Oakton T-100 Data Sheet

Oakton
T-100 Waterproof Turbidimeter Operation Instructions
T-100 Turbidimeter
Getting Started
This instrument operates on the nephelometric principle of turbidity measurement and is designed to meet the criteria specifi ed in ISO 7027 and DIN 27027 standards.
Using a Phillips screwdriver, remove the screws from the battery cover and install (4) AAA batteries (included). Tighten the screws to retain a waterproof seal when completed.
Sample Vial
Sample Well
Index Mark
Liquid Crystal Display
Keypad
Light Shield Cover
- for covering the vial
Keypad Functions
Powers on and shuts off the meter. The meter automatically shuts off 20 minutes after last key press.
Initiates the calibration mode. Press during calibration mode to abort the calibration and enter Standby “
mode.
When in measurement mode, the READ/ENTER key is used to perform a measurement. Single Measurements: When the key is pressed and released immediately (less than 0.3 seconds), the display will blink “
” for 10 times and then
display the measured value. Continuous Measurements: If the READ/ENTER key is pressed and held, the instrument will perform a continuous measurement during which the display is updated every 2 seconds. This can be used for indexing vials. (This function is not available in calibration mode). After the READ/ENTER key is released, the instrument will automatically perform a single measurement.
During calibration mode, these keys are used to select the calibration point in an incremental/ decremental manner. Note: This meter uses an auto incrementing feature, i.e. after the successful calibration of one point it automatically selects the next calibration point, or automatically exits the calibration mode after the fourth calibration point. See also “Restoring Factory Calibration”.
Turbidity Calibration
The T-100 was calibrated and tested prior to leaving the factory. The T-100 kit includes (4) primary standards (0.02, 20.0, 100 and 800 NTU) to verify the meter calibration or to recalibrate the meter as needed. Before measuring samples for the fi rst time, perform a meter calibration with the primary standards. Four standard vials are included and labeled for each standard level. 800 NTU (CAL 1), 100 NTU (CAL 2), 20.0 NTU (CAL 3),
0.02 NTU (CAL 4).
Place the light shield cover over the vial to keep stray light from changing the calibration and sample measurement readings. In many environments, the light shield is not required as the vial cap is able to keep stray light from entering the sample well.
Indexing is not required due to the high quality of the glass vials. Simply align the index mark (arrow) on the vial with the index mark (arrow) on the meter.
Note: Do not shake the calibration standards as air entrapment will introduce error. Do not allow the calibration standards to freeze as this will cause permanent damage to the standards, making them inaccurate.
Calibration Procedure
Preparing the Calibration Standard Vials
Ensure there are no scratches or marks on the glass vial. If there are marks that could affect the turbidity measurement, select another vial. Before using the standards for the fi rst time, rinse the inside of the vial with a small amount of the same NTU standard that will be used to fi ll that vial.
1. Gently pour about 5 mL from the 60 mL stock standard into the vial.
2. Cap and swirl the vial so the inside of the vial is fully rinsed with the standard.
3. Pour the standard out of the vial and discard it.
4. Repeat steps 1 through 3.
5. Gently fi ll the vial using the 60 mL stock standard above the fi ll line on the vial and cap the vial.
6. Repeat this rinse and fi lling procedure for the other three vials. Note: The vial rinsing is critical for precision with the lower
NTU standards.
Use these calibration standard vials daily as a check, and also periodically for calibration as needed. When the standard reading of 20.0, 100, or 800 NTU drifts more than 10 % of the standard’s NTU value, the solution should be replaced with another aliquot from the plastic bottle following the steps listed above. Note: 0.02 NTU standard read back value should be <0.1 NTU.
Calibration Sequence
Place the CAL 1
standard into the sample
well and press “CAL
CAL 1
800 NTU
Blinks
Press ENTER to accept
Blinks Blinks
Place the CAL 2
CAL 2
standard into the
100 NTU
sample well
Press ENTER to accept
Blinks
Ready To Measure
Blinks
Press ENTER to accept
Place the CAL 4
CAL 4
standard into the
0.02 NTU
sample well
Press ENTER to accept
Place the CAL 3
CAL 3
standard into the
20.0 NTU
sample well
Restoring Factory Calibration
1. With the meter off, press and hold s key.
2. Power on the meter using ON/OFF. Release s key when “
(User-Reset) appears in the display.
3. The display shows “ “
”.
4. Use s or t key to choose “
” for about 2 seconds and then shows
” or “ ”.
= To restore meter back to factory calibration values
= To retain last calibrated values
5. Press READ/ENTER key to confi rm. When “ meter performs a reset, and will blink “
” is selected, the
” to indicate that it is
reading in measurement mode.
Turbidity Measurement
Insert vial containing sample or calibration standards before powering on. Alternatively, from “
” mode,
press READ/ENTER.
Calibration Standards Battery Indicator
Vial is currently Reading in measurement mode
Reading in (Nephelometric Turbidity Units (NTU) is displayed. “ message will occur if a vial is not present.
” error
“X.X” is software revision number
Turbidity Measurement
Good techniques are important for accurate turbidity measurements. For best results, use clean sample vials, properly position the vial in the sample well, cover the vial with the light shield cover, use proper handling of standards, use supplied cloth to keep vials clean and scratch free, and perform meter calibration as needed.
Preparation of Sample Vial
1. Obtain a clean, dry sample vial.
2. Handle the sample vial only by the cap to avoid fi ngerprints on the glass.
3. Rinse the vial with approximately 10 mL of the sample, capping the vial with the black screw cap and gently inverting it several times. Discard the used sample and repeat.
4. Fill the rinsed vial with the sample up to the mark indicated in the vial. Cap the vial with the supplied black screw cap.
5. Wipe the vial with the soft, lint-free cloth supplied. Ensure that the outside of the vial is dry, clean and free from smudges.
6. Apply a thin fi lm of silicone oil (supplied) on the sample vial (see image below).
7. Wipe with a soft cloth to obtain an even distribution over the entire vial’s surface. The purpose of oiling the vial is to fi ll small scratches and to mask the imperfection in the glass. Do not apply large quantity of oil as this may collect dirt and dust.
8. The sample vial is now ready to be inserted into the sample well for measurement.
Applying a thin fi lm of silicon to the sample vial
Fill line
Oakton
T-100 Waterproof Turbidimeter Operation Instructions
Measurement Procedure
1. Turn meter off, and place on a fl at, level surface.
2. Place the sample vial inside the sample well and align the vial’s index mark with the meter’s index mark.
Align index mark on the vial with the index mark on the turbidimeter
3. Push the vial down until it is seated.
4. Place the light shield cover over the vial that is inserted into the sample well.
5. Turn on the meter by pressing the ON/OFF key. After the power-up sequence, the meter goes to measurement mode and the display blinks “
* When meter is in “
”. The measured reading appears in the display.
” mode after calibration it is ready for
measurement. Press the READ/ENTER key. The display blinks “
” until the measured reading appears.
Notes:
• NEVER pour liquid directly into the sample well of the instrument.
Always use a vial. The instrument will only accurately measure the turbidity of a sample when vials sealed with the black caps are used. The black cap serves as both seal and a primary light shield.
• NEVER attempt to clean the sample well. The optics may
be damaged.
• For battery conservation, the instrument automatically powers off
20 minutes after the last key pressed.
Measurement Sequence
Place sample
vial into the
sample well
Sample
Unknown
NTU
Power on meter or from Standby mode, press and release READ/ENTER
” blinks until stable,
then displays measured value
Troubleshooting Guide
The T-100 turbidimeter routinely performs self-diagnostics, and will automatically generate messages to provide you with specifi c diagnostic information.
Message Description Corrective Actions
Calibration Error. The meter is unable to recognize the 800 NTU Calibration Standard.
Calibration Error. The meter is unable to recognize the 100 NTU Calibration Standard.
Calibration Error. The meter is unable to recognize the 20.0 NTU Calibration Standard.
Calibration Error. The meter is unable to recognize the 0.02 NTU Calibration Standard.
Check or replace the 800 NTU calibration standard.
Check or replace the 100 NTU calibration standard.
Check or replace the
20.0 NTU calibration standard.
Check or replace the
0.02 NTU calibration standard.
General Calibration Error. There is not suffi cient signal to achieve the appropriate
Perform recalibration with all (4) standards.
resolution.
Ensure the vial is
Excessive stray light detected.
properly seated in the sample well. Use light
shield cover. Lamp Failure. Return unit. “Over Range”; value is above
maximum measurement range. Low battery indication. The
batteries need to be replaced.
Dilute sample.
Replace batteries.
Routine Maintenance and Care
The supplied carrying case is optimal for protecting the instrument. If you do not plan on leaving the instrument in the supplied carrying case, when not in use, ensure that the instrument has been turned off and that a clean sample vial fi tted with a black cap has been placed in the sample well. This will ensure that a minimal amount of dust and/or debris will be able to settle on the optics of the instrument.
Proper measurement of the turbidity of a sample requires the use of a vial that is free of marks, smudges, scratches and bacterial growth. Sample vials must be handled with absolute care to avoid contamination or damage, which might change the optical characteristics of the glass. Scratches, fi ngerprints, and water droplets on the sample vial or inside the sample well can cause stray light interference leading to inaccurate readings.
Cleaning the vial is accomplished by washing the interior and exterior of the vial in a detergent solution. Once cleaned, the vial should be rinsed thoroughly 8 to 10 times with clean distilled water to eliminate the possibility of detergent buildup and streaking.
Vials can also be acid washed periodically and coated with a special silicone oil to fi ll small scratches and mask the imperfections in the glass. Since the silicone oil required for this application should have the same refractive characteristics as glass, it is recommended that the oil be obtained from us. Care should be taken not to apply excessive oil that could attract dirt or contaminate the sample well of the meter. Once the oil has been applied to the vial, the excess oil should be removed with a lint-free cloth. The result should be a sample vial surface with a dry appearance, but with all imperfections fi lled with oil.
Sample vials should always be handled from the top or by the cap to avoid fi ngerprints or smudges. After a vial has been fi lled with a sample and capped, the outside surface should be wiped with a clean, lint-free absorbent cloth until it is dry. Cleaned and dried vials should be stored with the black caps on. The vials can be stored in the carrying case. During normal operation you may use any typical glass cleaner along with a lint free cloth or tissue (Kimwipes
®
), to clean the
outside of the vials. Condensation may appear on the vial when your sample is very cold
and the relative air humidity is high. When this happens, the turbidity that you read may be higher than the actual turbidity due to the light scattered by the condensate on the vial. To alleviate this problem, coat the vial with an anti-fogging agent, or by running warm water over the vial for a short period of time to warm the sample prior to measurement.
Intended Use, Maintenance & Precautions
This instrument is designed for turbidity measurement of water-based solutions. For routine maintenance dust or wipe the display using a damp cloth. If necessary, warm water or a mild water based detergent can be used. Immediately remove any spilled substance from contact with the meter using the proper cleaning procedure for the type of spill.
• Do not use this equipment in potentially explosive atmospheres.
• Ensure that no liquid enters the instrument.
• Do not use any aggressive cleaning chemicals (solvents or similar agents).
• There are no user serviceable parts inside. Attempts to service internal parts may void the warranty.
• Not intended for medical applications or patient use.
WARNING: No modifi cation of this equipment is allowed.
Instrument Operating Conditions Operating Ambient Temp. 0 to 50 ºC Operating Relative
Humidity
0 to 90 %, non-condensing at 30 ºC
Storage Temp. -20 to +60 ºC (instrument only)
Storage Relative Humidity
0 to 90 %, non-condensing at 30 ºC
Pollution Degree 2 Overvoltage Category II Weight 200 g Size (L x W x H) 15.5 x 6.8 x 4.6 cm Battery Requirement 4 x AAA (LR03) 1.5 V batteries Vibration Shipping/handling per ISTA #1A Shock Drop test in packaging per ISTA #1A
Certifi cations/Compliance
FCC part 15 class A, TUV 3 in 1, CE, RoHS
Ordering Information
Waterproof T-100 handheld turbidimeter
35635-00
with set of 4 calibration standards (800, 100,
20.0 & 0.02 NTU), sample vials, lint-free cloth, silicone oil, batteries, and hard carrying case
Waterproof T-100 handheld turbidimeter,
35635-05
sample vials, lint-free cloth, silicone oil, batteries, and hard carrying case
35635-52
Calibration kit set – standard solutions (0.02,
20.0, 100, 800 NTU) 60 mL each and (4) vials
35653-55 Pack of 3 sample vials 00159II Silicone oil (10 mL) 00131SH /
32X366401
Replacement light shield cover
67X357201 Replacement cloth 09376-00 AAA batteries 12/pack
Oakton Instruments
625 East Bunker Court, Vernon Hills, IL, 60061, USA Tel: 1-888-462-5866 • Fax: 1-847-247-2984 info@4oakton.com • www.4oakton.com
68X357701 08/15 Rev10
Oakton
Instrucciones de funcionamiento del turbidímetro a prueba de agua T-100
Turbidímetro T-100
Primeros pasos
Este instrumento funciona de acuerdo con el principio nefelométrico de medición de turbidez y su diseño cumple los criterios especifi cados por las normas ISO7027 y DIN27027.
Con ayuda de un destornillador de estrella, extraiga los tornillos de la tapa de las pilas e introduzca las (4) pilas AAA (incluidas). Apriete los tornillos para mantener el sellado impermeable.
Vial para muestras
Puerto para muestras
Marca indicadora
Pantalla de cristal líquido
Teclado
Cubierta protectora
de luz
(para cubrir el vial)
Funciones del teclado
Enciende y apaga el medidor. El medidor se apaga automáticamente 20minutos después de que se presiona una tecla por última vez.
Inicia el modo de calibración. Presione durante el modo de calibración para anular la calibración y pasar al modo en espera “
”.
Cuando se presiona en el modo de medición, la tecla
READ/ENTER se usa para llevar a cabo una medición. Mediciones individuales: Cuando se presiona
la tecla y sesuelta inmediatamente (en menos de 0,3segundos), lapantalla parpadeará con el mensaje “
” 10veces ydespués mostrará el
valor medido. Mediciones continuas: Si se presiona y mantiene pulsada la tecla READ/ENTER, el instrumento llevará a cabo una medición continua durante la cual la pantalla se actualizará cada 2segundos. Esto se puede utilizar para indexar archivos. (Esta función no está disponible en el modo de calibración). Una vez que se suelta la tecla READ/ENTER, el instrumento realizará una medición automáticamente.
Durante el modo de calibración, estas teclas se usan para seleccionar el punto de calibración en un orden ascendente o descendente. Nota: Este medidor usa una característica de aumento automático; es decir, después de calibrar con total éxito un punto, selecciona automáticamente el siguiente punto de calibración o sale de manera automática del modo de calibración después del cuarto punto de calibración. Vea también «Restauración a la calibración de fábrica».
Calibración de la turbidez
El T-100 ha sido calibrado y probado antes de salir de fábrica. El kit del T-100 incluye (4) patrones primarios (0,02; 20,0; 100 y 800 NTU) para comprobar la calibración del medidor o para recalibrarlo cuando fuera necesario. Antes de medir muestras por primera vez, realice una calibración del medidor con los patrones primarios. Se incluyen cuatro viales con patrones etiquetados según el nivel del estándar. 800 UNT (CAL 1), 100 UNT (CAL 2), 20,0 UNT (CAL 3), 0,02 UNT (CAL 4).
Coloque el protector de luz sobre el vial para evitar que la luz dispersa modifi que la lectura de la medición de la muestra o el calibrador. En muchos ambientes, no es necesario el protector de luz, ya que el propio tapón del vial impide que la luz dispersa entre en el puerto para muestras.
La indexación no es necesaria debido a la alta calidad de los viales de vidrio. Simplemente alinee la marca indicadora (fl echa) del vial con la marca indicadora (fl echa) del medidor.
Nota: No agite los patrones de calibración, ya que el aire atrapado puede provocar errores. No deje que se congelen los patrones de calibración, puesto que esto haría que perdieran su exactitud y quedarían invalidados.
Procedimiento de calibración
Preparación de los viales con patrones de calibración
Asegúrese de que el vidrio del vial no tenga ninguna marca o rayón. Si hubiera alguna marca que pudiera afectar a la medición de la turbidez, use otro vial. Antes de usar los patrones por primera vez, enjuague el interior del vial con una pequeña cantidad del mismo patrón UNT que se usará para rellenar el vial.
1. Vierta cuidadosamente en el vial unos 5ml de la solución patrón de 60ml.
2. Tape y gire el vial de manera que el interior se enjuague completamente con el patrón.
3. Vacíe el patrón del vial y deséchelo.
4. Repita los pasosdel 1 al 3.
5. Rellene con cuidado el vial usando la solución patrón de 60ml por encima de la línea de rellenado marcada en el vial y tápelo.
6. Repita este procedimiento de enjuague y rellenado para los otros tres viales.
Nota: El enjuagado de los viales es crucial para la precisión con los
patrones UNT más bajos.
Use estos viales como patrón de calibración diaria o como comprobación y, asimismo, úselos regularmente cuando necesite realizar una calibración. Cuando la lectura del patrón de 20,0, 100 u 800 UNT difi era más de un 10% del valor de UNT marcado, se deberá cambiar la solución por otra alícuota del frasco de plástico siguiendo los pasos descritos anteriormente.
Nota: El valor límite del patrón de 0,02 UNT debe ser <0,1UNT.
Secuencia de calibración
Coloque el estándar CAL 1 en el puerto para muestras
y pulse “CAL”
CAL 1
800UNT
Parpadea
Pulse ENTER para aceptar
Parpadea Parpadea
Coloque el estándar
CAL 2
CAL 2 en el puerto
100UNT
para muestras
Pulse ENTER para aceptar
Parpadea
Listo para medir
Parpadea
Pulse ENTER para aceptar
Coloque el
CAL 4
estándar CAL 4
0,02UNT
en el puerto para muestras
Pulse ENTER para aceptar
Coloque el
CAL 3
estándar CAL 3
20,0UNT
en el puerto para muestras
Restauración a la calibración de fábrica
1. Con el medidor apagado, mantenga presionada la tecla s.
2. Encienda el medidor con la tecla ON/OFF. Suelte la tecla s
cuando la pantalla muestre “
3. La pantalla mostrará “ continuación “
”.
4. Use las teclas s o t para elegir “
= Para restaurar los valores de calibración de fábrica del
” (Reinicio del usuario).
” durante unos 2 segundos y a
” o “ ”.
medidor.
= Para mantener los últimos valores de calibración.
5. Pulse la tecla READ/ENTER para confi rmarlo. Cuando selecciona “
”, el medidor lleva a cabo un reinicio y parpadeará el mensaje
” para indicar que está leyendo en modo de medición.
Medición de la turbidez
Introduzca el vial que contiene la muestra o los patrones de calibración antes de encender el equipo. También, desde el modo “ puede pulsar READ/ENTER.
Patrones de calibración Indicador de las pilas
”,
El vial se encuentra actualmente leyendo en el modo de medición
“X.X” es el número de versión del software
Se muestra la lectura en unidades nefelométricas de turbidez (UNT). Elmensaje de error “ aparece si no se ha colocado ningún vial.
Medición de la turbidez
Es muy importante una buena técnica para obtener medidas precisas de la turbidez. Para obtener mejores resultados, utilice viales de muestras limpios, correctamente colocados en el puerto para muestras, cubra el vial con la cubierta protectora de luz, manipule adecuadamente los patrones, utilice los paños suministrados para mantener los viales limpios y sin rayones y lleve a cabo la calibración del medidor cuando sea necesario.
Preparación del vial para muestras
1. Disponga un vial para muestras limpio y seco.
2. Manipule el vial para muestras únicamente tomandolo por la tapa, para evitar dejar huellas en el vidrio.
3. Enjuague el vial con aproximadamente 10ml de la muestra, tapando el vial con la tapa negra de rosca y dele la vuelta suavemente varias veces. Deseche la muestra usada y repita la operación.
4. Rellene el vial enjuagado con la muestra hasta la marca señalada en el vial. Tape el vial con la tapa negra de rosca suministrado.
5. Limpie el vial con el paño suave y sin pelusa que se suministra. Asegúrese de que el exterior del vial está seco, limpio y sin manchas.
6. Aplique una fi na capa de aceite de silicona (suministrado) sobre el vial de la muestra (vea la imagen siguiente).
7. Use un paño fi no para distribuirlo por toda la superfi cie del vial. El fi n del aceite en el vial es rellenar pequeños rayones y disimular las imperfecciones del vidrio. No aplique demasiado aceite, ya que entonces podría arrastrar partículas de polvo y suciedad.
8. Ahora el vial para muestras ya está preparado para introducirse en el puerto para muestras para la medición.
Aplicación de una fina película de silicona al vial de la muestras
Rellenar hasta la línea
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