wide range of applications.
If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com.
This instrument is in compliance with the directives.
TABLE OF CONTENTS
Preliminary Examination............................. 3
General Description .................................... 3
Functional Description Probe...................... 4
Functional Description Meter...................... 5
Specifications ............................................. 6
Initial Probe Preparation ............................. 7
Dissolved Oxygen Calibration ..................... 9
Temperature Calibration ............................ 15
Taking Measurements .............................. 16
Probe & Membrane Maintenance ............. 17
Battery Replacement ................................ 19
Accessories.............................................. 20
Warranty ................................................... 21
CE Declaration of Confirmity .................... 22
2
PRELIMINARY EXAMINATION
Remove the instrument from the packing ma­terial and examine it to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer.
Each meter is supplied with:
DO Meter
DO Probe (HI 76401)
Membrane cap (2 pcs)
O-ring (2 pcs)
Protective cap
30 mL electrolyte solution (HI 7041S)
Screwdriver for calibration purposes
1 x 9V battery
Instruction manual
Note: Save all packing material until you are
sure that the instrument functions correctly. All defective items must be returned in the original packaging with the supplied accessories.
GENERAL DESCRIPTION
HI 8043 is a portable meter for Dissolved
Oxygen measurements. It is housed in a lightweight case, with an easy-to-read LCD. Dissolved oxygen and temperature measure­ments can be performed in the field (waste­water treatment, fish-farming, water analysis, etc.) as well as in the laboratory without compromising accuracy. Dissolved oxygen is indicated in mg/l (ppm) and this value is compensated for the tem­perature effect (ATC). The dissolved oxygen probe has a membrane covering the polarographic sensors and a built­in thermistor for temperature measurements and compensation. The thin permeable mem-
3
brane isolates the sensor elements from the sample tested, but allows oxygen to enter. A voltage is applied across the sensor, and the oxygen that has passed through the mem­brane reacts causing the current to flow, hence determining a reading. A convenient feature of the instrument is its standby mode which keeps the probe polarized and ready for instant measurements.
FUNCTIONAL DESCRIPTION PROBE
1. D.O. Probe
2. Protective Cap
3. Watertight Shielded Cable
4. Probe Body
5. O-Ring Seal
6. Silver Chloride Anode
7. Platinum Cathode (sensor)
8. Oxygen Permeable PTFE Membrane
9. Membrane Cap
4
FUNCTIONAL DESCRIPTION
1
3
DO meter
STB
OFF
HI 8043
°C
O
2
42 5
9
6 7
ZERO SLOPE °C
8
s
ins
rum n
1.Liquid Crystal Display
2."OFF" (to switch the meter off)
3."STB" (to switch the meter on and polarize the probe. Use this standby position with­out switching the meter off if you are going to take further measurements)
4."°C" Measurement
5."O2" Measurement
6.ZERO Calibration Trimmer
7.SLOPE Calibration Trimmer
8.°C Calibration Trimmer
9.Rotary Switch
5
SPECIFICATIONS
Range DO 0.00 to 19.99 mg/l
Resolution DO 0.01 mg/l
Accuracy DO ±1.5% of full scale
Typical EMC DO ±1.5% of full scale Deviation °C ±1°C
Calibration Manual on 2 points Temperature Automatic from 0 to 30°C
Compensation (32 to 86°F) Probe HI 76401 polarographic
Battery 9V / 100 hours of continuous use Environment 0 to 50°C (32 to 122°F); 95% RH Dimensions 180 x 83 x 40 mm (7.1 x 3.3 x 1.6") Weight 650 g (23 oz.) with probe and
°C 0.0 to 50.0°C (32 to 122 °F)
°C 0.1°C
°C ±0.5°C
with 3 m cable
soft carrying case
6
INITIAL PROBE PREPARATION
Shipping
PROBE PREPARATION
All probes shipped from Hanna Instruments are dry. To hydrate the probe and prepare it for use, connect it to the meter and proceed as follows. 1 Remove the red and black
plastic cap. This cap is for
cap
shipping purposes and can be thrown away.
2 Wet the sensor by soak-
black
ing the bottom 2½ cm (1") of the probe in electrolyte
red
(HI 7041S) for 5 minutes.
3 Rinse the supllied mem-
brane (HI 76407A) with electrolyte while shaking it gently. Refill with clean electrolyte.
4 Gently tap the sides of the
membrane with your finger tip to ensure that no air bubbles remain trapped. To avoid damaging the mem­brane, do not tap the mem­brane directly on the bot­tom.
5 Make sure that the rubber O-ring sits prop-
erly inside the membrane cap.
6 With the sensor facing down, screw the
cap clockwise. Some electrolyte will over­flow.
When not in use, place the protective cap supplied in the kit with the meter.
7
PROBE POLARIZATION
When the probe is under polarization it is continuously fed with a voltage of approxi­mately 800 mV. Probe polarization is essential for stable mea­surements to be taken with the same recur­ring degree of accuracy. In the presence of the polarized probe, oxy­gen is continually "consumed" by passing through the sensitive diaphragm and dissolv­ing in the electrolyte solution contained in the probe. If this operation is interrupted, the electrolyte solution continues to be enriched with oxy­gen until it reaches an equilibrium with the surrounding solution. Whenever measurements are taken with a non-polarized probe, the oxygen level detected by the meter is both that of the tested sample as well as the oxygen present in the electro­lyte solution itself. By leaving the instrument in
OFF
STB
°C
O
the "STB" mode, which sig­nifies keeping the probe in a continual state of polariza­tion, the oxygen which is present in the electrolyte solution is progres­sively "consumed", and the following mea­surements detect only the quantity of oxygen present in the sample to be tested. Therefore, in order to keep the probe continu­ously polarized it is necessary to switch the meter to the "STB" mode and wait for at least 30 minutes. This should be done with the probe covered with the protective cap and filled with some electrolyte solution.
STB
Polarization is not maintained when the instrument is
OFF
°C
O
switched to the "OFF" posi­tion.
2
2
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