Teledyne GC-Pro-FID User Manual

INSTRUCTION, OPERATING AND
MAINTENANCE MANUAL FOR
GC-PRO FID
P/N M82956
DATE 3/28/13
Toxic and/or flammable gases or liquids may be present in this monitoring system. Personal protective equipment may be required when servicing this instrument. Hazardous voltages exist on certain components internally which may persist for
a time even after the power is turned off and disconnected. Only authorized personnel should conduct maintenance and/or servicing. Before
conducting any maintenance or servicing, consult with authorized supervisor/manager.
Teledyne Analytical Instruments
DANGER
GC-Pro FID
Copyright © 2013 Teledyne Analytical Instruments
All Rights Reserved. No part of this manual may be reproduced, transmitted, transcribed, stored in a retrieval system, or translated into any other language or computer language in whole or in part, in any form or by any means, whether it be electronic, mechanical, magnetic, optical, manual, or otherwise, without the prior written consent of Teledyne Analytical Instruments, 16830 Chestnut Street, City of Industry, CA 91748.
Warranty
This equipment is sold subject to the mutual agreement that it is warranted by us free from defects of material and of construction, and that our liability shall be limited to replacing or repairing at our factory (without charge, except for transportation), or at customer plant at our option, any material or construction in which defects become apparent within one year from the date of shipment, except in cases where quotations or acknowledgements provide for a shorter period. Components manufactured by others bear the warranty of their manufacturer. This warranty does not cover defects caused by wear, accident, misuse, neglect or repairs other than those performed by Teledyne or an authorized service center. We assume no liability for direct or indirect damages of any kind and the purchaser by the acceptance of the equipment will assume all liability for any damage which may result from its use or misuse.
We reserve the right to employ any suitable material in the manufacture of our apparatus, and to make any alterations in the dimensions, shape or weight of any parts, in so far as such alterations do not adversely affect our warranty.
Important Notice
This instrument provides measurement readings to its user, and serves as a tool by which valuable data can be gathered. The information provided by the instrument may assist the user in eliminating potential hazards caused by his process; however, it is essential that all personnel involved in the use of the instrument or its interface be properly trained in the process being measured, as well as all instrumentation related to it.
The safety of personnel is ultimately the responsibility of those who control process conditions. While this instrument may be able to provide early warning of imminent danger, it has no control over process conditions, and it can be misused. In particular, any alarm or control systems installed must be tested and understood, both as to how they operate and as to how they can be defeated. Any safeguards required such as locks, labels, or redundancy, must be provided by the user or specifically requested of Teledyne at the time the order is placed.
Therefore, the purchaser must be aware of the hazardous process conditions. The purchaser is responsible for the training of personnel, for providing hazard warning methods and instrumentation per the appropriate standards, and for ensuring that hazard warning devices and instrumentation are maintained and operated properly.
Teledyne Analytical Instruments, the manufacturer of this instrument, cannot accept responsibility for conditions beyond its knowledge and control. No statement expressed or implied by this document or any information disseminated by the manufacturer or its agents, is to be construed as a warranty of adequate safety control under the user’s process conditions.
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Safety Messages
Your safety and the safety of others are very important. We have provided many important safety messages in this manual. Please read these messages carefully.
A safety message alerts you to potential hazards that could hurt you or others. Each safety message is associated with a safety alert symbol. These symbols are found in the manual and inside the instrument. The definition of these symbols is described below:
GENERAL WARNING/CAUTION: Refer to the
instructions for details on the specific danger. These cautions warn of specific procedures which if not followed could cause bodily Injury and/or damage the instrument.
No
Symbol
CAUTION: HOT SURFACE WARNING: This warning is
specific to heated components within the instrument. Failure to heed the warning could result in serious burns to skin and underlying tissue.
WARNING: ELECTRICAL SHOCK HAZARD: Dangerous
voltages appear within this instrument. This warning is specific to an electrical hazard existing at or nearby the component or procedure under discussion. Failure to heed this warning could result in injury and/or death from electrocution.
Technician Symbol: All operations marked with this
symbol are to be performed by qualified maintenance personnel only.
NOTE: Additional information and comments regarding
a specific component or procedure are highlighted in the form of a note.
STAND-BY: This symbol indicates that the instrument is
on Stand-by but circuits are active.
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CAUTION: THE ANALYZER SHOULD ONLY BE USED FOR THE
PURPOSE AND IN THE MANNER DESCRIBED IN THIS MANUAL.
IF YOU USE THE ANALYZER IN A MANNER OTHER THAN THAT FOR WHICH IT WAS INTENDED, UNPREDICTABLE BEHAVIOR COULD RESULT POSSIBLY ACCOMPANIED WITH HAZARDOUS CONSEQUENCES.
This manual provides information designed to guide you through the installation, calibration and operation of your new analyzer. Please read this manual and keep it available.
Occasionally, some instruments are customized for a particular application or features and/or options added per customer requests. Please check the front of this manual for any additional information in the form of an Addendum which discusses specific information, procedures, cautions and warnings that may be specific to your instrument.
Manuals do get misplaced. Additional manuals can be obtained from Teledyne at the address given in the Appendix. Some of our manuals are available in electronic form via the internet. Please visit our website at: www.teledyne-ai.com.
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Additional Safety Information
DANGER
COMBUSTIBLE GAS USAGE
This is a general purpose instrument designed for use in a non-hazardous area. It is the customer's responsibility to ensure safety especially when combustible gases are being analyzed since the potential of gas leaks always exist.
WARNING
The customer should ensure that the principles of operating of this equipment are well understood by the user. Misuse of this product in any manner, tampering with its components, or unauthorized substitution of any component may adversely affect the safety of this instrument.
Since the use of this instrument is beyond the control of Teledyne, no responsibility by Teledyne, its affiliates, and agents for damage or injury from misuse or neglect of this equipment is implied or assumed.
WARNING: HYDROGEN GAS IS USED IN THIS INSTRUMENT AS
A FUEL. HYDROGEN IS EXTREMELY FLAMMABLE. EXTREME CARE MUST BE USED WHEN WORKING AROUND GAS MIXTURES CONTAINING FLAMMABLE GASES.
A successful leak check was performed at TAI on the sample system of this instrument prior to calibration, testing and shipping. Ensure that there are no leaks in the fuel supply lines before applying power to the system.
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Always purge the entire system before performing any maintenance and always leak check the system after removing any tubing or fittings on the sample system. See the procedures for purging and leak checking this instrument on the following pages.
If toxic gases or other hazardous materials are introduced into the sample system, the same precautions regarding leak checking and purging apply to the sample lines and sample supply or delivery lines.
WARNING: ELECTRICAL SHOCK HAZARD.
WITH THE EXCEPTION OF OPENING THE DOOR AND ADJUSTING THE PRESSURE REGULATORS, FLOW CONTROLLER, OR OBSERVING THE PRESSURE GAUGES AND THE FLOWMETER, ONLY AUTHORIZED AND SUITABLY TRAINED PERSONNEL SHOULD PERFORM WORK INSIDE OF THE INSTRUMENT. COMPONENTS WITHIN THE COVER ON THE INSIDE OF THE DOOR, INSIDE THE ISOTHERMAL CHAMBER (SAMPLE SYSTEM), AND ON THE ELECTROMETER-AMPLIFIER PC BOARD CONTAIN DANGEROUSLY HIGH VOLTAGE SUFFICIENT TO CAUSE SERIOUS INJURY OR DEATH.
There are the following three types of inaccessible
shock hazards within the Analyzer:
1. Line voltages and line related voltages such as 115 VAC which exists within the 230 VAC versions as well. These voltages stop when the Analyzer is turned off and the mains (line) cord is removed from the instrument.
2. The sensor anode supply voltage (approximately 250 VDC). This voltage exists on the Flame Guard, anode power supply, PCB, the motherboard, and the anode/igniter terminals on the sensor. THIS VOLTAGE WILL REMAIN HAZARDOUS FOR MANY MINUTES AFTER THE ANALYZER HAS BEEN TURNED OFF!
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3. External hazardous voltages which may be connected to the Analyzer alarm relay connections.
Procedure for Removal of Internal Inaccessible Shock Hazards
CAUTION: SERVICING OR MAINTENANCE OF THE ANALYZER
SHOULD ONLY BE DONE BY SUITABLE TRAINED PERSONNEL. TO AVOID THESE INACCESSIBLE
1. Switch off the power to the Analyzer and remove the main (line)
power cord from the Analyzer.
HAZARDOUS VOLTAGES WHEN SERVICING THE GC-PRO FID, PERFORM EACH OF THE FOLLOWING STEPS, IN THE ORDER GIVEN, BEFORE SERVICING BEGINS:
2. Remove all external voltages from the connections to the alarm
contacts.
3. Wait one minute.
4. Discharge the anode supply voltage. a. Connect one end of an insulated (to 1000 VDC or more)
clip lead to Analyzer chassis ground (the standoff for the upper right corner of the mother PCB).
b. Put one end of a 500V rated 1000 ohm resistor in the
other end of the clip lead.
c. Check the voltage between chassis ground (the standoff
for the upper right corner of the mother PCB) and the top side of R2 at PCB number B74671. It should be between
-5VDC and +5VDC. If is in that range, the inaccessible hazardous voltage removal procedure is completed, if not repeat steps 4.a and 4.b.
If it is absolutely necessary to work inside the instrument with power
on, use the ONE HAND RULE:
Work with one hand only.
Keep the other hand free without contacting any other object. This reduces the possibility of a ground path through the body in case of accidental contact with hazardous voltages.
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WARNING: THIS INSTRUMENT IS DESIGNED TO BE OPERATED
IN A NONHAZARDOUS AREA. THE ANALYZER USES HYDROGEN GAS AND/OR OTHER COMBUSTIBLE GASES IN ITS OPERATION. THIS EQUIPMENT, IF NOT USED AND MAINTAINED PROPERLY CAN BE AN EXPLOSION HAZARD. THE ANALYZER, DEPENDING ON THE APPLICATION, MAY ALSO USE TOXIC GASES. IT IS THEREFORE, THE CUSTOMER'S RESPONSIBILITY TO ENSURE THAT PROPER TRAINING AND UNDERSTANDING OF THE PRINCIPLES OF OPERATION OF THIS EQUIPMENT ARE UNDERSTOOD BY THE USER. SINCE THE USE OF THIS INSTRUMENT IS BEYOND THE CONTROL OF TELEDYNE, NO RESPONSIBILITY BY TELEDYNE, ITS AFFILIATES AND AGENTS FOR DAMAGE OR INJURY RESULTING FROM MISUSE OR NEGLECT OF THIS INSTRUMENT IS IMPLIED OR ASSUMED. MISUSE OF THIS PRODUCT IN ANY MANNER, TAMPERING WITH ITS COMPONENTS OR UNAUTHORIZED SUBSTITUTION OF ANY COMPONENT MAY ADVERSELY AFFECT THE SAFETY OF THIS INSTRUMENT.
CAUTION: WHEN OPERATING THIS INSTRUMENT, THE DOORS
MUST BE CLOSED AND ALL COVERS SECURELY FASTENED. THE GAUGES MUST BE IN PROPER WORKING ORDER. DO NOT OVERPRESSURIZE THE SYSTEM.
READ THIS MANUAL BEFORE OPERATING THE
INSTRUMENT AND ADHERE TO ALL WARNINGS INCLUDED IN THIS MANUAL.
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Table of Contents
Safety Messages .......................................................................... iii
Additional Safety Information ...................................................... v
List of Figures ............................................................................. xiii
List of Tables .............................................................................. xiv
Introduction ................................................................................... 1
1.1 Main Features of the Analyzer 1
1.2 Principle of Operation 2
1.3 Analyzer Description 3
1.4 Applications 6
Operational Theory ....................................................................... 7
2.1 Introduction 7
2.2 Modes of Operation 8
2.3 Analyzer Subsystems 8
2.3.1 Sample System 9
2.3.2 Gas Flow Control System 9
2.3.3 Fuel and Blanket Air Systems 10
2.3.4 Flame Ionization Detection Cell 10
2.4 Detection Cell 12
2.4.1 Electrometer-Amplifier 13
2.4.2 Anode Power Supply 14
2.4.3 Flame Guard Circuit 14
2.4.4 Flame Ignition Circuit 14
Installation ................................................................................... 15
3.1 Unpacking the Analyzer 15
3.2 Mounting the Analyzer 15
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3.3 User Connections 16
3.3.1 Electrical Power Connections 16
3.3.2 Electronic Connections 16
3.3.2.1 Primary Input Power 17
3.3.2.2 Fuse Installation 18
3.3.2.3 50-Pin Equipment Interface Connector 18
3.3.2.4 Analog Output 18
3.3.2.5 Alarm Relays 20
3.3.2.6 Digital Remote Cal Inputs 22
3.3.2.7 ‘Measure Once’ (or one shot measurement) contacts 23
3.3.2.9 Pin Out Table 23
3.3.2.10 RS-232 Port 26
3.3.3 Gas Connections 27
3.3.3.1 Effluent 29
3.3.3.2 Sample Bypass Vent 29
3.3.3.3 Fuel and Air Connections 30
3.3.3.4 Sample and Span Gas Connections 30
3.4 Placing the System in Operation 30
Operation ..................................................................................... 31
4.1 Equipment 32
4.2 Preliminary Power-Off Check List 33
4.3 Powering Up the Unit 33
4.4 Activating the Support Gases 35
4.4.1 Air 35
4.4.2 Carrier Gas 36
4.4.3 Span Gas 36
4.4.4 Fuel 36
4.5 Sample Pump 36
4.6 Flame Ignition 36
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4.6.1 Verification of the Flame Guard Circuit 39
4.6.2 Ignition and/or Flame Guard Circuit Failure 40
4.7 Analyzer Operation 40
4.7.1 Default Parameters 41
4.7.2 The HOME Screen 41
4.7.3 The MENU Screen 43
4.7.4 Standby 44
4.7.5 Overlay Chromatogram 45
4.7.6 Timing 47
4.7.7 Temperature 51
4.7.7.1 Thermocouple 52
4.7.7.2 Settings 53
4.7.7.3 PID Settings 53
4.7.7.4 Status 55
4.7.8 Group Setup 55
4.7.9 Analog Adjust 59
4.7.10 Calibration 60
4.7.10.1 Span 61
4.7.10.2 Alt Span 63
4.7.10.3 Auto cal 66
4.7.11 Self Test 67
4.7.12 Settings 69
4.7.12.1 Alarms 70
4.7.12.2 Range 73
4.7.12.3 Change Stream 74
4.7.12.4 Time 75
4.7.12.5 Password 76
4.7.12.6 Communication 77
4.7.13 Analysis Mode 79
4.7.13.1 T-Time 80
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4.7.13.2 T_Cycle 81
4.7.13.3 Chromatogram 82
4.7.13.4 VS Count 83
4.7.13.5 Cold Boot 83
Maintenance & Troubleshooting ................................................ 87
5.1 Measuring Circuit Electrical Checks 88
5.1.1 Anode Voltage Check 88
5.1.2 Electronic Stability 89
5.1.3 Printed Circuit Board Replacement 89
5.1.4 Collector Cable 90
5.2 Temperature Control Electronic Check 90
5.3 Ignition and/or Flame Guard Circuit Checks 91
5.4 Sampling System 92
5.5 Printed Circuit Board Descriptions 93
5.5.1 Flame Guard and Anode Power Supply PCB 93
5.5.2 Proportional Temperature Controller PCB 94
5.5.3 Electrometer-Amplifier PCB 95
Appendix ...................................................................................... 97
A.1 Specifications and Initial Settings: 97 A.2 Recommended Spare Parts List 98 A.3 Drawing List 99
Appendix B ................................................................................ 101
B1. VNC for GC-Pro FID 101
Appendix C ................................................................................ 107
C1 Addendum and Testing Results 107
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List of Figures
Figure 1-1: GP-Pro Front Panel ....................................................... 3
Figure 1-2: GC-Pro FID Rear Panel ................................................ 4
Figure 1-3: Internal PCB Arrangement ............................................ 5
Figure 1-4: GC-Pro FID Internal View ............................................. 6
Figure 2-1: Internal Temperature Controller Screens ...................... 9
Figure 2-2: Typical Piping Diagram for the GC-Pro FID Analyzer . 11
Figure 2-4: Onscreen Re-Ignition Button ....................................... 14
Figure 3-1: GC-Pro FID Electronic Connections ............................ 17
Figure 3-2: Equipment Interface Connector Pin Arrangement ....... 18
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List of Tables
Table 3-1: Analog Output Connections — Middle Connector ........ 19
Table 3-2: Analog Concentration Output—Example ..................... 20
Table 3-4: Alarm Relay Contact Pins — Top Connector ............... 21
Table 3-5: Remote Calibration Connections — Bottom Connector 22
Table 3-6: ‘Measure Once’ Relay Connections ............................. 23
Table 3-7: Pin out of Alarm Relay O/P (Top) 50 pin D-Sub
Connector .................................................................... 24
Table 3-8: Pin out of Analog Signal (Middle) 50 pin D-Sub
Connector .................................................................... 24
Table 3-9: Pin out of Standard (Bottom) 50 pin D-Sub Connectors25
Table 3-10: Commands via RS-232 Input ..................................... 26
Table 3-11: Required RS-232 Options .......................................... 26
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GC-Pro FID Introduction
Introduction
The GC-Pro FID Analyzer is a microprocessor controlled digital instrument incorporating a Flame Ionization Detector (FID) coupled with a gas separation column and switching valve designed to measure the quantity of aromatic hydrocarbons present in a positive pressure sample gas. Up to 8 channels of output are present for measuring specific analytes in a sample stream. Unlike other benzene or hydrocarbon analyzers, the GC-Pro FID Analyzer expands its diagnostic capabilities to look for other aromatics, like toluene, ethyl benzene, xylenes and other separable species. The GC-Pro FID Analyzer has multiple channels for measurement with enhanced versatility and capabilities. Due to its flexibility, it is vitally important that you refer to Appendix C for the specific factory setup for your application.
The GC-Pro FID features a modern user interface with a touch screen front panel facilitating operation, calibration, data collection and display. With the Ethernet connectivity feature, this new interface allows the instrument to be operated remotely with a VNC software application from another digital device whereby the analyzer can be accessed, controlled, data displayed etc. as if the analyzer were physically present.
Although the analyzer arrives already setup for your specific application, a gas chromatograph mode allows the user to program the instrument for measuring different species present in the sample.
1.1 Main Features of the Analyzer
The GC-Pro FID Analyzer is sophisticated yet simple to use. A touch screen display on the front panel provides access all phases of setup, calibration, operation, and troubleshooting on the GC-Pro FID.
The main features of the analyzer include:
Data acquisition and control functions supporting:
Pressure measurements, 5-Channels Flow (MFC) measurements, 3-Channels Oxygen measurements, 6-Channels
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Temperature measurements and control, 4-Channels 6-Channel Dew point Hygrometer measurements, 6-
Channel
Relay, (10) and solenoid outputs, (4) Alarm, (3) and over range indication outputs, (4) 4-20mA current loop outputs, 10 channels HMI through Maple touch sensitive display
The system operates at single phase AC, 110 or 220V 50/60
Hz.
High resolution, accurate readings of concentration. Versatile analysis with three user-definable analysis ranges. Microprocessor based electronics: 8-bit CMOS
microprocessor with 32 kB RAM and 128 kB ROM.
Auto ranging allows analyzer to automatically select the
proper preset range for a given measurement. Manual override allows the user to lock onto a specific range of interest.
Two adjustable concentration alarms and a system failure
alarm.
Extensive self-diagnostic testing at startup and on demand
with continuous power supply monitoring.
RS-232 serial digital port for use with a computer or other
digital communication device.
8-Analog outputs for concentration and range identification
(0-1 VDC standard and isolated 4-20 mA dc).
Superior Accuracy
1.2 Principle of Operation
The analyzer uses a gas separation column to separate the component of interest, for instance, benzene, from the other hydrocarbons in the sample gas. Using a carrier gas and a microprocessor actuated switching valve, the eluted gas is analyzed in
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GC-Pro FID Introduction
Flame Ionization Detector (FID) and the column is back flushed to accept the fresh sample for the next cycle. More information is provided
in Section 2.1 Introduction, under Operational Theory. The electrical
output of the electrometer-amplifier is directly proportional to the concentrations of the ionizable hydrocarbons present over the ranges of interest.
1.3 Analyzer Description
The standard analyzer is a rack mountable instrument designed to fit into a standard 19” instrument rack. The front interface screen is mounted on the left side of the panel. The right side of the panel includes the gas controls, pressure gauges and flowmeter. The front panel is shown in Figure 1-1.
Figure 1-1: GP-Pro Front Panel
Gas pressure gauges and controls are mounted on the front panel adjacent to the touch screen (human/machine interface abbreviated as HMI) display as shown in Figure 1-1.
At the rear of the instrument are ports for the introduction of air, fuel, zero, span, and sample gas as well as vent port connections. Three 50-pin user-interface cable connectors route input/output and alarm signals to external devices. RS232 and a network port are also available
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at the rear panel for connection to a remote computer or other digital communication device. Internally, there are two USB user connections which are used for updating firmware to the PCBs. Figure 1-2 shows the rear panel including the user connections for the standard instrument without the auto calibration manifold.
The analyzer is set up for either 120 VAC 60 Hz or 230 50/60 Hz operation depending on the customer’s requirements. The appropriate power cord for your unit is included with the analyzer.
Figure 1-2: GC-Pro FID Rear Panel
Internally, there are three isothermal chambers each separately controlled for precise control and separation of analyzed species. In the electronics section, internal PC boards are stacked in an assembly in an order based on inter connectivity needs between the PCBs as well as their association with other sub assemblies distributed within the system. See Figure 1-3.
Following is the card stack-up from top to bottom planned inside the system
Heater card 9261 controller card
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GC-Pro FID Introduction
Analog data acquisition card Analog signal conditioning card 89C5131 controller card
Figure 1-3: Internal PCB Arrangement
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Introduction GC-Pro FID
Figure 1-4: GC-Pro FID Internal View
1.4 Applications
Monitoring the benzene concentration of carbon dioxide gas
for use in the beverage industry.
Monitoring aromatic contamination in air liquefaction and
other gas production processes.
Gas purity certification. Detecting trace benzene in ambient air. Detecting atmospheric pollutants.
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Operational Theory
2.1 Introduction
The GC-Pro FID Analyzer uses a Flame Ionization Detector (FID) and a Gas Chromatograph (GC) Column to separate and analyze different factions of a volatile hydrocarbon sample. Using a carrier gas and a microprocessor actuated switching valve, a fixed volume of sample is pushed into the Column maintained at a constant temperature. The eluted gas is analyzed for benzene or other specific analyate configured for your specific application in a FID detector and the column is back flushed to accept the fresh sample for the next cycle. Actual separating and detecting sequence may vary depending on compounds of interest in the application for which the analyzer is configured.
The Flame Ionization Detector was selected for use in the GC-Pro FID Analyzer based on the positive performance and extensive experience in the use of this detector in other Teledyne analyzers. The FID has proven itself to be a rugged, stable, long life sensor giving years of trouble free operation in various applications. Also considering the fact that the required sensitivity of 100 ppb full scale was achieved, FID was considered a better choice over the limited life and less reliable Photo Ionization Detector.
A stainless steel packed column containing Chromosorb Diatomite is used at a constant temperature of 70°C. Using nitrogen as a carrier gas and a 5 ml sample loop, benzene elutes from the column within a few minutes. Additionally, a clear separation is observed from other aromatic hydrocarbons, namely toluene, ethyl benzene, and xylenes. The actual temperature setpoint and compound separation for your instrument may be different depending on the application. It is listed in
the Addendum and Testing Results section of Appendix C.
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2.2 Modes of Operation
The analyzer has 2 modes of operation depending on the position of the GC Sampling Valve (See Piping Diagram in Figure 2-2). They are: Sample Mode (position A) and Analysis Mode (position B).
1. Valve Position A—Sampling Mode
In this mode the analyzer configures the operational valve to back flush the column and charge the sample loop. The Sample Mode is programmed to continue for a 7 minute period by factory default; however, it is usually modified to match the needs of a particular process. The specific timing interval for
your system is listed in the Addendum and Testing Results
section of Appendix C. It is possible to set the Sample Mode duration up to 25 minutes.
2. Valve Position B—Analysis Mode
In this mode the analyzer configures the sampling valve to feed the gas in the sample loop through the column and to the detector. The eluted sample from the column is fed to the FID for the analysis of the compound of interest in the hydrocarbon stream. If configured to do so, the analyzer may read the detector for a programmed 5 second period at some point within this mode cycle to obtain a baseline reading for further calculation. This mode is usually programmed to continue until the compound of interest is fully eluted from the column. It is possible to set it up to 25 minutes.
During the Analysis Mode, a ‘Peak Detect’ period is programmed at which time the analyzer reads the detector output. The analyzer integrates the peak area during this time in conjunction with the baseline settings to calculate the concentration of the compound of interest. The calculation is performed at the end of the ‘Peak Detector’ period and the result is displayed at the end of Analysis Mode.
2.3 Analyzer Subsystems
The Model Analyzer is composed of three subsystems:
1. Sample System
2. Detector Cell
3. Electronic Signal Processing, Display and Control
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2.3.1 Sample System
All components used to control the sample and supporting gases, as well as the combustion portion of the detector cell, are located inside the analyzer chassis. They are accessible by opening the front door of the analyzer.
Adjustments are made using the appropriate control on the front panel.
The analyzer contains three separate isothermal chambers ‘SAMPLE’, ‘FID’, and ‘COLUMN’ that are controlled by internal temperature control PCBs. The temperature can be monitored and controlled using the touch screen main menu item ‘Temperature’. See Figure 2-1 and Section 4.7.7.
Figure 2-1: Internal Temperature Controller Screens
The sample chamber contains the 10-port GC switching valve and 2 sample loops. The ‘FID’ chamber contains the flame, pressure regulators, pressure gauges and flow restrictors used by the FID detector. The ‘COLUMN’ is housed in a separate ‘COLUMN’ enclosure and maintained at a temperature of 70° C by its PID temperature controller. The actual temperature setpoint for your instrument may be
different depending on the application. It is listed in the Addendum and Testing Results section of Appendix C.
2.3.2 Gas Flow Control System
The analyzer is equipped with ports for the introduction of air, fuel, carrier gas, span, and sample gas. It is imperative that these gases are supplied at constant pressures using two stage stainless steel diaphragm gas regulators. The recommended pressure range is 30 to 80 psig; however, the span gas should be supplied at a pressure of 20 psig to the restrictor fitting either on the optional auto calibration module or the span inlet on the rear panel.
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The Piping Diagram for the standard instrument is shown in Figure 2-2. A 10-port 2-position GC sampling valve is used to control and direct gas flows including sampling, back flush, and carrier gas. The fixed volume sample loop ensures the same volume of sample injection in the column every cycle.
If your instrument is fitted with the optional auto calibration module, a separate compartment containing of a pair of solenoid valves is installed for controlling the introduction of sample or span gas to the detector. Calibration can be performed automatically on a programmed schedule or manually using the front panel interface.
2.3.3 Fuel and Blanket Air Systems
Stable flow is achieved by maintaining a constant pressure across restrictors upstream from the cell. Each system incorporates an adjustable pressure regulator, pressure gauge, and restrictor. A flame out light is included to indicate when the flame fails. A fuel shut-off solenoid valve, mounted on the line that supplies fuel, stops the fuel flow in case of flame failure. This valve is located in line with the fuel port.
2.3.4 Flame Ionization Detection Cell
The carrier gas containing sample and fuel are combined within a tee fitting located in the isothermal chamber. The mixed gas is emitted from a burner within the sensor assembly. Blanket air is introduced into the sensor (or cell) by means of a separate fitting that is located in the base section of the assembly. The upper half of the assembly houses the anode-igniter, collector, and flame guard thermistor.
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Figure 2-2: Typical Piping Diagram for the GC-Pro FID Analyzer
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2.4 Detection Cell
The upper section of the stainless steel flame ionization cell houses the cylindrical collector electrode, the high voltage (+260 VDC) anode­igniter coil, and the sensing thermistor of the flame guard circuit (see cell cross-section in Figure 2-3).
WARNING: DANGEROUS HIGH VOLTAGE EXISTS AT THE
ANODE IGNITER COIL (+260 VDC). DO NOT ATTEMPT TO DISCONNECT THE IGNITER COIL CABLE OR DISASSEMBLE ANY OF THE FLAME IONIZATION CELL COMPONENTS WITHOUT TURNING OFF THE POWER AND DISCONNECTING THE POWER CORD.
The collector is interconnected with the electrometer-amplifier PC board by a coaxial cable. Although the cable and fittings are intended for coaxial service, the cable is actually being used as a shielded single­conductor connection.
The anode-igniter, as its name implies, serves two functions. When relay K2 at PCB part number B74671 is energized, the coil becomes an electrical heating element that glows red-hot and ignites the hydrogen fuel. When relay K2 at B74671 is de-energized, the coil is connected to the +260 volt DC terminal of the anode-flame guard power supply PC board. In this configuration, the necessary potential difference is established between the coil (anode) and collector to promote ionization of the burned hydrocarbons. The coil functions as the high voltage anode in all three-range positions of the selector switch.
The thermistor acts as the sensor in the flame guard circuit. Its ambient temperature resistance is in the 100 K ohms region. When the flame is ignited, its resistance is reduced by a factor of 100. The thermistor is coupled to a semiconductor control circuit on the anode­flame guard power supply PC board, which will be described in a following section.
The cell electrodes of both the anode-igniter and flame guard thermistor are connected to the electronics chassis by means of a plug-in cable.
The electrode section of the cell may be removed for inspection by turning off the power, disconnecting the electrode lead plug, and removing the screws, which retain the electrode assembly in the sensor body.
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2.4.1 Electrometer-Amplifier
The collector cable is coupled directly to a coaxial fitting located on the electrometer-amplifier PC board. The PC board is located on the side panel next to but outside of the isothermal chamber. It consists of an electrometer amplifier and an operational amplifier. This circuit is a very high-gain, current-to-voltage converter circuit, having an input impedance measuring in the billions of ohms. It is static sensitive and highly susceptible to contamination. Special care must be taken in handling this PC board.
Refer to Section 5.5.3: Electrometer-Amplifier PC Board for more
information concerning the electrometer-amplifier and the other printed circuits that follow.
Figure 2-3: Flame Ionization Cell
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2.4.2 Anode Power Supply
The high voltage anode power supply components are mounted on the anode power supply printed circuit board. High voltage regulation is achieved through the use of series-connected zener diodes. The simplicity of this circuit’s design can be attributed to the extremely low current demand of the anode circuit. The positive output voltage is nominally 125 volts. Output tolerance is ±10 volts from the specified 125 volts.
2.4.3 Flame Guard Circuit
A thermistor-controlled, transistorized switching circuit is employed to operate a relay in the event of a flame-out condition. A panel indicator light and fuel shut-off solenoid valve are operated by the relay to alarm personnel that a flame-out condition has occurred. The fuel shut-off solenoid valve stops the hydrogen flow.
2.4.4 Flame Ignition Circuit
The flame ignition circuit includes the anode-igniter electrode (in the detector cell), a transformer, and processor controlled relay. The circuit is automatically energized when the FID cools due to lack of flame.
If automatic ignition fails five times, there will be a message that reports this, and the flame can be re-ignited by pressing the re-ignite icon from the touch screen. See Figure 2-4 and Section 4.6.
Figure 2-4: Onscreen Re-Ignition Button
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Installation
Installation of the GC-Pro FID Analyzer includes:
1. Unpacking
2. Mounting
3. Gas connections
4. Electrical connections
5. Testing the system.
3.1 Unpacking the Analyzer
Although the analyzer is shipped with all the materials you need to install and prepare the system for operation. Carefully unpack the Analyzer and inspect it for damage. Immediately report any damage or shortages to the shipping agent.
3.2 Mounting the Analyzer
The GC-Pro FID is a general-purpose analyzer and is designed with (non-sealed) enclosures. It must be installed in an area where the ambient temperature is not permitted to drop below 32ºF or rise above 100ºF. In areas outside these temperatures, auxiliary heating/cooling must be supplied. The GC-Pro FID enclosure is oil and dust resistant and although it is designed to resist moisture, it should NOT be considered completely watertight. Mounting to walls or racks must be made securely. Avoid locations that are subject to extreme vibration and sway.
Sufficient space must be provided around and above the analyzer to accommodate the necessary electrical conduit and plumbing connections and top cover removal. The top cover must be allowed to be lifted off for possible service access to all components within the enclosure. Refer to the system/analyzer outline drawings for dimensions.
Regardless of configuration, the analyzer/system must be installed on a level surface with sufficient space allocated on either side for
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personnel and test equipment access. Subject to the foregoing, the Analyzer/system should be placed as close to the sample point as is possible.
All pertinent dimensions, connecting points, and piping details can be found in the drawings section as part of the outline, input-output, and piping diagrams. These drawings are specific to the instrument or system to which the manual applies.
3.3 User Connections
All user connections are made on the rear panel. Consult the input­output and outline diagrams in the drawing section of the manual. Not all the features displayed may be present in your system. Refer to any Addenda for additional information that may apply to your instrument.
3.3.1 Electrical Power Connections
The standard analyzer requires a supply of 100-125VAC, single­phase power. Power connections are made at the rear panel of the unit. Refer to the input-output diagram for more information. The electrical power service must include a high-quality ground wire. A high-quality ground wire is a wire that has zero potential difference when measured to the power line neutral. If you have the 220 VAC option, you will require 220 or 240 VAC, 50/60 Hz power. Check the analyzer input­output diagram, power schematic, outline, and wiring diagrams for incoming power specifications and connecting points.
CAUTION: PRIMARY POWER TO THE SYSTEM SHOULD NOT
BE SUPPLIED UNTIL ALL CUSTOMERS WIRING IS INSPECTED PROPERLY BY START-UP PERSONNEL.
3.3.2 Electronic Connections
Figure 3-1 shows the GC-Pro FID rear panel. There are connections for power, digital communications, and both digital and analog concentration output.
For safe connections, no uninsulated wiring should be able to come in contact with fingers, tools or clothing during normal operation.
CAUTION: USE SHIELDED CABLES. ALSO, USE PLUGS THAT
PROVIDE EXCELLENT EMI/RFI PROTECTION. THE PLUG CASE MUST BE CONNECTED TO THE CABLE
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SHIELD, AND IT MUST BE TIGHTLY FASTENED TO THE ANALYZER WITH ITS FASTENING SCREWS. ULTIMATELY, IT IS THE INSTALLER WHO ENSURES THAT THE CONNECTIONS PROVIDE ADEQUATE EMI/RFI SIELDING.
Figure 3-1: GC-Pro FID Electronic Connections
3.3.2.1
PRIMARY INPUT POWER
The power cord receptacle and fuse block are located in the same
assembly. Insert the power cord into the power cord receptacle.
CAUTION: POWER IS APPLIED TO THE INSTRUMENT'S
CIRCUITRY AS LONG AS THE INSTRUMENT IS CONNECTED TO THE POWER SOURCE.
The standard power supply requires 110 VAC, 50/60 Hz or 220
VAC, 50/60 Hz (optional) power.
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3.3.2.2 FUSE INSTALLATION
The fuse block, at the right of the power cord receptacle, accepts US or European size fuses. A jumper replaces the fuse in whichever fuse receptacle is not used.
3.3.2.3 50-PIN EQUIPMENT INTERFACE CONNECTOR
There are three 50-pin Equipment Interface Connectors installed on the rear panel of the GC-Pro FID. Figure 3-2 shows the pin layout of the Equipment Interface connectors. The arrangement is shown as seen when the viewer faces the rear panel of the analyzer. The pin numbers for each input/output function are given where each function is described in the paragraphs below.
Figure 3-2: Equipment Interface Connector Pin Arrangement
From top to bottom the signals handled by the individual connectors are as follows:
Top connector: Alarm relay connections Middle connector: Analog output signals Bottom connector: Standard connector for all additional
signals
See Section 3.3.2.9 for Pin-Out connections for each connector.
3.3.2.4 ANALOG OUTPUT
There are four DC output signal pins—two pins per output. These are found on the middle connector. For polarity, see Table 3-1. The outputs are:
0–1 VDC % of Range: Voltage rises linearly with increasing
concentration, from 0 V at 0 concentration to 1 V at full scale. (Full scale = 100% of programmable range.)
0–1 VDC Range ID: 0.20 V = Low Range
0.5 V = Medium Range
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0.80 V = High Range
4–20 mA DC % Range: Current increases linearly with
concentration, from 4 mA at 0 concentration to 20 mA at full scale. (Full scale = 100% of programmable range.)
4–20 mA dc Range ID: 6.8 mA = Range 1
12.0 mA = Range 2
16.8 mA = Range 3
Table 3-1: Analog Output Connections — Middle Connector
Pin Function
3 Channel 2, + 4-20 mA, floating
4 Channel 2, – 4-20 mA, floating
5 Channel 1, + 4-20 mA, floating
6 Channel 1, – 4-20 mA, floating
8 Channel 2, 0-1 VDC
23 Channel 2, 0-1 VDC, negative ground
24 Channel 1, 0-1 VDC
7 Channel 1, negative ground
Examples:
The analog output signal has a voltage which depends on gas concentration relative to the full scale of the range. To relate the signal output to the actual concentration, it is necessary to know what range the instrument is currently on, especially when the analyzer is in the auto ranging mode.
The signal output for concentration is linear over the currently selected analysis range. For example, if the analyzer is set on a range that was defined as 0-100 ppb benzene, then the output would be as shown in Table 3-2.
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Table 3-2: Analog Concentration Output—Example
Ppb Voltage Signal Current Signal Benzene Output (VDC) Output (mA DC)
0 0.0 4.0 10 0.1 5.6 20 0.2 7.2 30 0.3 8.8 40 0.4 10.4 50 0.5 12.0 60 0.6 13.6 70 0.7 15.2 80 0.8 16.8 90 0.9 18.4 100 1.0 20.0
3.3.2.5
ALARM RELAYS
The nine alarm-circuit connector pins connect to the internal alarm relay contacts. The pins for the alarm relays are available from the top interface connector. Each set of three pins provides one set of Form C relay contacts. Each relay has both normally open and normally closed contact connections. The contact connections are shown in Table 3-4. They are capable of switching up to 3 amperes at 250 VAC into a resistive load. The connectors are:
Threshold Alarm 1:
Can be configured as high (actuates when
concentration is above threshold), or low (actuates when concentration is below threshold).
Can be configured as failsafe or non-failsafe Can be configured as non-latching Can be configured out (defeated).
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Threshold Alarm 2:
Can be configured as high (actuates when
concentration is above threshold), or low (actuates when concentration is below threshold).
Can be configured as failsafe or non-failsafe Can be configured as non-latching Can be configured out (defeated).
System Alarm:
Actuates when DC power supplied to circuits is
unacceptable in one or more parameters. Permanently configured as failsafe and latching. Cannot be
defeated.
Note: Reset by pressing the STANDBY button to remove power.
Then press STANDBY again and any other button except SYSTEM to resume. Further detail can be found in Chapter 4, Section 4.7.4.
Table 3-4: Alarm Relay Contact Pins — Top Connector
Pin Contact
45 Threshold Alarm 1, normally closed contact
28 Threshold Alarm 1, moving contact
46 Threshold Alarm 1, normally open contact
42 Threshold Alarm 2, normally closed contact
44 Threshold Alarm 2, moving contact
43 Threshold Alarm 2, normally open contact
36 System Alarm, normally closed contact
20 System Alarm, moving contact
37 System Alarm, normally open contact
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3.3.2.6 DIGITAL REMOTE CAL INPUTS
The digital remote calibration signals are available on the bottom connector. They input accepts 0 V (off) or 24 VDC (on) for remote
control of calibration. (See Remote Calibration Protocol below.) See
Table 3-5 for pin connections.
Span: Floating input. A 5–24 V input across the + and – pins puts the
analyzer into the Span mode If cycle mode is ‘Continuous’. Either
side may be grounded at the source of the signal. A 0–1 volt across
the terminals allows Span mode to terminate when done. A
synchronous signal must open and close external span valve appropriately.
Cal Contact: This relay contact is closed while analyzer is spanning.
(See Remote Calibration Protocol below.)
Table 3-5: Remote Calibration Connections — Bottom Connector
Pin Function
10 + Remote Span 12 – Remote Span 40 Cal Contact 41 Cal Contact
Remote Calibration Protocol: To properly time the Digital Remote Cal
Inputs to the GC-Pro FID Analyzer, the customer's controller must monitor the Cal Relay Contact.
When the contact is OPEN, the analyzer is analyzing, the Remote Cal Inputs are being polled, and a span command can be sent.
When the contact is CLOSED, the analyzer is already calibrating. It will ignore your request to calibrate, and it will not remember that request.
Once a span command is sent, and acknowledged (contact closes), release it. If the command is continued until after the span is complete, the calibration will repeat and the Cal Relay Contact (CRC) will close again.
For example:
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1. Test the CRC. When the CRC is open, send a span command
until the CRC closes (The CRC will quickly close.)
2. When the CRC closes, remove the span command.
When CRC opens again, the span calibration is done, and the sample
is being analyzed.
3.3.2.7 ‘MEASURE ONCE (OR ONE SHOT MEASUREMENT) CONTACTS
There are three dedicated relay contacts and these are available from the bottom Equipment Interface Connector. They are assigned to indicate status of ‘measure once’ (or one shot measurement). Contacts are normally open, and they close when GC-Pro TCD switches to that particular range.
Table 3-6: ‘Measure Once’ Relay Connections
Pin Function
9 + Start Measurement Digital Input 11 - Start Measurement Digital Input 21 IDLE Contact 1 38 IDLE Contact 2 22 IN MEASUREMENT Contact 1 39 IN MEASUREMENT Contact 2 19 MEASUREMENT DONE Contact 1 18 MEASUREMENT DONE Contact 2
MEASUREMENT DONE contact only closes for 5 seconds at end of measurement cycle. After that IDLE contact closes. However reading is display and analog output stays till new measurement is requested.
Digital input range is 5 to 24 vdc to start measurement.
3.3.2.9
PIN OUT TABLE
The following table summarizes all the outputs/inputs available on the three 50 pin D-Sub connectors on the back panel of the analyzer.
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Table 3-7: Pin out of Alarm Relay O/P (Top) 50 pin D-Sub Connector
pin # Description
1 Alarm Relay # 9, NC contact 2 Alarm Relay # 9, C contact 27 3 Alarm Relay # 9, NO contact 28 4 Alarm Relay # 10, NC contact 29 5 Alarm Relay # 10, C contact 30 6 Alarm Relay # 10, NO contact 31 7 Alarm Relay # 11, NC contact 32 8 Alarm Relay # 11, C contact 33
9 Alarm Relay # 11, NO contact 34 10 Alarm Relay # 12, NC contact 35 11 Alarm Relay # 12, C contact 36 12 Alarm Relay # 12, NO contact 37 13 Alarm Relay # 13, NC contact 38 14 Alarm Relay # 13, C contact 39 15 Alarm Relay # 13, NO contact 40 16 Alarm Relay # 14, NC contact 41 17 Alarm Relay # 14, C contact 42 18 Alarm Relay # 14, NO contact 43 19 Alarm Relay # 15, NC contact 44 20 Alarm Relay # 15, C contact 45 21 Alarm Relay # 15, NO contact 46 22 Alarm Relay # 16, NC contact 47 23 Alarm Relay # 16, C contact 48 24 Alarm Relay # 16, NO contact 49 25 Alarm Relay # 17, NC contact 50
pin # Description
AlarmRelay#17,Ccontact
26
AlarmRelay#17,NOcontact AlarmRelay#18,NCcontact AlarmRelay#18,Ccontact AlarmRelay#18,NOcontact +15VDC AnalogGround +15VDC AnalogGround +15VDC Ch.#1,4‐20madcinput,HOT AnalogGround +15VDC Ch.#2,4‐20madcinput,HOT AnalogGround +15VDC Ch.#3,4‐20madcinput,HOT AnalogGround +15VDC Ch.#4,4‐20madcinput,HOT AnalogGround Ch.#5,4‐20madcinput,HOT Ch.#6,4‐20madcinput,HOT +15VDC SpareAnalogInput
Table 3-8: Pin out of Analog Signal (Middle) 50 pin D-Sub Connector
pin # Description
1 4-20 ma Out, Ch. # 3- HOT 2 4-20 ma Out, Ch. # 3- RET 27 Analog Ground 3 4-20 ma Out, Ch. # 4- HOT 28 0-1 vdc Out, Ch. # 9 - HOT 4 4-20 ma Out, Ch. # 4- RET 29 0-1 vdc Out, Ch. # 10 - HOT 5 4-20 ma Out, Ch. # 5- HOT 30 Analog Ground 6 4-20 ma Out, Ch. # 5- RET 31 O2 sensor Hot Input #2 (NI) 7 4-20 ma Out, Ch. # 6- HOT 32 O2 sensor Return Input #2 (NI) 8 4-20 ma Out, Ch. # 6- RET 33 Thermistor for O2 sensor #2 ((NI) 9 4-20 ma Out, Ch. # 7- HOT 34 Thermistor for O2 sensor #2 (NI)
pin # Description
26 0-1 vdc Out, Ch. # 8 - HOT
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pin # Description
10 4-20 ma Out, Ch. # 7- RET 35 O2 sensor Hot Input #3 (NI) 11 4-20 ma Out, Ch. # 8- HOT 36 O2 sensor Return Input #3(NI) 12 4-20 ma Out, Ch. # 8- RET 37 Thermistor for O2 sensor #3 (NI) 13 4-20 ma Out, Ch. # 9- HOT 38 Thermistor for O2 sensor #3 (NI) 14 4-20 ma Out, Ch. # 9- RET 39 O2 sensor Hot Input #4 (NI) 15 4-20 ma Out, Ch. # 10- HOT 40 O2 sensor Return Input #4 (NI) 16 4-20 ma Out, Ch. # 10- RET 41 Thermistor for O2 sensor #4 (NI) 17 Analog Ground 42 Thermistor for O2 sensor #4 (NI) 18 Analog Ground 43 O2 sensor Hot Input #5 (NI) 19 0-1 vdc Out, Ch. # 3 - HOT 44 O2 sensor Return Input #5 (NI) 20 0-1 vdc Out, Ch. # 4 - HOT 45 Thermistor for O2 sensor #5 (NI) 21 Analog Ground 46 Thermistor for O2 sensor #5 (NI) 22 0-1 vdc Out, Ch. # 5 - HOT 47 O2 sensor Hot Input #6 (NI) 23 0-1 vdc Out, Ch. # 6 - HOT 48 O2 sensor Return Input #6 (NI) 24 Analog Ground 49 Thermistor for O2 sensor #6 (NI) 25 0-1 vdc Out, Ch. # 7 - HOT 50 Thermistor for O2 sensor #6 (NI)
pin # Description
(NI) = Not Implemented
Table 3-9: Pin out of Standard (Bottom) 50 pin D-Sub Connectors
pin # Description
1 2 27 3 + Output 4-20 ma - Channel 2 28 Alarm 1 C Contact 4 - Output 4-20 ma - Channel 2 29 5 + Output 4-20 ma – Channel 1 30 6 - Output 4-20 ma – Channel 1 31 7 - Output 0-1 v (Channel 1) 32 Exhaust Solenoid Hot 8 + Output 0-1 v (Channel 2) 33 Sample Solenoid Hot
9 34 Range 4 Contact/ not used 10 Remote Span + 35 Range 4 Contact/not used 11 36 Alarm 3 NC Contact 12 Remote Span - 37 Alarm 3 NO Contact 13 38 Range 1 Contact 14 39 Range 2 Contact 15 40 Calibration Contact 16 Span Solenoid Return 41 Calibration Contact 17 Span Solenoid Hot 42 Alarm 2 NC Contact 18 Range 3 Contact 43 Alarm 2 NO Contact 19 Range 3 Contact 44 Alarm 2 C Contact 20 Alarm 3 C Contact 45 Alarm 1 NC Contact
pin # Description
26
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pin # Description
21 Range 1 Contact 46 Alarm 1 NO Contact 22 Range 2 Contact 47 23 - Output 0-1 v (Channel 2) 48 Exhaust Solenoid Return 24 + Output 0-1 v (Channel 1) 49 25 50 Sample Solenoid Return
pin # Description
3.3.2.10 RS-232 PORT
The digital signal output is a standard RS-232 serial communications port used to connect the analyzer to a computer, terminal, or other digital device. It requires a standard 9-pin D connector.
Input: The input functions using RS-232 that have been implemented
to date are described in Table 3-8.
Table 3-10: Commands via RS-232 Input
Command Description AS <enter> Auto Span immediately (continuous mode)
SV <enter> Switch to Span Valve ZV <enter> Switch to Zero Valve AV <enter> Switch to Analyze Valve C1 <enter> If in 1Shot mode, start a cycle C2 <enter> If in 1Shotm modde, start a span cycle PMA <enter> Switch to standard message PMB <enter> Switch to FID output mode PMC <enter> Switch to Query Mode (used for interface with
OPC server)
Implementation: The RS-232 protocol allows some flexibility in its
implementation. Table 3-9 lists certain RS-232 values that are required by the Standard Mode GC-Pro FID implementation.
Table 3-11: Required RS-232 Options
Baud 9600 Byte 8 bits
Parameter Setting
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Parity none Stop Bits 1 Message Interval Sent at the end of each cycle.
3.3.3 Gas Connections
The analyzer gas connection diagram identifies the various gas connection points as to function and location. Figure 3-1 shows the gas connection points for the standard instrument without the optional auto calibration module. If the optional auto calibration manifold is present, sample and span gas connections would be made to labeled fittings on the manifold.
Figure 3-3: Gas Connections
Note: For instruments without the auto calibration option, the
customer must provide means of switching sample and span gas to the analyzer. It is recommended that you use a tee with appropriate valves as opposed to disconnecting the sample gas connection when span gas is required.
Gas connections to the instrument are made at the 1/8”or 1/4” stainless steel tube fittings provided on the rear panel. Note that the
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optional purge (not shown) and sensor vent fittings are 1/4” while all other gas connections are 1/8”.
It is recommended that all gas tubing leading to the connections on the back of the analyzer be of the coiled type. This will facilitate sliding the unit out of the case without disconnecting the gas supply to the analyzer.
Before tubing is connected to the system, it must be decontaminated to eliminate any hydrocarbon deposits. Using a small torch, heat each length of tubing while passing nitrogen through it until it glows red. Begin at the nitrogen source end and proceed down the length of the tube, “chasing” the red glow (and hydrocarbon deposits) down to the open end of the tube. Cap the tubing while not in use with suitable non­contaminating caps.
All sample, calibration, and supporting gas lines, which deliver gas to the analyzer, must be decontaminated before connection; vent lines do not.
When connecting the various gas lines to the system, be absolutely certain that no “dead ends” are left; that is, no unused branch lines should be left capped off, where pockets might form of material that is not representative of the current contents of the line, or which might keep contaminants from being purged out of the system.
CAUTION: THE GASES USED MUST BE OF THE HIGHEST
QUALITY, ULTRA ZERO GRADES, AS SHOWN BELOW. FAILURE TO DO SO WILL RESULT IN CONTAMINATION AND FAILURE TO DETECT AT THE REQUIRED ACCURACY.
AIR: USE WATER PUMPED AIR WITH THC LESS THAN
0.1 PPM. DO NOT USE OIL PUMPED AIR UNDER ANY CIRCUMSTANCES.
FUEL: HYDROGEN GAS, 100%, ZERO QUALITY WITH THC
LESS THAN 0.5 PPM.
CARRIER GAS: NITROGEN GAS, ULTRA ZERO GRADE WITH THC
LESS THAN 0.05 PPM.
Normally, four supporting gases of different composition (see
Section 4.1: Equipment) will be required to operate the analyzer. The
recommended composition is specified Appendix C: Addendum and Testing Results. The gases should be supplied from cylinders that are
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GC-Pro FID Installation
equipped with the type of regulator specified in the aforementioned sections.
CAUTION: UNDER NO CIRCUMSTANCES SHOULD YOU
EMPLOY A REGULATOR THAT IS NOT EQUIPPED WITH A METALLIC DIAPHRAGM ANYWHERE IN THE SYSTEM.
The regulators should be inspected prior to installation to be sure that they are oil-free. Failure to comply with these directives will result in a constant drift in analyzer output, as organic compounds will outgas into the plumbing system at a rate that is related to the ambient temperature. Use 316 stainless steel, dual-stage stainless steel diaphragm regulators only in fuel, sample, and blanket air lines; shutoff valves should be used downstream from each regulator.
Place the supply cylinders as close to the analyzer as possible, and connect to the analyzer with new tubing. Be sure that all plumbing connections are free of leaks.
Note: Use only stainless steel tubing throughout the system.
Consult the assembly, piping, outline drawings, and any Addenda included with this manual to determine if special conditions apply.
3.3.3.1 EFFLUENT
All the gases introduced into the detection cell vent from one fitting at the rear of the analyzer. TAI recommends that the cell be permitted to vent directly to the atmosphere wherever possible.
If a vent line is required, the installation must include a drop-out pot to collect the water that is formed by the burning of the hydrogen fuel. The vent line must be constructed so that water and dirt cannot collect in it.
3.3.3.2 SAMPLE BYPASS VENT
The sample bypassed by the back-pressure regulation system vents from a separate port at the rear of the analyzer. If a vent line is required, it must be installed so that water and dirt cannot accumulate in it.
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3.3.3.3 FUEL AND AIR CONNECTIONS
The fuel used to provide combustion should be hydrogen gas, zero quality with certified THC of less than 0.5 ppm and supplied at a pressure of 40 psig. The compressed air, ultra zero gas quality with THC less than 0.1 ppm should be used and supplied at a pressure of 40 psig. Connect the fuel and air sources to the instrument according to the gas connection diagram included at the back of this manual.
3.3.3.4 SAMPLE AND SPAN GAS CONNECTIONS
The sample and span gas connections are made at the rear panel. If the optional auto calibration module is installed, the sample and span gas will connect to this module. If no auto calibration module is present, these gases connect to the labeled fittings on the rear panel.
Set the supply pressure for sample and span gas to 20 psig.
3.4 Placing the System in Operation
See Section 4 for information on starting the analyzer for the first time. Make sure that all electrical connections have been made correctly and all connectors are fully seated. Make sure all gas connections are correct and leak–free.
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Operation
This section of the manual describes how to setup and operate the GC-Pro FID Analyzer. It includes preliminary steps and equipment needed for operation, initial startup, and then the actual operation of the analyzer using the touch screen interface is described. You should read this chapter in its entirety and become familiar with the operating characteristics of this system before starting the analyzer for the first
time. The Addendum and Testing Results section of Appendix C lists the
software revision and default settings for your specific analyzer.
The GC-Pro FID Analyzer incorporates a HMI interface that uses a touch-sensitive LCD display with menus logistically grouped for easy, intuitive access to all functions. The features supported by the newly designed system HMI interface include:
1. Sensor data acquisition, data logging and system health
monitoring performed through the touch-screen display.
2. Firmware up-grades of the 89C5131 PCB can be carried out
through an internal USB 2.0 interface
3. Firmware up-grade for the 9261 controller board can be carried
out through the USB 2.0 interface using the SAMBA tool.
4. Stand alone testing of the 89C5131 PCB can be performed
through the debug hyper terminal (9600Kbps) connection on the rear panel.
Operation of the analyzer including setup functions are performed from the touch screen. The HOME screen is the main display screen and the MENU screen allows the user to enter any phase of operation, calibration, and setup simply by touching the specific on-screen button. See Section 4.7.
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4.1 Equipment
The following supporting gases and hardware will be required to
operate the (standard) analyzer:
1. Fuel: A cylinder containing a hydrogen gas, zero gas quality
composition will be required to supply the fuel for the flame ionization burner. The cylinder is to be equipped with an oil-free metallic diaphragm regulator (dual stage).
2. Blanket Air: A cylinder of compressed air, zero gas quality will
be required to maintain the proper atmosphere within the cell. The cylinder is to be equipped with an oil-free, dual stage, metallic diaphragm regulator.
3. Carrier Gas: A cylinder of nitrogen gas, zero gas quality,
equipped with dual stage metallic diaphragm regulator is required.
4. Span Gas: A cylinder or a permeation device system, capable of
generating known concentration of benzene and/or other aromatic hydrocarbons of interest, will be required to standardize the analyzer.
5. Sample Pressure Regulation: An oil-free, metallic diaphragm
regulator must be installed at the sample point when possible; see
Section 3.3.3 Gas Connections.
CAUTION: THE GASES USED MUST BE OF THE HIGHEST
QUALITY, ULTRA ZERO GRADES, AS SHOWN BELOW. FAILURE TO DO SO WILL RESULT IN CONTAMINATION AND FAILURE TO DETECT
THE REQUIRED ACCURACY.
AT
AIR: USE WATER PUMPED AIR WITH THC LESS THAN 0.1 PPM. DO NOT USE OIL PUMPED AIR UNDER ANY CIRCUMSTANCES.
FUEL: HYDROGEN GAS, 100%, ZERO QUALITY WITH THC LESS THAN 0.5 PPM.
CARRIER GAS: NITROGEN GAS, ULTRA ZERO GRADE WITH THC LESS THAN 0.05 PPM.
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4.2 Preliminary Power-Off Check List
Make the following checks of the installation before proceeding further into the start-up procedure:
1. Check to see that the sample and supporting gas installation is in
accordance with the specifications called for in the installation and application sections of the manual (Chapter 3). Be sure that the supporting gases are of the proper composition and are connected to the correct fittings at the rear of the analyzer.
2. Check to see that the electrical installation conforms to the
instructions contained in the installation section (Chapter 3) and on the input-output diagram.
3. Remove the top cover and check to see that the printed circuit
boards and cables are firmly seated in their respective sockets.
4. Confirm that recorder and alarm connections are properly made.
4.3 Powering Up the Unit
Before applying power to the analyzer for the first time perform the following checks:
1. Make sure that the proper power 120/220 VAC 50/60 Hz is
available.
2. Connect the AC power cord to the rear panel and then plug the
other end into the mains supply. As soon as power is established, the unit will turn on.
3. Check that the Power, CPU, and COM LEDs illuminate and the
Teledyne Logo screen appears on the display.
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4. Momentarily, the Teledyne screen will be replaced with a second
start-up screen that lists the Model, Serial Number, Software Version and other parameters specific to your instrument.
5. A one hour warm up time is required for the internal heaters to
come up to the required temperature and stabilize. The screen will indicate a countdown as the warm up period progresses.
6. During the warm up period activate the support gases as
described in Section 4.4.
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7. Following the warm up, the system will initiate a self-diagnostic
routine and display the results as either “OK” or “Failed”
8. After the self diagnostic test has completed the instrument will
attempt to ignite the flame. See Section 4.6.
4.4 Activating the Support Gases
The instrument gas controls are located on the front panel adjacent to the touch screen display as shown in Figure 1-1. Make sure that the following support gases are available at the analyzer:
Air: (HC-free) for combustion Carrier gas: (usually nitrogen but refer to Appendix C for
your specific application.
Fuel: 100% hydrogen Span gas: Typically 70-90% of measured component on
the range of interest in a clean background gas. Refer to Appendix C for the specific span gas composition for your application.
4.4.1 Air
1. Set the air source regulator to 40 psig.
2. Adjust the analyzer air regulator until the air pressure gauge
reads the recommended air pressure of 7.0 psig.
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After the air is flowing through the sensor and warm-up time has
been completed, activate the following gases:
4.4.2 Carrier Gas
Set the carrier gas source regulator to 80 psig and adjust the analyzer sample regulator until the sample pressure gauge reads the recommended sample pressure of 7.0 psig.
4.4.3 Span Gas
1. Feed span gas to the analyzer (see Section 4.4.3). Gas switching
can be performed manually or handled through the auto calibration valves (if the option is added). See Section 4.7.10.3.
2. Observe that the analyzer sample flow meter reads from 0.3 to
1.0 SCFH.
4.4.4 Fuel
1. Open the main valve on the fuel source and set the fuel pressure
regulator to 40 psig.
2. Adjust the fuel regulator until its pressure gauge reads the
recommended pressure of 4.0 psig.
Note: Adjust fuel settings only when the red LED (flame failure
light) is off.
4.5 Sample Pump
A built-in sample pump is provided to draw sample gas from ambient air. The gas flow rate should be maintained at about 1000 to 1200 cc/minute using the Front Panel flow control valve (clockwise increases flow). See Figure 1-1.
4.6 Flame Ignition
After the warm up countdown on the display reaches zero, open the gas control door and observe that the amber heater lamp is blinking (indicating that the temperature controller is maintaining the temperature setpoint) and the red Flame Out lamp on the front panel is on. See Figure 1-1.
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The GC-Pro FID will automatically attempt a flame ignition sequence following the warm up period which has been preset at the factory.
If the ignition process fails, the instrument will attempt to ignite the flame 4 more times. If it continues to fail after the fifth attempt, a flame failure message will appear on the display. If this occurs refer to Section
5.
Attempting to reignite the flame by touching the “RE-IGNITE” button will display a confirmation window as shown below.
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Operation GC-Pro FID
Again the ignition process will start if user selects the “OK” button.
The number of attempts will be updated on the screen below.
The above process will repeat until the flame ignites successfully.
The status will be updated as shown in the next screen.
Once the ignition process is successful the HOME screen will appear
on the display.
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4.6.1 Verification of the Flame Guard Circuit
Prior to using the analyzer for the first time, the operation of the flame guard circuit should be checked. This circuit has been checked at the factory, but should be re-verified during start-up. Use the following procedure after ignition of the flame has been achieved:
1. Turn off the fuel at the supply cylinder.
2. Observe the fuel pressure gauge on the analyzer control panel. The
gauge indication will decay as the fuel in the line is exhausted. When the gauge reading reaches near zero, the flame will extinguish as the fuel solenoid shuts off the fuel supply. The display will indicate an ignition failure followed by a request to re­ignite.
3. The analyzer will automatically try to re-ignite. After 5 attempts, it
will display: flame failure, check air, fuel and the flame failure LED will be on.
4. Open the cylinder supply valve and re-ignite the flame by
pressing the ‘OK’ button on the Re-ignite screen.
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4.6.2 Ignition and/or Flame Guard Circuit Failure
If the flame ignition or guard circuits do not operate as described in the above two sections, set the instrument fuel regulator to the recommended pressure. If still fails to ignite, proceed as directed in
Chapter 5: Maintenance & Troubleshooting.
4.7 Analyzer Operation
Although the GC-Pro FID has been programmed for your application at the factory, it can be further configured at the operator level. Depending on the specifics of the application, this might include all or a set of the following procedures:
1. Setting system parameters Establish a security password, if desired, requiring operator
to log in.
Establish and start an automatic calibration cycle (if equipped
with the optional auto calibration module).
2. Routine operation.
Calibrate the instrument. Choose auto ranging or select a fixed range of analysis. Set alarm setpoints and modes of alarm operation.
3. Special functions setup. Calibrate analog output, select analog output source.
Procedures for accessing and/or changing parameters as well as analyzer operation are detailed in the sections to follow. All functions can be accessed from the MENU screen which is accessible via the center button on the HOME screen.
The default screen is the HOME screen (see Section 4.7.2). This is the analysis display and shows details regarding the current sample being analyzed. However, the user can go directly to any function supported by the analyzer by pressing the MENU button. The only exception to this is when the instrument is powered up. It will go through a warm-up period, followed by a diagnostic self-test routine as explained in Section 4.3.
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4.7.1 Default Parameters
The versatility of this analyzer usually results in significant changes being made to parameters over the course of time to better suit a particular application. Occasionally processes change requiring alteration to alarms, filter settings etc. At some time, it may be beneficial to reset the analyzer to the default conditions as it was when shipped from the factory. Below is a listing of the default parameters used in configuring the typical GC-Pro FID instrument. Your specific
application may require different settings. Refer to the Addendum and Testing Results section of Appendix C for any specific changes or
recommendations that apply to your application.
Range/Application: Refer to the Addendum and Testing
Results section of Appendix C
Range: Manual Alarms: Defeated, 20ppb, 50ppb, HI, NON-
FAILSAFE, NON-LATCHING
Auto Span Timing: Defeated, every 7 days, at 12 hours Span: 80 ppb Password: 11111
4.7.2 The HOME Screen
The HOME screen is the default display and represents the Analysis Mode of the instrument. It is a set of two screens that present
information regarding the current measurement state. The HOME screen is where the maximum information about the instrument is displayed.
The Group name/tag is listed on the left most column and the concentration for groups are displayed in PPB, PPM or % depending on the range and value. The Enabled group is represented by the glowing LED. Each group has three user settable ranges R1, R2, and R3 and the current range index is displayed in the Group row. It is possible to view the VS (Volt-second) count by touching the “Vs Count” button.
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The phase cycle (forward or reverse) and corresponding phase timer along with the cell ADC value are displayed in the lower box. The green LED within the rectangle starts blinking whenever a peak is detected for active time frames (groups) running in the respective cycle.
The ten groups are split into two screens showing five on each screen. Either screen can be displayed by selecting “NEXT” and “PREV” on the HOME screen.
A “Cold Boot” button is located on the bottom left corner of the HOME screen that when pressed will allow the user to revert back to factory settings or retain the current instrument settings. See Section
4.7.13.5 for additional details regarding a cold boot.
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Each group has buttons associated with it (T_Time and T-Cycle) that will bring up a graph displaying the analysis trend in the group with respect to time or cycle. With these buttons, the user can evaluate the instantaneous analysis as opposed to waiting for a complete cycle to terminate. See Section 4.7.13 for more details.
4.7.3 The MENU Screen
Instrument parameters can be accessed and set by pressing the “MENU” button on the HOME screen. This brings up the following MENU screen:
Any function can be entered by touching the respective icon. The
functions are:
Standby (lower left corner on display) Home (home icon at bottom center) Overlay Chromatogram Timing Temperature Group Setup Analog Adjust Calibration Self Test
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Settings Firmware Upgrade
These functions are described in the sections that follow.
4.7.4 Standby
This function allows you to place the instrument in STANDBY
mode.
CAUTION: STANDBY SHUTS DOWN POWER TO THE DISPLAYS
ONLY. INTERNAL CIRCUITS ARE STILL ENERGIZED AND ELECTRICAL SHOCK HAZARD STILL EXISTS.
To place the instrument in STANDBY status press the “Standby” button at the lower left corner of the display. The following Confirmation screen will pop up.
Selecting ‘OK” puts the system goes into a sleep mode and
following window will be displayed on the screen.
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To come out of standby mode, touch the “WAKE UP” button. An informational pop up screen will appear for approximately one minute displaying a message “Please wait……”.
4.7.5 Overlay Chromatogram
Selecting “Overlay Chromatogram” brings up the following screen:
The above screen displays the overlay chromatogram with the ADC values on y axis plotted against the sample number on the x axis. To display the graph onscreen, touch the “PLOT” button. To clear the screen touch “REFRESH”.
Use the “Scale” button to change the X axis or Y axis scaling.
Note: The chromatogram will be displayed for a maximum of 1020
samples. The chromatogram will not display if the total sum of the forward phase duration & backward phase duration is more than 1020 seconds.
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Operation GC-Pro FID
In this screen, low and high limits on the X and Y axes can be input. The maximum limit for X-High is 1020 i.e., 1020 seconds. So the maximum cycle time (forward + backward) time should not exceed 1020 seconds (17 min) for the overlay chromatogram.
The user can also select the number of channels to be plotted on the overlay chromatogram screen by selecting the “Setting” icon from the MAIN menu. Doing so will display the Setting submenu screen as shown below.
From this menu, touch the “Overlay Chro’gram” button. This will bring up the CHANNEL SELECTION window as shown below.
Use the UP ARROW to select the number of channels then touch ENTER to confirm the selection or CANCEL to abort the selection and return the previous selection. This screen also provides the color
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indicators for the plot on the various channels. These colors are fixed and cannot be changed.
4.7.6 Timing
Timing controls the parameters of the valve and data acquisition. It
is specific to the setup of the instrument and must be determined at the
factory or TAI trained personnel. Refer to the Addendum and Testing Results section of Appendix C for the specific timing settings used for
your system and application. Do not change these values unless directed by Customer Service at TAI. For further information please contact TAI Customer Service.
In the event the timing must be changed or viewed, touch the
“Timing” icon on the MENU screen. The following screen is displayed.
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The window screen is used to set the forward and backward duration in MM:SS format. After setting the required duration, select the ENTER button to save the values.
If the onscreen LED is red, all available buttons will be disabled and timing cannot be adjusted. Wait until the LED turns green again before resuming any button presses.
Note: The chromatogram will be displayed up to a maximum of
1320 samples i.e. if the sum of the forward plus backward phase duration is more than 1320 seconds. Beyond that value, that the chromatogram will not be displayed.
With the LED green, the “Parameters” icon can be selected to view and edit several parameters for each time frame, as shown in the screen below.
The above screen displays the Phase, Begin Time and End Time along with the active ON/OFF field. The screen also contains an EDIT button that can be used to view or modify all the parameters for the selected timeframe, as shown below.
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The parameters can be modified by either touching the UP arrows or
by entering the values in input fields.
In order to input the Begin/End Time, touch on the Green “EDIT
TIME” button. This causes an input window to appear as shown below.
In this screen, the Begin/End Time can be changed (minutes and seconds) by touching the requisite box. A pop up numerical keypad appears onscreen that allows the direct input of numerical values.
If an inappropriate value is input, for example a Begin time greater than the End time or an End time which exceeds the selected (FWD+BCK) phase duration, an onscreen warning will appear as shown below.
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Once a valid input has been entered as shown in the example screen above, the display will return to the Parameter window, which will now reflect the modified values.
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After modifying the above parameters touch the ENTER button to save the new inputs. A confirmation window will pop up before actually saving the inputs. Select OK to save, otherwise touch CANCEL to reject the new inputs.
4.7.7 Temperature
Temperature control is a critical factor in GC analysis. The GC-Pro FID Analyzer incorporates three dedicated temperature controllers.
FID Temperature (Sensor) GC Column Temperature (Column) Sample Chamber (Sample)
Refer to the Addendum and Testing Results section of Appendix C
for the specific temperature setpoints used for your system and application. Do not change these values unless directed by Customer Service at TAI. For further information please contact TAI Customer Service.
Caution: The temperature settings have been carefully
determined and set at the factory for your application. Temperature is a key factor in determining the accuracy of the resultant analysis. It is recommended that the user consult TAI before making any changes to the temperature setpoints as listed in Appendix C of this manual.
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To monitor the temperatures, check the status of a thermocouple or
change a temperature controller setpoint select “Temperature” from the
MAIN screen. The following screen will display.
4.7.7.1 THERMOCOUPLE
Selecting “Thermocouple” from the Temperature menu shows the actual temperature reading (°C) of the three sections: Sample, Sensor, and Column.
The temperature sensor value will be displayed in degrees Centigrade. If the values are within the limits the green LED will be illuminated. The LED will be red if the values are above or below the
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setpoint limits. The screen also displays the date and time of the thermocouple data acquisition. The values are updated every five seconds.
4.7.7.2 SETTINGS
To redefine the limits and offset for the thermocouple values, press “Settings” from the Temperature screen. The following screen will appear.
Pressing any data box will bring up an onscreen numerical keyboard that allows data input. When finished making setpoint, limit and offset changes, press ENTER to return to the Temperature screen.
4.7.7.3 PID SETTINGS
The temperature controllers used in the GC-Pro are three-term controllers with proportional (Kp), Integral (KI), and derivative (Kd) settings. Together, these parameters determine the overall control and response of the instrument.
Optimum values for Kp, KI, and Kd have been determined at the factory and set for your instrument. The PID Settings menu from the Temperature main menu will display the current values for each of the three heaters and allow the user to modify the setting.
To access the parameters, press PID Settings from the Temperature screen.
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Pressing PID Settings will bring up the following screen that displays the current settings for each of the three temperature controllers.
You can adjust any of the three PID constants by touching the data box and entering a new value into the numerical entry box that pops up. Once the value has been entered, press ENTER on the entry box to accept the value and dismiss the numerical entry box. After all parameters have been set, save the values by pressing ENTER on the lower left corner of the screen. This will return you to the Temperature main screen.
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4.7.7.4 STATUS
The STATUS screen displays the status for the three thermocouple sensors. If a thermocouple is open or damaged, this condition will be indicated by the message “Broken” in the corresponding sensor column. Otherwise, if a thermocouple is operating properly “Normal” will be displayed in the sensor column.
4.7.8 Group Setup
Group Setup assigns to each compound a name, a range given in Range settings and an associated peak window that is determined in Timing settings. These values should not be modified unless directed by TAI customer Service.
When the Group Setup icon on Main Menu is selected, the following screen is displayed.
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The Group Setup is function split into two screens covering Croups 0-4 and 5-9 on individual setup screens. The Group Setup screen gives the option to display either half of the Groups by touching the relevant icon. When user touches the “Group 0-4” icon, a new window appears as shown below.
From these screens (0-4 and 5-9) a specific group or groups can be selected, names (tag) assigned, a range assigned as well as concentration peaks (Sxx) added or subtracted.
A group is selected by touching the adjacent LED. When selected it the LED icon should turn green.
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A tag is limited to three characters (letters or numbers 0-9). A tag can be assigned by touching any three keys provided in the on-screen keypad after selecting the tag field for the relevant group. You must
press ENTER on the keypad to assign the tag before moving to another
setting or group, otherwise the tag will NOT be assigned.
To assign a range, touch the UP arrow button adjacent to the range of the selected group.
Once all the required inputs have been made, select ENTER to save. A confirmation window pops up to confirm the inputs or cancel.
Note: You can view the first of the Enabled Sxx on the Group
Setup screen for the respective Groups. If none of the Sxx are enabled S** will be displayed. Details for enabling the Sxx are given below.
It is possible to add or subtract concentration peaks to groups using the SUM function available from the Group Select screen.
Selecting SUM from a selected group brings up an additional screen.
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This screen has three inputs for ten peaks S00 through S09. The possible inputs are Subtract, Add, and NA (Not Applicable). The user can assign these inputs by touching the UP arrow button available. After touching the ENTER button to save the inputs, a confirmation window pops up.
Note: After selecting the ENTER button there will be a delay of
few seconds to update the inputs. All other buttons (i.e. home, cancel, back etc) available on the screen will be disabled during the delay period.
As an example, assume Groups G00 and G01 have been setup to monitor two different hydrocarbons with peaks associated as follows:
Group Assigned Peak
G00 S00 G01 S01
Then, it is possible to setup a group to monitor total hydrocarbon as G03 which would have both hydrocarbon peaks assigned to it by using the SUM function:
Group Assigned Peak
G00 S00 G01 S01 G02 S01 + S02
Similarly, group setup inputs can be provided for the other five
groups by selecting Group 5-9 icon on the first Group Setup screen.
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4.7.9 Analog Adjust
The GC-Pro FID Analyzer has ten 4-20 mA DC output channels that can be assigned to the various groups. Any group can be assigned to any output channel and it is also possible to assign groups to multiple channels.
Channel 0 and channel 2 are unique channels. For these channels the user can assign gain and offset values to the output. Channel 0 has an additional feature called “WAVE” which when selected will assign the ADC counts to the 4-20 mA output for the group assigned to channel 0.
Note: The WAVE function will not be accessible until a group has
been assigned to channel 0.
WAVE is only visible on channel 0 but it may be changed back to GROUP by pressing the WAVE button again. The WAVE button toggles between WAVE and GROUP.
Selecting Analog Adjust from the MAIN screen brings up the following screen.
Pressing GROUP and assigning a specific group to Channel 0, the screen changes to:
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where WAVE function is now available.
Any group that is available (see Section 4.7.8 Group Setup) can be
assigned to any output channel.
To assign a group to a channel: Press the UP Arrow button under group and it will start with G00, pressing UP again increments it to G01, and so on. After G09, it will return to G00.
4.7.10 Calibration
The SPAN function is used to calibrate the analyzer. Span can be performed either manually or automatically with the auto calibration function if equipped. Typically, each group will require a separate calibration.
The analyzer is calibrated using span gas as described in Section 4.1.
See also Appendix C Addendum and Testing Results for any specific
requirements regarding span gas for your application. This section assumes that this gas has been properly connected and the line checked for leaks.
To initiate a span calibration, touch the Calibration icon on the MAIN screen. The following screen is displayed.
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4.7.10.1 SPAN
When user touches SPAN the following screen is displayed.
This screen allows the user to select which group or groups to calibrate. There are two separate screens, one for groups 0 through 4 and another for groups 5 through 10. Both screens function identically and allow the user to input the concentration of the known span gas for each group, set the concentration unit as parts per billion (ppb), parts per million (ppm) or percent (%) and span calibrate the group or groups.
Selecting “GROUP 0-4” brings up the following screen:
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A similar screen displays if Group 5-9 is selected.
A lit green LED next to a group indicates the group is enabled (selected) for calibration. An unlit green LED means the group has not been selected and will not be calibrated. Touching on the group’s LED will toggle the LED between lit (enabled) and unlit (deselected).
The SPAN value inputs for each selected group in any of the three units PPB, PPM or Percent can be entered by touching the respective yellow LED next to the correct unit input box. A numerical keyboard will pop up allowing the user to input the known composition of the
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span gas. After inputting the value, press ENTER on the pop up keyboard to input the value into the box.
Only inputs with the glowing yellow LED will be affected. When user touches the ENTER button the inputs with the glowing yellow LED will be saved following confirmation on the pop up screen.
To initiate the calibration, touch the “SPAN BEGIN” button and then “OK” on the next pop up screen to calibrate the analyzer for the selected groups.
Once calibration is complete, the display will revert to the HOME screen. The same procedure can be followed for calibrating groups 5-9.
4.7.10.2 ALT SPAN
If a particular compound of interest is not available or not contained in the span gas, another compound existing in the span gas can be used for the alternate calibration. This requires assigning a factor that results in a best fit approximation to the calibration standard normally required for that group. These factors must be determined by the factory since entering an incorrect value will seriously affect the measurement capability of the instrument for that group. For this reason, TAI recommends contacting customer service before using the Alt Span function.
Touch the ALT SPAN listing on the Calibration screen to enter the Alt Span function. The following screen is displayed:
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The function is split into two screens addressing to Groups 0-4 and 5-9. The screen below shows the display addressing Groups 0-4 (Group 5-9 screen is similar).
In this screen a dark green color on the LED in the “Include” column adjacent to a group indicates that Alt Span is currently disabled for that group. A bright green LED indicates that Alt Span is enabled for the corresponding group. The Alt Factor value can be entered into the box in two phases i.e., an integer part using the UP arrow on the left and a fractional part using the UP arrow on the right.
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One the appropriate values have been entered select ENTER to save the factor. A confirmation screen will arise asking the user to confirm the changes before saving.
After confirmation, a display screen will appear where the user can be the currently saved factor. If you “Cancelled” the entry on the last screen, the previous Alt Span factor will be used.
To initiate an Alt Span calibration, touch “OK” to bring up the next screen to select which group to span on or “CANCEL” to exit the Alt Span function.
After pressing “OK” the next screen appears.
Use the “UP/DOWN” arrows to enter the group to span on and then press “ENTER” to begin the calibration or “CANCEL” to exit the function.
Once the calibration has completed the HOME screen will appear on the display.
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Use the same procedure for performing an Alt Span on any member
or members in Groups 5-9.
4.7.10.3 AUTO CAL
The GC-Pro FID Analyzer can be fitted with an external auto calibration module as an option. This feature provides automatic switching of sample and calibration gases and allows the operator to program calibration events to occur automatically
Note: If your instrument is not fitted with an auto calibration
module, the auto calibration screens will still appear on the display but will be non-functional.
Note: Before setting up an AUTO CALIBRATION, be sure you
understand the Span function as described in Section
4.7.10.1 and follow the procedures given there for inputting the calibration gas compositions for each group etc. Auto Span performs a span calibration using the target span value set that has been set in the Span feature menu.
To setup an auto calibration cycle for a span events to occur in a certain number of days/hours select the “Auto Cal” button from the Calibration screen. The Auto Cal screen is displayed.
A dark green color of the LED button adjacent to the Auto Span indicates that Auto Span is disabled while a bright green color means that the Auto Cal feature is enabled.
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Touching the text box adjacent to either Days or Hours brings up a numeric keypad for entering the time between calibration events (up to 255 day and/ or 24 hours). On numeric display user can see max and min numeric value he can enter. After entering the value, press ENTER to place the value into the onscreen box (days or hours). When the correct values have been loaded into the Days and the Hours boxes, touch the Green LED adjacent to Auto Cal to toggle it to the lit (bright green) state. This enables the Auto Span feature. Or toggle it to the unlit (dark green) state to disable auto calibration.
After pressing ENTER, a confirmation window pops up. Selecting “OK” all inputs will be registered and the auto cal status as determined by the state of the green LED will become active.
Touching the CANCEL button will abort the present inputs and revert back to the last saved values and state.
Auto Cal countdown (if enabled) will begin as soon as the display returns to the HOME screen by pressing the HOME icon.
4.7.11 Self Test
The GC-Pro FID has a built-in self-diagnostic testing routine which automatically runs whenever the instrument is powered up. The self­testing routine can also be run by the operator at any time by pressing the Self-Test icon on the MAIN screen.
In the self-test routine, preprogrammed signals are sent through the power supply, output board, preamp board and sensor circuit. The return signal is analyzed, and at the end of the test the status of each function is displayed on the screen as either “GOOD” or “BAD”. If any of the functions fail, the System Alarm is tripped.
Note: The self diagnostics will interrupt analysis temporarily.
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To initiate a self-test from the MAIN screen press the Self Test icon
and then select either “Main Board” or “9261 Board”
Selecting “Main Board” displays the following screen:
After about one minute the results of the self test is displayed as “GOOD” or “BAD” for the various tests. Once the diagnostic test has begun, it cannot be stopped. After performing the self test the display will revert back to the Self Test screen where you can continue the diagnostics by selecting “9261 Board”.
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After about one minute the results of the self tests are displayed as “GOOD” or “BAD”. The T1 to T4 tests analyze the 4 thermocouples for continuity. Once the user enters into this screen there is no option for stopping the self test in the middle. After performing the self test the screen automatically reverts back to the self test screen.
4.7.12 Settings
Touching the Settings icon brings up a screen with eight functions that are used to customize the analyzer to your specific needs. The functions available are:
ALARMS: Used to set the alarm setpoints and determine
whether each alarm will be active or defeated, HI or LO acting, and failsafe or not.
RANGE: Used to set up three analysis ranges that can be
switched manually.
CHANGE STREAM: Used to manually switch between
sample and calibration gas.
PASSWORD: Used to establish password protection or
change the existing password.
OVERLAY CHROMATOGRAM: TIME: Used to set the current date and time on the
instrument.
INSTRUMENT INFORMATION: Displays Manufacturer,
Model, and Software version of the instrument.
COMMUNICATION: Selects between four different RS232
protocols.
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Pressing the “Settings” icon displays the following screen:
4.7.12.1 ALARMS
The GC-Pro FID provides two concentration alarms with relays. When an alarm condition exists, the relay or relays will change state. The relays are available from the 50-pin Equipment Connector as described in Section 3.3.2.5 and 3.3.2.9. The alarms screens are used to configure how the concentration alarms operate.
There are two identical screens within the ALARMS function, one for setting the parameters on ALARM 1 and the other for ALARM 2.
Pressing the ALARMS button brings up a screen where you can change or view the alarm parameters for either Alarm 1 or Alarm 2.
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Selecting ALARM 1 displays the following screen:
From this screen you can make Alarm 1 active or defeated, configure it as a high or low alarm, failsafe or non-failsafe and whether the alarm will be latching or non-latching by touching the respective LED’s.
The user can enter the trigger value (alarm setpoint) by touching in the Trigger Value box. This causes a numeric keypad to display for entering the value. Hit ENTER to close down the keypad and enter the value into the Trigger Value box.
The user can also select the group to which the Alarm will be associated by using the UP/DOWN arrows adjacent to the Source box.
The configurable items are as follows:
DEFEATED: If an alarm is defeated, its relay is de-energized,
regardless of failsafe condition. A defeated alarm does not react to a transition over its trip point in either direction.
HIGH: If an alarm is set as HIGH, it will not create a new alarm
condition (see latching) if the analysis concentration is below the trip point, if the analysis concentration is above the trip point, then an alarm condition will be created or maintained.
FAILSAFE: A non-defeated alarm that is in FAILSAFE mode energizes an alarm relay in a non-alarm condition and de-energizes an
alarm relay in an alarm condition.
Note: Failsafe condition of an alarm is a software property. This
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is not related to relays that have both normally-open and normally-closed terminals.
LATCHING: The latching property configures the alarm such that the
user must manually relieve the alarm condition even though the concentration no longer violates the trip point of the alarm. So, if an alarm is NON-LATCHING, and the analysis concentration temporarily drifts above the trip point of a HIGH alarm, the alarm condition occurs only during the time the concentration is above the trip point. If that alarm were LATCHING, the alarm condition would persist (even though the concentration is no longer above the trip point), until the user released it.
RELEASING A LATCHED ALARM: When alarm conditions are
present, the relay associated with that alarm changes state. To reset from an alarm condition, enter the Alarm 1 or Alarm 2 screen and disable the alarm. Then re-enable the alarm. If the alarm condition still exists, the alarm will again trigger.
TRIGGER POINT: This is the threshold at which an active alarm can
enter into alarm condition. If an alarm is HIGH, ACTIVE, and set at
20.00 ppb, then when the analysis concentration is at or above 20.00 ppb an alarm condition is initiated or maintained.
CAUTION: IT IS NOT GOOD PRACTICE TO SILENCE AN
EXISTING ALARM BY SETTING THE ALARM ATTRIBUTE TO ‘DEFEAT”. THE ALARM WILL NOT AUTOMATICALLY RETURN TO “ACTIVE” STATUS. IT MUST BE RESET BY THE OPERATOR. IF IT IS NOT RESET, YOUR PROCESS WILL BE RUNNING WITHOUT THE SAFEGUARDS THIS INSTRUMENT IS DESIGNED TO PROVIDE.
When finished configuring the alarms, touch the ENTER button at the bottom right corner of the screen. A confirmation window will pop up and by selecting “OK” the new alarm configuration will be the active settings. Then, by touching the HOME icon, all alarm 1 inputs will be saved permanently. Touching the CANCEL button will abort the inputs and return the previously saved values.
The ALARM 2 screen is an identical screen for configuring ALARM 2.
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Note: An alar m in 'alarm condition' is signaling that action must
be taken such as correcting the alarm or the analysis concentration. If an active (not defeated) alarm has been set to HIGH at 20.0 ppb, and the analysis concentration is above that level, then the 'alarm condition' is occurring.
4.7.12.2 RANGE
There are three settable analysis ranges on the GC-Pro FID Analyzer. Both upper and lower bounds may be set. The value of each limit on the currently selected range affects the corresponding upper and lower value of the voltage and current of the analog outputs of the analyzer as well as contact closures (if present) indicating which range is current. The analog outputs from the 50–pin Equipment connector (see Section 3.3.2.3 and Table 3-1) represent the proportion of the analysis concentration to the currently selected range limit.
RANGE LIMITS: Ranges may be set for ppb, ppm, or percent
analysis however, range 3 can only be set at a value greater than range 2 and range 2 can only be set at a value greater than range 1.In addition, the lower bound on each range must always be less than the upper bound.
To set the ranges select “Range” from the SETTINGS screen. The following screen will appear:
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Once the input range has been decided, press the corresponding LED icon to turn it on. Touch the input box and a numerical keypad will display from which you can enter the upper range limit (the lower limit on each range is always zero). Once the value is entered, press ENTER to dismiss the keypad and enter the value into the range box selected.
When finished, touch the ENTER button and the inputs with the glowing yellow LED will be converted in other available units and a confirmation pop up window will appear. Press “OK” button to proceed further.
Repeat the procedure for the other two ranges.
If the range values entered by the user does not follow the order R3>R2>R1 then a warning will display.
Touching the “OK” button allows the user to input the values again. If the input values follow the order R3>R2>R1; a final confirmation window pops up on the screen. Select OK to save or CANCEL ignore the entered inputs.
4.7.12.3 CHANGE STREAM
The Change Stream function is used to manually select between sample and calibration (span and zero) gases.
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Note: If the analyzer is equipped with the Auto Calibration
feature, input from this screen will override the Auto Calibration status.
To manually change the gas stream sent to the analyzer, press Change Stream from the SETTINGS screen. The following screen will appear:
Touch the UP arrow to toggle the display between ANALYZE/SPAN /ZERO. Pressing UPDATE will select the displayed stream and open the corresponding valve. Use CANCEL to abort the selection.
The user can return to the analyze mode by pressing the HOME icon or go back to the SETTINGS screen by touching the BACK button.
4.7.12.4 TIME
The date and time are set from the Time screen. Select Time from the SETTINGS screen.
Touching any of the Date and Time value boxes will bring up a numerical keypad that allows the date and tie to be input. The time settings entered in this screen sets the RTC which is interfaced to 9261
board on the I2C interface.
After selecting Time, the following below screen displays:
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After entering each value press the “Enter” button on the keypad to input the number and move to the next field. When all inputs have been made, press the ENTER button on the display screen and then respond to the confirmation display that appears.
Pressing “OK” saves the new date and time settings.
4.7.12.5 PASSWORD
There are two functions in the GC-Pro FID that if misused can result in significant changes to the instrument. These are: Default Settings from a Cold Boot (Section 4.7.13.5) and Firmware Upgrade. These functions are therefore password protected functions.
The password is assignable by the user or the default password “11111” can be used. The password can be any number between 1 and
99999.
To assign a new password, press “Password” from the SETTINGS screen. The following screen will appear:
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Touching the password box will display a numeric keypad allowing the new password to be entered. Press ENTER on the keypad to dismiss the keypad and insert the new password into the box.
Pressing the HOME icon installs the password and places the analyzer back into the analyze mode. Pressing BACK also installs the new password but returns the display to the SETTINGS screen.
4.7.12.6 COMMUNICATION
There are four different serial communications modes available to the user and these are accessible from the Communications screen.
The available modes are:
Detect Mode: Used with a laptop computer running custom
TAI software and is designed to interact with the chromatogram screen. (Contact TAI for software upgrade).
Query Mode: A specialized communication protocol that
enables interaction with the analyzer via an OPC server.
Profi Mode: This mode is compatible with a Teledyne
Valve Box (VB1-VB5) used in switching gas streams to an analyzer.
STD Mode: The standard mode outputs a text string every
two seconds that includes concentration, range, and alarm status. If there are multiple
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components (groups) being analyzed, the output will cycle through each component in sequence.
Press the Communications icon on the SETTINGS screen to enter
the communications function.
The user can shift between different serial modes by selecting the “Serial Mode” from the above screen and then on the next screen using the UP arrow button, cycle through the modes until the desired mode is
presented. Select the mode using the ENTER button.
Selecting Serial Number from the Communications Screen produces another screen which allows the user to input the serial number for the
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analyzer which is used by the RS232 when in Profi mode to identify the analyzer. Use the UP Arrow and then select the ENTER button next to each channel. The following example screen has the analyzer serial number set to 473200. The default serial is 100000.
4.7.13 Analysis Mode
Analysis mode is the default mode of the instrument where measurements are updated after each cycle (forward + reverse) and displayed on the HOME screen.
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The GC-Pro FID is analyzing in both the forward and reverse cycles and measurement value integrated over the last complete cycle is shown in the display box adjacent to the group identifier (G00-G09, Bnz, etc.) for any group that has been activated (LED lit). See Group Setup for activating a group. The cycle direction and time into the cycle are shown in the lower box as is the current ADC output value. The current analysis range is indicated next to the Group LED.
4.7.13.1 T-TIME
Each group has “T_Time” and “T-Cycle” selectable buttons associated with it that will bring up a graph displaying the analysis trend in the group with respect to time or cycle. With these buttons, the user can evaluate the instantaneous analysis as opposed to waiting for a complete cycle to terminate.
The T_Trend screen shows the analysis trend with respect to time.
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This screen displays the concentration behavior or trend for the
group on y axis against the time into the cycle on the x axis.
Low and High values can be set for the y axis using the “L” and “H” boxes below the graph. Touching the “Update” button will reformat the y axis index with the new input.
It is possible to view the instantaneous value by touching the trend graph at the location of interest and the corresponding value will be displayed in “Watch Line” box at the top right corner.
Note: The LOW and HIGH values must be updated by the user
as soon as system is powered on.
Note: The trend graph will not be plotted continuously; it needs to
be refreshed manually. To refresh the trend screen, press the HOME button to return to the HOME screen and then re-enter the trend screen by pressing trend button.
4.7.13.2 T_CYCLE
Similar to the above function, the T_Cycle button displays a graph of group concentration versus cycles.
The T_Cycle is display is shown below.
Both X-axis (number of cycles) and y-axis (concentration) can be changed by touching the “Setting” button. The maximum number of cycles that can be plotted is 300.
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4.7.13.3 CHROMATOGRAM
The Chromatogram function is available from the HOME screen using the “Chromatogram” button on the lower right corner of the screen. This function displays the ADC count as a function of the number of samples taken (seconds). It is useful for troubleshooting as well as setting up new applications.
Selecting “Chromatogram” from the HOME screen brings up the following screen:
Touching the “PLOT” button will display the graph on the screen and touching the “Refresh” button will clear it. Low and high limits on both the X and Y axis can be changed by touching the “Setting” button. This will cause the following screen to appear:
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Note: The Chromatogram will be displayed for maximum 1020
samples. The chromatogram will not be displayed if the total sum of the forward and backward phase duration is greater than 1020 seconds.
Note: User can view the Y axis value in digital format by entering
the corresponding X axis value in the field provided with X= symbol.
Values for the X and Y axis are entered by touching the input box. A numerical keypad appears that allows for numeric entry. Press ENTER on the keypad to enter the value into the appropriate box and dismiss the keypad. Repeat for each input box requiring an entry or change. Upon final entry, press Chromatogram button to return to the Chromatogram screen. The new X-axis and Y-axis values will be displayed on the screen. The limit for X-High is 1020 i.e., 1020 seconds. So the maximum cycle time which is the sum of the Forward and Backward phase duration should not exceed 1020 seconds (17 min) for the chromatogram.
4.7.13.4 VS COUNT
The VS (Volt-seconds) count is a measure of the conditioned signal coming from the detector. It corresponds to the strength of the output signal from the detector. The VS measure is a relative value and has no absolute relationship to concentration between groups.
4.7.13.5 COLD BOOT
The “Cold Boot” button on the HOME screen provides the user with the option of resuming the system with user configured settings or restoring the analyzer back to the default factory settings for all parameters.
The Cold Boot function is a password protected function. The default password is ‘11111’. If the password has been changed (see Section 4.7.12.5) then the new password must be entered to gain entry into the function that allows a change from the current setting.
Pressing “Cold Boot” from the HOME screen brings up the following screen:
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Selecting “Current Setting” causes the analyzer to use all the functions and settings that are presently in force, i.e. no change to the presently saved system configuration. A confirmation window pops up whereby selecting ‘OK” causes the instrument to start up as normal with the present configuration. Pressing “Cancel” reverts the display to the previous screen with no change.
However, if Factory Settings is selected, a Password Entry screen will display requiring the user to input the system password (Default Password is “11111”). After the password is input an “Access Check” pop up window will display requiring the Password to be re-entered. Press “OK” when done.
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The validation LED should glow green which means the password has been entered correctly otherwise, the password is incorrect and you will be required to enter it again.
Since this function may drastically alter the settings on the analyzer, once the password has been re-entered correctly and “OK” is pressed, a final Warning screen will appear.
Pressing “OK” will then reset the analyzer to the default configuration with the parameters set as described in Appendix C.
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