IKA HB digital Operating Instructions Manual

Operating instructions EN 4
Source language: German
Veiligheidsinstructies NL 12 Säkerhetsanvisningar SV 13 Sikkerhedshenvisninger DA 14 Sikkerhetsanvisninger NO 15 Turvallisuusohjeet FI 16 Bezpečnostní pokyny a informace
CS 17
Biztonsági óvintézkedések HU 18
Varnostni napotki SL 19 Bezpečnostné pokyny SK 20 Ohutusjuhised ET 21 Drošības norādījumi LV 22 Saugos nurodymai LT 23 Указания за безопасност BG 24 Instrucțiuni de siguranță RO 25 Υποδείξεις ασφαλείας EL 26
HB digital
20000017437
2
Device setup/Display
Device setup
Fig. 1
B A
E
F
G
C
D
H
J
F
A Power socket B Mains switch C Rotating/pressing knob D USB interface E Key “Lock“ F Handle G Bath insert H Display J IR interface
3
Display
Fig. 2 Fig. 3 Fig. 4
Fig. 7Fig. 6Fig. 5
Fig. 8 Fig. 9 Fig. 10
Fig. 12Fig. 11
4
EN
Contents
Explication of warning symbols
Declaration of conformity
We declare under our sole responsibility that this product corresponds to the directives 2014/35/EU, 2014/30/EU and 2011/65/EU and conforms with the following standards or normative documents: EN 61010-1, EN 61010-2-010, EN 61326-1, EN 60529 and EN ISO
12100.
Source language: German
Page Device setup/Display 2
Declaration of conformity 4 Explication of warning symbols 4 Safety instructions 5 Correct use 6 Unpacking 6
Commissioning 6 Interfaces and outputs 8 Maintenance and cleaning 9 Error codes 10 Warranty 10 Technical Data 11
DANGER
DANGER
CAUTION
WARNING
NOTICE
Indicates an (extremely) hazardous situation, which, if not avoided, will result in death, serious injury.
Indicates a potentially hazardous situation, which, if not avoided, can result in death, serious injury.
Indicates a potentially hazardous situation, which, if not avoided, can result in injury.
Indicates practices which, if not avoided, can result in equipment damage.
DANGER - note on hazards arising from a hot surface.
5
• Read the operating instructions completely before starting up and follow the safety instructions.
• Keep the operating instructions in a place where they can be accessed by everyone.
Ensure that only trained staff work with the device.
• Follow the safety instructions, guidelines, occupational health and safety and accident prevention regulations.
• Wear your personal protective equipment in accordance with the hazard category of the medium to be processed. Otherwise there is a risk of splashing liquids.
• Set up the device in a spacious area on an even, stable, clean, non-slip, dry and fireproof surface.
• Prior to each use, always check the device for damage. Do not use damaged components.
CAUTION
Only process and heat up media that has a flash point higher than the adjusted safe temperature lim­it of the heating bath that has been set. The safe temperature limit of the heating bath must always be set to at least 25 °C lower than the fire point of the media used.
DANGER
Risk of burns! During operation, the heating bath housing can get hot.
When emptying the device use only the handles to carry and hold it.
• Prior to filling or emptying the heating bath, the device must be switched off and disconnected from the power supply at the plug.
• Only fill or empty the heating bath when it is cold.
• Empty the heating bath prior to transporting it.
• Never operate the heating bath without tempering medium.
DANGER
The preferred tempering medium in the heating bath is water (up to approx. 80 °C) or the low-viscosity silicone oils (50 mPas) with a flash point > 260 °C are also permitted. There is a risk of burning when us­ing tempering media with lower flashpoints!
• Before use, calculate the optimum filling level of the tempering medium! Pay special attention to the change in volume caused by heating and the displacement that occurs when immersing an object, for example, an evaporating flask.
• When using the heating bath in combination with a rotary evaporator, the heating bath temperature must not be allowed to rise to a value higher than the boiling point of the solvent at normal pressure, since if the evaporating flask glass were to break there would be a hazard due to liquid spraying out (for instance breakage of the evaporating flask glass during distilla­tion of water using a silicone oil bath).
CAUTION
When working with the IKA rotary evaporator, be aware of a hazard arising from breakage of the evap­orating flask glass.
CAUTION
Be aware of a hazard due to lack of grip on a wet evaporating flask, in particular when operating the IKA HB digital heating bath with silicone oil!
• When using as a water bath, the use of demineralised water is recommended.
• Always observe the minimum filling level of one litre when using oil as the tempering medium.
• Ensure that the interfaces are not soiled.
• Beware of hazards due to flammable materials.
• Only process media that will not react dangerously to the extra energy produced through processing. This also applies to any extra energy produced in other ways, e.g. through light irradia­tion.
• Do not operate the device in explosive atmospheres, with haz­ardous substances or under water.
• The device will automatically restart in mode C following any interruption to the power supply.
• The device can only be disconnected from the mains supply by pulling out the mains plug or the connector plug.
• The socket for the mains cord must be easily accessible.
• The voltage stated on the type plate must correspond to the mains voltage.
Socket must be earthed (protective ground contact).
• Protect the device and accessories from bumps and impacts.
• The device may only be opened by experts.
• Solvents can be hazardous to health. Therefore comply with the relevant warnings and refer to the relevant safety data sheet (Internet).
• If silicone oil is used as a tempering medium, in the event that the evaporating flask fractures there is a risk that on mixing with the aqueous solvents (contents of the evaporating flask) the hot oil will foam up and spurt out in conjunction with a rapid in­crease in volume (formation of bubbles by the solvent).
Safety instructions
6
Unpacking
Commissioning
• Unpacking
- Unpack the device carefully,
- Any damage should be notified immediately to the shipping agent (post, rail or logistics company).
• Scope of delivery
- Heating bath IKA HB digital
- Power supply cable
- USB cable
- Operating instructions
- Warranty card
Correct use
• Use
The IKA tempering baths HB digital is laboratory device and is suitable for directly tempering substances filled into the bath con­tainer. They are also suitable for indirect tempering of substances filled in glass containers when the glass containers are immersed in the actual tempering medium. A rotary glass container is particularly advantageous, for example, when used in conjunction with an
IKA rotary evaporator.
CAUTION
The device is not intended to pre­pare food!
• Area of use (only indoors)
- Laboratories - Schools
- Pharmacies - Universities
This device is suitable for use in all areas except:
- Residential areas
- Areas that are connected directly to a low-voltage supply net­work that also supplies residential areas.
The safety of the user cannot be guaranteed:
- If the device is operated with accessories that are not supplied or recommended by the manufacturer;
- If the device is operated improperly or contrary to the manufac­turer’s specifications;
- If the device or the printed circuit board are modified by the third parties.
Observe the ambient conditions (temperature, humidity, etc.) list­ed under “Technical Data”.
The unit is ready for service when the mains plug has been plugged in.
Prior to commissioning the device, determine the filling quantity of the tempering medium due to the used evaporator piston size (approx. 2.5 l tempering medium by using a standard 1 l evapora­tor piston).
• Switch on the device using the mains switch (B).
• At every start, the display will show all display segments (Fig. 2) and the software version (Fig. 4).
Note: Only the display segments shown on Fig. 3 are available in functions for the current device.
• The set operating mode (A/B/C) is indicated on the top of the display (Fig. 5).
• The heating bath temperature is held constant by the control circuit and is additionally monitored by the safety circuit.
In the event of an error occurred in the control circuit, the heat-
ing bath is switched off permanently by the safety circuit.
An error in the control or safety circuits is shown on the display. The heating function can no longer be started.
• When switching off the heating function and the medium tem­perature is higher than 50 °C, the display will alternately show OFF and HOT (Fig. 6, Fig. 8).
Activate the SET function by turning and pressing the rotating/ pressing knob (C).
• Switch on the device using the mains switch (B), when the ope­ning screen (Fig. 5) appears and the setting for the safety tem­perature is activated for 5 seconds. “SAFE TEMP.“ flashes on the display, see also “Setting the safety temperature“.
• The display then switches from “SAFE TEMP.“ to “TEMP.“ and the SET function is activated. (Fig. 6)
• Set the desired heating bath temperature by turning the rota­ting/pressing knob (C).
• The SET function flashes every few seconds.
• Confirm the value by pressing the rotating/pressing knob (C).
• If not confirmed, the set value is not saved.
• The SET function stops flashing.
• Start the heating process by pressing the rotating/pressing knob (C).
Setting the target temperature
7
Safety circuit
The adjustable safety circuit prevents the temperature of the heat­ing bath from getting too high as a result of:
- a controller error,
- the rotating/pressing knob having been accidentally turned. Once the safety temperature has been reached, the device switch­es off permanently. Furthermore, dry running of the heating bath is detected. The de­vice switches off permanently. The dry running function detects both accidental heating of the heating bath without liquid and dry running caused by water evaporation starting at a set temperature of 60 °C. The error mes­sage E 26 appears and the heating bath is switched off perma­nently. To remedy this error, see “Error codes”. When the safety circuit is set, an upper temperature limit between 50 and 190 °C is defined.
Silicone oils as tempering media When increased safety is not necessary the temperature of the
safety circuit stays at 190 °C.
Temperature of the tempering medium rises to a maximum of
190 °C in the case of an error. Then the safety circuit switches the heating bath permanently off.
Demineralised water as the tempering medium When increased safety is not necessary, the adjustment knob of
safety circuit stays all the way to the right. As long as there is any demineralised water in the heating bath, the temperature of the tempering medium rises to a maximum of 100 °C, in the case of
Operating mode A
• Switch on the device at the mains switch (B).
• The heating function is switched off.
• Safe Temp (safety temperature) will appear for 5 seconds. (Fig.
5)
• The target value is set to 20 °C.
• The controller tempering medium is set to water.
• The heating function must be restarted following a power fail­ure.
• The following settings are possible/adjustable:
- the target value,
- the safety circuit,
- the controller tempering medium.
• Mode A always appears on the top of the screen.
Factory setting: Mode A
Operating mode B
• Switch on the device at the mains switch (B).
• The heating function is switched off.
• Safe Temp (safety temperature) will appear for 5 seconds.
• The target value is set to 20 °C or the most recent temperature setting.
• The controller tempering medium is set to water or the most recent medium setting.
• The heating function must be restarted following a power failu­re.
• The following settings are possible/adjustable:
- the target value setting,
an error. If the water is evaporated completely, the temperature of the tempering medium rises to a maximum of 190 °C. Then the safety circuit switches off the heating bath permanently.
Temperature-sensitive or easily flammable media in the ro-
tary evaporator
When the pre-set bath temperature may not be exceeded under
any circumstances set the safety temperature as described be­low.
Adjusting the safety temperature
- Set the desired safety temperature by turning the rotating/pres­sing knob (C) within the 5 seconds of the “SAFE TEMP.“ appear­ing on the display after the device is switched on. (Fig. 5)
Checking the safety circuit
- The safety circuit has to be checked by the user once a year.
- Fill the heating bath with 1 liter of water as tempering medium.
- Set the safety temperature to 100 °C.
- Set the set temperature to 80 °C.
- Start the heating function by pressing the rotating/pressing knob (C).
- When the set temperature is reached, turn the heating bath off and on again at the mains switch (B).
- Set the safety temperature to 70 °C.
- The medium temperature is thus 10 K above the safety tem­perature, the safety circuit trips, the display shows E 24. (Fig. 7)
- the controller tempering medium.
• The safety circuit is set to the most recently set value and cannot be adjusted.
• Mode B always appears on the top of the screen.
Operating mode C
• Switch on the device at the mains switch (B).
• The heating function is switched on or off depending on the last selected setting.
• Safe Temp (safety temperature) will appear for 5 seconds.
• The last target value set in mode B applies.
• The setting controller tempering medium set before the device was last switched off in mode B applies.
• The following settings cannot be adjusted:
- the target value,
- the safety circuit,
- the controller tempering medium.
• Mode C always appears on the top of the screen.
Switching the operating modes
• Switch the device off at the mains switch (B).
• Press and hold rotating/pressing knob (C) and switch the device on at the mains switch (B). Release the rotating/pressing knob (C) after 2 seconds. The new operating mode appears and fla­shes 3 times on the top of the screen.
• Sequence A, B, C, A etc.
Setting the operating modes
Setting the safety temperature
8
The operating settings can be locked by pressing and holding the key (E) for 2 seconds, preventing any inadvertent changes during ope­ration. The lock symbol appears on the screen when this function is activated. (Fig. 10)
Press and hold the key (E) again for 2 seconds to unlock the operating settings. The lock symbol disappears when function is deactivated.
Interfaces and outputs
The device can be operated by computer via an USB interface using the laboratory software labworldsoft®.
Note: Please comply with the system requirements together with the operating instructions and help section included with the software.
USB interface
The Universal Serial Bus (USB) is a serial bus for connecting the device to the PC. Equipped with USB devices can be connected to a PC during operation (hot plugging). Connected devices and their properties are automatically recognized. Use the USB interface in conjunction with labworldsoft
®
for op-
eration in “Remote” mode and also to update the firmware.
USB device drivers
First, download the latest driver for IKA devices with USB inter­face from:
http://www.ika.com/ika/lws/download/usb-driver.zip
Install the driver by running the setup file. Then connect the IKA device through the USB data cable to the PC. The data communi­cation is via a virtual COM port.
Command syntax and format
The following applies to the command set:
- Commands are generally sent from the computer (Master) to the lab device (Slave).
- The lab device sends only at the computer’s request. Even fault indications cannot be sent spontaneously from the lab device to the computer (automation system).
- Commands are transmitted in capital letters.
- Commands and parameters including successive parameters are separated by at least one space (Code: hex 0x20).
Data transfer via IR interface
IR
Key “Lock“
IR interface
Controlling the medium temperature
The medium temperature is limited by the set safety temperature, controlled by means of a PID controller and measured by the PT 1000 temperature sensor, and the medium is heated up as quickly as pos­sible without overshooting to the set temperature. The PID controller adapts to the different tempering media and en­sures optimum temperature control with minimum temperature drift and fluctuation. Optimum control is only achieved when the medium is mixed using a rotating evaporator piston.
- Set the desired medium temperature between room temperature and 180 °C by turning the rotating/pressing knob (C). The max. medium temperature setting is the safety temperature minus 10 °C.
- Start the heating function by pressing the rotating/pressing knob (C).
- An animated heating symbol appears on the display. (Fig. 9)
- The heating bath is heated up to the set temperature.
- The set and actual temperature referred to the medium are shown on the display. (Fig. 9)
Select tempering medium
- If a target value > 90 °C is set, the PID controller is adapted specially for oil.
- The “OIL“ symbol appears on the display. (Fig. 11)
- If the target value is reset to 20 °C the PID controller is adjusted again specially to water.
- The “OIL“ symbol will disappear from the display. (Fig. 9)
The heating bath transfers data via IR interfaces. These interfaces are located on the left display side of the heating bath or on the right side of the drive unit. Do not place any objects between the two operating units as otherwise the data transfer may be interrupted!
Remote Mode
Using the laboratory device software “labworldsoft
®
” and the rota­ry evaporator RV 10 digital/control the device can be operated in “Remote” mode. In this mode, the device can no longer be hand­operated. (Fig. 12) Note: Please comply with the system requirements together with the operating instructions and help section included with the software.
Fig. 13
9
NAMUR Commands Function
IN_NAME Read the device name IN_PV_2 Read medium temperature actual value IN_SP_2 Read medium temperature set value OUT_SP_2 V Set medium temperature set value IN_SP_3 Read safety temperature set value OUT_SP_3 V Set safety temperature value IN_SP_74 Read medium type set value
(1 - water, 0 - oil)
OUT_SP_74 V Set medium type value
(1 - water, 0 - oil)
START_2 Start heating STOP_2 Stop heating
Maintenance and cleaning
The device is maintenance-free. It is only subject to the natural wear and tear of components and their statistical failure rate.
Cleaning
Remove the device from the mains before cleaning.
Only use cleaning materials recommended by IKA:
Dirt Cleaning agent
Dyes Isopropyl alcohol Building materials
Water containing detergent/isopropyl alcohol
Cosmetics
Water containing detergent/isopropyl alcohol Food Water containing detergent Fuels Water containing detergent Other materials Please consult IKA
Wear protective gloves during cleaning the devices. Electrical devices may not be placed in the cleansing agent for the purpose of cleaning. Do not allow moisture to get into the device when cleaning. Before using another than the recommended method for clean­ing or decontamination, you must ascertain with IKA that this method does not destroy the device.
Ordering spare parts When ordering spare parts, please give:
- Device type,
- Serial number, see rating plate,
- Position number and description of spare part, see www.ika.com,
- Software version.
Repairs
Please only send devices in for repair that have been cleaned and are free of materials which might present health haz­ards.
For this, use the “certificate of compliance” form which you can obtain from IKA or can download a version for printing from the IKA website at www.ika.com. If your appliance requires repair, return it in its original packaging. Storage packaging is not sucient when sending the device - also use appropriate transport packaging.
USB cable A - B
This cable is used to connect the USB interface to a PC.
USB Micro B
USB A
- Each individual command (incl. parameters and data) and each response are terminated with Blank CR LF (Code: hex 0x20 hex 0x0d hex 0x20 hex 0x0A) and have a maximum length of 80 characters.
- The decimal separator in a number is a dot (Code: hex 0x2E).
The above details correspond as far as possible to the recommendations of the NAMUR working party (NAMUR recommendations for the design of electrical plug connections for analogue and digital signal transmission on individual items of laboratory control equipment, rev. 1.1). The NAMUR commands and the additional specific IKA commands serve only as low level commands for communication between the lab device and the PC. With a suitable terminal or communications program these commands can be transmitted directly to the lab device. The IKA software package, labworldsoft®, provides a convenient tool for controlling lab device and collecting data under MS Windows, and includes graphical entry features, for motor speed ramps for example. The following table summarises the (NAMUR) commands understood by the IKA equipment.
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