Hanna instruments HI 98160 User Manual

ALT
LIGHT
HI 98160
Microprocessor Logging pH/ORP Meter
LOG
RANGE CAL
SALES AND TECHNICAL SERVICE CONTACTS
Australia:
Tel. (03) 9769.0666 • Fax (03) 9769.0699
China:
Tel. (10) 88570068 • Fax (10) 88570060
Egypt:
Tel. & Fax (02) 2758.683
Germany:
Tel. (07851) 9129-0 • Fax (07851) 9129-99
Instruction Manual
HI 98160
Portable Waterproof
Microprocessor
Logging GLP
Greece:
Tel. (210) 823.5192 • Fax (210) 884.0210
Indonesia:
Tel. (21) 4584.2941 • Fax (21) 4584.2942
Japan:
Tel. (03) 3258.9565 • Fax (03) 3258.9567
Korea:
Tel. (02) 2278.5147 • Fax (02) 2264.1729
Malaysia:
Tel. (603) 5638.9940 • Fax (603) 5638.9829
Singapore:
Tel. 6296.7118 • Fax 6291.6906
South Africa:
Tel. (011) 615.6076 • Fax (011) 615.8582
Taiwan:
Tel. 886.2.2739.3014 • Fax 886.2.2739.2983
Thailand:
Tel. (662) 619.0708.11 • Fax (662) 619.0061
United Kingdom:
Tel. (01525) 850.855 • Fax (01525) 853.668
USA:
Tel. (401) 765.7500 • Fax (401) 765.7575
pH / ORP Meter
MAN98160R1 09/04
For e-mail contacts and a complete list of Sales and Technical offices, please see www.hannainst.com.
www.hannainst.com
Dear Customer, Thank you for choosing a Hanna Instruments Product. Please read this instruction manual carefully before using the instru-
ment. This manual will provide you with all the necessary information for the
correct use of the instrument, as well as a precise idea of its versatility in a wide range of applications.
If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com
This instrument is in compliance with the directives.
TABLE OF CONTENTS
PRELIMINARY EXAMINATION ..................................................................... 3
GENERAL DESCRIPTION ........................................................................... 3
FUNCTIONAL DESCRIPTION ....................................................................... 5
SPECIFICATIONS .................................................................................. 6
INITIAL PREPARATION .............................................................................. 7
SETUP MODE .................................................................................. 8
TAKING pH MEASUREMENTS ................................................................. 11
TAKING ORP MEASUREMENTS ............................................................... 12
TAKING TEMPERATURE MEASUREMENTS ................................................ 12
AUTO ENDPOINT MODE ........................................................................ 13
pH CALIBRATION PROCEDURE ............................................................... 13
ELECTRODE CONDITION ........................................................................ 16
mV CALIBRATION PROCEDURE .............................................................. 16
TEMPERATURE CALIBRATION PROCEDURE .............................................. 17
LOGGING FUNCTION ............................................................................. 18
GOOD LABORATORY PRACTICE (GLP) ..................................................... 20
LCD BACKLIGHT ............................................................................... 22
DATA TRANSFER TO PC ......................................................................... 22
BATTERY REPLACEMENT ....................................................................... 24
TEMPERATURE CORRELATION FOR HANNA pH SENSITIVE GLASS ................ 25
ELECTRODE CONDITIONING AND MAINTENANCE ...................................... 26
ACCESSORIES ...................................................................................... 29
WARRANTY ......................................................................................... 31
WARRANTY
All Hanna Instruments meters are warranted for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions.
Electrodes and probes are warranted for a period of six months.
This warranty is limited to repair or replacement free of charge. Damages due to accident, misuse, tampering or lack of prescribed
maintenance are not covered. If service is required, contact the dealer from whom you purchased the
instrument. If under warranty, report the model number, date of purchase, serial number and the nature of the failure. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization number from the Cus­tomer Service department and then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packaged for complete protection.
Hanna Instruments reserves the right to modify the design, con­struction and appearance of its products without advance notice.
Recommendations for Users
Before using this product, make sure that it is entirely suitable for the environment in which it is used. Operation of this instrument in residential area could cause unaccept­able interferences to radio and TV equipments, requiring the operator to take all necessary steps to correct interferences. The glass bulb at the end of the electrode is sensitive to electrostatic discharges. Avoid touching this glass bulb at all time. During calibration of instruments, ESD wrist straps should be worn to avoid possible damage to the electrode by electrostatic discharge. Any variation introduced by the user to the supplied equipment may degrade the instrument's EMC performance. To avoid electrical shock, do not use these instruments when voltages at the measurement surface exceed 24VAC or 60 VDC. To avoid damages or burns, do not perform any measurement in microwave ovens.
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HI 2031B Glass-body, semimicro, conic tip, refillable FC 100B Plastic-body (Kynar®), double junction, refillable, for
food industry.
FC 200B Plastic-body (Kynar®), single junction, conic, Viscolene,
non-refillable, for meat & cheese.
FC 210B Glass-body, double junction, conic, Viscolene, non-
refillable, for milk & yogurt.
FC 220B Glass-body, triple ceramic, single junction, refillable, for
food processing.
FC 911B Plastic-body (Kynar®), double junction, refillable with
built-in amplifier
HI 1413B Glass-body, single junction, flat tip, Viscolene for sur-
face measurement.
ORP ELECTRODES (with BNC connector & 1 m cable)
HI 3131B Glass-body, refillable, Pt sensor HI 3230B Plastic-body (Ultem®), gel-filled, Pt sensor HI 4430B Plastic-body (Ultem®), gel-filled, Gold sensor
OTHER ACCESSORIES
HI 710031 Rugged carrying case HI 740027 1.5V AA size alkaline batteries (4 pcs) HI 76405 Electrode holder HI 7662 Temperature probe with 1 m (3.3') cable HI 8427 pH and mV simulator HI 931001 pH and mV simulator with display HI 920011 5 to 9-pin cable for connection to PC
Ultem® is registered Trademark of "General Electrics Co."
Kynar® is registered Trademark of "Pennwalt Corp."
PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer.
Each meter is supplied complete with:
• HI1230B/C pH electrode, double junction, plastic body, BNC
connector with protective sleeve, 1 m (3.3') cable
• HI7662 temperature probe with 1 m (3.3') cable
• HI70004 pH 4.01 buffer solution, 20 ml sachet (1 pc)
• HI70007 pH 7.01 buffer solution, 20 ml sachet (1 pc)
Instruction manual
1.5V AA size alkaline batteries (4 pcs)
Rugged carrying case.
Note: Save all packing material until you are sure that the
instrument functions correctly. All defective items must be returned in their original packaging together with the sup­plied accessories.
GENERAL DESCRIPTION
HI98160 is a portable logging microprocessor-based pH/ORP/tempera­ture meter.
All pH measurements are automatically compensated for temperature (ATC or MTC). The instrument housing is made of rugged, lightweight material, making it truly portable.
Eight memorized buffers (1.68, 3.00, 4.01, 6.86, 7.01, 9.18, 10.01 and 12.45 pH) and wrong buffer recognition technology make pH calibration simple and error free. One or two-point procedure can be performed.
The meter is also equipped with a stability indicator and backlight feature for comfortable reading even in excessively dark environments.
An user friendly interface provides clear messages regarding errors, functions and more.
The GLP features provide a guarantee of data consistency. Measurements can be performed with lab-grade precision in the field as
well as in the laboratory. An alarm time-out is available to alert the user if too much time has
elapsed since the last pH calibration and that re-calibration may be required.
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The meter provides a controlled access to calibration and GLP settings through a password protection method.
The Battery Error Preventing System (BEPS) recognizes batteries level and automatically switches the meter off when batteries are too weak to support proper function.
To prolong battery life, the backlight feature is automatically disabled when the batteries are getting low; a clear indication is displayed on LCD to warn the user of this condition. However, the meter continues to measure correctly even when the low battery indication is dis­played.
The meter can store measurements in memory upon user request for retrieval at a later time.
HI98160 also allows transfer of data to computer through the RS232 interface.
In addition, the meter allows the user to enter an ID code to uniquely identify the instrument. Made of tough, lightweight ABS material, the water-resistant rugged casing is built to last. The meter is in compliance with IP67 standards: dust-tight, pro- tected against the effects of temporary immersion in water and designed to provide laboratory results and accuracy under harsh industrial conditions.
ACCESSORIES
pH CALIBRATION SOLUTIONS
HI 70004P pH 4.01 Buffer Sachets, 20 ml sachet, 25 pcs HI 70007P pH 7.01 Buffer Sachets, 20 ml sachet, 25 pcs HI 70010P pH 10.01 Buffer Sachets, 20 ml sachet, 25 pcs
HI 7001M pH 1.68 Buffer Solution, 230 ml HI 7004L pH 4.01 Buffer Solution, 500 ml HI 7006L pH 6.86 Buffer Solution, 500 ml HI 7007L pH 7.01 Buffer Solution, 500 ml HI 7009L pH 9.18 Buffer Solution, 500 ml HI 7010L pH 10.01 Buffer Solution, 500 ml
ELECTRODE STORAGE & CLEANING SOLUTIONS
HI 70000P Electrode Cleaning Sachets, 20 ml sachet, 25 pcs HI 70300L Storage Solution, 460 ml HI 7061L General Cleaning Solution, 460 ml HI 7073L Protein Cleaning Solution, 460 ml HI 7074L Inorganic Cleaning Solution, 460 ml HI 7077L Oil & Fat Cleaning Solution, 460 ml
REFILL ELECTROLYTE SOLUTIONS
HI 7071 3.5M KCl + AgCl Electrolyte, 4x50 ml HI 7072 1M KNO3 Electrolyte, 4x50 ml HI 7082 3.5M KCl Electrolyte, 4x50 ml, for double junction electrodes
ORP PRETREATMENT SOLUTIONS
HI 7091L Reducing Pretreatment Solution, 460 ml HI 7092L Oxidizing Pretreatment Solution, 460 ml
pH ELECTRODES (with BNC connector & 1 m cable)
HI 1230B/C Plastic-body (Ultem®), double junction, gel-filled, BNC
protective sleeve
HI 1230B Plastic-body (Ultem®), double junction, gel-filled HI 1043B Glass-body, double junction, refillable, combination HI 1053B Glass-body, triple ceramic, conic shape, refillable, HI 1083B Glass-body, micro, Viscolene HI 1131B Glass-body, single junction, refillable HI 1330B Glass-body, semimicro, single junction, refillable HI 1331B Glass-body, semimicro, single junction, refillable HI 1332B Plastic-body (Ultem®), double junction, refillable
Ultem® is registered Trademark of "General Electrics Co."
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ON / OFF
ALT
LIGHT
HI 98160
Microprocessor Logging pH/ORP Meter
LOG
RANGE CAL
For refillable electrodes:
Refill it with fresh electrolyte (HI7071 for single junction or HI7082 for double junction). Allow the electrode to stand upright for 1 hour.
Follow the Storage Procedure above.
CLEANING PROCEDURE
General Soak in Hanna HI7061 General Cleaning Solution for approximately 1 hour.
Removal of films, dirt or deposits on the membrane/junction:
- Protein Soak in Hanna HI7073 Protein Cleaning
Solution for 15 minutes.
- Inorganic Soak in Hanna HI7074 Inorganic Cleaning
Solution for 15 minutes.
- Oil/grease Rinse with Hanna HI7077 Oil and Fat Cleaning
Solution.
IMPORTANT: After performing any of the cleaning procedures rinse
the electrode thoroughly with distilled water, drain and refill the reference chamber with fresh electrolyte, (not necessary for GEL filled electrodes) and soak the electrode in HI70300 Storage Solution for at least 1 hour before taking measurements.
TROUBLESHOOTING
Evaluate your electrode performance based on the following possibilities.
• Noise (Readings fluctuate up and down) could be due to:
- Clogged/Dirty Junction: Refer to the Cleaning Procedure above.
- Loss of shielding due to low electrolyte level (in refillable electrodes only): refill with fresh HI7071 for single junction or HI7082 for double junction electrodes.
• Dry Membrane/Junction: Soak in Storage Solution HI70300
for at least 1 hour.
• Drifting: Soak the electrode tip in warm Hanna Solution HI7082 for one hour then flush tip with distilled water. Refill with
fresh HI7071 for single junction electrodes and HI7082 for double junction electrodes.
• Low Slope: Refer to the cleaning procedure above.
• No Slope: Check the electrode for cracks in glass stem or bulb
and replace the electrode.
• Slow Response/Excessive Drift: Soak the tip in Hanna Solu­tion HI7061 for 30 minutes, rinse thoroughly in distilled water and then follow the Cleaning Procedure above.
FUNCTIONAL DESCRIPTION
1) Socket for temperature probe
2) RS232 connector
3) BNC connector for pH electrode
4) Liquid Crystal Display (LCD)
5) ON/OFF key, to turn the meter on and off
6) ALT key, to alternate key function
7) RANGE / GLP key, to select measurement ranges, to display time
and date, and to view calibration data (with ALT)
8) CAL / AutoEnd key, to enter pH calibration mode or (with ALT)
to enter Auto Endpoint mode
9) / CFM key, to move down or confirm values (with ALT)
10) LOG / RCL key, to store or recall measurements (with ALT)
11) / FNC key, to move up or enter setup mode (with ALT)
12) LIGHT / DEL key, to turn the LCD backlight on and off and to
delete stored data (with ALT)
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