Yamato Scientific Vacuum controller User Manual

INSTRUCTION MANUAL
FOR
Vacuum Controller
The 2nd Edition
The 2nd Edition
The 2nd EditionThe 2nd Edition
VR100
Yamato Scientific
Yamato Scientific Co
2-1-6,
2-1-6, Nihonbashi Honcho, Chuo-
2-1-6, 2-1-6,
Congratulations on your selection of Yamato Scie ntific’s VR100! Please read these operating instructions, user notes and the warranty card thoroughly before the initial operatio n of your VR100. This will ensure proper operati ng procedures and extended life for the unit. Please keep the operating instructions together with the warranty card for easy access whenever you need them.
Nihonbashi Honcho, Chuo-ku
Nihonbashi Honcho, Chuo-Nihonbashi Honcho, Chuo­Tokyo 103-8432 JAPAN
Tokyo 103-8432 JAPAN
Tokyo 103-8432 JAPANTokyo 103-8432 JAPAN
Co...., Ltd.
, Ltd.
CoCo
, Ltd., Ltd.
ku
kuku
TABLE OF CONTENTS
Explanation of Picture Display......................................................................................1
Cautions in Using with Safety.......................................................................................2
Notes to Users................................................................................................................3
Description and Function of Each Part.....................................................................................3
Requiremen ts for Installa tion....................................................................................................5
Handling Precautions ....................................................................................................9
Corrosive Resistance.............................................................................................................11
Operation ......................................................................................................................12
The Fixed Value Control.........................................................................................................13
Changing the Set point While the Fixed Value Control Operates............................................14
The Ramp Control..................................................................................................................15
The Free Mode ......................................................................................................................16
Shutdown...............................................................................................................................17
Restart...................................................................................................................................17
Shifting to Oth er Operation .....................................................................................................18
Using the Function Menu.............................................................................................19
Calibrating Measurements.....................................................................................................20
Editing the Set point of the Ramp control...............................................................................21
Error ..............................................................................................................................24
Maintenance..................................................................................................................25
Daily Inspection and Maintenance..........................................................................................25
Replacing Fuse......................................................................................................................26
After Service and Warranty..........................................................................................27
If a Service Call is required:...................................................................................................27
Troubleshooting .....................................................................................................................27
Specifications...............................................................................................................28
Wiring Diagram.............................................................................................................29
Replacement Parts Table.............................................................................................30
Reference......................................................................................................................31
Dangerous Substances..........................................................................................................31
Pressure Conversion..............................................................................................................32
Explanation of Character on the display.................................................................................32
Explanation of Picture Display
MEANING OF ILLUSTRATED SYMBOLS
Illustrated Symbols
Various symbols are used in this safety manual in order to use the unit without danger of injury and damage of the unit. A list of problems caused by ignoring the warnings and improper handling is divided as shown below.Be sure that you understand the warnings and cautions in this manual before operating the unit.
Warning
Caution
If the warning is ignored, there is the danger of a problem that may cause a serious accident or even fatality.
If the caution is ignored, there is the danger of a problem that may cause injury/damage to property or the unit itself.
Meaning of Symbols
This symbol indicates items that urge the warning (including the caution). A detailed warning message is shown adjacent to the symbol.
This symbol indicates items that are strictly prohibited. A detailed message is shown adjacent to the symbol with specific actions not to perform.
This symbol indicates items that should be always performed. A detailed message with instructions is shown adjacent to the symbol.
1
Cautions in Using with Safety
WARNING
Do not use the unit in an area where there is flammable or explosive gas.
••••
Never use the unit in an area where there is flammable or explosive gas. The unit is not explosion-proof. An arc may be generated when the power switch is turned on or off, and fire/explosion may result.
Always ground the unit.
••••
Always ground the unit on the power equipment side in order to avoid electrical shock due to a power surge.
If a problem occurs, you should:
••••
If smoke or strange odor should come out of the unit for some reason,
off
the circuit breaker and the main power. Immediately contact a service technician for inspection. If this procedure is not followed, fire or electrical shock may resul t. Never perform repair work yourself, since it is dangerous and not recommended.
Do not use the power cord if it is bundled or tangled.
••••
Do not use the power cord if it is bundled or tangled. If it is used in this manner, it can overheat and fire may be caused.
turn off
the power key right away, then
turn
Do not process, bend, wring, or stretch the power cord forcibly.
••••
Do not process, bend, wring, or stretch the power cord forcibly. Fire or electrical shock may result.
Substances that can not be used.
••••
Never use explosive substances, flammable substances and substances that include explosive or flammable ingredients in the unit. Explosion or fire may occur.
Do not disassemble or modify the unit.
••••
Do not reconfigure the unit. Fire or electrical shock may be caused.
CAUTION
During a thunder storm
••••
During a thunder storm, If this procedure is not followed, fire or electrical shock may be caused.
turn off
the power key immediately, then
turn off
the circuit breaker and the main power.
2
Main unit
Front view
Notes to Users
Description and Function of Each Part
Control panel
Power Switch
Power Cord
Rear view
Fuse Box
Connection for Evaporator Port for Hose: Outside Diameter 10mm, Nominal Size 1/8 x 5/16
Connection for Aspirator Port for Hose Outside Diameter 10mm, Nominal Size 1/8 x 5/16
3
Control Panel
Main Display:
Solenoid Valve Lamp (LED):
Blind Window:
Edit Mode Display Lamp
(LED) Operation Mode Display
Lamp Set Mode Display Lamp
Leak Lamp
Operation Menu Key
Function Menu Key
Up/Down Key
Enter Key
Displays measureme nts, set points ( indicated as ~h Pa), literal informations in the ramp control editing, etc.
Lit while the solenoid valve for control opens. Indicates a blinking
abnormality occurred. Lights up
selected. indicates a selected operation mode. It is lit while
operation, and blinked in the set mode and the edit mode. Nothing is indicated in the free mode.
lit when settings and edits are done. lit while the leak valve opens. used to select one of the following operations.「the fixed
value control」,「the ramp control」,「the free mode used to select the function;「the measurement
calibrating mode」in the fixed value control and 「the edit mode」 in the ramp control.
used to change the set point. used to decide or input set points and modes, such as
operation, calibration, edit.
「編集」
「異常」
(Means
(Means
EDIT
TROUBLE
) when the edit mode is
) when an
4
Requirements for Installation
Installation to Rotary Evaporator RE400/500/440/540
1. 2.
Unscrew the screw which fix the rubber-leg of the body.
Rubber leg Metal Fixture
3. 4.
Fix the metal fixture to the rear of the control unit with four screws.
Control Unit of RE400/500
Fix the metal fixture provided as standard accessories with flat-head screws.
Put the power plug of the vacuum regulator in the outlet at the rear of the control unit.
5.
Finished View
Power Cord Plug
VR100
RE400/500/440/540 Being the auto lift style, the body-outlook of
RE440/540 is not the same as the drawing on the left.
5
Warn ing
Warning
WarningWarning
Do not use the unit in an area where there is flammable or explosive gas.
Never use the unit in an area where there is flammable or explosive gas. The unit is not explosion-
proof. An arc may be generated when the power switch is turned ON or OFF, and fire/explosion may result.
Always ground the unit.
Connect VR100’s power plug to a receptacle with grounding connectors.
Do not forget to ground VR100, to protect you and the uni t from electr ical sho ck in cas e of pow er surge.
Choose a receptacle with grounding connectors as often as possible.
Do not connect the grounding wire to a gas pipe, or by means of a light ni ng ro d or t ele pho ne line. A fire
or electrical shock will occur.
If only bipolar receptacles are available for
VR100, connect an optional grounding adapter to VR100’s power plug. Check the polarity of the receptacle before connecting the adapter to the receptacle. Connect the adapter’s grounding wire (green) to a grounding terminal to the power supply. Contact our sales representative in your vicinity or our service center for additional information or assistance.
100V receptacle with grounding terminals
Power plug
100V bipolar receptacle
Grounding wire
6
Choose a correct power distribution board or receptacle.
Choose a correct power distribution board or receptacle that meets VR100’s rated electric capacity.
Electric capacity : AC100 V, 1A
Do not connect VR100 to an outlet that differs from the above spe cif ic ations because a fire or electrical
shock will occur.
Install on a level area.
Do not installation VR100
on a non level surface. This will cause hazards to the operator and create problems during actual operation.
Choose a proper place for installation.
Do not install VR100 in a place where:
Flammable gas or corrosive gas is generated.
Ambient temperature exceeds 35°C, also bellow 5°C.
Ambient temperature fluctuates violently.
There is direct sunlight.
There is excessive humidity and dust.
There is constant vibrations.
Keep the clearance over 15cm around VR100.
7
Caution
Caution
CautionCaution
Handling of power code.
Do not entangle the power cord. This will cause overheating and possibly a fire.
Do not bend or twist the power cord, or apply excessive tension to it. This may cause a fire and
electrical shock.
Do not lay the power cord under a desk or chair, and do not allow it to be pinched in order to prevent it
from being damaged and to avoid a fire or electrical shock.
Keep the power cord away from any heating equipment such as a room heater. The cord's insulation
may melt and cause a fire or electrical shock.
If the power cord becomes damaged (wiring exposed, breakage, etc.), immediately turn off the power
at the rear of the product and shut off the main supply power. Then contact your nearest dealer for replacement of the power cord. Leaving it may cause a fire or electrical shock.
Connect the power plug to the outlet which is suppl ied appr opriate pow er and voltage . If the p ow er cord
is connected the supply which is also connected to a aspirator or a vacuum pomp etc., with no sufficient power and voltage, the product may not operate properly because the power would fall.
Piping
Vacuum hoses (outside diameter 12 x inside diameter 6mm) are required. These are not included in
accessories.
Refer to figure below in order to pipe. Stickers that indicate where to connect are attached at the rear.
Connect the pipes correctly in accordance with each indication of them.
Power code
to condenser's decompression port of ROTARY EVAPORATOR
The rear of the body
to suction port of ASPIRATOR
Vacuum Hose
8
Warn ing
Warning
WarningWarning
Approaching Thunderstorm
If a thunderstorm approaches in the distance, immediately turn off the power at the rear panel and shut
off the supply power. Leaving the power turned on may cause a fire or electrical shock.
During Power Failure
In case of power failure, the leak valve opens, the atmosphere in the system of the rotary evaporator is
released, and the solenoid valve for control is shut. It prevents spout of organic solvent in distillation, and back-flow of water from the aspirator.
After power failure was repaired, the set mode is automatically switched to the fixed value control. The
indicator displays the set pressure blinking. The leak valve opens and the solenoid valve for control shuts.
The product is not interlocked with neither the rotary evaporator nor bath. Care should be taken that
each movement of them is not the same after the power failure. If power failes wh ile the evaporator is revolving, it starts revolving after power failure was repaired.
Make sure that the aspirator and the cold circulating device etc. is working properly when you start
the vacuum control again.
Handling Precautions
Aspirator Shutdown
The device must be stoppe d be fore y o u st op the aspirator. If not,ba ck- f low ,from the aspirator's bath to
the pressure senser,may occur.In case of back-flow, the indicator may not display accurate values,or the sensor may be damaged.
Using the Product
The product is not a pressure measurement apparatus. Do not use it for calibration.
There are not functions for vacuum and pressure raising in the product itself. The product is used to
control the pressure in the system. The operation runs in order to reach to the pressure which is set depending on the rise of pressure, by connecting to a decompression device of aspirator etc. The rise of pressure (depending on the steam pressure of sample) is that occurs when the rotary evaporator operates distillations.
Corrosive Samples
The product's connections to gas are made of materials given in Table 1. Especially metal piping parts
and gas-joint for pressure sensor are corroded by strong acids and strong alkalines. Do not use the product for distillation of strong acids and strong alkalines.
As the product's gas-joints are exposed to low-concentrated steam that can not be trapped by the
condenser (cooler),the joints are not corroded soon. However a sort of rubber might swell depending on the kind of solvent or frequency of use. If pressure in the system is not held,or,an abnormality is shown the indicator ,please contact us.
Make sure that vacuum hoses are connected correctly ,to 「pressure」 and to「load」.
9
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