The information contained in this document is subject to change without notice.
Teflon® is a registered trademark of E.I. duPont de Nemours and Co., Inc.
Viton® is a registered trademark of E.I. duPont de Nemours and Co., Inc.
Freon12® is a registered trademark of E.I. duPont de Nemours and Co., Inc.
SNOOP
®
is a registered trademark of NUPRO Co.
Manual Part Number 081854-P
January 2001
Printed in U.S.A.
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
P
REFACE
SAFETY SUMMARY
To avoid explosion, loss of life, personal injury and damage to this equipment and
on-site property, all personnel authorized to install, operate and service the Model 340
Trace Moisture Analyzer should be thoroughly familiar with and strictly follow the
instructions in this manual. Save these instructions.
DANGER is used to indicate the presence of a hazard which will cause severe
personal injury, death, or substantial property damage if the warning is ignored
WARNING is used to indicate the presence of a hazard which can cause severe
personal injury, death, or substantial property damage if the warning is ignored.
CAUTION is used to indicate the presence of a hazard which will or can cause minor
personal injury or property damage if the warning is ignored.
NOTE is used to indicate installation, operation, or maintenance information which is
important but not hazard-related.
WARNING: ELECTRICAL SHOCK HAZARD
Do not operate without doors and covers secure. Servicing requires access to
live parts which can cause death or serious injury. Refer servicing to qualified
personnel.
For safety and proper performance this instrument must be connected to a
properly grounded three-wire source of power.
Alarm switching relay contacts wired to a separate power source must be
disconnected before servicing.
081854-P Rosemount Analytical January 2001
Model 340 Trace Moisture Analyzer
P1
REFACE
P
WARNING: POSSIBLE EXPLOSION HAZARD
This analyzer is of a type capable of analysis of sample gases which may be
flammable. If used for analysis of such gases, the detection section of the
analyzer must be either in an explosion proof enclosure suitable for the hazard
classification of the gas, or protected by a continuous dilution purge system in
accordance with Standard ANSI/NFPA-496-1986 (Chapter 8) or IEC Publication
79-2-1983 (Section Three).
If explosive gases are introduced into this analyzer, the sample containment
system must be carefully leak checked upon installation and before initial
startup, during routine maintenance and any time the integrity of the sample
containment system is broken, to ensure that the system is in leak proof
condition. Leak check instructions are provided in Section 4.2.
Internal leaks resulting from failure to observe these precautions could result in
an explosion, causing death, personal injury or property damage.
WARNING: HIGH PRESSURE GAS CYLINDERS
Fuel, air and calibration gas cylinders are under pressure. Mishandling of gas
cylinders could result in death, injury or property damage. See General
Precautions for Handling and Storing High Pressure Cylinders, in the rear of this
manual.
CAUTION: PARTS INTEGRITY
Tampering or unauthorized substitution of components may adversely affect
safety of this product. Use only factory documented components for repair.
P2
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
SPECIFICATIONS - GENERAL
NON-PORTABLE ANALYZERS
CATALOG NUMBER 193000
AC Power1: 107 to 127 VAC 50/60 Hz ±0.5 Hz, 80 Watts maximum
Sample System Materials: 316 stainless steel, Viton, Teflon
Case: General purpose, panel mounting, purgeable
CATALOG NUMBER 193001
AC Power1: 107 to 127 VAC 50/60 Hz ±0.5 Hz, 80 Watts maximum
Sample System Materials: Brass, aluminum, neoprene, Buna-N, stainless
steel.
Case: General purpose, panel mounting, purgeable
REFACE
P
2
2
C
ATALOG NUMBER
193004
AC Power1: 107 to 127 VAC 50/60 Hz ±0.5 Hz, 80 Watts maximum
Sample System Materials: 316 stainless steel, Viton, Teflon
Case: Detector module: Class I, Group D, Division 1.
Control Module: General purpose, purgeable
PORTABLE ANALYZERS
C
ATALOG NUMBER
AC Power: 107 to 127 VAC 50/60 Hz ±0.5 Hz, 20 Watts maximum
Sample System Materials: Brass, aluminum, neoprene, Buna-N, stainless
steel.
Case: Portable with carrying handle.
C
ATALOG NUMBER
DC Power: ±15 VDC from self-contained battery pack.
Sample System Materials: Brass, aluminum, neoprene, Buna-N, stainless
steel.
Case: Portable with carrying handle.
193005
193006
3
2
1
When requested by customer as a "special", the Model 340 Trace Moisture Analyzer has been modified for operation on
230 VAC power.
To verify AC power requirements for an analyzer, see the instrument name-rating plate.
If the instrument has the 230 VAC power modification, the following drawings are applicable:
780213 Schematic Diagram, 230 VAC Operation
2
Air purge. When installed with user supplied components, meets requirements of Type Z purge per ANSI/NFPA 496-
3
Air purge. When installed with user supplied components, meets requirements of Type Z purge per ANSI/NFPA 496-
1986, Chapter 2, for installation in Class I, Division 2 locations per National Electrical Code (ANSI/NFPA-70) for
analyzers sampling non-flammable gases. Analyzer sample flammable gases must be contained in a suitable explosion
proof enclosure or protected by a continuous dilution purge.
1986, Chapter 2, for installation in Class I, Division 2 locations per National Electrical Code (ANSI/NFPA-70).
Model 340 Trace Moisture Analyzer
P3
REFACE
P
SPECIFICATIONS - PERFORMANCE
R
ANGES
0 to 10, 0 to 50, 0 to 100, 0 to 500, 0 to 1000 ppm H2O by volume
ACCURACY
±5% of fullscale (not applicable to 0 to 10 ppm range or to hydrogen or oxygen
sample stream containing less than 25 ppm H2O
S
ENSITIVITY
Less than 1 ppm
BYPASS FLOW
Adjustable of 0 to 2 cubic feet per hour (940 cc/min.) is standard in nonportable instruments, and is obtainable for portable instruments through use of
optional flowmeter accessory
A
MBIENT TEMPERATURE
0°F to 120°F (-18°C to 49°C)
R
ECORDER POTENTIOMETRIC OUTPUT
All analyzers provide selectable output of 0 to 10 mV, 0 to 100 mV, 0 to 1 V, or
0 to 5 V
Output (mA)Maximum Permissible Load (ohms)
0 to 5 800
1 to 5 8000
4 to 20 2000
10 to 50 700
SPECIFICA TIONS - ALARM OPTION (PANEL MOUNT ANALYZERS ONLY)
S
ETPOINT ACCURACY
±1/2 of fullscale, or 25 mV
R
EPEATABILITY
1% of fullscale
S
ETPOINT RANGE
0 to 100% or 0 to 5 VDC, displayed on front panel meter
H
YSTERESIS
2% of fullscale is standard, adjustable by changing resistor on circuit board
P4
O
UTPUT
(1) isolated (2) 190 VDC or VAC maximum, (3) 1.5 amperes AC or DC
maximum
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
SPECIFICATIONS - SAMPLE
S
AMPLE FLOW RATE
100 cc/minute
SAMPLE PRESSURE
Standard range 10 to 100 psig (69 to 690 kPa).
Low Pressure Sampling Accessory provides range of 10 inches mercury
vacuum to +10 psig.
S
AMPLE TEMPERATURE
32°F to 120°F (0°C to 80°C)
S
AMPLE INLET/OUTLET CONNECTIONS
1/8 inch bulkhead tube fittings (Double ferrule compression type)
REFACE
P
081854-P Rosemount Analytical January 2001
Model 340 Trace Moisture Analyzer
P5
REFACE
P
CUSTOMER SERVICE, TECHNICAL ASSISTANCE AND FIELD SERVICE
For order administration, replacement Parts, application assistance, on-site or factory
repair, service or maintenance contract information, contact:
Rosemount Analytical Inc.
Process Analytical Division
Customer Service Center
1-800-433-6076
RETURNING PARTS TO THE FACTORY
Before returning parts, contact the Customer Service Center and request a Returned
Materials Authorization (RMA) number. Please have the following information when
you call: Model Number, Serial Number, and Purchase Order Number or Sales Order
Number.
Prior authorization by the factory must be obtained before returned materials will be
accepted. Unauthorized returns will be returned to the sender, freight collect.
When returning any product or component that has been exposed to a toxic, corrosive
or other hazardous material or used in such a hazardous environment, the user must
attach an appropriate Material Safety Data Sheet (M.S.D.S.) or a written certification
that the material has been decontaminated, disinfected and/or detoxified.
Return to:
Rosemount Analytical Inc.
4125 East La Palma Avenue
Anaheim, California 92807-1802
USA
TRAINING
A comprehensive Factory Training Program of operator and service classes is
available. For a copy of the Current Operator and Service Training Schedule contact
the Technical Services Department at:
Rosemount Analytical Inc.
Phone: 1-714-986-7600
FAX: 1-714-577-8006
D
OCUMENTATION
The following Model 340 Trace Moisture Analyzer instruction materials are available.
Contact Customer Service or the local representative to order.
081854 Instruction Manual (this document)
P6
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
I
NTRODUCTION
1
The Model 340 Trace Moisture Analyzer automatically and continuously measures water
vapor concentrations, up to a maximum of 1000 ppm, in a gaseous sample stream. The
determination is based on the simultaneous absorption and electrolysis of water. The
instrument has a wide range of applications, in monitoring many gases used in
manufacturing processes. (Suitable and unsuitable sample gases are listed in Section 1.2.)
Permissible sample pressure range for the standard instrument is 10 to 100 psig. Optional
sampling accessories permit monitoring gas streams at atmospheric or sub-atmospheric
pressures.
The analyzer provides direct readout on a front panel meter and a selectable output for an
accessory potentiometric recorder. With all AC operated versions of the analyzer, a
selectable output for a current type recorder is obtainable through use of an optional plug in
the circuit board.
1.1 INSTRUMENT CONFIGURATIONS
The Model 340 Analyzer is made in the following configurations:
1. Panel Mounted Analyzer, Figure 1-1, with detector, electronic circuitry, and operating
controls housed in a single purgeable case. Available with internal flow system of either
stainless steel (193000 Analyzer) or brass (193001 Analyzer).
2. The 193004 Explosion Proof Analyzer, Figure 1-2. Designed for use in the chemical,
petrochemical, and petroleum industries, in applications where the sample stream
contains flammable gases, or where explosive vapors may be present at the installation
site. Control section is similar to that of the Panel Mounted Analyzer. Detector section is
contained in an explosion proof housing that meets the requirements for installation
under hazardous conditions specified as Class 1, Group D, Division 1, in the National
Electrical Code. Flow system is of stainless steel.
3. Portable Analyzer, Figure 1 -3. Available for operation on either 115 VAC, 50/60 Hz
(193005 Analyzer) or ±15 VDC from a self contained battery pack (193006 Analyzer).
Except where specifically stated otherwise, information in this manual applies to all versions
of the instrument.
081854-P Rosemount Analytical January 2001
Model 340 Trace Moisture Analyzer
1
NTRODUCTION
I
Alarm Setpoint
Accessory
Note:: Illustration applicable to 193000 and 193001 Analyzers
IGURE
F
1-1. P
ANEL MOUNTED TRACE MOISTURE ANALYZER
Alarm Setpoint
Accessory
IGURE
F
2
Detector SectionControl Section
Note:: This instrument is no longer available – Consult Factory
1-2. E
XPLOSION-PROOF TRACE MOISTURE ANALYZER
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
Note:: Illustration applicable to 193005 and 193006 Analyzers
NTRODUCTION
I
IGURE
F
1-3. P
ORTABLE TRACE MOISTURE ANALYZER AND FLOWMETER ACCESSORY
1.2 SAMPLE GASES
WARNING: POSSIBLE EXPLOSION HAZARD
This analyzer is of the type capable of analysis of sample gases which may be
flammable. If used for analysis of such gases, the detection section of the analyzer
must be either in an explosion proof enclosure suitable for the hazardous
classification of the gas , or, protected by a continuous dilution purge system in
accordance with Standard ANSI /N FPA-496 -1986 (Chapter 8) or IEC Publication
79-2-1983 (Section Three).
If explosive gases are introduced into this analyzer, the sample containment system
must be carefully leak checked upon installation and before initial startup, during
routine maintenance and any time the integrity of the sample containment system is
broken, to ensure that the system is in leak proof condition. Leak check instructions
are provided in Section 4.2.
Internal leaks resulting from failure to observe these precautions could result in an
explosion causing death, personal injury or property damage.
Determination of whether a sample stream of a particular composition is suitable for
monitoring depends on its compatibility with the construction materials in a) the detector
cell, and b) the instrument flow system. In all instruments, the detector cell utilizes a thin film
of phosphorous pentoxide (P2O6) on rhodium electrodes. Depending on the intended
081854-P Rosemount Analytical January 2001
Model 340 Trace Moisture Analyzer
3
NTRODUCTION
I
application of a given instrument version, its internal flow system is constructed of either
stainless steel (for corrosion resistance) or brass (for non-corrosive sample gases only).
Gases that react with P206 to produce additional water
Example: alcohols, HF.
Gases that react with construction materials of the instrument
Gases that react with P2O6 to alter required absorption characteristics of the P2O
film
6
Examples: ammonia, amines.
Gases that polymerize to form a solid or liquid phase (they gradually desensitize the
detector cell by coating or clogging)
Example: Unsaturated hydrocarbons - alkynes, alkadienes and alkenes.
Gases that contain particulate solid or liquid materials such as dust and dirt found in
furnace atmosphere gases.
These must be avoided or filtered out upstream; oil mist or dust from some types of dryers
can clog the detector cell or desensitize the P2O6 film by forming a layer over the film.
4
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
I
NSTALLATION
2
2.1 FACILITY PREPARATION
Sections 2.1.1 through 2.1.4 provide information that may be required prior to installation.
2.1.1 O
For significant dimensions of the instrument, refer to the appropriate Drawing at the back of
the manual.
2.1.2 I
Drawing 194759 shows electrical interconnection for the 193004 Explosion Proof Analyzer.
Note::
Separate conduits should be used for the power cable and the interconnection cable.
2.1.3 L
Ambient temperature range for all analyzers is 0°F to 120°F (-18°C to 49°C). Additional
requirements, specific to the various analyzer configurations, are given in the following:
193000 and 193001 Panel Mounted Analyzers
Install in a clean area, not subject to excessive vibration or extreme temperature variations.
Preferably, the instrument should be mounted near the sample stream, to minimize
transport time.
UTLINE AND MOUNTING DIMENSIONS
NTERCONNECTION DIAGRAM (EXPLOSION PROOF ANALYZERS ONLY
OCATION
)
193004 Explosion Proof Analyzer
Detector Section: Criteria for installation site are proximity to sample point, protection from
environment, and accessibility for servicing. Protect the unit adequately against shock and
extreme vibration.
Control Section: Principal criteria for the installation site is that it must be outside the
hazardous area. Hazardous locations are defined in Article 500 of the National Electrical
Code. An additional consideration is convenience in taking readings and servicing the unit.
081854-P Rosemount Analytical January 2001
Model 340 Trace Moisture Analyzer
5
NSTALLATION
I
2.1.4 U
Electrical power requirements are listed in the following table:
193000 and 193001 Panel Mounted Analyzers
193004 Explosion Proof Analyzer
Unpack instrument carefully. For a list of items supplied in the shipping kit, refer to Section
Ten.
2.3 ELECTRICAL CONNECTIONS
Depending on the particular options used, electrical setup may entail insertion of various
selector plugs into appropriate positions in the associated circuit boards. Locations of circuit
boards and other components within the several analyzer configurations are shown in
Figures 2-1 and 2-2. Locations of selector plugs on the individual circuit boards are shown
in Figure 2-3.
IGURE
F
6
2-1. I
NTERIOR OF PANEL MOUNT ANALYZER
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
NSTALLATION
I
Make electrical connections in the following sequence:
1. If a recorder is to be used, select the particular output required and make the
appropriate cable connections as explained in Section 2.3.1 (potentiometric recorder) or
Section 2.3.2 (current recorder). All analyzers provide potentiometric output. Current
output is obtainable from AC operated instruments only, through use of the optional
current output circuit board.
2. If an alarm system is to be used, select the desired function and connect the output as
explained in Section 2.3.3 Alarm output is obtainable from panel mounted instruments
only, through use of the Alarm Setpoint Accessory and Universal Alarm Board in
combination.
3. W ith Explosion Proof Analyzer, interconnect detector and control modules per Section
2.3.4.
4. Supply electrical power to analyzer per Section 2.3.5.
IGURE
F
081854-P Rosemount Analytical January 2001
2-2. I
NTERIOR OF EXPLOSION PROOF ANALYZER
Model 340 Trace Moisture Analyzer
7
NSTALLATION
I
IGURE
F
IGURE
F
8
2-3. L
2-4. U
OCATIONS OF SELECTOR PLUGS ON CIRCUIT BOARDS
NIVERSAL ALARM BOARD CONNECTIONS
January 2001 Rosemount Analytical 081854-PModel 340 Trace Moisture Analyzer
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