You have made an excellent choice.
JULABO thanks you for the trust you have placed in us.
This operating manual has been designed to help you gain an understanding of the operation and
possible applications of our circulators. For optimal utilization of all functions, we recommend that you
thoroughly study this manual prior to beginning operation.
Printed in Germany Changes without prior notification reserved
Important: keep operating manual for future use
The JULABO Quality Management System
Temperature control devices for research and industry are developed,
produced, and distributed according to the requirements of ISO 9001 and
ISO 14001. Certificate Registration No. 01 100044846
Unpacking and inspecting
Unpack the unit and accessories and inspect them for possible transport damage. Damage should be
reported to the responsible carrier, railway, or postal authority, and a damage report should be
requested. These instructions must be followed fully for us to guarantee our full support of your claim
for protecting against loss from concealed damage. The form required for filing such a claim will be
provided by the carrier.
Lift the unit only with a crane (see pictures) using the lifting strands and the wooden crate .
The recessed grips on the side are not suited for this purpose!
11. REMOTE CONTROL ........................................................................................... 66
11.1. Setup for remote control ...................................................................................... 66
11.2. Communication with a PC or a superordinated data system ............................... 67
11.3. List of commands ................................................................................................ 68
11.4. Status messages / error messages ..................................................................... 71
12. CLEANING THE UNIT ......................................................................................... 72
13. MAINTAINING / REPAIRING THE UNIT ............................................................. 75
4
Operating manual
1. Intended use
JULABO Temperature Systems have been designed for temperature application to specific fluids in a
external closed system (oop circuit). The units feature pump connections for temperature control of
external systems (loop circuit).
JULABO circulators are not suitable for direct temperature control of foods, semi-luxury
foods and tobacco, or pharmaceutical and medical products. Direct temperature control
means unprotected contact of the object with the bath medium (bath fluid).
1.1. Description
Besides the cooling unit, the main functional elements are the heater, circulation pump and control
electronics. Via an external Pt100 control sensor, a self-optimizing, electronic proportional
temperature control (PID characteristic) adapts the heat supplied to the thermal requirements of
the external system.
The high pump capacity can be reduced by regulating the motor speed in five grades. It may thus
be adapted to sensitive vessels.
LH47: The cooling unit may be cooled with air.
LH50: The cooling unit may be cooled with water.
Setting is rapid and simple using the splash-proof keypads. The operating elements consist of the
local operating board with a bright VFD-Info-Display, as well as the removable control module RD
connected with a cable.
The microprocessor technology allows four temperature values to be stored and indicated on the
DIALOG-DISPLAY (LCD) of the control module RD: working temperature, high and low
temperature warning limits as well as pump pressure stage.
The digital RS232 / RS485 port permits modern process engineering without additional interface.
The excess temperature protection (safety temperature), a safety feature functioning independent
of the regulator circuit, is adjusted and indicated via the VFD-Info-Display.
The integrated programmer allows programming of setpoint and time values for six temperature
profiles.
The following analog sockets are available:
- The REG+E-PROG socket for setpoint selection via an external, analog programmer.
At the same time, this socket provides three analog outputs for temperature recorders.
- The external Pt100 socket for external control.
- The alarm output for an external signal.
- The stand-by input for external emergency switch-off.
5
Operator responsibility – Safety instructions
2. Operator responsibility – Safety instructions
The products of JULABO ensure safe operation when installed, operated, and maintained according
to common safety regulations. This section explains the potential dangers that may arise when
operating the circulator and also specifies the most important safety precautions to preclude these
dangers as far as possible.
The operator is responsible for the qualification of the personnel operating the units.
The personnel operating the units should be regularly instructed about the dangers involved with
their job activities as well as measures to avert these dangers.
Make sure all persons tasked with operating, installing, and maintaining the unit have read and
understand the safety information and operating instructions.
When using hazardous materials or materials that could become hazardous, the circulator may be
operated only by persons who are absolutely familiar with these materials and the unit. These
persons must be fully aware of possible risks.
If you have any questions concerning the operation of your unit or the information in this manual,
please contact us!
Contact:
Safety instructions for the operator:
Avoid strikes to the housing, vibrations, damage to the operating-element panel (keypad, display),
and contamination.
Make sure the product is checked for proper condition regularly (depending on the conditions of
use). Regularly check (at least every 2 years) the proper condition of the mandatory, warning,
prohibition and safety labels.
Make sure that the mains power supply has low impedance to avoid any negative effects on the
instruments being operated on the same mains.
This unit is designed for operation in a controlled electromagnetic environment. This means that
transmitting devices (e.g., cellular phones) should not be used in the immediate vicinity.
Magnetic radiation may affect other devices with components sensitive to magnetic fields (e.g.,
monitors). We recommend maintaining a minimum distance of 1 m.
Permissible ambient temperature: max. 40 °C, min. 5 °C.
Permissible relative humidity: 50 % (40 °C).
Do not store the unit in an aggressive atmosphere. Protect the unit from contamination.
Do not expose the unit to sunlight.
Appropriate operation
Only qualified personnel is authorized to configure, install, maintain, or repair the unit.
Persons who operate the circulator must be trained in the particular tasks by qualified personnel. The
summarized user guidance (short manual) and the specification table with information on individual
parameters are sufficient for this.
6
Use
The bath can be filled with flammable materials. Fire hazard!
There might be chemical dangers depending on the bath medium used.
Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data
sheets).
Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well
ventilated areas.
Only use recommended materials (bath fluids). Do not use poisonous, vitriolic or corrosive bath
fluids..
When using hazardous materials or materials that could become hazardous, the operator must affix
the enclosed safety labels (1 + 2) to the front of the unit so they are highly visible:
1
2
or
2
Particular care and attention is necessary because of the wide operating range.
There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.
Warning label W00: Colors: yellow, black
Danger area. Attention! Observe instructions.
(operating manual, safety data sheet)
Mandatory label M018: Colors: blue, white
Carefully read the user information prior to beginning operation.
Scope: EU
Semi S1-0701 Table A1-2 #9
Carefully read the user information prior to beginning operation.
Scope: USA, NAFTA
Warning label W26: Colors: yellow, black
Hot surface warning.
(The label is put on by JULABO)
Observe the instructions in the manuals for instruments of a different make that you connect to the
circulator, particularly the corresponding safety instructions. Also observe the pin assignment of plugs
and technical specifications of the products.
7
Operator responsibility – Safety instructions
2.1. Disposal
The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or
synthetic oil. For disposal, follow the instructions in the material safety data sheets.
This unit contains the refrigerants R-404A and R-23, which at this time are not considered harmful to
the ozone layer. However, over the long operating period of the unit, disposal rules may change.
Therefore, only qualified personnel should handle the disposal.
Valid in EU countries
See the current official journal of the European Union – WEEE directive.
Directive of the European Parliament and of the Council on waste electrical and
electronic equipment (WEEE).
This directive requires electrical and electronic equipment marked with a crossedout trash can to be disposed of separately in an environmentally friendly manner.
Contact an authorized waste management company in your country.
Disposal with household waste (unsorted waste) or similar collections of municipal
waste is not permitted!
2.2. EC Conformity
The products described in the operating instructions conform to the requirements
of the following European guidelines:
Directive of the European Parliament and of the Council on the approximation of the laws of the
Member States relating to machinery.
Low voltage regulations with respect to legal harmonization of the member countries concerning
electric devices for use within certain voltage limits.
EMC guideline with respect to legal harmonization of the member countries concerning
JULABO GmbH warrants its products against defects in material or in workmanship, when used under
appropriate conditions and in accordance with appropriate operating instructions
for a period of ONE YEAR.
Extension of the warranty period – free of charge
With the ‘1PLUS warranty’ the user receives a free of charge extension to the warranty of up to 24
months, limited to a maximum of 10 000 working hours.
To apply for this extended warranty the user must register the unit on the JULABO web site
www.julabo.de
GmbH’s original invoice.
JULABO GmbH reserves the right to decide the validity of any warranty claim. In case of faults
arising either due to faulty materials or workmanship, parts will be repaired or replaced free of charge,
or a new replacement unit will be supplied.
Any other compensation claims are excluded from this guarantee.
, indicating the serial no. The extended warranty will apply from the date of JULABO
9
Operator responsibility – Safety instructions
2.4. Technical specifications
Mains power connection
400 V/3P/50 Hz
LH 47 LH 50
V /
360-440 V/3PNPE/50 Hz 360-440 V/3PNPE/50 Hz
Hz
Current input (at 230 V) A 12 20
Working temperature range °C -47 ... 250 -50 ... 250
Temperature stability K ±0.01 ... ±0.05 ±0.01 ... ±0.05
Cooling capacity
Pressure pump, adjustable
pressure min ... max. at 0 liter
discharge, max. at 0 bar
Pressure pump, adjustable
pressure min ... max. at 0 liter
discharge, max. at 0 bar
grade
bar
l/min
grade
bar
l/min
1
2
3
4
5
0.5
0.7
1.1
1.3
1.7
16
19
23
26
30
1
0.7
17
2
0.9
19
3
1.4
24
Viscosity, max. 50 mm²/s (50 cSt)
Noise level, 1 m distance dBA 72 ----Ambient temperature °C 5 ... 40 5 ... 40
Filling volume Heat exchanger
Reservoir
liters
liters
2.5
3.2 … 8.4
10
3.2 … 8.4
Overall dimensions (WxDxH) cm 40x55x127 40x55x127
Weight kg 150 182
All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.
Pump data in relation to fluids with a specific density of 1 kg/dm3
4
1.8
27
5
2.3
31
10
Mains power connection
LH 47 LH 50
V / Hz 207-253 V/3PPE/60 Hz 207-253 V/3PPE/60 Hz
230 V/3P/60 Hz
Current input (at 230 V) A 13 27
Working temperature range °C -47 ... 250 -50 ... 250
Temperature stability K ±0.01 ... ±0.05 ±0.01 ... ±0.05
Cooling capacity
Pressure pump, adjustable
pressure min ... max. at 0 liter
discharge, max. at 0 bar
Pressure pump, adjustable
pressure min ... max. at 0 liter
discharge, max. at 0 bar
grade
bar
l/min
grade
bar
l/min
1
2
3
4
5
0.5
0.7
1.1
1.3
1.7
16
19
23
26
30
1
0.7
17
2
0.9
19
3
1.4
24
Viscosity, max. 50 mm²/s (50 cSt)
Noise level, 1 m distance dBA 72 ----Ambient temperature °C 5 ... 40 5 ... 40
Filling volume Heat exchanger
Reservoir
liters
liters
2.5
3.2 … 8.4
10
3.2 … 8.4
Overall dimensions (WxDxH) cm 40x55x127 40x55x127
Weight kg 150 182
All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.
Pump data in relation to fluids with a specific density of 1 kg/dm3
4
1.8
27
5
2.3
31
11
Operator responsibility – Safety instructions
Temperature selection digital
via Removable control module RD indication on DIALOG-Display (LCD)
remote control via personal computer indication on monitor
Temperature indication VFD-Info-Display
DIALOG-DISPLAY (LCD)
Resolution K 0.01 from -9.99 °C to +249.99 °C
Pump pressure display on VFD-Info-Display in five grades
Liquid level display on VFD-Info-Display in five grades
Absolute Temperature Calibration
(ATC1) K ±3
(ATC2) K ±9
Temperature control ICC - Intelligent Cascade Control, self-optimizing
Cascade, parameter can be called-in and modified
Working temperature sensor Pt 100
Safety temperature sensor Pt 100
Electrical connections:
Computer interface RS232 or RS485
Programmer input -100 °C to 400 °C = 0 to 10 V or 0 to 20 mA or 4 to 20 mA
Temperature recorder outputs 0 to 10 V (0 V = -100 °C, 10 V = 400 °C)
0 to 20 mA (0 mA = -100 °C, 20 mA = 400 °C)
4 to 20 mA (4 mA = -100 °C, 20 mA = 400 °C)
Stand-by input
External alarm device 24-0 V DC / max. 25 mA
External measurement and control sensor Pt100, 4-lead technique
Control connector (10) Output voltage: 230 V / max. 0.1 A
Safety installations according to IEC 61010-2-010:
Excess temperature protection >TANK< adjustable from 0 °C ... 320 °C
Excess temperature protection >RES< adjustable from 0 °C ... 220 °C
Low level protection float switch
Liquid level display optical, 5-graded
Classification according to DIN 12876-1 class III FL
Supplementary safety installations
High temperature warning function optical + audible (in intervals)
Low temperature warning function optical + audible (in intervals)
Supervision of the working sensor plausibility control
Reciprocal sensor monitoring between
working and safety sensors difference >50 K
Alarm indication optical + audible (permanent)
12
Environmental conditions according to IEC 61 010-1:
Use only indoor.
Altitude up to 2000 m - normal zero.
Ambient temperature: see Technical specifications
Air humidity:
Max. rel. humidity 80 % for temperatures up to +31 °C,
linear decrease down to 50 % relative humidity at a temperature of +40 °C
Max. mains fluctuations of ±10 % are permissible.
Overvoltage category II
Pollution degree 2
Caution:
The unit is not suitable for use in explosive atmosphere
Protection class according to IEC 60 529: IP31
The unit corresponds to Class I
Standards for interference resistance according to EN 61326-1
This unit is an ISM device classified in Group 1 (using high frequency for internal purposes) Class A
(industrial and commercial range).
13
Operator responsibility – Safety instructions
2.5. Cooling water connection
Cooling water pressure (IN / OUT ) max. 6 bar
Difference pressure (IN - OUT ) 3.5 to 6 bar
Cooling water temperature <20 °C
Notice: Cooling water circuit
Risk of oil leaking from the refrigeration system (compressor) of the recirculating
cooler into the cooling water in case of a fault in the cooling water circuit!
Observe the laws and regulations of the water distribution company valid in the
location where the unit is operated.
Notice:
Danger of corrosion of heat exchanger due to unsuitable quality of cooling
water.
Due to its high content of lime, hard water is not suitable for cooling and causes
scale in the heat exchanger.
Ferrous water or water containing ferrous particles will cause formation of rust
even in heat exchangers made of stainless steel.
Chlorinated water will cause pitting corrosion in heat exchangers made of
stainless steel.
Due to their corrosive characteristics, distilled water and deionized water are
unsuitable and will cause corrosion of the bath.
Due to its corrosive characteristics, sea water is not suitable.
Due to its microbiological (bacterial) components, which settle in the heat
exchanger, untreated and unpurified river water and water from cooling towers is
unsuitable.
In addition to the safety warnings listed above, warnings are posted throughout the
manual. These warnings are designated by an exclamation mark inside an equilateral
triangle. “Warning of a dangerous situation (Attention! Please follow the
documentation).”
The danger is classified using a signal word.
Read and follow these important instructions.
Warning:
Describes a possibly highly dangerous situation. If these instructions are not followed,
serious injury and danger to life could result.
Caution:
Describes a possibly dangerous situation. If this is not avoided, slight or minor injuries
could result. A warning of possible property damage may also be contained in the
text.
Notice:
Describes a possibly harmful situation. If this is not avoided, the product or anything in
its surroundings can be damaged.
3.2. Explanation of other notes
Note!
Draws attention to something special.
Important!
Indicates usage tips and other useful information.
3.3. Safety instructions
Follow the safety recommendations to prevent damage to persons or property.
Further, the valid safety instructions for working places must be followed.
Only connect the unit to a power socket with earthing contact (PE – protective
earth)!
The power supply plug serves as safe disconnecting device from the line and
must be always freely accessible.
Place the instrument on an even surface on a pad made of non-inflammable
material.
Do not stay in the area below the unit.
Make sure you read and understand all instructions and safety precautions listed
in this manual before installing or operating your unit.
Set the safety temperature.
Never operate the unit without bath fluid in the bath.
15
Safety notes for the user
Pay attention to the thermal expansion of bath oil during heating to avoid
overflowing of the fluid.
Prevent water from penetrating into the hot bath oil.
Do not drain the bath fluid while it is hot!
Check the temperature of the bath fluid prior to draining (by switching the unit on
for a short moment for example).
Employ suitable connecting tubing.
Avoid sharp bends in the tubing, and maintain a sufficient distance from
surrounding walls.
Make sure that the tubing is securely attached.
Regularly check the tubing for material defects (e.g. for cracks).
Never operate damaged or leaking equipment.
Always turn off the unit and disconnect the mains cable from the power source
before performing any service or maintenance procedures, or before moving the
unit.
Always turn off the unit and disconnect the mains cable from the power source
before cleaning the unit.
Always empty the bath before moving the unit.
Transport the unit with care.
Sudden jolts or drops may cause damages in the interior of the unit.
Observe all warning labels.
Never remove warning labels.
Never operate equipment with damaged mains power cables.
Repairs are to be carried out only by qualified service personnel.
Some parts of the bath cover and the pump connections may become extremely
warm during continuous operation. Therefore, exercise particular caution when
touching these parts.
Caution:
The temperature controlling i.e. of fluids in a reactor constitutes normal temperature
system practice.
We do not know which substances are contained within these vessels.
Many substances are:
inflammable, easily ignited or explosive
hazardous to health
environmentally unsafe
i.e.: dangerous
The user alone is responsible for the handling of these substances!
16
The following questions shall help to recognize possible dangers and to reduce the
risks to a minimum.
Are all tubes and electrical cables connected and installed?
Note:
sharp edges, hot surfaces in operation, moving machine parts, etc.
Do dangerous steams or gases arise when heating?
Is an exhaust needed when working?
What to do when a dangerous substance was spilled on or in the unit?
Before starting to work, obtain information concerning the substance and
determine the method of decontamination.
Caution: Escape of vapors / gas
The necessity of degassing requires that a closed system is not entirely sealed.
Especially at increased working temperatures vapor / gas may escape.
Ensure sufficient ventilation at the place of installation!
Notice:
When you have finished the application, it is recommended to keep on circulating the
liquid in the bath or the external system for some time. Simultaneously set the
working temperature to +20 °C to allow the temperature in the system to decrease
slowly.
Thus fractional over-heating of the bath liquid is prevented.
Notice:
Please check the safety device from time to time.
Excess temperature protection according to IEC 61010-2-010
With a screw driver turn back the adjustable excess temperature protection until
the shut-down point (actual temperature).
Low level protection
To check the function of the float of this unit it cannot be operated manually.
The 5-graded level display should therefore be observed whenever refilling.
If the bath liquid thickens or cracks, the instrument should be cleaned and
checked by qualified personnel.
17
Operating controls and functional elements
4. Operating controls and functional elements
Front view LH47 LH50
air-cooled water-cooled
18
1 Mains power switch, illuminated
2 Local operating board
3 Socket board - description see page 20
4 Removable control module RD
5 Filling funnel (hinged)
1
6
7 Venting grid, removable
8 Drain with drain port
2 Local operating board
2.1
0
Motor protection circuit breaker for compressor motor
2 Mains circuit breakers (resettable) 10 A for the pump-motor
4 Mains circuit breakers (resettable) 16 A
VFD-Info-Display
Header: Control indicators see section 2.2
Line 1: Actual value Int or Ext
To swap, press the key
Line 2: Working temp. setpoint, constantly S xxx.xx
or indication of the safety temperature (TANK)
(see below)
2.2
Line 3: Miscellaneous values
To swap, press the key
or indication of the safety temperature (RES)
Control indicators in the header:
Heating / Cooling / Alarm / Remote control
Temperature indication Internal or External actual value
Temperature indication in °C or °F
Display for the adjusted pump pressure stage (five grades),
adjustable via the key
Liquid level display (five grades)
for the reservoir.
.
(see below)
19
Operating controls and functional elements
2.3
2.4
2.5
2.6
2.7
Int
Key to swap line 3 on the VFD
ID xx Identification no. of control module RD
L xx Capacity in %
E xxx.xx or I xxx.xx Actual value (external or internal)
P x.xx Pump pressure in bar
Key to swap line 1 on the VFD
Actual value Int or Ext alternating with line 3
Key to indicate the safety temperature on the VFD
Line 2: TANK - Safety temperature in internal bath
Line 3: RES - Safety temperature in internal reservoir
Adjustable excess temperature protection (safety temperature)
Used for setting the safety temperature in the internal bath, called
"TANK" on the display
Adjustable safety temperature.
Used for setting the safety temperature in the internal reservoir,
called "RES" on the display
2.8
3 Socket board
3.1
3.2
3.3
3.4
3.5
REG+E-PROG
STAND-BY
ALARM
EXT. Pt100
SERIAL
Key for automatic filling and air purge of the unit as well as the
connected external system.
Connector for external measurement and control sensor
Interface RS232/RS485
3.6
20
Connector: control cable of control module RD
RD
4
4.0
Control module RD
Setp: 120. 00 °C
IntAct 21.00°C
ExtAct : 20. 00 °C
Contro l: Intern
DIALOG-DISPLAY (LCD) Standard indication
Line 1: Setpoint in °C
Line 2: Internal actual value in °C
Line 3: External actual value in °C
Line 4: Control type: internal / external control
Indicating messages (e. g. warnings)
4.1
4.2
4.3
4.4
4.5
>Setp. : 12 0. 00 °C
Overt.:255.00°C
Subtmp:-55.00°C
St.Pump: 2
>Configuration
Control param.
Profile Start
Int. Programmer
Start / stop key
To switch the circulation pump, heating element and cooling unit.
SET Menu Key - Indicating and setting setpoint values
Set the following values:
in Line 1: the working temperature Setp.: Line 2: the high temperature limit Overt.: Line 3: the low temperature limit Subtmp:Line 4: the pump pressure stage St.Pump:
Control type: internal / external control
To swap, the unit has to be in the STOP MODE.
Indicated in line 4 on the DIALOG-DISPLAY (LCD)
MENU key - for selecting the menu functions
(Menu see page 42)
Cursor keys - Select menu items
4.6
4.7
4.8
4.9
....
P-key Selecting parameters
Escape key 1) Cancel entries
2) Return to a higher menu level
Enter key 1) Store value / parameter
2) Next lower menu level
Numeric keypad: numerals 0 to 9; minus / decimal point
21
Operating controls and functional elements
Rear
22
A
A M P
A M P
10
11
Si1
Control connector
230 V / max. 0.1 A
Si3
16
A
M
P
16
M
P
Si4 Si2
4 Mains circuit breakers (resettable) 16 A
16
F1 and F3 Compressor
16
F2 and F4 Heater, Pump
11a
1
0
12
13 + 14
15
16
17 + 18
19
19a
Motor protection circuit breaker for compressor motor
Mains power cable with plug
Pump connectors
Return Feed M16x1
Overflow connector M16x1
Connector for expansion vessel M16x1
Cooling water connectors LH41 G3/4" external thread
IN - inlet OUT - outlet
Castor without brake (at the back)
Castor with brake (at the front)
23
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