Hamilton VisiWater DO Operating Instructions Manual

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VisiWater™ DO Sensors
Operating Instructions
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TABLE OF CONTENTS
Table of Contents
TABLE OF CONTENTS
1 General Information ................................................ 4
1.1 Intended Use ................................................................. 4
1.2 About this Operating Instruction .................................. 4
2 Liability .. ................................................................... 4
3 Safety Precautions and Hazards ........................... 5
3.1 General Precautions .................................................... 5
3.2 Operation of VisiWater DO Sensor .............................. 5
3.3 Earthing ....................................................................... 6
3.4 Electrical Safety Precautions ....................................... 8
3.5 Chemical, Radioactive or Biological
Hazard Precautions ..................................................... 9
4 Product Description ................................................ 9
4.1 General Description ..................................................... 9
4.2 Hardware Description ................................................ 10
4.3 Optical DO measurement .......................................... 11
4.4 VisiWater DO sensor with
Micro-Transmitter inside ............................................ 11
5 Installation .............................................................. 12
5.1 Unpacking ................................................................. 12
5.2 Configure the VisiWater DO sensor with
Hamilton Device Manager (HDM) .............................. 12
5.2.1 Installing the Hamilton Device Manager .......... 12
5.2.2 Installing DTMs ................................................ 13
5.2.3 Connecting a VisiWater DO
Sensor to HDM ............................................... 13
5.2.4 Setting User Level ........................................... 13
5.2.5 Configuring the VisiWater DO
Sensor Parameters .......................................... 14
5.2.6 Configuring the calibration settings ................. 15
5.2.7 Configuring the temperature settings ............ 15
5.2.8 Configuring the analog interface for
your process control system ........................... 16
5.2.9 Defining a measuring point name for
identification of the process ............................ 16
5.3 Install VisiWater DO sensor in
your Measuring Loop ................................................. 16
5.3.1 Mechanical Process Connection .................... 16
5.3.2 Cable Pin Designation ..................................... 17
5.3.3 Controlling 4–20 mA current interface
signals by pulse-width modulation .................. 17
5.3.4 Electrical Connection for Analog
4–20 mA Connection ...................................... 19
5.3.5 Electrical connection for the
digital RS485 interface .................................... 20
6 Operation .............................................................. 22
7 Maintenance ......................................................... 22
7.1 Verify Sensor Status and ODO Cap Functionality ...... 22
7.2 Replacing the ODO Cap ............................................ 23
7.3 Calibration .................................................................. 23
7.3.1 Automatic Standard Calibration with HDM ..... 24
7.3.2 Zero Point Calibration (Point Zero Oxygen) ..... 24
7.3.3 Calibration in Air (Calibration Point Air) ............ 25
7.4 Product calibration .................................................... 25
8 Troubleshooting ..................................................... 27
8.1 Sensor Self-Diagnostic .............................................. 27
8.1.1 W a r n i n gs ......................................................... 27
8.1.2 Errors .............................................................. 28
8.2 Getting Technical Support ......................................... 29
8.3 Returning VisiWater DO sensor for Repair ................. 29
9 Disposal ................................................................ 29
10 Technical Specifications ...................................... 30
11 Ordering Information ............................................. 31
11.1 VisiWater DO sensor ................................................. 31
11.2 Parts and Accessories .............................................. 31
11.3 Services .................................................................... 32
Hamilton Warranty
Please refer to the General Terms of Sales (GTS).
Important note
Copyright © 2016 Hamilton Bonaduz AG, Bonaduz Switzerland. All rights reserved. The reproduction of any part of this document in any form is forbidden without the express written agreement of Hamilton Bonaduz AG.
Contents of this manual can be modified without previous announcement. Technical modifications reserved. Greatest possible care was used on the correctness of the information in this manual. If errors should be discovered nevertheless, Hamilton Bonaduz AG is pleased to be in­formed about it. Regardless of this, Hamilton Bonaduz AG cannot assume liability for any errors in this manual or for their consequences.
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GENERAL INFORMATION • LIABILITY SAFETY PRECAUTIONS AND HAZARDS
1 General Information
1.1 Intended Use
The VisiWater DO sensors are intended for the measurement of dissolved oxygen (DO) in water application.
ATTENTION! VisiWater DO sensor is not intended
for hazardous atmospheres.
The VisiWater DO sensor has a built-in temperature sensor (NTC 22 kOhm). This temperature sensor is to be used only for monitoring the sensor conditions, not for controlling the process temperature.
1.2 About this Operating Instruction
These Operating Instructions are designed to support the inte­gration, operation and qualification of the VisiWater DO sensors.
To achieve this, it will describe the features of VisiWater DO sen­sor and its integration in Process Control Systems (PCS). Both the hardware and the communication between the VisiWater DO sensor and Process Control Systems are detailed in this manual. After reading this manual the user should be capable of installing and operating VisiWater DO sensors.
NOTE: The VisiWater DO sensor is not intended and specified as a safety device. A SIL (Safety Integrity Level) certification is not available. It is in the sole responsibility of the user to validate the VisiWater DO sensor according the safety requirements of his application.
3 Safety Precautions and Hazards
ATTENTION! Read the following safety instruc­tions carefully before installing and operating the VisiWater DO sensor.
3.1 General Precautions
For safe and correct use of VisiWater DO sensor, it is essential that both operating and service personnel follow generally ac­cepted safety procedures as well as the safety instructions given in this document, the VisiWater DO sensor operation instruction manual.
The specification given in chapter 10 as regards temperature, pressure etc. may under no circumstances be exceeded. Inap­propriate use or misuse can be dangerous.
ATTENTION! Essential information for avoiding
personal injury or damage to equipment.
NOTE: Important instructions or interesting information.
2 Liability
The liability of Hamilton Bonaduz AG is detailed in the document “General Terms and Conditions of Sale and Delivery”.
Hamilton is expressly not liable for direct or indirect losses arising from use of the sensors. It must in particular be insured in this con­junction that malfunctions can occur on account of the inherently limited useful life of sensors contingent upon their relevant applica­tions. The user is responsible for the calibration, maintenance and regular replacement of the sensors. In the case of critical sensor ap­plications, Hamilton recommends using back-up measuring points in order to avoid consequential damages. The user is responsible for taking suitable precautions in the event of a sensor failure.
Cleaning, assembly and maintenance should be performed by per­sonnel trained in such work. Before removing the sensor from the measuring setup, always make sure the no process medium can be accidentally spilled. When removing and cleaning the sensor, it is recommended to wear safety goggles and protective gloves.
The sensor can not be repaired by the operator and has to be sent back to Hamilton for inspection.
Necessary precautions should be taken when transporting the sensors. For repair or shipment the sensor should be sent back in the original reusable packaging box. Every VisiWater DO sensor sent back for repair must be decontaminated.
If the conditions described in these operating instructions manual are not adhered to or if there is any inappropriate interference with the equipment, all of our manufacturer’s warranties become obsolete.
3.2 Operation of VisiWater DO Sensor
VisiWater DO sensors must be used for their intended applications, and in optimum safety and operational conditions. The specifica­tions (such as temperature or pressure) defined in the section entitled ‘Technical Specification’ must not be exceeded under any circumstances (Chapter 10).
Make sure that the PG13,5 thread and the O-ring are not dam­aged when screwing the sensor into the process. O-rings are consumable parts which must be exchanged regularly (at least once per year). Even when all required safety measures have
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SAFETY PRECAUTIONS AND HAZARDS SAFETY PRECAUTIONS AND HAZARDS
been complied with, potential risks still exist with respect to leaks or mechanical damage to the armature. Wherever there are seals or screws, gases or liquids may leak out undetected. Always make sure that no process medium can be accidentally spilled before removing the sensor from its measurement setup. Do not put stress on the system by vibration, bending or torsion.
Before use, verify that the sensor is properly configured for your application.
ATTENTION! When unscrewing the PG13,5 thread connection never turn the sensor at the sensor head because you can loosen the ODO Cap from the sensor shaft and fluid can reach the interior of the sensor.
ATTENTION! To avoid humidity problems, make sure that the ODO Cap is always attached firmly to the sensor shaft, and that the O-ring between the shaft and cap is undamaged.
Make sure that following cross sensitivities and resistances of ODO Caps are respected.
Option 1: The Metal tank is connected to earth
The sensor shaft is connected to the metal tank over the PG13,5 thread
Green/Yellow Cable
Cross sensitivities and resistances of ODO Cap H0
Measurement not influenced by Carbon Dioxide
Wetted parts resistant to Ethanol
Wetted parts not resistant to Chlorine, Ozone and Organic Solvents such as Acetone, Tetrahydrofuran (THF*)
Cross sensitivities and resistances of ODO Cap H2
Measurement not influenced by Carbon Dioxide, lipophilic compounds
Wetted parts resistant to Organic Solvents such as Ethanol*, Acetone*, (THF*), Heptan*, Dimethylformamide*
Wetted parts not resistant to Chlorine and Ozone Gases
*Tested for 30 min at 25°C
3.3 Earthing
The sensor has to be mounted at the mounting location electro­statically conductive (< 1MOhm). It is recommended to assign the sensor shaft to earth (PE potential equalization) especially in electromagnetically noisy environments. This significantly improves noise immunity and signal quality. The PG13,5 thread is connected to the metallic housing of the VisiWater DO sensor. Two options for connecting the sensor to the process environ­ment are available.
Figure 1: Metal tank with earth connection
NOTE: If the tank is not connected to earth, Option 2
has to be applied.
Option 2: Glass or plastic tank (not connected to earth)
The glass or plastic tank has no connection to earth and therefore it is necessary to connect the sensor shaft via a screw clamp to earth.
Green/Yellow Cable
Figure 2: Glass or plastic tank without earth conne ction
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SAFETY PRECAUTIONS AND HAZARDS PRODUCT DESCRIPTION
Below several examples how to connect the shaft of the sensor directly to earth as required in Figure 2 are shown.
External earth cable
ATTENTION! Switch off the power supply and unplug the connector before dismounting the VisiWater DO sensor.
3.5 Chemical, Radioactive or Biological Hazard Precautions
Selection of the appropriate safety level and implementation of the required safety measures for working with VisiWater DO sensor is the sole responsibility of the user.
If working with hazardous liquids observe and carry out the main­tenance procedures, paying particular attention to cleaning and decontamination. If VisiWater DO sensor becomes contaminated with biohazardous, radioactive or chemical material, it should be cleaned. Failure to observe and carry out the maintenance procedures may impair the reliability and correct functioning of the measuring module.
Figure 3: Example clamps for conne cting the earth to armature and metallic housing of the tank.
3.4 Electrical Safety Precautions
Do not connect the sensor to a power source of any voltage beyond the range stated in the power rating Technical Specifi­cations (Chapter 10).
Make sure the cable is intact and properly plugged to avoid any short circuit.
Keep VisiWater DO sensor away from other equipment which emits electromagnetic radio frequency fields, and minimize static electricity in the immediate environment of the optical measuring parts. Carefully follow all the instructions in chapter 5.3 to avoid electrical damage to the sensor. The contacts must be clean and dry before sensor is connected to the cable.
4 Product Description
4.1 General Description
Hamilton’s optical sensor has been the first optical dissolved oxygen (DO) sensor for process measurement. With their micro transmitter, VisiWater DO sensors enable direct communication to the process control system via 4–20 mA standard signal or digital Modbus.
VisiWater DO sensor optical technology improves the measuring performance and simplifies maintenance. Improvements com­pared to conventional electrochemical (amperometric) sensors include flow independence, rapid start-up with no polarization time, and simplified maintenance.
With the transmitter integrated, VisiWater DO sensors provide more reliable measurements directly to your process control system. The µ-transmitter located in the sensor head stores all relevant sensor data, including calibration and diagnostic informa­tion, simplifying calibration and maintenance.
Key benefits include:
• Optical measurement
• No separate transmitter needed
• Simple maintenance with robust industrial design
• Easy to install
• Direct analog or digital Modbus communication to the process control system via 4–20 mA standard signal.
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PRODUCT DESCRIPTION PRODUCT DESCRIPTION
4.2 Hardware Description
The VisiWater DO sensor consists of a sensor head with inte­grated electronic and a sensor shaft in contact with the measured medium. The sensor shaft is terminated by the optical dissolved oxygen (ODO) cap, carrying the oxygen sensitive luminophore. During development, special attention was paid to an optimum sanitary design. All materials in contact with the solution meet the FDA requirement.
Fix cable
Sensor Head with micro transmitter
4.3 Optical DO measurement
The optical measurement principle is based on the so-called luminescence quenching. The luminescence of certain organic pigments (luminophore) is quenched in the presence of oxygen. The luminophore absorbs the excitation light and release a part of the absorbed energy by emission of fluorescence. In the pres­ence of oxygen, energy transfer takes place from the excited luminophore to oxygen. The luminophore does not emit fluore­cence and the measurable fluorescence signal decreases.
1
Fluorescence process (without oxygen)
Light (excitation)
Luminophore
Light Absorption Excited State
2
Quenching in the presence of oxygen
Fluorescence
(emission)
Process connection PG13,5 stainless steel
O-ring
Sensor shaft with stainless steel
Energy transfer
O
2
No fluorescence
Light Absorption Excited State
Figure 5: Fluorescence quenching by oxyge n
O
2
4.4 VisiWater DO sensor with Micro-Transmitter inside
With the micro-transmitter integrated, VisiWater DO sensors offer fully compensated signal directly to the process control system. Communication protocols include standard analog 4–20 mA. The micro transmitter located in the sensor head stores all relevant sensor data, including calibration and diagnostic information, simplifying calibration and maintenance.
ODO Cap with oxyge n-sensitive luminophore (sensory element), ODO Cap serial number, reference number and stainless steel heat number
Figure 4: VisiWater DO sensor hardware description.
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INSTALLATIONINSTALLATION
5 Installation
5.1 Unpacking
1) Unpack carefully the VisiWater DO sensor. Enclosed you will find the VisiWater DO sensor, the Declaration of Quality, the VisiWater DO sensor Instruction Manual, and the Stainless Steel material Certificate.
2) Inspect the sensor for shipping damages or missing parts.
5.2 Configuring the VisiWater DO sensor with Hamilton Device Manager (HDM)
Two pieces of software are required to configure and set up the VisiWater DO sensor. The Hamilton Device Manager (HDM) soft­ware is required as frame application based on FDT (Field Device Tool). The Device Type Manager (DTM) file is required to configure and manage all VisiWater DO sensors in HDM. To configure the VisiWater DO sensor you will need a USB RS485 Modbus Con­verter and power supply.
5.2.2 Installing DTMs
1) Download the Zip File «Arc Sensor DTM Setup» from the Hamilton webpage www.hamiltoncompany.com (search for Hamilton DTMs).
2) Unpack the downloaded ZIP-File.
3) Do not plug the USB RS485 Modbus Converter before the installation of the DTM is completed.
4) Install the DTM and follow the instructions on the screen.
5) Plug your USB RS485 Modbus Converter to the USB-port of your computer. The driver installs automatically under Windows the drivers saved on the computer under Windows
®
7. Use the “Found new Hardware” Wizard to install
®
X P.
5.2.3 Connecting a VisiWater DO Sensor to HDM
1) Connect the sensor to an external power supply.
2) Start HDM.
3) Open “Device Catalogue” in View.
4) Update the DTM Device Catalogue by clicking “update”.
5) Add the selected “Modbus Serial Port”. Right click on “My network” and select “Add” for the Device Type.
USB RS485 Modbus Converter VisiWater DO
HDM
Figure 7: VisiWater DO sensor configuration with HDM
Power Supply
5.2.1 Installing the Hamilton Device Manager
1) Download the ZIP file “Hamilton Device Manager” from the Hamilton webpage www.hamiltoncompany.com (search for Hamilton Device Manager).
2) Unpack the downloaded ZIP-File.
3) Install the “Hamilton Device Manager” by double clicking “setup.exe” and follow the instructions on the screen.
6) The Modbus Serial Port is added to the “My network” list.
7) Double click on the “Modbus Serial Port”. Set the appropriate COM Port and validate with “Apply”.
8) “Scan for devices”. The available sensors appear on the N etwo rk View.
9) Select the desired sensor. Right click and select “GO online”. The sensor is online if it shows in bold font and offline if it shows in normal font.
Figure 8: VisiWater DO Sensor connected to the HDM (symbolic figure)
5.2.4 Setting User Level
1) Select the desired sensor and check it is online. If not “Go online” with right click on the sensor.
2) Double click on the bold sensor name.
3) Set the appropriate operator level and press “Apply”.
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INSTALLATION INSTALLATION
Parameter Default Name Description password Configuration Location
User The Users Not required Not required System [U] can only read basic data from sensor
Administrator The Admini- 18111978 Not required System [A] strators can also calibrate sensor s
Specialist Additionally 16021966 Must System [S] the specialist can configure the sensors.
Figure 9: User levels
5.2.5 Configuring the VisiWater DO Sensor Parameters
1) Select the desired sensor and check it is online. If not “Go online” with right click.
2) Double click on the bold sensor name.
3) Set operator level to “S” and press “Apply” (Chapter 5.2.4).
4) Configure the measurement parameters.
Parameter Default Name Description Value Configuration Location
Sensing Sensing 243515 Must Measurement/ Material Material are application Parameter different types dependent of ODO Cap which can be set by entering the Ref number of the ODO Caps
5.2.6 Configuring the calibration settings
Parameter Default Name Description Value Configuration Location
Drift DO Higher drift 0.05%/min Recommend Calibration/ will interrupt default Calibration the calibration parameter Settings process. Warning comes up “drift ox ygen”
Drift T Higher drift 0.5 K/min Recommend Calibration/ will interrupt default Calibration the calibration parameter Settings process. War­ ning comes up “drift temperature”
Parameter Default Name Description Value Configuration Location
DO Unit These are the %vol. Required measurement Values physical units %vol., %sat., ug/l ppb, mg/l ppm, mbar
T unit These are the °C Required Measurement/ temperature Values physical units K, °F, °C
Salinity The concentra- 0 mS/cm Default Measurement/ tion of dissolve parameter Parameter oxygen in recommended saturated water is dependent on the salinit y
Air The partial 1013 mbar Required, Measurement/ pressure pressure of application Parameter oxygen is dependent proportional to the atmospheric pressure or the pressure of the air supply to the process
Measuring The measuring 3 sec. Interval interval can be default Parameter set between parameter 1 sec. and 300 sec. The LED flashes once in the set measure interval
Moving The sensor 0 (auto) average uses a moving default Parameter average over parameter the measuring points
Recommended
Recommended
Measurement
Measurement/
Measurement/
/
5.2.7 Configuring the temperature settings
Parameter Default Name Description Value Configuration Location
Customer User defines 0°C to 60°C Recommend Status/ temperature temperature default Quality, range range for DO parameter Counters reading. No and DO reading Tempe- above 60°C ratures possible
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INSTALLATION INSTALLATION
5.2.8 Configuring the analog interface for your process control system
Parameter Default Name Description Value Configuration Location
Interface The output of 4 20 mA Recommended Interface/ Mode the 4-20 mA default Analog can be configure linear, bilinear or with a fix value
Value at Defined 0%-vol Must Interface/ 4 mA measurement application Analog value for 4 m A dependent Output output
Value at Defined 62.85-%vol Must Interface/ 20 mA measurement application Analog value for dependent Output 20 mA output
Mode in Current output No output Recommended Interface/ event of mode in case default Analog warning of warnings parameter Output
Mode in Current output Continuous Recommended Interface/ event of mode in case output default Analog errors of errors parameter Output
Output in Current output 3.5 mA Recommended Interface/ event of in case of default Analog warning warnings parameter Output
Output in Current output 3.5 mA Recommended Interface/ event of in case of default Analog error error parameter Output
Output for T Current output 3.5 mA Recommended Interface/ out of limit in case of default Analog temperature parameter Output out of limit
Before installing the armatures, you should test that the seal is tight and the parts are all in working order. Ensure that there is no damage to the sensor or the armature. Check whether all O-rings are in place in the appropriate grooves and are free of damage. To avoid any mechanical damage to O-rings on assembly, they should be slightly greased.
Please note that O-rings are wetted parts and greasy compounds must comply to your FDA application needs.
5.3.2 Cable Pin Designation
1
2
3
4
Shield
5
5.2.9 Defining a measuring point name for identification of the process
Parameter Default Name Value Settings Location Descriptions
Measuring User can 243650 – 1234 Optional Information / point define a Info sensor name Userspace for better identification of the mea­ suring point
5.3 Install VisiWater DO sensor in your Measuring Loop
5.3.1 Mechanical Process Connection
The VisiWater DO sensor mechanical design is compatible with all Hamilton process housings, including FlexiFit, Retractex, RetractoFit and Hygienic Sockets.
Figure 11: Requirements for electrical connection of VisiWate r DO sensors
Pin Color Function
1 White - 4-20 mA Interface # 1
2 Brown Power Supply: + 24 VDC (7 to 30 V) Start-up power: 1 W Continuous power consumption: 600 mW
3 Green GND
4 Yellow RS485 (A)
5 Gray RS485 (B)
Shield Green-Yellow not connected
5.3.3 Controlling 4–20 mA current interface signals by pulse-width modulation
Hamilton VisiWater DO sensors use the method of pulse-width modulation (PWM) to adjust the DC currents of the 4–20 mA interfaces corresponding to the measured values. In principle, the pulse width (ti) of a rectangular signal with a constant frequency, the pulse duty factor (ti/T), is modulated and afterwards de-
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INSTALLATION INSTALLATION
modulated by a low-pass filter to generate continuous analog DC signals. The resulting value yi corresponds to the average of the PWM signal (see Figures 12 and 13). The PWM-loads of the Sensors have low-pass filters which are not able to eliminate all AC fractions of the used PWM frequency of 5 kHz due to techni­cal impossibilities. Therefore, the current signals of the 4–20 mA interfaces are still overlaid by a certain AC which should be masked by lag smearing or input filters of the current input card of the process control system (PCS). Recommended PCS settings are a sampling rate below 3.5 kHz, an averaging over more than 1 s, and the use of galvanically separated inputs to avoid oscilla­tions. It is also possible to use mathematical functions or isolating amplifiers for signal processing filtering if necessary. For detailed technical advice about suitable isolating amplifiers, please contact Hamilton technical support.
Analog interface 1 and 2
Galvanically not isolated, pulse width modulation with 5 kHz, recommended PCS settings:
• Use galvanically separated inputs
• Sampling rate < 3 kHz and ≠ n * 5 kHz
• Average over > 1 s
5.3.4 Electrical Connection for Analog 4–20 mA Connection
The 4–20 mA interface enables direct connection of the VisiWa­ter DO sensor to a data recorder, indicator, control unit or PCS with analog I/O. The VisiWater DO sensor works as a current sink sensor and is passive. Connect the sensor according to the pin designations (Chapter 5.3.2). The 4–20 mA interface of the VisiWater DO sensors is pre-configured with default values for the 4–20 mA range, and measurement unit. Configure the 4–20 mA interface according to your requirements for proper measurement (Chapter 5.2.8).
Examples of circuit arrangement
Figure 12: Progress of a rectangular signal with a period T and a pulse duration t
Figure 13: Progre ss of a rectangular signal with a period T and a pulse duration t2 for the generation of an analog signal with the value y
for the generation of an analog signal with the value y1.
1
.
2
ATTENTION! The VisiWater DO sensor generates the 4-20 mA signals by pulse with modulation (PWM) which is not compatible to all PCS systems. Also a galvanic separation between the power supply and the PCS is necessary for correct sensor functionality when used in 4-20 mA setups. Figure 12 illustrates a solution for the problem.
Sensor
4–20 mA c urrent
White
Brown
Green
-
input
+
Brown
Green
+
-
output
Pin 1
4–20 mA regulation
Sensor power
Pin 2
U (7–30 VDC) Po wer Supp ly Sens or
Pin 3
Figure 14: Three-wire loop wiring diagram for the 4 –20 mA interface.
Sensor
Pin 1
4–20 mA regulation
Sensor power
Pin 2
Pin 3
Figure 15: The safest form of wiring, using an ex ternal isolation amplifier. The figure represents 4–20 mA interface. (For detailed technic al advice, please contact the technical support at Hamilton.)
White
4–20 mA c urrent
U (7–30 VDC) Po wer Supp ly Sens or
PCS
0 VDC; GND
-
u
+
+ 24 VDC
0 VDC; GND
PCS
+
u
-
0 VDC; GND
+ 24 VDC
0 VDC; GND
Analog Input
Analog Input
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INSTALLATION INSTALLATION
5.3.5 Electrical connection for the digital RS485 interface
The digital RS485 interface enables communication with VisiWater DO sensor for performing measurements, for cali­brating the sensor and for changing the sensor’s configuration parameters. VisiWater DO sensor are always connected to digital controlling devices as a Modbus slave. To function, they require a power supply (Pin 2 and 3, see below). The section entitled “Configuring the VisiWater DO sensor parameters” describes operation in digital mode.
Additional information:
The Modbus RTU communication protocol corresponds to the Modbus-IDA standard (see www.modbus.org). VisiWater DO sen­sor uses an open register set developed by Hamilton. Additional information about the register content and structure can be found in the programmers manual under www.hamiltoncompany.com
The Modbus physical layer is described in detail with require­ments on cabling and line termination in the “Modbus Serial
>
line Protocol and Implementation Guide” www.modbus.org Technical Resources / Modbus Specifications / Modbus Serial line Protocol and Implementation Guide.
Example of circuit arrangement
Sensor
Pin 2
Pin 3
Pin 4
Pin 5
Figure 17: Wiring diagram for the RS485 inte rface.
Master device Distributors
SDA(-)
SDB(+)
RDA(-)
RDB(+)
+ 24 VDC
Common
120 Ohm
line termination
(option)
#1
A/A'
B/B'
+ 24 VDC
Common
#2
A/A'
B/B'
+ 24 VDC
Common
#3
A/A'
B/B'
+ 24 VDC
Common
Power supply
+24 VDC
+
-
0 VDC; G roun d
PCS
A
RS 485
B
Ground
#n
n≤31
A/A'
B/B'
+ 24 VDC
Common
120 Ohm
line termination
(option)
ATTENTION! Because all sensors are delivered with factor y-default settings, each sensor must be configured for its specific application before first use (see the section entitled “Configuring VisiWater DO sensor”).
The pins for digital the RS485 interface have the following designation with respect to cable conductor colors:
Sensor fix cable Color
Power supply: +24 VDC Brown (7 to 30 VDC), max. power consumption 1 W.
Power supply: Ground Green
RS485 (A) Yellow
RS485 (B) Gray
Cable shield green-yellow
Figure 18: Multi-drop bus wiring for the Modbus two-wire mode. Each sensor functions as a Modbus slave.
The serial Modbus connection between the RS485 port of the master and the corresponding interfaces of the sensors has to be ensured according to the EIA/TIA RS485 standard. Only one sensor can communicate with the master at any time.
NOTE: In order to avoid signal reflection on the lines the use of line termination resistors (120 Ohm each) is recom­mended. The effect of signal reflections becomes more relevant with long cable length and/or high baud rates.
NOTE: In the connection scheme shown above, each sensor must have the unique Modbus device address for proper communication.
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OPERATION MAINTENANCE MAINTENANCE
6 Operation
WARNING: Only use the sensor within the specifications (Chapter 10). Failure to do so may lead to damages or measure- ment failure.
1) Remove the protective caps from the VisiWater DO sensor shaft
2) Check the O-ring on the sensor shaft and verify if the ODO Cap is screwed firmly to the sensor shaft (Chapter 7.2)
3) Verify if the sensing material is correct for the ODO Cap type which can be set by entering the Ref number of the ODO Caps
4) Verify the functionality of the sensor including the ODO cap (Chapter 7.1)
5) Calibrate the sensor (Chapter 7.3)
6) Connect the sensor to the process control system (Chapter 5.3)
7) Verify the measurement in air on your control system
8) Mount the sensor to the armature or process connection (Chapter 5.3)
NOTE: No oxygen measurement is performed at a temperature higher than 6C to protect the optoelec- tronics and enhanced the sensor lifetime.
4) Control the quality of the ODO cap in Sensor Status / Quality Counter and Temperature / Quality Indicator and change the ODO cap if required (Chapter 7.2).
The sensor is performing correctly. No errors or warnings have been registered.
At least an error or a warning has been registered. Verify the sensor errors and warnings in Sensor Status.
No communication between the sensor and the HDM. This may be due to a hardware failure.
Figure 19: Description of the trafc lights on the HDM
7.2 Replacing the ODO Cap
The exchange of ODO Cap can be performed very easily:
1) Unscrew the ODO cap from the shaft (Figure 20).
2) Exchange the O-ring.
NOTE: To ensure a correct measurement by changing a ODO Cap type e.g. ODO Cap H0 reference number of the ODO Cap should be congured in the Sensing Material register (See chapter “Conguring the VisiWater DO Sensor Parameters. Firmware version ODOUM042.hex ore higher is required.
>
ODO Cap H2 the
7 Maintenance
Periodic maintenance routines need to be run in order to ensure safe and reliable operation and measurement of sensor and the accessories.
ATTENTION! Avoid any contact of the equipment
with corrosive media.
3) Screw firmly the new ODO Cap onto the sensor shaft again.
4) Perform sensor calibration (Chapter 7.3).
NOTE: If the ODO Cap is mounted very firmly on the shaft, and if you cannot obtain a good grip on the stainless steel with your fingers, a silicone tube between your fingers and metal may supply a better grip.
O-ring
unscrew
Figure 20: Replacing the ODO Cap
7.1 Verify Sensor Status and ODO Cap Functionality
1) Power the sensor and connect the sensor to HDM.
2) Control the traffic lights (Figure 15).
3) Please refer to the troubleshooting (Chapter 8) for the next steps if the traffic light is not green.
7.3 Calibration
The VisiWater DO sensors provide two kinds of sensor calibra- tion: automatic standard calibration, and product calibration. The automatic standard calibration and the product calibration may be performed using HDM (see chapter 5.2)
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MAINTENANCE MAINTENANCE
N
2
7.3.1 Automatic Standard Calibration with HDM
VisiWater DO sensors are calibrated at two points: in air and in an oxygen-free environment. During calibration, the sensor controls automatically the stability of the oxygen and temperature signals.
NOTE: For greater measurement accuracy ensure that temperature difference between calibration medium and process medium is minimal.
7.3.2 Zero Point Calibration (Point Zero Oxygen)
1) Power the sensor and connect it to HDM.
2) Select the sensor to calibrate in “Network View”.
3) Go in System and select “Operator Level”.
4) Log in an appropriate Operator Level (Administrator or Specialist). More details in chapter 5.2.4.
7.3.3 Calibration in Air (Calibration Point Air)
1) Select the sensor to calibrate in “Network View”.
2) Go in System and select “Operator Level”.
3) Log in an appropriate Operator Level (Administrator or Specialist). More details in chapter 5.2.
4) Go to “Calibration” and select “Calibration Point Air”.
5) Hold the sensor for at least three minutes under stable conditions in air over stirred water to account for humidity (Figure 22).
6) Select the calibration command “Auto” and press “Apply”.
7) Verify the Calibration status in air. It should indicate “Calibration successful”.
5) Go to Calibration and select “Point Zero Oxygen”.
6) Immerse the sensor into an oxygen-free environment (Figure 21) for e.g. nitrogen gas with min. purity of 5.0 and nitrogen flow rate: 0.5 mL/min with 3 to 4 bar pressure (no overpressure). Let the system equilibrate and ensure stable conditions for at least three minutes.
7) Select the calibration command “Auto” and press “Apply”.
8) Verify the Calibration status in Zero Oxygen. It should indicate “Calibration successful”.
Sensor for calibration in zero oxygen
Tube: on the top open (no overpressure)
Valve for setting the flow of 0.5 L/min
O
2
H2O
Magnetic stirrer
Figure 22: Calibration setup in saturated medium
NOTE: Calibration with air-saturated water is less
accurate due to the slow saturation process of air in water.
NOTE: The value of the saturated oxygen concentration at different temperatures, different pressures and air humidity play an important role for the calibration of dissolved oxygen. VisiWater DO sensor refers to a concentration in water saturated air and from the factory settings of atmospheric pressure of 1013 mbar at 25°C.
Nitrogen with purity of 5.0
Figure 21: Zero point calibration setup
7.4 Product calibration
The product calibration is an in-process calibration procedure in order to adjust the measurement to specific process conditions. Product calibration is an additional calibration procedure to a standard calibration.
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MAINTENANCE TROUBLESHOOTING
If product calibration is activated, the VisiWater DO sensor cali­bration curve is calculated from the data of last calibration at point 1 and from the data of the product calibration (Figure 23). In order to restore the original standard calibration curve, the product cali­bration can be at any time by selecting on the Product calibration command “cancel”. A new standard calibration cancels a product calibration as well.
Figure 23: Ef fect of a product calibration (CP6) on an existing standard calibration function based on the Zero Point Calibration (CP 1) and the Air Calibration (CIP 2).
8 Troubleshooting
8.1 Sensor Self-Diagnostic
VisiWater DO sensors provide a self-diagnostic functionality to detect and identify the most common sensor malfunctions. Both interfaces, analog 4–20 mA or digital Modbus, may provide warning and error messages. The analog 4–20 mA interface can be configured according to the NAMUR recommendations to in­dicate an abnormal event (See Chapter 5.2.8). Use HDM for moni­toring the sensor status and for troubleshooting. The following types of messages are provided by the self-diagnosis function.
NOTE: Errors cannot be ignored and corrective action is immediately necessary.
NOTE: Warnings can be ignored but the warning will be displayed continuously until the corrective action is successfully completed.
NOTE: The product calibration is possible for DO values
in the range of 2 to 55 %-vol (20 – 550 mbar pO
).
2
A product calibration is performed as follows:
1) Connect the sensor to HDM.
2) Select the sensor to calibrate in “Network View”.
3) Go in System and select “Operator Level”.
4) Log in an appropriate Operator Level (Administrator or Specialist). More details in chapter 5.2.
5) Go to Calibration and select “Calibration Point Product”.
6) Select under product calibration command Initialize and press Apply.
7) Perform an initial measurement while taking a sample from the process.
8) Perform a laboratory measurement of the sample at the same temperature as it was measured in the process.
9) Assign the laboratory value in the HDM to the value of the Initial measurement (Product value to assign). This new DO value is accepted and automatically active, if the difference between initial measurement and laboratory values is not greater than 20 %-sat units.
10) Verify the Calibration status in product calibration. It should say active + assigned.
NOTE: Alternatively, the product calibration may be
performed with a field device on side the measuring point.
NOTE: For additional information about the sensor status and the diagnostics features refer to the sensor operation instruction manual or the programmer`s manual.
8 .1 .1 W a r n i n g s
Warning Cause / Solution
DO reading below The oxygen reading is too low lower limit (DO < 0%-sat). Make a new zero-point calibration (Chapter 7.3.2).
DO reading above The oxygen reading is too high upper limit (DO > 500 %-sat). Make a new calibration in oxygen saturated medium. (See chapter 7.3.3). If not successful, replace the sensor cap.
DO reading unstable If continuously happening, use a new cap or check the process regulation. If the problem still appears, call our Technical Support.
T reading below The temperature is below the user defined lower limit measurement temperature range. If the process temperature is outside this range, the sensor will not perform DO readings.
T reading above The temperature is above the user upper limit defined measurement temperature range. If the process temperature is outside this range, the sensor will not perform DO readings.
Measurement The measurement interval is set to 0 or not running the measurement temperature is out of the range.
DO calibration Perform a calibration in order to ensure recommended reliable measurement (Chapter 7.3).
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TROUBLESHOOTING DISPOSAL
8.2 Getting Technical Support
Warning Cause / Solution
DO last calibration The last calibration failed. The sensor is not successful using the old successful calibration values. In order to ensure reliable measurement perform a new calibration (Chapter 7.3).
DO replace Replace the ODO Cap and calibrate the sensor cap sensor. This warning remains active as long as the sensor quality is below 35%.
4–20 mA value The measurement value is below the below 4 mA lower limit of the 4–20 mA interface output. Reconfigure the 4–20 mA interface (Chapter 5.2.8).
4–20 mA value The measurement value is above the above 20 mA upper limit of the 4–20 mA interface output. Reconfigure the 4–20 mA interface (Chapter 5.2.8).
4–20 mA current The 4–20 mA interface is not able to set-point not met regulate the current requested for the current measurement value according to your 4–20 mA interface configuration. Check the 4–20 mA wiring and supply voltage (Chapter 5.3.4).
Sensor supply The sensor supply voltage is too low for voltage too low the sensor to operate correctly. Ensure stable supply voltage within the sensors specifications.
Sensor supply The sensor supply voltage is too high for voltage too high sensor to operate correctly. Ensure stable supply voltage within the sensors specifications.
If a problem persists even after you have attempted to correct it, contact Hamilton`s Customer Support: Please refer to the contact information at the back of this operating instruction.
8.3 Returning VisiWater DO sensor for Repair
Before returning a VisiWater DO sensor to Hamilton for repair, contact our Customer Service (see Chapter 8.2) and request a Returned Goods Authorization (RGA) number.
Do not return a VisiWater DO sensor to Hamilton without an RGA number. This number assures proper tracking of your sensor. VisiWater DO sensors that are returned without an RGA number will be sent back to the customer without being repaired.
Decontaminate the VisiWater DO sensor and remove health haz­ards, such as radiation, hazardous chemicals, infectious agents etc. Provide complete description of any hazardous materials that have been in contact with the sensor.
9 Disposal
8.1. 2 E r ro r s
Errors (failures) Cause / Solution
DO reading failure Sensor cap is missing or the sensor is broken.
) exceeds Measured partial pressure of oxygen is
DO p(O
2
air pressure higher than the air pressure set by the operator. Reconfigure the air pressure parameter (Chapter 5.2.5).
T sensor defective The internal temperature sensor is defect, please call our Technical Support.
DO sensor The DO sensor cap has been removed. cap missing Do not immerse the sensor in a measurement solution. Mount an ODO Cap and calibrate the sensor prior measurement (Chapter 6).
Red channel failure Measurement channel failure. Please call our Technical Support.
Sensor supply The sensor supply voltage is below 6 V. voltage far too low Please check your power supply.
Sensor supply The sensor supply voltage is above 40 V. voltage far too high Please check your power supply.
Temperature reading The measured temperature is below the far below min operation temperature.
Temperature reading The measured temperature is above the far above ma x operation temperature.
The design of Hamilton sensors optimally consid­ers environmental compatibility. In accordance with the EC guideline 2002/96/EG Hamilton sensors that
are worn out or no longer required must be sent to a dedicated collection point for electrical and electronic devices, alternatively, must be sent to Hamilton for disposal. Sensors must not be sent to an unsorted waste disposal point.
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TECHNICAL SPECIFICATIONS
ORDERING INFORMATION
10 Technical Specifications
4–20 mA current range 3.5 to 22 mA
Accuracy at 25 °C 1 ± 0.05%-vol
21 ± 0.2%-vol 50 ± 0.5%-vol 100 ± 10%-vol
Analog Interface 1 4–20 mA
Certificate Yes
Configurable Values DO: mbar; %-sat; %-vol; μg/l;
mg/l; ppb/ppm (dissolved oxygen); Temperature: °C
Diameter 12 mm
Digital Interface RS485 Modbus
Drift at Room Temp. under Constant Conditions < 1% per week
Electrical Connector Fix cable with open end wires
Electrolyte None
Measurement Principle Oxygen dependent
luminescence quenching
Measuring Range 4 ppb to 40 ppm (DO) or
0.1 to 1000 mbar (pO
Wetted parts Stainless steel 1.4435, Silicone
Process Temperature 0 – 60 °C
Operating Voltage 7 to 30 VDC
Oxygen Consumption None
Pressure Range 0 to 12 bar
Process Connection PG13,5
Stainless Steel 1.4435
Protection Rating IP 68
Response Time t98% < 30 s at 25°C, from air
to nitrogen
Serial Number Yes
Temperature Sensor NTC 22 kOhm
)
2
11 Ordering Information
Parts below may only be replaced by original spare parts.
11.1 VisiWater DO Sensor
Ref Description Interface
243650 VisiWater DO Arc 120 FC10* 4-20 mA, Modbus
* FC10 = 10 m fix cable
11.2 Parts and Accessories
Ref Description Wetted parts
243515 ODO Cap H0 Stainless steel 1.4435 Silicone (FDA and USP Class VI approved)
Application: For general application in biotechnology, water treatment and monitoring as well as in breweries, wineries and soft drink processing.
Ref Description Wetted parts
243505 ODO Cap H2 Stainless steel 1.4435 PTFE (USP Class VI)
Application: For fermentation processes where sterilization in place (SIP) is performed in media containing higher amounts of lipophilic compounds. It comes with a hygienic design.
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ORDERING INFORMATION ORDERING INFORMATION
Ref Qualification (IQ/OQ)
243999-07 IQ/OQ per sensor measuring point
Description: Documentation of the initial operation and calibration of the measuring system, provision of the measuring and testing equipment, check and certification (without travel costs)
243999-08 Ever y further IQ/OQ of the same kind per
Ref Product Name
242411 USB RS485 Modbus Converter
Description: Designed for wired communication between HDM and VisiWater DO Arc FC10 sensor.
11. 3 S e r vi ce s
Ref Training sessions
243999-12 On-site training (half-day)
Description: Impar ting of fundamental knowledge about pH/ORP/Conductivity/DO/cell density sensor measuring technology incl. documents and participation confirmation, excl. travel costs
sensor measuring point
243999-14 IQ/OQ Documentation per sensor gauge incl. report documents and instructions for qualification
Ref Maintenance
243999-10 Maintenance per DO measuring point
Description: Check of the response behavior, calibration with air and nitrogen 5.0, replacement of the electrolytes, cleaning of the internal body, check of the temperature probe, check of the sensor quality with VisiWater DO sensor, incl. calibration certificate
243999-13 Every further maintenance of the same kind per sensor measuring point
NOTE: These services are only available in the
following locations: Europe, Africa and China.
Ref Service packages
243999-17 PREMIUM service package DO sensor
243999-20 BASIC service package DO sensor
Ref Service tools
238999-4456 DO service case
Ref Initial operation and calibration
243999-05 Initial operation per sensor measuring point
Description: Sensor parametrization, connection of the sensor cable, calibration of the measuring chain (without transmitter/SPS), check and certification, provision of the measuring and testing equipment as well as orientation of the operator personnel
243999-06 Every further initial operation of the same kind per sensor measuring point
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NOTES NOTES
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Windows is a registered trademark or trademark of Microsoft Corporation in the United States and/or other countries.
© 2016 Hamilton Bonaduz AG. All rights reserved.
624821/01 — 06/ 2016
Web: www.hamiltoncompany.com USA: 800-648-5950
Europe: +41-58 -610 -10-10
Hamilton Americas & Pacific Rim
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Via Crusch 8 CH-7402 Bonaduz, Switzerland Tel: +41-5 8- 610-10-10 Fax: +41-58- 610-00-10 contact.pa.ch@hamilton.ch
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