PASCO SP-9268A User Manual

Instruction Manual and Experiment Guide
STUDENT
SPECTROMETER
012-02135F
10/03
Copyright © January 1991 $7.50
®
10101 Foothills Blvd. • P.O. Box 619011 • Roseville, CA 95678-9011 USA
Phone (916) 786-3800 • FAX (916) 786-8905 • email: techsupp@PASCO.com
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Model Name 012–0xxxxA
34
012-02135F Spectrometer
T ab le of Contents
Section Page
Equipment Return .............................................................................................ii
Introduction ......................................................................................................1
Equipment ........................................................................................................2
Equipment Setup...............................................................................................3
Measuring Angles of Diffraction ....................................................................... 4
Using the Diffraction Grating ............................................................................5
Using the Prism.................................................................................................6
Maintenance .....................................................................................................8
Appendix: Using the Gaussian Eyepiece ...........................................................9
Technical Support ..................................................................................... back cover
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Spectrometer 012-02135F
Copyright, W arranty and Equipment Return
Please—Feel free to duplicate this manual subject to the copyright restrictions below.
Copyright Notice
The PASCO scientific Model SP-9268A Student Spec­trometer manual is copyrighted and all rights reserved. However, permission is granted to non-profit educational institutions for reproduction of any part of this manual providing the reproductions are used only for their laboratories and are not sold for profit. Reproduction under any other circumstances, without the written consent of PASCO scientific, is prohibited.
Limited Warranty
PASCO scientific warrants this product to be free from defects in materials and workmanship for a period of one year from the date of shipment to the customer. PASCO will repair or replace, at its option, any part of the product which is deemed to be defective in material or workmanship. This warranty does not cover damage to the product caused by abuse or improper use. Determi­nation of whether a product failure is the result of a manufacturing defect or improper use by the customer shall be made solely by PASCO scientific. Responsibil­ity for the return of equipment for warranty repair belongs to the customer. Equipment must be properly packed to prevent damage and shipped postage or freight prepaid. (Damage caused by improper packing of the equipment for return shipment will not be covered by the warranty.) Shipping costs for returning the equipment, after repair, will be paid by PASCO scientific.
Equipment Return
Should this product have to be returned to PASCO scientific, for whatever reason, notify PASCO scientific by letter or phone BEFORE returning the product. Upon notification, the return authorization and shipping instructions will be promptly issued.
NOTE: NO EQUIPMENT WILL BE ACCEPTED FOR RETURN WITHOUT AN AUTHORIZATION.
When returning equipment for repair, the units must be packed properly. Carriers will not accept responsibility for damage caused by improper packing. To be certain the unit will not be damaged in shipment, observe the following rules:
1. The carton must be strong enough for the item shipped.
2. Make certain there is at least two inches of packing material between any point on the apparatus and the inside walls of the carton.
3. Make certain that the packing material can not shift in the box, or become compressed, thus letting the instrument come in contact with the edge of the box.
Address: PASCO scientific
10101 Foothills Blvd. P.O. Box 619011
Roseville, CA 95678-9011 Phone: (916) 786-3800 FAX: (916) 786-8905
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012-02135F Student Spectrometer
Introduction
In principle, a spectrometer is the simplest of scientific instruments. Bend a beam of light with a prism or dif­fraction grating. If the beam is composed of more than one color of light, a spectrum is formed, since the vari­ous colors are refracted or diffracted to different angles. Carefully measure the angle to which each color of light is bent. The result is a spectral "fingerprint," which car­ries a wealth of information about the substance from which the light emanates.
In most cases, substances must be hot if they are to emit light. But a spectrometer can also be used to investigate cold substances. Pass white light, which contains all the colors of the visible spectrum, through a cool gas. The result is an absorption spectrum. All the colors of the vis­ible spectrum are seen, except for certain colors that are absorbed by the gas.
The importance of the spectrometer as a scientific instru­ment is based on a simple but crucial fact. Light is emit­ted or absorbed when an electron changes its orbit within an individual atom. Because of this, the spectrometer is a powerful tool for investigating the structure of atoms. It's also a powerful tool for determining which atoms are present in a substance. Chemists use it to determine the constituents of molecules, and astronomers use it to de­termine the constituents of stars that are millions of light years away.
In its simplest form, a spectrometer is nothing more than a prism and a protractor. However, because of the need for very sensitive detection and precise measurement, a real spectrometer is a bit more complicated. As shown in Figure 1, a spectrometer consists of three basic compo­nents; a collimator, a diffracting element, and a tele­scope.
The light to be analyzed enters the collimator through a narrow slit positioned at the focal point of the collimator lens. The light leaving the collimator is therefore a thin, parallel beam, which ensures that all the light from the slit strikes the diffracting element at the same angle of incidence. This is necessary if a sharp image is to be formed.
The diffracting element bends the beam of light. If the beam is composed of many different colors, each color is diffracted to a different angle.
The telescope can be rotated to collect the diffracted light at very precisely measured angles. With the tele­scope focused at infinity and positioned at an angle to collect the light of a particular color, a precise image of the collimator slit can be seen. For example, when the telescope is at one angle of rotation, the viewer might see a red image of the slit, at another angle a green im­age, and so on. By rotating the telescope, the slit images corresponding to each constituent color can be viewed and the angle of diffraction for each image can be mea­sured. If the characteristics of the diffracting element are known, these measured angles can be used to determine the wavelengths that are present in the light.
SOURCE
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COLLIMATOR
SLIT
LIGHT
RED LIGHT
COLLIMATOR
PARALLEL BEAM
Figure 1 Spectrometer Diagram
DIFFRACTION GRATING
1
GREEN LIGHT
(OR PRISM)
TELESCOPE
ANGLE OF DIFFRACTION
EYE PIECE
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