Hanna Instruments HI 38039 User Manual

Instruction Manual
HI 38039
Iron Low Range
Test Kit with
Checker Disc
www.hannainst.com
Dear Customer, Thank you for choosing a Hanna Product. Please read the instruction sheet carefully before using the
test kit. It will provide you with the necessary information for correct use of the kit. If you need additional information, do not hesitate to e-mail us at tech@hannainst.com.
Each kit is supplied with:
HI 3834-0 Reagent, packets (100 pcs);
• 1 checker disc (containing a mirror, a mirror holder
• and the 38039 disc);
2 glass vials with caps;
• 1 plastic pipette (3 mL).
Note: Any damaged or defective item must be returned in
its original packing materials.
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
Range 0 to 1.0 mg/L (ppm) as Fe Smallest Increment 0.02 mg/L (ppm) Fe Analysis Method Colorimetric Sample Size 15 mL Number of Tests 100 Case Dimensions 235x175x115 mm (9.2x6.9x4.5") Shipping Weight 436 g (15.4 oz)
SIGNIFICANCE AND USESIGNIFICANCE AND USE
SIGNIFICANCE AND USE
SIGNIFICANCE AND USESIGNIFICANCE AND USE
Generally, ground and surface water contains no more than 1 mg/L (ppm) iron; but due to mining and industrial drainage, higher levels of iron have been observed. Iron in water appears to be more of a nuisance than a hazard. The presence of iron can stain laundry and give water a bittersweet taste.
The Hanna Test Kit determines the iron concentration in water by conversion of the ferrous (Fe fast and easy. The checker disc makes it simple to obtain the iron level in water.
Note: mg/L is equivalent to ppm (parts per million).
CHEMICAL REACTIONCHEMICAL REACTION
CHEMICAL REACTION
CHEMICAL REACTIONCHEMICAL REACTION
Iron can exist as ferrous (Fe2+) or ferric (Fe3+) ions. The Hanna Test Kit determines total iron levels in water via a colorimetric method. First all ferric ions are reduced by sodium sulfite to ferrous ions. Phenanthroline complexes with ferrous ion to form an orange colored solution. The color intensity of the solution determines the iron concentration.
INSTRUCTIONSINSTRUCTIONS
INSTRUCTIONS
INSTRUCTIONSINSTRUCTIONS
READ THE ENTIRE INSTRUCTIONS BEFORE USING THE KIT
• Verify that the mirror, its holder and the disc are pre­installed in the checker disc. If not, install them as shown in the figure.
ISTR38039 09/00 PRINTED IN ITALY
2+
) state. The test is
• Using the plastic pipette, fill each glass vial with 15 mL of sample (up to the mark).
• Insert one of the vials into the left hand opening of the checker disc. This is the blank.
• Add to the other vial 1 packet of HI 3834-0 re­agent. Replace the cap and shake to mix.
• Wait for 3 minutes to allow reac­tion to occur. This is the reacted sample.
• Remove the cap and in­sert the reacted sample into the right hand open­ing of the checker disc.
• Hold the checker disc so that a light source illumi­nates the samples from the top.
15 mL
• Keep the checker disc at a distance of 30-40 cm (12­16") from the eyes to match the color while having a uniform background (e.g. a white sheet). Rotate the disc while looking at the color test windows and stop when you find the color match. Read the value in the result window directly in mg/L (or ppm) of Iron.
For best results: Perform the reading three times and
take the average value (divide by 3 the sum of the three numbers). Intensely colored samples will make the color matching difficult and they should be adequately treated before performing the test. Sus­pended matter in large amounts should be removed by prior filtration.
Caution: Ultraviolet radiation may cause fading of colors.
When not in use, keep the disc protected from light, in a cool and dry place.
Interferences: Molybdate and Molybdenum above 50 ppm,
calcium above 10000 ppm (as CaCO above 100000 ppm, chloride above 185000 ppm.
REFERENCESREFERENCES
REFERENCES
REFERENCESREFERENCES
1987 Annual Book of ASTM Standard, Volume 11.01 Water (1), pages 531-535.
Standard Methods for the Examination of Water and Wastewater, 16
The chemicals contained in this kit may be hazardous if improperly handled. Read the relevant Health and Safety Data Sheet before performing this test.
th
Edition, pages 215-219.
HEALTH AND SAFETYHEALTH AND SAFETY
HEALTH AND SAFETY
HEALTH AND SAFETYHEALTH AND SAFETY
), magnesium
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