Labconco 7900000, 7900001, 7900002, 7900003, 7900010 User Manual
...
7900000
7900001
7900002
7900003
7900010
7900011
7900012
7900013
7910000
7910001
7910010
7910011
7910012
7910013
7910014
7910015
RapidVap Vacuum, N2 & N2/48
Evaporation Systems
Models
Warranty
Labconco Corporation provides a warranty to the original buyer for the repair or replacement of parts and
reasonable labor as a result of normal and proper use of the equipment with compatible chemicals. Broken
glassware and maintenance items, such as filters, gaskets, light bulbs, finishes and lubrication are not
warranted. Excluded from warranty are products with improper installation, erratic electrical or utility supply,
unauthorized repair and products used with incompatible chemicals.
The warranty for RapidVap® Vacuum, N2 & N2/48 Evaporation Systems will expire one year from date of
installation or two years from date of shipment from Labconco, whichever is sooner. Warranty is nontransferable and only applies to the owner (organization) of record.
Buyer is exclusively responsible for the set-up, installation, verification, decontamination or calibration of
equipment. This limited warranty covers parts and labor, but not transportation and insurance charges. If the
failure is determined to be covered under this warranty, the dealer or Labconco Corporation will authorize
repair or replacement of all defective parts to restore the unit to operation. Repairs may be completed by 3rd
party service agents approved by Labconco Corporation. Labconco Corporation reserves the rights to limit this
warranty based on a service agent’s travel, working hours, the site’s entry restrictions and unobstructed access
to serviceable components of the product.
Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages
of any kind. This warranty is exclusive and in lieu of all other warranties whether oral, or implied.
Copyright © 2017 Labconco Corporation. The information contained in this manual and the accompanying
products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves
the right to make periodic design changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be
accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery
carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by
various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to
user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact
Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525
or 1-816-333-8811, between the hours of 7:30 a.m. and 5:30 p.m., Central Standard Time.
Part #7490100, Rev. K
ECO #L122
ORIGINAL INSTRUCTIONS
T
T
AABBLLEE
O
O
FF
C
C
OONNTTEENNTTSS
CHAPTER 1: INTRODUCTION 1
About This Manual 2
Typographical Conventions 3
Your Next Step 3
CHAPTER 2: PREREQUISITES 5
Electrical Requirements 5
Location and Exhaust Requirements 6
Vacuum Pump Requirements 6
Vacuum Line Traps 7
Nitrogen Supply Requirements 8
Space Requirements 8
Tools Required 8
Your Next Step 8
CHAPTER 3: GETTING STARTED 9
Unpacking Your RapidVap 9
RapidVap Components 10
Setting Up Your RapidVap 12
Vacuum Pump Connection 12
Sample Block 13
Nitrogen Gas Connection 15
Exhaust Port 15
Electrical Connection 15
Calibrate the Vacuum Sensor 15
Chemical Attack on RapidVap Components 15
Solvent Safety Precautions 17
Your Next Step 18
CHAPTER 4: USING YOUR RAPIDVAP 19
Planning 19
Glassware Selection and Speed Setting Guidelines 20
Loading Glassware Into the RapidVap 22
Heat Setting Guidelines 23
Time Setting Guidelines 27
RapidVap Controls 29
Operating the RapidVap Controls 30
Operating The RapidVap 32
Operational Notes 33
Interrupting a Cycle After it Has Begun 33
End Alarms 33
RS-232 Communications 34
RS-232 Programming Syntax 34
RS-232 Hardware Required 36
CHAPTER 5: MAINTAINING YOUR RAPIDVAP 37
CHAPTER 6: MODIFYING YOUR RAPIDVAP 39
Changing the Sample Blocks 39
Installing the Optional Lid Heater 40
CHAPTER 7: TROUBLESHOOTING 41
APPENDIX A: RAPIDVAP AND RAPIDVAP N2 COMPONENTS 45
APPENDIX B: RAPIDVAP DIMENSIONS 52
APPENDIX C: RAPIDVAP SPECIFICATIONS 54
Wiring Diagram (115V) 56
Wiring Diagram (230V) 57
Evaporation Rates 58
RapidVap Vacuum Models 58
RapidVap N2 Models 59
RapidVap N2/48 Models 63
APPENDIX D: RAPIDVAP ACCESSORIES 65
RapidVap Vacuum Model Accessories 65
RapidVap N2 Model Accessories 68
RapidVap N2/48 Model Accessories 70
1
Original instructions
C
C
HHAAPPTTEERR
1
1
I
I
NNTTRROODDUUCCTTIIOONN
Congratulations on your purchase of a Labconco RapidVap. Labconco
manufactures two types of RapidVaps - one utilizes vacuum and the other utilizes
nitrogen as an aid to evaporation. Each model is available for operation on 115V
or 230V.
Superior evaporation rates are achieved by the unique blending of several gentle
forces on the sample. Samples are subjected to a gyrating motion causing the
liquid to form a vortex configuration which greatly increases the surface area and
hence the ability to evaporate. A precisely controlled amount of thermal energy
can be supplied to the sample to heat it. In the vacuum model, the sample can be
subjected to a decreased pressure by the application of a regulated vacuum. In
summary, the vacuum model RapidVap performance is maximized by increasing
the sample’s surface area, increasing temperature and decreasing pressure.
In the RapidVap N2, a stream of nitrogen or dry gas is directed downward onto the
surface of the sample. This reduces the partial pressure directly over the liquid to
speed evaporation and helps remove the solvent as it evaporates. In summary, the
RapidVap N2 performance is maximized by increasing the sample’s surface area,
increasing temperature and directing gas over the sample.
The gyrating motion imparted to the sample causes other, more subtle effects to
occur. Excellent mixing of the components in the liquid sample is obtained. Also,
as the liquid forms the vortex shape, a centrifugal force is established which forces
the liquid outward against the tube walls. This helps prevent bumping and in turn
allows the evaporation rate to be optimized.
The microprocessor which controls the operation of the heater and the motor
provides excellent regulation and reproducibility of protocols. The end of the run
can be signaled by the automatic end point system or by a manually preset timer.
Nine different protocols can be stored in memory so exact test parameters can be
easily repeated.
Product Service 1-800-522-7658
Chapter 1: Introduction
2
Original instructions
About This Manual
This manual is designed to help you learn how to install, use, and maintain your
RapidVap. Instructions for performing routine maintenance and making minor
modifications to your RapidVap are also included.
Chapter 1: Introduction provides a brief overview of the RapidVap, explains the
organization of the manual, and defines the typographical conventions used in the
manual.
Chapter 2: Prerequisites explains what you need to do to prepare your site before
you install your RapidVap. Electrical and exhaust requirements are discussed as
well as vacuum pump or nitrogen requirements.
Chapter 3: Getting Started contains the information you need to properly unpack,
inspect, install, and test your RapidVap.
Chapter 4: Using Your RapidVap discusses the basic operation of your RapidVap.
Information on how to arrange the samples inside your RapidVap and select an
operating cycle is included.
Chapter 5: Maintaining Your RapidVap explains how to perform routine
maintenance on your RapidVap.
Chapter 6: Modifying Your RapidVap describes how to install other blocks and the
optional lid heater.
Chapter 7: Troubleshooting contains a table of problems you may encounter while
using your RapidVap, including the probable causes of the problems, and
suggested corrective actions.
Appendix A: RapidVap and RapidVap N2 Components contains labeled diagrams
of the components of the RapidVaps.
Appendix B: RapidVap Dimensions contains comprehensive diagrams showing the
dimensions for the RapidVap and RapidVap N2.
Appendix C: RapidVap Specifications contains product specifications. Wiring
diagrams for both the 115V and 230V RapidVaps are also included.
Appendix D: RapidVap Accessories lists the part numbers and descriptions of all of
the accessories available for your RapidVap.
Product Service 1-800-522-7658
Chapter 1: Introduction
3
Original instructions
!
V
N
!
Typographical Conventions
Recognizing the following typographical conventions will help you understand and
use this manual:
Book, chapter, and section titles are shown in italic type (e.g., Chapter 3:
Getting Started).
Steps required to perform a task are presented in a numbered format.
Comments located in the margins provide suggestions, reminders, and
references.
Critical information is presented in boldface type in paragraphs that are
preceded by the exclamation icon. Failure to comply with the information
following an exclamation icon may result in injury to the user or permanent
damage to your RapidVap.
Les informations critiques sont présentées en caractères gras dans les
paragraphes qui sont précédés par le point d'exclamation. Le non respect de
l'information suite à un point d'exclamation peut entraîner des blessures pour
l'utilisateur ou des dommages permanents à votre RapidVap.
Important information is presented in capitalized type in paragraphs that are
preceded by the pointer icon. It is imperative that the information contained in
these paragraphs be thoroughly read and understood by the user.
Information that is specific to a particular model of RapidVap is preceded by a
letter icon. The V icon indicates the text is specific to the Vacuum model. The
N icon indicates the text is specific to the RapidVap N2 model.
CAUTION – See Manual. When this symbol is on the unit it indicates a
caution that is detailed in this manual.
ATTENTION – Voir le manuel. Lorsque ce symbole est allumé l'unité, il
indique une mise en garde qui est détaillée dans ce manuel.
Your Next Step
If your RapidVap needs to be installed, proceed to Chapter 2: Prerequisites to
ensure your installation site meets all of the requirements. Then, go to Chapter 3:
Getting Started for instructions on how to install your RapidVap and make all of
the necessary connections.
For information on the operational characteristics of your RapidVap, go to Chapter
4: Using Your RapidVap.
If your RapidVap is installed and you need to perform routine maintenance on the
RapidVap, proceed to Chapter 5: Maintaining Your RapidVap.
Product Service 1-800-522-7658
Chapter 1: Introduction
4
Original instructions
For information on making modifications to the configuration of your RapidVap
go to Chapter 6: Modifying Your RapidVap.
Refer to Chapter 7: Troubleshooting if you are experiencing problems with your
RapidVap.
Product Service 1-800-522-7658
5
Original instructions
C
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HHAAPPTTEERR
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2
P
P
RREERREEQQUUIISSIITTEESS
V
!
Before you install your RapidVap, you need to prepare your site for installation.
Carefully examine the location where you intend to install your RapidVap. You
must be certain that the area is level and of solid construction. In addition, an
exhaust means must be provided and a source of nitrogen must be available for the
RapidVap N2. An electrical source must be located near the installation site.
Carefully read this chapter to learn:
the electrical supply requirements.
the exhaust requirements.
the nitrogen supply requirements for the RapidVap N2.
the vacuum pump requirements for the RapidVap Vacuum.
Refer to Appendix C: RapidVap Specifications for complete RapidVap electrical
and environmental conditions, specifications and requirements.
If the unit is not operated as specified in this manual it may
impair the protection provided by the unit.
Si l'appareil n'est pas utilisé comme spécifié dans ce manuel, il
peut compromettre la protection offerte par l'appareil.
Electrical Requirements
If your RapidVap is a Vacuum model, a dedicated electrical outlet is required.
This outlet requires a 20 Amp circuit breaker or fuse for models rated at 115V (60
Hz). A 10 Amp circuit breaker or fuse is required for models rated at 230V (50/60
Hz). 115V models are equipped with a 20 Amp NEMA 5-20P plug. 230V models
are equipped with a 16 Amp CEE 7/7 plug. It may be necessary to remove the
plug and install a different plug to match the available receptacle.
Product Service 1-800-522-7658
Chapter 2: Prerequisites
6
Original instructions
N
V
N
V
!
!
If your RapidVap is a Nitrogen model, a dedicated electrical outlet is required.
This outlet requires a 15 Amp circuit breaker or fuse for models rated at 115V (60
Hz) or an 8 Amp circuit breaker or fuse is required for 230V (50/60 Hz) models.
115V models are equipped with a 20 Amp NEMA 5-20P plug. 230V models are
equipped with a 16 Amp CEE 7/7 plug. It may be necessary to remove the plug
and install a different plug to match the available receptacle.
Do not use any detachable power cord that is not adequately rated for the unit.
N'utilisez pas de cordon d'alimentation amovible qui n'est pas suffisamment
puissant pour l'unité.
Location and Exhaust Requirements
The RapidVap Vacuum Evaporation System should be located within a fume hood
if hazardous or flammable solvents are used. In all cases, regardless of the solvent
used, it is strongly recommended that the vacuum pump is located and vented in a
fume hood.
The RapidVap N2 Evaporation System should be located within a fume hood if
hazardous or flammable solvents are used. In all cases, regardless of the solvent
used, it is recommended that the exhaust hose is vented into a fume hood or other
laboratory ventilation device.
Do not position the unit so that it is difficult to operate the main
disconnect device.
Ne pas placer l'appareil de sorte qu'il est difficile de faire
fonctionner le dispositif de déconnexion principal.
Vacuum Pump Requirements
A vacuum pump must be provided by the user. For most applications, it is
recommended that the vacuum pump is capable of a free air flow of 63 L/min and
1.5 mbar vacuum although, in some applications other pumps may be satisfactory
or be required. The inlet fitting on the vacuum pump must be suitable for 0.50 I.D.
hose.
Biological samples, for example, are often dissolved in water, a high boiling point
solvent, and are often heat liable. Such samples require the high vacuum
achievable with a mechanical vacuum pump, usually with an ultimate vacuum of
7 x 10-3 mBar to achieve a good evaporation rate.
Product Service 1-800-522-7658
Chapter 2: Prerequisites
7
Original instructions
!
!
On the other hand, samples dissolved in methylene chloride, a low boiling point
solvent, can be efficiently concentrated using a water aspirator.
The nomograms in Chapter 4: Using Your RapidVap will help determine the
boiling point of a solvent at pressures below atmospheric. This can serve as a
guide to the appropriate vacuum source.
TO INSURE THAT AGGRESSIVE SAMPLES USED IN THE
RAPIDVAP DO NOT DAMAGE THE VACUUM PUMP, IT IS
RECOMMENDED THAT ALL INTERNAL WETTED PARTS
ARE PTFE OR PTFE COATED. TO PREVENT A HAZARDOUS
CONDITION, THE PUMP MUST BE SUITABLE FOR
HANDLING THE VAPORS FROM THE SOLVENTS THAT
WILL BE EVAPORATED IN THE RAPIDVAP.
CAUTION: When selecting the vacuum pump it is very
important to consider the flammability of the solvents that will
be used. If the solvents are flammable, an explosion proof
vacuum pump is recommended.
ATTENTION: Lors de la sélection de la pompe à vide, il est très
important d'examiner l'inflammabilité des solvants qui seront
utilisés. Si les solvants sont inflammables, d'une pompe à vide à
l'épreuve des explosions est recommandé
Vacuum Line Traps
When using a mechanical pump which is not corrosion resistant, a trap must be
used in the vacuum line to prevent damage from solvent vapors. This is most often
a condenser-type trap chilled with dry ice/acetone. When evaporating acids, it is
advisable to include a soda lime acid trap in the vacuum line. This adds additional
protection for the pump.
Several components within the RapidVap are made from
stainless steel and can be degraded if exposed to acids. Before
evaporating acids, be sure to contact Labconco.
Plusieurs composants du RapidVap sont en acier inoxydable et
peuvent être dégradés s'ils sont exposés à des acides. Avant de
s'évaporer acides, n'oubliez pas de contacter Labconco.
A moisture trap and radioisotope trap are also available. When evaporating high
boiling point solvents, a liquid trap should be positioned between the RapidVap
and the vacuum pump to prevent liquid from entering the pump. Refer to
Appendix D: RapidVap Accessories for ordering information.
Product Service 1-800-522-7658
Chapter 2: Prerequisites
8
Original instructions
N
Nitrogen Supply Requirements
The 1/4" I.D. hose on the rear of the RapidVap N2 must be attached to a source of
nitrogen or other suitable gas. Pressure must NOT exceed 20 psi. A regulator
must be supplied by the user. The nitrogen supply must be capable of 0.6 CFM
flow rate for the 8 place RapidVap N2. The RapidVap N2/48 requires a flow rate
of 3.5 CFM. A suitable barb or compression fitting must be supplied by the user.
Space Requirements
Refer to Appendix C: RapidVap Specifications for dimensional drawings of the
RapidVap.
Tools Required
Common hand tools are required to set up the RapidVap. A screwdriver or 5/16"
socket is needed to attach hose clamps. A tubing cutter or knife is needed to
shorten exhaust hoses. If the sample block must be installed or exchanged,
attaching nuts on the RapidVap Vacuum and RapidVap N2 require a 7/16" socket.
The manifold guides, which secure the block on the RapidVap N2/48, require a
9/16" socket.
Your Next Step
After you have determined that the location for your RapidVap accommodates the
installation and operational requirements, you are ready to unpack and install your
RapidVap. Proceed to Chapter 3: Getting Started.
Product Service 1-800-522-7658
9
Original instructions
C
C
HHAAPPTTEERR
3
3
G
G
EETTTTIINNGG
S
S
TTAARRTTEEDD
!
The United
States Interstate
Commerce
Commission
rules require
that claims be
filed with the
delivery carrier
within fifteen
(15) days of
delivery.
Now that the site for your RapidVap is properly prepared, you are ready to unpack,
inspect, install, and test your RapidVap. Read this chapter to learn how to:
unpack and move your RapidVap.
set up your RapidVap.
connect the vacuum pump or nitrogen source to your RapidVap.
connect the electrical supply source to your RapidVap.
properly exhaust your RapidVap.
calibrate the vacuum sensor.
solvent safety precautions.
Depending upon which model of RapidVap you are installing, you will need
common hand tools including a flat blade screw driver, a 7/16" socket and an
adjustable wrench to complete the instructions in this chapter.
The RapidVap weighs over 70 lbs. (33 Kg). The carton allows
for lifting with a mechanical lift truck or hand truck. If you
must lift the RapidVap manually, use at least two (2) persons
and follow safe-lifting guidelines.
Unpacking Your RapidVap
Carefully unpack your RapidVap and inspect it for damage that may have occurred
in transit. If your RapidVap is damaged, notify the delivery carrier immediately
and retain the entire shipment intact for inspection by the carrier.
DO NOT RETURN GOODS WITHOUT THE PRIOR
AUTHORIZATION OF LABCONCO. UNAUTHORIZED
RETURNS WILL NOT BE ACCEPTED.
Product Service 1-800-522-7658
Chapter 3: Getting Started
10
Original instructions
Catalog #
RapidVap Description
79000-00
RapidVap Vacuum System – 115V
79000-01
RapidVap Vacuum System – 230V
79000-02
RapidVap Vacuum System – 115V with lid heater
79000-03
RapidVap Vacuum System – 230V with lid heater
79000-10
RapidVap Vacuum System – 115V with RS 232 Interface
79000-11
RapidVap Vacuum System – 230V with RS 232 Interface
79000-12
RapidVap Vacuum System – 115V with lid heater with RS 232 Interface
79000-13
RapidVap Vacuum System – 230V with lid heater with RS 232 Interface
Plus the Following:
Part #
Component Description
78286-04
Hose - Vacuum
14888-00
Two (2) Clamps
13364-00
13365-00
Power Cord – 115V
or
Power Cord – 230V
19116-00
Washer (3)
19092-21
Acorn Nut (3)
12556-00
Heat Transfer Grease
74901-00
User’s Manual
74848-00
Cable Assembly RS232 (Models 79000-10, -11, -12, -13)
IF YOUR RAPIDVAP WAS DAMAGED IN TRANSIT, YOU
MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT
CARRIER. LABCONCO CORPORATION AND ITS DEALERS
ARE NOT RESPONSIBLE FOR SHIPPING DAMAGES.
Do not discard the carton or packing material for your RapidVap until you have
checked all of the components and installed and tested the RapidVap.
RapidVap Components
As previously mentioned, Labconco manufactures two types of RapidVap, the
Vacuum and the Nitrogen models. Each model is available in 115V or 230V.
The different RapidVap models require different assembly components. Locate
the model of RapidVap you received in the following tables. Verify that the
components listed are present and undamaged.
Product Service 1-800-522-7658
Chapter 3: Getting Started
11
Original instructions
Catalog #
RapidVap Description
79100-00
RapidVap N2 Evaporation System – 115V
79100-01
RapidVap N2 Evaporation System – 230V
79100-10
RapidVap N2 Evaporation System – 115V with RS 232 Interface
79100-11
RapidVap N2 Evaporation System – 230V with RS 232 Interface
Plus the Following:
Part #
Component Description
79131-01
Exhaust Hose
19660-00
One (1) Clamp
79255-00
Eight (8) Sample Tube Caps
13364-00
13365-00
Power Cord – 115V
or
Power Cord – 230V
12556-00
Heat Transfer Grease
74901-00
User’s Manual
74848-00
Cable Assembly RS232 (Models 79100-10, -11)
Catalog #
RapidVap Description
79100-12
RapidVap N2/48 Evaporation System – 115V
79100-13
RapidVap N2/48 Evaporation System – 230V
79100-14
RapidVap N2/48 Evaporation System – 115V with RS 232 Interface
79100-15
RapidVap N2/48 Evaporation System – 230V with RS 232 Interface
Plus the Following:
Part #
Component Description
79131-00
Exhaust Hose – 6 ft.
19660-00
One (1) Clamp
13364-00
13365-00
Power Cord – 115V
or
Power Cord – 230V
12556-00
Heat Transfer Grease
74901-00
User’s Manual
74488-00
Manifold Guide (3)
19116-00
Washer (3)
74848-00
Cable Assembly RS232 (Models 74100-14, -15)
Since users’ preference of sample size varies, the sample holding block is not
included with the RapidVap Vacuum System or the RapidVap N2/48 Evaporation
System. The correct size block must be selected and ordered separately. Refer to
Appendix D: RapidVap Accessories for block selection.
If you do not receive one or more of the components listed for your RapidVap, or
if any of the components are damaged, contact Labconco Corporation immediately
for further instructions.
Product Service 1-800-522-7658
Chapter 3: Getting Started
12
Original instructions
V
Optional vacuum
pump exhaust hose
to ventilation device
Hose
Vacuum hose
Clamp all connections
Optional liquid trap or
chilled trap or
secondary trap
Vacuum pump
inlet fitting
Vacuum pump
power connection
Setting Up Your RapidVap
After you verify the RapidVap components, move your RapidVap to the location
where you want to install it. Then, follow the steps listed below.
Vacuum Pump Connection
Connect the pump inlet to the fitting at the right hand rear corner of the RapidVap
using the hose and clamps provided. Route the hose to prevent kinks. Clamp all
connections securely. Plug the pump into the pump receptacle on the back of the
unit and turn the pump switch on if it is so equipped. When evaporating high boiling
point solvents, a liquid trap should be positioned between the RapidVap and the
vacuum pump to prevent liquid from entering the pump. It is recommended that the
vacuum pump is located inside a fume hood. If that is not possible, the exhaust of
the pump should be directed to a laboratory fume hood or other laboratory
ventilation device.
Product Service 1-800-522-7658
Chapter 3: Getting Started
13
Original instructions
There is a switch on the back of the RapidVap Vacuum that is used to select the
operation of an optional RapidVap Trapping Valve. When the RapidVap is used
without the Trapping Valve as shown above, set the switch to the “Off” position.
Sample Block
If the RapidVap was not shipped with the sample block installed then it must be
installed by the user. The sample block must be securely attached to its mounting
plate. Note the asymmetric hole pattern of the three thru mounting holes. Locate
the three flat washers either nuts or manifold guides that were shipped with the
RapidVap. The RapidVap Vacuum uses nuts while the RapidVap N2/48 uses
guide rods.
Apply a small amount of heat transfer grease that was shipped with the RapidVap
to the end of the temperature sensor probe that extends up from the bottom of the
chamber. Position the block over the three studs in the chamber. Install the flat
washers and either nuts or guide rods. Tighten securely.
Product Service 1-800-522-7658
Chapter 3: Getting Started
14
Original instructions
!
Nut or guide rods – 3 required
Washer – 3 required
Block
Mounting stud
Temperature sensor
Apply heat
transfer grease
Never lift the lid if the block is moving. Samples may splash
out.
Ne jamais soulever le couvercle si le bloc est en mouvement. Les
échantillons peuvent gicler.
Never operate the RapidVap without the sample block securely
fastened in place. Excessive vibration will occur.
Ne jamais faire fonctionner le RapidVap sans le bloc
d'échantillon fixé solidement en place. Des vibrations excessives
se produira.
Never attempt to reach into the chamber if the block is moving.
Ne jamais tenter de mettre la main dans la chambre si le bloc
est en mouvement.
Product Service 1-800-522-7658
Chapter 3: Getting Started
15
Original instructions
N
N
V
Nitrogen Gas Connection
Turn the gas supply off. Install a barb fitting suitable for a 1/4" I.D. hose into the
“out” port of the regulator. Clamp securely. Alternately, a compression fitting
may be used that is suitable for a hose with a 3/8" O.D. and 1/4" I.D.
THE NITROGEN PRESSURE MUST NEVER BE ALLOWED
TO EXCEED 20 PSI. (103 KPA)
Exhaust Port
If the RapidVap N2 is not located in a fume hood, attach one end of the two inch
diameter venting hose that is supplied with the RapidVap to the exhaust port on the
right side of the unit. Clamp securely. Route the other end to a fume hood or
other laboratory ventilation device.
Electrical Connection
Plug the power cord into the receptacle on the back of the RapidVap and plug the
other end into a suitable wall power receptacle.
Calibrate the Vacuum Sensor
The vacuum sensor can be calibrated to room ambient atmospheric pressure. To
do this, determine the atmospheric pressure using a known reference device such
as a mercury barometer. Press and hold the vacuum release button on the
RapidVap while turning on the RapidVap power switch. Use the increase or
decrease buttons to make the vacuum display agree with the reference pressure.
Press run to store the calibration in memory.
Chemical Attack on RapidVap
Components
Your RapidVap Evaporation System is designed to be chemical resistant to most
compounds that are commonly used in the concentration processes that are
performed in it. However, by necessity, the RapidVap is comprised of a number of
different materials, some of which may be attacked and degraded by certain
chemicals. The degree of degradation is obviously dependent on the concentration
and duration of exposure. Some of the major components of the RapidVap that are
susceptible to degradation are as follows:
Product Service 1-800-522-7658
Chapter 3: Getting Started
16
Original instructions
Acids
Bases
Solvents
COMPONENT
MATERIAL
Acetic Acid 20%
Boric Acid
Formic Acid
Hydrobromic Acid 20%
Hydrochloric Acid 20%
Nitric Acid 20%
Sulfuric Acid 10%
Trifluoroacetic Acid (TFA)
Ammonium Hydroxide
Potassium Hydroxide
Acetone
Acetonitrile Chloroform
Dimethyl Formamide
Dimethyl Sulfoxide (DMSO)
Ethanol
Ethyl Acetate
Hexanes
Isoproponal
Methylene
Chloride
Toluene
Manifold N2/48
Acetal
C C C D D D C D C
Exhaust Elbow N2
Polyamid (Nylon)
D D D D D D D C D C
Blower Fan N2
Polyamid (Nylon)
D D D D D D D C D C
Exhaust Hose N2
Polyethylene
C C C C C C C
Vacuum Fittings
Polypropylene
C C
Blower Housing N2
Polypropylene
C C
Vacuum Hose
PVC D C D D D D D D C D D D D Trim Ring
Bromyl Butyl
C D D D D D D D
O- Rings
Neoprene
D D C D D C D D D D D D
Block Hardware
Stainless Steel
Nozzle N2
Stainless Steel
D D D
Vacuum Sensor
Stainless Steel
D D D
C- Moderate Degradation- Questionable Use
D- Severe Degradation- Infrequent use recommended- immediate thorough cleaning required
If a rotary vane vacuum pump is used, most compounds used in the RapidVap
will degrade the oil if allowed to enter the pump. Generally, a rotary vane
pump is not suitable for use with the RapidVap.
Diaphragm vacuum pumps sold by Labconco have wetted parts either made
from PTFE or protected by PTFE coatings and are suitable for nearly all
procedures.
Glass lids are suitable for use with all common compounds.
When using compounds in the RapidVap that are hostile to the materials of
construction, it is imperative that the equipment is properly maintained.
After each run, clean up all residues, spills, and materials that might have
splashed in the chamber using agents suitable for the substance involved.
When using a rotary vane pump the oil in the pump should be checked often. It
must be changed if it is cloudy, shows particles or is discolored. The useful life
of vacuum pump oil can be extended if the vacuum pump is operated for an
extended period of time after the RapidVap run is over. This allows
contaminants to be purged from the hot oil. This must be done with the inlet to
the pump blocked off to prevent air from free flowing through the pump. If the
pump is operated at an elevated vacuum level, oil will be expelled from the
pump and damage will occur.
Product Service 1-800-522-7658
Chapter 3: Getting Started
17
Original instructions
!
With prudent maintenance your RapidVap will provide years of service. Warranty
on the effected parts will be void if maintenance has obviously been neglected. If
you have questions about using specific compounds in your RapidVap, contact
Labconco Technical Service at 1-800-821-5525 or 816-333-8811 or e-mail
labconco@labconco.com.
Solvent Safety Precautions
The RapidVap is not classified as “explosion proof.” It has been designed with
safety as a primary consideration and should be used in a prudent manner using
“good laboratory practices.” It has been designed for use with compounds as
described in the United States National Electrical Code Class I, Group D. The
block that holds the sample tubes may be programmed to run as hot as 100°C,
however, the heater element may normally run at 110°C. A thermal fuse limits the
heater to a maximum temperature of 130°C. It is important that the solvents used
are compatible with these temperatures. Do not evaporate solvents that have an
autoignition temperature below 180°C. Do not evaporate solvents that are
classified as Group A, B, or C by the National Electrical Code. Evaporate only
non-flammable or Group D solvents with autoignition temperatures 180°C or
above. Use of other compounds could cause an explosion.
Solvents used in the RapidVap may be flammable or hazardous.
Use extreme caution and keep sources of ignition away from the
solvents. When using flammable or hazardous solvents, both
the RapidVap and the vacuum pump should be operated inside
a fume hood.
If a sample is spilled in the chamber it must immediately be
cleaned up.
Hazardous materials such as strong acids or bases, radioactive
substances and volatile organics, must be handled carefully and
promptly cleaned up if spilled.
Several components of the RapidVap which are located inside
the chamber are made of stainless steel which can be attacked
by acids. Use of acids such as trifluoroacetic acid can result in
degradation of the product and the vacuum pump if the
vacuum system is being used. Use care when using aggressive
liquids which can damage the RapidVap and thoroughly clean
the RapidVap after each use. Contact Labconco before
evaporating acids.
WARNING: The disposal of substances used in connection with
this equipment may be governed by various Federal, State or
local regulations. All users of this equipment are urged to
Product Service 1-800-522-7658
Chapter 3: Getting Started
18
Original instructions
become familiar with any regulations that apply in the user’s
area concerning
the dumping of waste materials in or upon water, land or air
and to comply with such regulations.
AVERTISSEMENT: L'élimination des substances utilisées
dans le cadre de ce matériel peut être régie par diverses
réglementations fédérales, provinciales ou locales. Tous les
utilisateurs de cet équipement sont invités à se familiariser avec
tous les règlements qui s'appliquent dans le domaine de
l'utilisateur concernant le déversement de déchets dans ou sur
l'eau, la terre ou de l'air et de se conformer à ces règlements.
Your Next Step
The installation and setup of your RapidVap is now complete. To learn how to
load and operate your RapidVap, proceed to Chapter 4: Using Your RapidVap. To
make a modification to the configuration of your RapidVap, proceed to Chapter 6:
Modifying your RapidVap. To perform additional diagnostics on your RapidVap,
proceed to Chapter 7:Troubleshooting. To learn about the maintenance
requirements for your RapidVap, proceed to Chapter 5: Maintaining Your
RapidVap.
Product Service 1-800-522-7658
19
Original instructions
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After your RapidVap has been installed as detailed in Chapter 3: Getting Started,
you are ready to begin using your RapidVap. Read this chapter to learn how to:
set operating parameters.
operate the controls.
properly select and position glassware inside your RapidVap.
understand the display.
interrupt a cycle after it has begun.
Do not use the RapidVap in a manner not specified by the
manufacturer (refer to Appendix C: RapidVap Specifications).
The electrical protection properties of the RapidVap may be
impaired if the RapidVap is used inappropriately.
Planning
Thoroughly understand procedures and the equipment operation prior to beginning
work. The unique performance of the RapidVap Vacuum is dependent upon the
proper balance of heat, vacuum and vortexing action. If the proper balance is not
established, it is possible to damage or lose a portion of the sample. Therefore, if
you are unfamiliar with the RapidVap or are attempting a new protocol, it may be
helpful to make a trial run that is void of the sample you are attempting to
concentrate.
Select the size of the sample tube so it is compatible with the block. Tubes should
not be loose in the block. Blocks are available with holes for various size tubes.
Refer to Appendix D: RapidVap Accessories for available block sizes and pages 19
and 20 for recommended usable tube volumes and vortex speeds.
Product Service 1-800-522-7658
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