Yamato Scientific DP610, DP410, DP200, DP300 User manual

Thank you for choosing DP Series Vacuum Drying
Ovens by Yamato Scientific Co., Ltd.
For proper equipment operation, please read this instruction manual thoroughly before use. Always keep equipment documentation safe and close at hand for convenient future reference.
Warning: Read instruction manual warnings and
cautions carefully and completely before proceeding.
VACUUM DRYING OVENS
Model DP200/300/410/610
Instruction Manual
Yamato Scientific Co., Ltd.
Printed on recycled paper
TABLE OF CONTENTS
1. SAFETY PRECAUTIONS ........................................................................................................... 1
Explanation of Symbols ......................................................................................................................... 1
Symbol Glossary ................................................................................................................................... 2
Warnings and Cautions ......................................................................................................................... 3
2. PRE-OPERATION PROCEDURES ............................................................................................ 4
Installation Precautions & Procedures .................................................................................................. 4
Vacuum System Information ................................................................................................................. 9
3. COMPONENT NAMES AND FUNCTIONS ............................................................................... 11
Unit Overview 1 ................................................................................................................................... 11
Control Panel ....................................................................................................................................... 13
4. OPERATION PROCEDURE ..................................................................................................... 14
Prior Confirmation ............................................................................................................................... 14
Decompression/Purge Procedure ....................................................................................................... 14
Setting Date & Time ............................................................................................................................ 15
Keypad Tone Function ........................................................................................................................ 16
Mode and Function Flow ..................................................................................................................... 17
Constant Temperature Mode .............................................................................................................. 18
Auto Stop Mode ................................................................................................................................... 20
Auto Start Mode................................................................................................................................... 22
Programmed Operation ....................................................................................................................... 24
Building Programs ............................................................................................................................... 27
Keypad Lock Function ......................................................................................................................... 31
Calibration Offset Function .................................................................................................................. 32
Recovery Modes ................................................................................................................................. 33
CO2 Emissions & Power Consumption Settings ................................................................................ 34
Data Backup & Reset .......................................................................................................................... 35
Data Monitoring ................................................................................................................................... 36
Independent Overheat Prevention Device .......................................................................................... 37
5. HANDLING PRECAUTIONS .................................................................................................... 38
6. MAINTENANCE PROCEDURE ................................................................................................ 43
Inspection and Maintenance ............................................................................................................... 43
7. EXTENDED STORAGE & DISPOSAL ..................................................................................... 44
Extended Storage / Unit Disposal ............................................................................................................. 44
Disposal Considerations...................................................................................................................... 44
8. TROUBLESHOOTING .............................................................................................................. 45
Error Code Guide ................................................................................................................................ 45
Troubleshooting Guide ........................................................................................................................ 46
9. SERVICE & REPAIR ................................................................................................................ 48
10. SPECIFICATIONS .................................................................................................................. 49
11. ACCESSORIES ...................................................................................................................... 51
Optional Accessory Guide ................................................................................................................... 51
12. WIRING DIAGRAM................................................................................................................. 53
13. WEAR ITEMS ......................................................................................................................... 57
14. LIST OF HAZARDOUS SUBSTANCES ................................................................................. 58
15. SETUP CHECKLIST ............................................................................................................... 59
A Word Regarding Symbols
Various symbols are provided throughout this text and on equipment to ensure safe operation. Failure to comprehend the operational hazards and risks associated with these symbols may lead to adverse results as explained below. Become thoroughly familiar with all symbols and their meanings by carefully reading the following text regarding symbols before proceeding.
Warning
Caution
Signifies a situation which may result in minor injury (Note 2) and/or property damage (Note 3)
(Note 1) Serious injury is defined as bodily wounds, electrocution, bone
breaks/fractures or poisoning, which may cause debilitation requiring extended hospitalization and/or outpatient treatment.
(Note 2) Minor injury is defined as bodily wounds or electrocution, which will not
require extended hospitalization or outpatient treatment.
(Note 3) Property damage is defined as damage to facilities, equipment, buildings or
other property. Note 1 Serious injury is defined as bodily wounds,
Symbol Meanings
Signifies warning or caution. Specific explanation will follow symbol.
Signifies restriction. Specific restrictions will follow symbol.
Signifies an action or actions which operator must undertake. Specific instructions will follow symbol.
Signifies a situation which may result in serious injury or death (Note 1)
1. SAFETY PRECAUTIONS
Explanation of Symbols
1
General Warning
Danger!:
High Voltage
Danger!:
Extremely Hot
Danger!:
Moving Parts
Danger!:
Blast Hazard
General Caution
Caution:
Electrical Shock
Hazard!
Caution: Burn
Hazard!
Caution: Do Not
Heat Without
Water!
Caution: May
Leak Water!
Caution: Water
Only
Caution: Toxic
Chemicals
General
Restriction
No Open Flame
Do Not
Disassemble
Do Not Touch
General Action
Required
Connect Ground
Wire
Level Installation
Required
Disconnect Power
Inspect
Regularly
Warning
Caution
1. SAFETY PRECAUTIONS
Symbol Glossary
Restriction
Action
2
Warning
Never operate equipment near combustible gases/fumes.
Do not install or operate DP series unit near flammable or explosive gases/fumes. Unit is NOT fire or blast resistant. Negligent use could cause a fire/explosion. See List of Hazardous Substances (P.58).
Always ground equipment.
Always ground this unit properly to avoid electric shock.
DO NOT operate equipment when abnormalities are detected.
If smoke or unusual odors begin emitting from unit, or if any other abnormalities are detected, terminate operation immediately, turn off main power switch (Earth Leakage Breaker - ELB) and disconnect power cable. Continued operation under such conditions may result in fire or electric shock.
DO NOT operate with bundled or tangled power cable.
Operating unit with the power cable bundled or otherwise tangled, may cause power cable to overheat and/or catch fire.
DO NOT damage power cable.
Damaging the power cable by forcibly bending, pulling or twisting may cause fire or electric shock to the operator.
NEVER disassemble or modify equipment.
Attempting to dismantle or modify unit in any way, may cause malfunction, fire or electric shock.
DO NOT touch hot surfaces.
Some surfaces on this unit become extremely hot during operation. Exercise vigilance in order to avoid getting burned.
DO NOT insert multiple power cables into a single outlet.
Inserting multiple cords into a single outlet, using branch outlets or extension cords, may cause power cable to overheat and/or catch fire. Other issues may include a drop in voltage, which may affect performance, resulting in failure to control or maintain proper temperatures.
Caution
DO NOT operate equipment during thunderstorms.
In the event of a thunderstorm, terminate operation and turn off main power switch (ELB) immediately. A direct lightning strike may cause damage to equipment, or result in fire or electric shock.
1. SAFETY PRECAUTIONS
Warnings and Cautions
3
Do not install DP series unit:
where flammable or corrosive gases/fumes will be generated. where exterior temperature will exceed 35ºC, will fall below 5ºC or will fluctuate. in excessively humid or dusty locations. where there is constant vibration. where power supply is erratic. in direct sunlight or outdoors.
Install DP series oven(s) in a location with sufficient space and ventilation as specified as below.
Install unit on a level and even surface. Failure to do so may result in abnormal vibrations or noise, possibly causing complications and/or malfunction.
Approximate unit weight: DP200: approx. 45kg, DP300: approx. 72kg, DP410: approx. 210kg, DP610: approx. 310kg. Handle with care. Transportation and installation should always be done by two or more people.
Min. 20cm
Min. 20cm
Equipment
Door
DP200: Min. 40cm DP300: Min. 50cm DP410: Min. 65cm DP610: Min. 80cm
Min. 20cm
2. PRE-OPERATION PROCEDURES
1. Choose an appropriate installation site.
Installation Precautions & Procedures
2. Install on a level surface.
4
In the event of an earthquake or other unforeseen incident, equipment may unexpectedly shift or fall, causing injury. Taking preventative steps to install unit in a safe location, away from room access doors and out of other danger is strongly recommended.
Install unit so that side panel heat vents (see Unit Overview 1 on P.11 for location) are unobstructed and allowed to sufficiently diffuse heat. Failure to do so may result in excessive temperatures inside the unit control panel, causing possible degraded CPU board performance, malfunction or fire. See installation specifications above.
Install unit where it will be free from liquid spray and other moisture. Failure to do so may result in control mechanisms becoming wet, causing malfunction, electrical shock and/or fire.
Never install near flammables or explosives. This unit is NOT fire or blast resistant. Simply switching the main power switch (ELB) “ON” or “OFF” can produce a spark, which could relay during operation, causing a fire or explosion when near flammable or explosive fluids, chemicals or gases/fumes. See “List of Hazardous Substances” (P.58).
Explosives
Flammables
2. PRE-OPERATION PROCEDURES
Installation Precautions & Procedures
3. Install in a safe location.
4. Install in a well-ventilated area (DP200/300 only).
5. Install in a dry location.
6. Install in a location free of flammables and explosives.
5
Connect power cable to a suitable facility outlet or terminal, according to the following electrical requirements.
Electrical requirements:
DP200 Single phase 100V AC 50/60Hz 7A DP300 Single phase 100V AC 50/60Hz 11A DP410 Single phase 200V AC 50/60Hz 11.5A DP610 Single phase 200V AC 50/60Hz 16A
Check the line voltage on outlet or terminal to be used and properly evaluate whether to utilize
a line being shared by other equipment. If the unit is not activated by turning on the main power switch (ELB), take an appropriate course of action, such as connecting the unit to a dedicated power source.
Multiple power cables connected to a single outlet may cause unit input voltage to drop,
resulting in degraded heating and temperature control performance.
Never operate unit with power cable bundled or tangled; and do not modifiy, bend, forcibly twist or pull on power cable. Doing so may cause fire and/or electrical shock.
Do not risk damage to power cable by positioning it under desks or chairs, or by pinching it between objects. Doing so may cause fire and/or electrical shock.
Do not place power cable near kerosene/electric heaters or other heat-generating devices. Doing so may cause power cable insulation to overheat, melt and/or catch fire, which may result in electric shock.
Turn off main power switch (ELB) immediately and disconnect from facility terminal or outlet, if power cable becomes partially severed or damaged in any way. Failure to do so may result in fire or electric shock. Contact a local dealer or Yamato sales office for information about replacing power cable if it is damaged.
Always connect power cable to appropriate facility outlet or terminal.
7. Connect to power supply.
8. Handle power cable with care.
2. PRE-OPERATION PROCEDURES
Installation Precautions & Procedures
6
Ground wire must be connected to a proper grounding line or teminal in order to avoid
electrical shock.
Never connect ground wire to gas lines or water pipes. Never connect ground wire to telephone grounding lines or lightening rods. Doing so may
result in fire or electric shock.
Never insert multiple plugs into a single outlet. Doing so may result in power cable
overheating, fire or drop in voltage.
Connect to grounded outlet.
Outlet with ground receptacle When no grounding terminal is found:
Grounding to Electrical Equipment Technical
Standards, Section 19, class D (Grounding
Resistance Max. 100Ω) is required in Japan.
Contact a local dealer, electrician, or Yamato Sales office for location-specific electrical requirements.
Use grounded adapter for ungrounded outlets.
Outlet with no ground receptacle Ground adapter
Insert grounded power plug into ground
adapter. Connect grounding wire (green) from ground adapter to a ground terminal.
Grounding to Electrical Equipment Technical Standards, Section 19, class D (Grounding
Resistance Max. 100Ω) is required in Japan where no grounding terminal is provided. Contact a local dealer, electrician, or Yamato Sales office for location-specific electrical requirements.
Connect terminals securely to facility terminal or to an appropriate connector.
Plugs and connectors are not included with this unit. Ground unit properly to facility outlet or terminal as required.
Never connect ground wire to gas lines, water pipes, telephone grounding lines or lightening rods. Doing so may result in fire or electrical shock.
Confim that the facility main breaker is OFF before connecting the round terminals from the power cable. No power plugs or connectors of any kind are included with DP410/610. Where required, purchase an appropriate plug and properly connect using the round terminals.
Wire color
Terminal
Black
Live side
White
Neutral side
Green
Ground
Ungrounded outlet 100V AC only
Ground adapter
Grounded plug
Grounding wire
with Y-terminal
W
G Grounded plug
3 (three) Round Terminals for M5 screws
Green (to grounding terminal)
Black (to facility terminal)
White (to facility terminal)
Grounding prong
2. PRE-OPERATION PROCEDURES
Installation Precautions & Procedures
9.(1) Ground wire MUST be connected properly (DP200/300 at 100V AC).
9.(2) Ground wire MUST be connected properly (DP410/610 220V AC).
10. Observe wire color designation when connecting to facility terminal (DP410/610 200V AC) See table below.
7
11. DO NOT disassemble or modify.
Attempting to disassemble or modifiy this unit in any way may result in malfunction, fire or electric shock.
Position the 2 (two) adjustable leveling feet, located on the undercarriage of DP410/610 units.
After unit is installed, position the adjustable leveling feet using the following procedure: Rotate leveling feet down until unit stands
securely on the floor.
Check for any gaps between the floor and
4 (four) contact points (e.g. the 2 ‘two’ front leveling feet and the 2 ‘two’ rear
casters).
Once unit is secure, tighten both leveling
feet stop nuts firmly against the topmost nut, to prevent leveling feet from turning under vibration.
2. PRE-OPERATION PROCEDURES
Installation Precautions & Procedures
12. Position adjustable leveling feet (DP410/DP610 only).
8
Item
Model (Pump Connection Port Size)
Manufacturer
or Supplier
Vacuum
Pump
Model
(sold
separately)
Effective
Pump
Displacement
(at 50/60Hz) in litters/min.
Pump
Inlet Size
Required vacuum line components
DP200/300 (Pump connection port
18mm)
Yamato Science
PD53*1
50/60
18 mm
15 mm ID vacuum hose
Qty 1
PX52*1
PD103
100/120
27 mm
15 mm ID vacuum hose 25 mm ID vacuum hose Reducing pipe(18/27)
A(Brass)/C(Stainless St.)
Qty 1 Qty 1 Qty 1
PD138*1
135/162
PX137*1
135/162
30 mm
DP410/610 (Pump
connection port
NW25
flange)
Yamato
Science
PD138
*1
135/162
27 mm
25 mm ID vacuum hose Vacuum hose adapter Clamp (NE20/25) Center ring (NW25)
Qty 1 Qty 1 Qty 1 Qty 1
PD203*1
200/240
PX137
135/162
30 mm
PX202
200/240
Adixen
M(T)2010
142/170
NW25
flange
Flexible hose Clamp (NW20/25) Center ring (NW25)
Qty 1 Qty 2 Qty 2
M(T)2015
208/250
M(T)2010C
142/170
M(T)2015C
208/250
Kashiyama
NeoDry15E
250
NW25
flange
Flexible hose Clamp (NW20/25) Center ring (NW25)
Qty 1 Qty 2 Qty2
2. PRE-OPERATION PROCEDURES
Vacuum System Information
Vacuum System Information Vacuum pumps and vacuum line components (sold separately) for DP series ovens
(1) Vacuum pump models and vacuum line components (sold separately), required for DP series
ovens, are shown in Table 2.1. Select an appropriate vacuum pump and vacuum line components (sold separately) using the table below. Note that an appropriate check valve must also be selected for vacuum pumps (sold separately). Vacuum line components are also offered as options and available upon request.
Table 2.1 Vacuum pump models and required line components (sold separately) for DP series ovens
Note
*1 These pump models can be fitted with components for the KF-style quick-coupling flange, as on
all Adixen pump models.
If an existing vacuum pump is to be connected to a new DP series unit, and their inlet sizes do not
match, use an appropriate reducing joint.
(2) Be sure to use the proper vacuum line components between vacuum pump (sold separately) and
DP series unit to prevent any vacuum leaks.
(3) If an existing pump cabinet is to be used for a new vacuum pump (sold separately) installation on
DP models 410/610, be sure to place the vacuum pump (sold separately) inside of the cabinet so that the oil gauge faces front and can be easily viewed and regularly inspected.
9
φ18mm OD
DP200/DP300 pump connection port
Reducing joint A(Brass) or C(Stailess St.)
Vacuum hose(φ15mm ID )
Vacuum hose (φ25mm ID)
DP410/610 pump connection port
NW25 flange
Clamp
Clamp
Center ring
Center ring
Vacuum hose adapter
Flexible hose
Vacuum hose (φ25mm ID)
Connection port sizeφ30mm, φ27mm
Connection port sizeφ30mm, φ27mm
Connection port size NW25 flange
Clamp
Center ring
Rotary Vacuum Pump PD138/203, PX137/202 etc.
Rotary Vacuum Pump KF25 quick-coupling specifications for M(T)2010/2015/2021, PD/PX etc.
(Note)
components inside broken line are optional
Air-cooled Dry Vacuum Pump NeoDry 15E
2. PRE-OPERATION PROCEDURES
Vacuum System Information
Vacuum System Information Vacumm pump and vacuum line components (sold separately) for DP series ovens
10
Control Panel
Independent
Overheati
Door Handle
Viewing Window
Vacuum Gauge
Pump Valve Knob
(closes with CW rotation)
Purge Valve Knob
(closes with CW rotation)
Caution-Rating Spec. sticker
Heat Vents
Terminal Block Cover (Terminal Block: option)
Main Power Switch (ELB) Legs
Serial No. sticker
Door
Heat Vents
Pump Port
Purge Port
Power Cable w/plug
3. COMPONENT NAMES AND FUNCTIONS
DP200/300 overview
Unit Overview 1
11
Round Terminals
Purge Port
Pump Port
N2 Gas Inlet
(optional)
4(four) Casters
Safety Cover (DP610 only)
Door
Viewing Window
Flow Meter
(option)
Pump Valve Knob
(closes with CW rotation)
Purge Valve
(closes with CW rotation)
Vacuum Pump Cabinet Door
Vacuum Pump
(sold separately)
Pump slide tray (optional)
Caution-Rating sticker
Serial No. sticker
Door Handle
Independent Overheat Prevention Device
Vacuum Gauge
Control Panel
Main Power Switch (ELB)
External Vacuum Pump Switch (optional)
Adjustable Leveling Feet (2 two’ on undercarriage)
Digital Pirani Vacuum Gauge (optional)
Memory Recorder (option)
Terminal Block
(optional)
Power Cable
(Round terminals)
DP410/610 overview
3. COMPONENT NAMES AND FUNCTIONS
Unit Overview 2
12
No
Name
Description
1
Upper Display
Readout for temperature reading (current chamber temp), error codes, etc.
2
Lower Display
Readout for temperature setting, clock, timer, etc.
3
Function Indicator Lamps
Illuminates (one or more) to show which function is currently running or active
4
Mode Indicator Lamps
Illuminates (only one) to show which mode is currently running.
5
REMOTE Indicator Lamp
Illuminates while remote comm (optional item) transmission is in progress.
6
ERROR Indicator Lamp
Illuminates when an error occurs.
7
OPERATE Indicator Lamp
Illuminates during operation. Flashes in operation standby mode.
8
HEATER Indicator Lamp
Illuminates when heaters are receiving power.
9
EVENT Indicator Lamp
Illuminates when event output (optional item) is transmitted.
10
FIXED TEMP Indicator
Lamp
Illuminates during constant temperature operation.
11
PROGRAM Indicator Lamp
Illuminates during programmed operation. Flashes while entering program settings.
12
AUTO START Indicator
Lamp
Illuminate during auto start operation.
13
AUTO STOP Indicator
Lamp
Illuminates during auto stop operation.
14
MODE key
Press to switch between operation modes, ⑩~⑬ on control panel.
15
POWER key
Press and hold to switch between unit idle and unit standby.
16
DISP key
Press to switch between monitoring options in lower display.
17
START/STOP key
Press to start or stop an operation.
18
MENU key
Press to switch between setting options.
19
Esc key
Press to return to previous menu without finalizing settings.
20
▲(Up) key
Press to increase setting value.
21
▼(Down) key
Press to decrease setting value.
22
key
Press to move cursor left.
23
ENTER key
Press to finalize setting items.
24
Independent Overheat
Prevention Device
Set device to keep unit from exceeding a certain temperature.
24
3. COMPONENT NAMES AND FUNCTIONS
Control Panel
13
4. OPERATION PROCEDURE
Prior Confirmation
(1) Power source and ground wire
Be sure to connect power cable to an appropriate power source and confirm that ground wire is connected.
(2) Main power switch (ELB)
Turn ELB ON. Test ELB function once a month or before extended operation. See Maintenance Procedures (P.43) for details. Check the lower display on the control panel when ELB is turned on and confirm it is showing current time.
(3) Independent Overheat Prevention Device (IOPD)
Be sure to set IOPD temperature 20ºC over the chamber temperature setting. Test IOPD function before each instance of extended operation. See Maintenance Procedures (P.43) for details.
(4) Vacuum line connection
Be sure to connect unit securely to vacuum pump (sold separately).
(5) Vacuum pump (sold separately)
Check vacuum pump oil level and be sure it is free of contamination.
Decompression/Purge Procedure
(1) Decompressing unit chamber
1. Close purge valve.
2. Close the pump valve.
3. Turn vacuum pump ON.
4. Open the pump valve. Note: open pump valve gradually when processing powdery or frothy test samples.
(2) Repressurizing unit chamber
1. Close pump valve.
2. Open purge valve to allow ambient pressure back into chamber.
3. Open Pump Valve.
4. Shut vacuum pump OFF.
Note: open purge valve gradually when processing powdery test samples.
14
The backup battery installed in DP series units, is a wear item and has an estimated life of approximately 5 years. Replacing battery within the 5-year lifespan is recommended.
Contact a local dealer or Yamato sales office to request a replacement battery. If unit has
program data in memory, make a data backup file before replacing backup battery. See Data Backup (P.35) in this section for details.
To set the current date & time,after replacing backup battery, follow the steps below.
1
Turn on power.
Turn ON the main power switch (ELB), located on the right panel of the DP series units. Lower display on the control panel will show the time. This indicates that the machine is in idle.
Press and hold to display the standby screen. Upper display shows current temperature in the chamber while lower display shows current temperature setting. This indicates that the machine is in standby.
2
Use the MENU key to view date and time in displays
Press repeatedly until FUNC appears in lower
display, then press .
When [bUZZ] is shown in the lower display, press
to view the year in upper display, and month/date in lower display.
is used to advance to next item is used to return to previous item
4. OPERATION PROCEDURE
Setting Date & Time
15
3
Set the date.
Setting the year/month/date and clock.
Year and month/date are shown on upper and lower
displays respectively.
Press . Settable value begins flashing.
Set calendar year with and . Press .
Set month/date with and . Press .
Press to change digit (flashing) positions.
4
Set the time.
Press .
Press and set current time with and
press .
Set time in conformance to the 24-hour time system (e.g. military time, continental time or railway time).
※Press to change digit (flashing) positions.
Press twice to return to initial screen when
time/date settings are completed.
1
Set keypad tone.
Press repeatedly until FUNC is shown, then
press to bring up bUZZ in lower display. Press
. oFF begins flashing in upper display.
Select one of three keypad tone modes using
and press .
on: Activates tone for all keys. (factory default). CLK: Activates tone for POWER and ENTER keys
only.
oFF: Deactivates tone for all keys.
Press the key twice to go back to initial screen
when keypad tone settings are completed.
4. OPERATION PROCEDURE
Setting Date & Time
Keypad Tone Function
16
Mode and Function Flow
4. OPERATION PROCEDURE
17
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