Hach-Lange FP 360 sc User Manual

DOC023.52.90161

FP 360 sc

User Manual
01/2010, Edition 1B
© HACH-LANGE GmbH, 2010. All rights reserved. Printed in Germany
Table of Contents
Section 1 Specifications ........................................................................................................................ 5
Section 2 General information............................................................................................................... 7
2.1 Safety information............................................................................................................................... 7
2.1.1 Use of hazard information.......................................................................................................... 7
2.1.2 Precautionary labels .................................................................................................................. 7
2.2 Product overview ................................................................................................................................ 8
2.3 Measuring principle............................................................................................................................. 8
2.4 Product components........................................................................................................................... 8
2.4.1 FP 360 sc sensor ...................................................................................................................... 9
2.5 Function test ....................................................................................................................................... 9
Section 3 Installation............................................................................................................................ 11
3.1 Connect sensor cable....................................................................................................................... 11
3.2 Installation options............................................................................................................................ 13
3.2.1 Installation with the chain mount kit ......................................................................................... 13
3.2.2 Installation of chain mount kit for sensors with cleaning unit ................................................... 13
3.2.2.1 Install the cleaning unit hose........................................................................................... 13
3.2.3 Installation with flow cell........................................................................................................... 15
Section 4 Operation.............................................................................................................................. 17
4.1 User interface and navigation ........................................................................................................... 17
4.2 Sensor setup..................................................................................................................................... 17
4.3 Sensor data logger ........................................................................................................................... 17
4.4 Menu structure.................................................................................................................................. 18
4.4.1 SENSOR STATUS................................................................................................................... 18
4.4.2 SENSOR SETUP..................................................................................................................... 18
4.5 Calibration......................................................................................................................................... 20
4.5.1 Factory calibration.................................................................................................................... 20
4.5.2 Process calibration/adjustment................................................................................................ 20
4.5.2.1 Determination of factors and adjustment of slope........................................................... 20
4.5.2.2 Multi-point calibration ...................................................................................................... 21
4.5.3 Check the zero point................................................................................................................ 21
4.5.4 Adjustment of slope and zero point; multi-point calibration......................................................21
4.5.4.1 Adjust the slope (FACTOR) ............................................................................................ 21
4.5.4.2 Adjust the zero point (OFFSET)...................................................................................... 22
4.5.4.3 Multi-point calibration (2 to 5-point calibration) ............................................................... 22
Section 5 Maintenance ......................................................................................................................... 23
5.1 Maintenance schedule...................................................................................................................... 23
5.2 Maintenance for the connectors on the sensor................................................................................. 23
5.3 Cleaning the measurement windows................................................................................................ 24
3
Table of Contents
Section 6 Troubleshooting ...................................................................................................................25
6.1 Error messages.................................................................................................................................25
6.2 Warnings ...........................................................................................................................................25
6.3 Replacement parts ............................................................................................................................25
Section 7 Replacement parts and accessories ..............................................................................27
7.1 Sensor options ..................................................................................................................................27
7.2 Replacement parts ............................................................................................................................27
7.3 Accessories.......................................................................................................................................27
Section 8 Contact information ............................................................................................................29
Section 9 Warranty and Liability..........................................................................................................31
Appendix A Modbus register ..............................................................................................................33
Index.......................................................................................................................................................35
4

Section 1 Specifications

Specifications are subject to change without notice.
Measurement
UV fluorescent measurement process for polycyclic aromatic
Measurement method
Low measurement range
Measuring range
High measurement range
Display units ppb, ppm, μg/L, mg/L
Reproducibility 2.5% of measurement value at a constant temperature
Measurement accuracy
Limit of detection 1.2 ppb (PAH)
Hydrocarbons (PAH) Excitation wavelength: 254 nm Emission (measurement) wavelength: 360 nm
0 to 50 ppb and 0 to 500 ppb in relation to PAH calibration standard, corresponding to 0.1 to 1.5 ppm and 0.1 to 15 ppm of oil calibration standard
0 to 500 ppb and 0 to 5000 ppb in relation to PAH calibration standard, corresponding to 0.1 to 15 ppm and 0.1 to 150 ppm of oil calibration standard
5% of measurement value ±2% from measurement range limit at a constant temperature
Response time 10 s (T90)
Calibration
Sensor software
Software version From 1.14
Equipment properties
Measurement sensor Stainless steel version 2.8 kg, titanium version 1.8 kg
Weight
Flow cell Approximately 0.6 kg, including installation board approximately 2.0 kg
Sensor Max. 30 bar
Pressure range
Flow cell Max. 1 bar
Measurement sensor (Ø × length)
Dimensions
Flow cell (L × W × D)
Measurement sensor
Materials
Flow cell
Shackle Stainless steel 1.4301
Factory calibration with UV fluorescence calibration standard, custom adaptation possible
68 mm x 306 mm (2.68 in. x 12.05 in.) (without plugs or suspension pin) 68 mm x 399 mm (2.68 in. x 15.71 in.) (including suspension pin) 68 mm x 413 mm (2.68 in. x 16.26 in.) (with additional cleaning option)
98 mm x 98 mm x 150 mm (3.86 in. x 3.86 in. x 5.91 in.) (without fittings), installation board: 600 x 300 x 10 mm (23.62 in. x 11.81 in. x 0.39 in.)
Housing: stainless steel 1.4571 or titanium Optic bracket: POM Housing bolts: stainless steel 1.4571 Measurement window: synthetic quartz glass (Suprasil) Gaskets (housing): Viton Gaskets (measurement window): NBR (Nitrile Butadiene Rubber)
Housing: POM Installation board: PVC Gaskets: NBR (Nitrile Butadiene Rubber) Fittings: nickel-plated brass
5
Specifications
Environment considerations
Sample temperature 1 to 40 °C (34 to 104 °F)
–5 to +45 °C (23 to 113 °F)
Ambient temperature
Sensor distance - wall/ground min. 100 mm (3.94 in.) (recommended)
Miscellaneous
Cable length 1.5 or 10 m, extension cable up to total maximum length of 40 m
Measurement sensor wetted by at least half from the measuring medium: –25 to +55 °C (-13 to 131 °F)
Connection information
Inspection interval
Maintenance requirements
Compliance CE
Warranty 2 years
Sensor side 8-pin, type of protection IP68, PUR
Controller side M12, type of protection IP67
Every 2 years; 1/year service agreement by request, with warranty extension up to 5 years
Clean the measurement window, if necessary. Intervals are dependent on the measuring medium.

1.1 Dimensions

Figure 1 Sensor without and with cleaning unit
1 Sensor without cleaning unit 2 Sensor with cleaning unit
6

Section 2 General information

2.1 Safety information

Please read this entire manual before unpacking, setting up or operating this equipment. Pay attention to all danger and caution statements. Failure to do so could result in serious injury to the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not impaired, do not use or install this equipment in any manner other than that specified in this manual.

2.1.1 Use of hazard information

DANGER
Indicates a potentially or imminently hazardous situation which, if not avoided, will result in death or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation which, if not avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in minor or moderate injury.
Indicates a situation which, if not avoided, may cause damage to the instrument. Information that requires special emphasis.
Note: Information that supplements points in the main text.

2.1.2 Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.
This is the safety alert symbol. Obey all safety messages that follow this symbol to avoid potential injury. If on the instrument, refer to the instruction manual for operation or safety information.
This symbol indicates that a risk of electrical shock and/or electrocution exists.
This symbol shows that a UV lamp is used in the equipment.
Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal systems after 12 August 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of life equipment to the manufacturer for disposal at no charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return end-oflife equipment, producer-supplied electrical accessories, and all auxiliary items for proper disposal.
NOTICE
7
General information

2.2 Product overview

DANGER
This product is not suitable for use in potentially explosive atmospheres.
WARNING
The UV rays from the flash bulb are harmful to eyes and skin. Do not look directly through the measurement window during operation under any circumstances. Remove the measurement sensor from operation before carrying out any maintenance or installation work.
The FP 360 sc sensor is a UV fluorimeter used to continuously measure the concentration of PAH (polycyclic aromatic hydrocarbons) in water. The measurement values can be converted to reflect the total oil content for mineral oils using lab data.
The sensor may need to be installed with additional accessories depending on its area of application.
Area of application Installation with Sensor variants
Open channels, shafts, tanks (solid matter max. 200 mg/L)
Measurement media without solid matter with continuous, low sample throughput
Do not apply the sensor to any hard mechanical effects.

2.3 Measuring principle

The measuring principle is based on the fluorescent properties of PAHs. After excitation caused by UV rays, PAHs emit light with longer wavelengths after a short time delay. The intensity of this light is measured. This measuring principle is considerably more sensitive than absorption and scattered light measurement. It is possible to detect even the slightest trace of PAH contamination in water. PAHs are integral parts of most mineral oil products and are a very specific indicator of oil contamination in water bodies and process water.

2.4 Product components

Each sensor is supplied with
a connector cable with safety sleeve,
a shackle,
a basic user manual and
Chain mount kit Sensor with or without cleaning unit
Flow cell Sensor without cleaning unit
a CD.
The sensor is available in a variety of types (refer to section 7.1 on page 27). Refer to
Figure 2 to make sure that all components have been received. If any of these items are
missing or damaged, contact the manufacturer or a sales representative immediately.
8
General information

2.4.1 FP 360 sc sensor

Figure 2 FP 360 sc sensor
1 FP 360 sc measurement sensor 5 6 mm fitting for cleaning unit (depending on model)
sic user manual with CD 6 Safety sleeve
2 Ba 3 Me 4 Se
asurement window 7 Connector cable
nsor with cleaning unit (depending on model) 8 Shackle

2.5 Function test

CAUTION
Before power is applied, refer to the controller operation instructions.
After the components are removed from the package, do a function test.
1. Con
2. Ap
nect the connector cable to the sensor (8-pin polarized connector) and an
appropriate sc controller (5-pin polarized connector) (refer to section 3.1 on page 11).
ply power to the sc controller. The display is activated and the sensor goes to measurement mode. The sensor ticks quietly and regularly.
9
General information
3. Cover the sensor measurement window with a sheet of white paper (do not use
recycled paper).
4. Vary the distance between the measurement window and the paper. The measurement value on the display will change accordingly.
Note: In air, the measurement value displayed is not exactly zero due to reflections on the window surface (refer to section 4.5.3 on page 21).
10

Section 3Installation

Personal injury hazard. Only qualified personnel should conduct the tasks described in this section of the manual.
If the sensor is not fully inserted, sun protection is recommended in high ambient temperatures and intense solar radiation to protect against thermal and UV effects.

3.1 Connect sensor cable

Always put the cables and hoses in a position that does not bend or cause a trip hazard.
Before power is applied, refer to the controller operation instructions.
1. Connect the polarized socket on the connector cable to the sensor plug (8-pin plug) (refer to Figure 3 step 1).
DANGER
NOTICE
CAUTION
CAUTION
2. Push the
3. Hand-t
ighten the safety sleeve in position (step 3).
Figure 3 Connect the sensor cable to the sensor
safety sleeve on the plug (step 2).
4. Remo
5. Con
Note: Connector cables are available in various lengths (refer to section 7.2 on page 27). Maximum overall cable length is 40 m (131,23 ft).
ve the protective cap on the controller socket and keep it to seal the connector
opening in case the sensor must be removed.
nect the sensor to the controller using the keyed quick-connect fitting.
Hand-tighten (refer to Figure 4).
11
Installation
6
1 2
5
3
4
Figure 4 Connect the sensor to the controller
Figure 5 Pin configuration
Number Description Standard cable, cable color
1 +12 VDC brown 2 Ground black 3 Data (+) blue 4 Data (–) white 5 Screen Screen (gray) 6 Guide
12

3.2 Installation options

The sensor may need to be installed with additional optional accessories depending on the area of application (refer to section 7.3 on page 27).
Note: Refer to the documentation supplied with the accessories for detailed installation instructions.

3.2.1 Installation with the chain mount kit

The FP 360 sc sensor is installed with the chain mount kit in open channels, shafts and tanks.
Installation
Figure 6 FP 360 sc measurement sensor with chain mount kit

3.2.2 Installation of chain mount kit for sensors with cleaning unit

3.2.2.1 Install the cleaning unit hose
Note: An air hose is required, to operate the sensor with the optional cleaning unit. An oil-free compressed air (6 bar) and a solenoid valve or the HOAB compressed air cleaning system is also required (refer to section
With the HOAB compressed air cleaning system, replace the end of the hose connection that is connected to the compressed air on the underside of the instrument with the straight 6 mm fitting (refer to Figure 2 on page 9, item 5) supplied with the probe.
7.3 on page 27).
13
Installation
Figure 7 Install the cleaning unit hose
14
Figure 8 FP 360 sc measurement sensor with cleaning unit and chain mount kit

3.2.3 Installation with flow cell

The FP 360 sc sensor with flow cell is installed for samples free of solids and particulates and limited sample flows.
Installation
Figure 9 Installation with flow cell
15
Installation
16

Section 4 Operation

4.1 User interface and navigation

The sensor can be used with sc controllers from sc100. Refer to the controller documentation for keypad description and navigation information.

4.2 Sensor setup

When the sensor is connected for the first time, the sensor serial number is displayed as the name of the sensor. To change the sensor name:
1. Open the MAIN MENU.
2. Select SENSOR SETUP and confirm.
3. Select the corresponding sensor and confirm.
4. Select CONFIGURE and confirm.
5. Select EDIT NAME and confirm.
6. Edit the name and confirm to return to the SENSOR SETUP menu.
Complete sensor configuration in the same manner, with the following menu options selected:
SET PARAMETER
SELECT UNITS
AVERAGE
LOG SETUP
GAIN VALUE

4.3 Sensor data logger

There is a data log and event log available for each sensor. In the data log, the measurement data are stored at preset intervals; the event log stores events such as configuration changes, alarm messages and warning messages. Both logs can be exported to CSV format (refer to the controller manual).
17
Operation

4.4 Menu structure

4.4.1 SENSOR STATUS

SELECT SENSOR (if there is more than one sensor)
ERROR LIST Possible error messages: SENSOR ERROR
WARNING LIST

4.4.2 SENSOR SETUP

SELECT SENSOR (if there is more than one sensor)
CALIBRATE
SET OUTMODE Behavior of the outputs during calibration and zero point adjustment
HOLD ACTIVE SET TRANSFER
SENSOR MEASURE Current, uncorrected measurement value
CONFIGURE
FACTOR OFFSET 2 POINT 3 POINT 4 POINT 5 POINT
FACTOR
OFFSET
2 POINT
3 POINT
4 POINT
5 POINT
SET CAL DEFLT Security query, reset to (FACTOR=1, OFFSET=0)
Possible warning messages: TEST/MAINT, BULB CHANGE, LAST CONFIGUR, TARGET VALUE
Note: Refer to Section 6 on page 25 for a list of all possible error and warning messages together with a description of all necessary countermeasures to be taken.
FACTOR: 0.1 to 100 OFFSET: –1000 to +1000
Is shown when FACTOR has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
Is shown when OFFSET has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
Is shown when 2 POINT has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
Is shown when 3 POINT has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
Is shown when 4 POINT has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
Is shown when 5 POINT has been selected under CONFIGURE. Refer to section 4.5 on page 20 for detailed information.
18
4.4.2 SENSOR SETUP (Continued)
SELECT SENSOR (if there is more than one sensor)
CONFIGURE
EDIT NAME
SET PARAMETER
SELECT UNITS
AVERAGE
LOG SETUP
GAIN VALUE
SET DEFAULTS
DIAG/TEST
PROBE INFO
SENSOR NAME Device name EDIT NAME SERIAL NUMBER Device serial number RANGE 0 to 500 or 0 to 5000 MODEL NUMBER Item no. Sensor CODE VERSION Sensor software
COUNTER
OPERATING HOURS Operating hours counter MAINTENANCE Counter counting down days BULB CHANGE Counter counting down days
TEST/MAINT
SET OUTMODE Equipment output behavior in the SERVICE menu
HOLD ACTIVE SET TRANSFER
SIGNALS
LAMP CURR Flash lamp intensity
DIAG/TEST Zero point and slope check with external standards
REDADING OFFSET
CUBE CAL
Name can include up to 16 characters, DEFAULT CONFIG: sensor serial number
PAH: Measurement value related to PAH calibration standard OIL: Measurement value related to oil calibration standard DEFAULT CONFIG: PAH
ppb, ppm, μg/L, mg/L, DEFAULT CONFIG: ppb
1 to 300 s, DEFAULT CONFIG: 3 s
5 s, 30 s, 1 min, 2 min, 3 min, 4 min, 5 min, 6 min, 10 min, 15 min, 30 min, DEFAULT CONFIG: 10 min
Range 0 to 500 ppb: AUTO, 0.01 to 50, 0.01 to 500, Range 0 to 5000 ppb: AUTO, 0.01 to 500, 0.01 to 5000
DEFAULT CONFIG: AUTO Security query,
reset to preset configuration for all menu options listed above.
Password-protected access for the service
Operation
19
Operation

4.5 Calibration

4.5.1 Factory calibration

The calibration curve zero point and slope are preset. Retrospective calibration of these basic settings is generally not required outside of the inspection intervals.
Do regular zero point checks to make sure that impurities or faults are being detected (refer to section 4.5.3 on page 21).
If the zero signal increases due to the measuring medium components or the installation conditions, you can compensate for this influence via an offset correction. Carry out a lab analysis of the sample to do this. If there is no PAH/oil contamination in the measuring medium, enter the measurement value shown by the device as the offset (refer to section
4.5.4.2 on page 22).

4.5.2 Process calibration/adjustment

The sensor is pre-calibrated with various concentrations of a special calibration standard in ultra-pure water. These ideal measurement conditions rarely occur in reality. The measurement values shown are qualitative trend indicators if no adjustment is made to the on-site measurement conditions.
If you require quantitatively correct measurement values, either a slope adjustment or a multi-point calibration needs to be carried out. Both of these operations must be carried out on site using lab analysis data. Basic prerequisites for quantitative measurements are precise knowledge about the oil type in occurrence and constant measurement conditions, e.g. in cool water in a heat exchanger. If several oils are present in varying quantities, it is generally not possible to carry out a quantitative measurement.
If the measurement conditions change, you must check the accuracy of the results again through lab analyses and make any adjustments where necessary.
The measurement conditions can change in terms of
Composition of PAH or oil impurities
Distribution of impurities in water
Tem p
Measuring medium composition
Measurement sensor and measurement window
4.5.2.1 Determination of factors and adjustment of slope
To adjust the slope:
1. At the sensor installation site, draw a lab sample of the measuring medium and promptly analyze the sample for PAH and oil content.
2. Make a note of the measurement value shown on the controller at the time of the sample being taken. Make sure the correct unit is shown for the measurement value, e.g. as ppm oil.
3. Repeat steps 1 and 2 several times.
4. Use the sample value and the value shown on the controller at the time of sampling
to calculate a factor.
20
5. Find an average value from the factors.
6. Enter the factor as the slope (refer to section 4.5.4.1 on page 21).
Example for engine oil Example for naphthalene
Lab value: 4.0 ppm oil Measurement value shown Calculated factor: 1.67
1
At the time of sampling
1
: 2.4 ppm oil
Lab value: 420 ppb PAH Measurement value shown1: 120 ppb PAH Calculated factor: 3.5
It is advisable to adjust the slope if the following conditions apply:
Operation
If th
Th
e measuring sample is PAH-/oil free, the measurement value must almost be zero.
e factors calculated from the lab values must enable a sensible average value to be
derived.
If these conditions do not apply, do a multi-point calibration.
Note: If both the zero point and the slope must be changed, use a 2-point calibration (refer to section 4.5.4.3 on page 22).
4.5.2.2 Multi-point calibration
In the event of a multi-point calibration, enter the lab value as the target value and the value shown as the actual value. Make sure that all values are entered in the same unit, e.g. oil in ppm. (refer to section 4.5.4.3 on page 22).

4.5.3 Check the zero point

Medium: ultra-pure water
T
arget value: < 1 ppb. Clean the window in the event of deviations.
Use a glass container (not plastic) large enough to enable the measurement to be taken with an 8 to 10 1000 mL glass beaker). Place a black, non-reflective underlay under the container and switch off artificial lights during the measurement process.
Note: In air, the measurement value displayed is not exactly zero due to reflections on the window surface. This is standard sensor behavior and not an indicator of malfunction.
cm distance between the measurement window and the base (e.g. a
Note: Always use can contain organic compounds.
ultra-pure water. Distilled water and demineralized water are not suitable as these

4.5.4 Adjustment of slope and zero point; multi-point calibration

4.5.4.1 Adjust the slope (FACTOR)
1. Open the MAIN MENU.
2. Select SENSOR SETUP an
3. Sele
4. Select CALIB
5. Select CONFIGURE
6. Sele
7. Enter
8. Go
ct the corresponding sensor and confirm.
RATE and confirm.
and confirm.
ct FACTOR and confirm.
the calculated factor and confirm.
back to the MAIN MENU or the Measurement mode display.
d confirm.
21
Operation
4.5.4.2 Adjust the zero point (OFFSET)
1. Open the MAIN MENU.
2. Select SENSOR SETUP and confirm.
3. Select the corresponding sensor and confirm.
4. Select CALIBRATE and confirm.
5. Select CONFIGURE and confirm.
6. Press OFFSET and confirm.
7. Enter the required offset and confirm.
8. Go back to the MAIN MENU or the Measurement mode display.
4.5.4.3 Multi-point calibration (2 to 5-point calibration)
Note: Multi-point calibration means that the pairs must be input in ascending order.
1. Open the MAIN MENU.
2. Select SENSOR SETUP and confirm.
3. Select the corresponding sensor and confirm.
4. Select CALIBRATE and confirm.
5. Select CONFIGURE and confirm.
6. Select the type of calibration, e.g. 2 POINT and confirm.
7. Select 1PAIR and confirm.
8. Edit the TARGET VALUE and confirm.
9. Edit the ACTUAL VALUE and confirm.
10. Repeat the process for 2PAIR and confirm.
11. Go back to the MAIN MENU or the Measurement mode display.
22

Section 5 Maintenance

The inside of the sensor is maintenance-free.
The cleanliness of the measurement window in the sensor head has an impact on the accuracy of measurements. Check the measurement window at regular intervals to make sure it is clean. The required frequency of these checks is dependent on the measuring medium. Also do a check in the event of unusually high measurement values and clean the measurement window if necessary (refer to section 5.3 on page 24).
For sensors with a cleaning unit, adjust the frequency of cleaning to the measurement conditions. The inspection interval must be shortened to reflect any increase in solid matter.
Individual components of the suspension device (shackle and chain of the chain mount kit) are made of stainless steel and may corrode.

5.1 Maintenance schedule

NOTICE
Interval Maintenance task
Visual inspection System inspection Every 2 years Check plugs and flash bulb. Calibration check Every 2 years Check calibration
1
When operated according to factory settings and appropriate use
Contact the manufacturer's service department every 2 years to arrange sensor inspection, testing, calibration and seal replacement. The flash bulb is also replaced every 4 years.
Application-dependent Check for contamination and corrosion.

5.2 Maintenance for the connectors on the sensor

The 8-pin connector on the sensor is designed for constant usage under water. The connector is lubricated with high-performance grease at the factory and does not require any additional maintenance from the recommended sensor inspection cycles.
To maintain the performance of the connectors:
Protect the neoprene components of the connector against high temperatures and intense solar radiation. If this cannot be avoided, moisten the dried out neoprene components with clean, clear water. Subsequently, loosen the connector.
The pins must always be lightly lubricated. Only apply a very thin film of lubricant. Recommended lubricants are Loctite The lubricant must not come into contact with the measurement window.
8021 as a spray or Molykote 44 Medium.
1
Rinse out grains of sand and solid matter from the cable socket.
To loosen the connector, unscrew the safety sleeve and pull out the plug longitudinally.
Avoid flexing the plug and pulling on the cable.
Do not loosen the connector at ambient temperatures below 0 °C. Heat the neoprene
components carefully to temperatures above 0 °C and then loosen the connector.
Avoid kinks or tight bend in the cables.
23
Maintenance

5.3 Cleaning the measurement windows

Cleaning agents can be hazardous to health. Wear protective equipment and avoid direct contact with cleaning fluids.
Other cleaning agents can damage the material. Damage caused by cleaning carried out incorrectly is not covered by the warranty.
1. Rinse the sensor with fresh water until all attached solid matter has been removed.
2. Use pure acetone and a soft, clean cloth (e.g. camera lens cleaning paper) to
carefully remove the deposits on the measurement window. Avoid sharp objects on the measurement window surface.
3. Rinse the residue from the cleaning agent with fresh water.
CAUTION
NOTICE
24

Section 6 Troubleshooting

6.1 Error messages

Possible sensor errors displayed by the sc controller.
Displayed errors Definition Resolution
SENSOR ERROR Electronic defect Call manufacturer customer service

6.2 Warnings

Possible sensor warning messages displayed by the sc controller.
Displayed warnings Definition Resolution
DIAG/TEST Counter expired Call manufacturer customer service BULB CHANGE Counter expired Call manufacturer customer service
LAST CONFIGUR
TAR GET VAL UE
Changed configuration was not accepted
With multi-point calibration, values not entered in ascending order
Send configuration again
Enter calibration values in ascending order

6.3 Replacement parts

Designation Quantity Service life
Flash bulb 1 4 years O-Rings 4 2 years
25
Troubleshooting
26

Section 7 Replacement parts and accessories

7.1 Sensor options

Description Cat. no.
Range 0 to 50/500 ppb, stainless steel housing, cable length 10 m without cleaning unit LXV441.99.11101 Range 0 to 50/500 ppb, stainless steel housing, cable length 10 m with cleaning unit and fittings
ot in connection with flow cell)
(n Range 0 to 50/500 ppb, stainless steel housing, cable length 1.5 m without cleaning unit LXV441.99.11301 Range 0 to 50/500 ppb, titanium housing, cable length 10 Range 0 to 50/500 ppb, titanium housing, cable length 10 m with cleaning unit and fittings (not
in connection with flow cell) Range 0 to 50/500 ppb, titanium housing, cable length 1.5 m without cleaning unit LXV441.99.12301 Range 0 to 500/5000 ppb, stainless steel housing, cable length 10 m without cleaning unit LXV441.99.21101 Range 0 to 500/5000 ppb, stainless steel housing, cable length 10 m with cleaning unit and
fittings (not in conn Range 0 to 500/5000 ppb, stainless steel housing, cable length 1.5 m without cleaning unit LXV441.99.21301 Range 0 to 500/5000 ppb, titanium housing, cable length 10 m without cleaning unit Range 0 to 500/5000 ppb, titanium housing, cable length 10 m with cleaning unit and fittings
(not in connection with flow cell) Range 0 to 500/5000 ppb, titanium housing, cable length 1.5 m without cleaning unit LXV441.99.22301
ection with flow cell)
m without cleaning unit LXV441.99.12101
LXV441.99.11201
LXV441.99.12201
LXV441.99.21201
LXV441.99.22101
LXV441.99.22201

7.2 Replacement parts

Description Cat. no.
Connector cable 1.5 m LZY623 Connector cable 10 m Shackle, stainless steel 1.4301 LZY668 Gasket and screw set for flow cell Fitting set for flow cell LZY626 Pressure ring and angle bracket for flow cell Chain mount kit instructions DOC273.99.90164 Flow cell instructions DOC273.99.90165
LZY624
LZY625
LZY674

7.3 Accessories

Description Cat. no.
Extension cable (5 m/16.40 ft) LZX848 Extension cable (10 m/32.81 ft) Extension cable (15 m/49.21 ft) LZX850 Extension cable (20 m/65.62 ft) Extension cable (30 m/98.43 ft) LZX852 Flow cell on prefabricated wall including gasket set V4A chain mount kit LZX914.99.11110 HOAB compressed air cleaning system, 230 V HOAB compressed air cleaning system, 115 V, HACH Lange version 6860003.99.0001 Hose for air and measuring medium 5 m, 6/4 mm external/internal diameter Hose for air and measuring medium 10 m, 6/4 mm external/internal diameter LZY620 Hose for air and measuring medium 25 m, 6/4 mm external/internal diameter LZY621
LZX849
LZX851
LZY669
6860103.99.0001
LZY619
27
Replacement parts and accessories
7.3 Accessories (table continued)
Description Cat. no.
Hose for measuring medium 5 m, 8/6 mm external/internal diameter LZY672 Hose for measuring medium 10 m, 8/6 mm external/internal diameter LZY673
28

Section 8 Contact information

HACH Company World Headquarters
P.O. Box 389 Loveland, Colorado 80539-0389 U.S.A. Tel (800) 227-HACH (800) -227-4224 (U.S.A. only) Fax (970) 669-2932 orders@hach.com www.hach.com
HACH LANGE GMBH
Willstätterstraße 11 D-40549 Düsseldorf Tel. +49 (0)2 11 52 88-320 Fax +49 (0)2 11 52 88-210 info@hach-lange.de www.hach-lange.de
HACH LANGE
Rorschacherstrasse 30 a CH-9424 Rheineck Tel. +41 (0)71 886 91 11 Fax +41 (0)71 886 91 66 info@hach-lange.ch www.hach-lange.ch
Repair Service in the United States:
HACH Company Ames Service 100 Dayton Avenue Ames, Iowa 50010 Tel (800) 227-4224 (U.S.A. only) Fax (515) 232-3835
HACH LANGE LTD
Pacific Way Salford GB-Manchester, M50 1DL Tel. +44 (0)161 872 14 87 Fax +44 (0)161 848 73 24 info@hach-lange.co.uk www.hach-lange.co.uk
HACH LANGE FRANCE S.A.S.
8, mail Barthélémy Thimonnier Lognes
F-77437 Marne-La-Vallée cedex 2 Tél. +33 (0)8 20 20 14 14 Fax +33 (0)1 69 67 34 99 info@hach-lange.fr www.hach-lange.fr
Repair Service in Canada:
Hach Sales & Service Canada Ltd. 1313 Border Street, Unit 34 Winnipeg, Manitoba R3H 0X4 Tel (800) 665-7635 (Canada only) Tel (204) 632-5598 Fax (204) 694-5134 canada@hach.com
HACH LANGE LTD
Unit 1, Chestnut Road Western Industrial Estate IRL-Dublin 12 Tel. +353(0)1 46 02 5 22 Fax +353(0)1 4 50 93 37 info@hach-lange.ie www.hach-lange.ie
HACH LANGE SA
Motstraat 54 B-2800 Mechelen Tél. +32 (0)15 42 35 00 Fax +32 (0)15 41 61 20 info@hach-lange.be www.hach-lange.be
Repair Service in Latin America, the Caribbean, the Far East, Indian Subcontinent, Africa, Europe, or the Middle East:
Hach Company World Headquarters, P.O. Box 389 Loveland, Colorado, 80539-0389 U.S.A. Tel +001 (970) 669-3050 Fax +001 (970) 669-2932 intl@hach.com
HACH LANGE GMBH
Hütteldorferstr. 299/Top 6 A-1140 Wien Tel. +43 (0)1 9 12 16 92 Fax +43 (0)1 9 12 16 92-99 info@hach-lange.at www.hach-lange.at
DR. LANGE NEDERLAND B.V.
Laan van Westroijen 2a NL-4003 AZ Tiel Tel. +31(0)344 63 11 30 Fax +31(0)344 63 11 50 info@hach-lange.nl www.hach-lange.nl
HACH LANGE APS
Åkandevej 21 DK-2700 Brønshøj Tel. +45 36 77 29 11 Fax +45 36 77 49 11 info@hach-lange.dk www.hach-lange.dk
HACH LANGE LDA
Av. do Forte nº8 Fracção M P-2790-072 Carnaxide Tel. +351 214 253 420 Fax +351 214 253 429 info@hach-lange.pt www.hach-lange.pt
HACH LANGE KFT.
Vöröskereszt utca. 8-10. H-1222 Budapest XXII. ker.
Tel. +36 (06)1 225 7783 Fax +36 (06)1 225 7784 info@hach-lange.hu www.hach-lange.hu
HACH LANGE AB
Vinthundsvägen 159A SE-128 62 Sköndal Tel. +46 (0)8 7 98 05 00 Fax +46 (0)8 7 98 05 30 info@hach-lange.se www.hach-lange.se
HACH LANGE SP.ZO.O.
ul. Opolska 143 a PL-52-013 Wrocław Tel. +48 (0)71 342 10-83 Fax +48 (0)71 342 10-79 info@hach-lange.pl www.hach-lange.pl
HACH LANGE S.R.L.
Str. Căminului nr. 3 Sector 2 RO-021741 Bucureşti Tel. +40 (0) 21 205 30 03 Fax +40 (0) 21 205 30 17 info@hach-lange.ro www.hach-lange.ro
HACH LANGE S.R.L.
Via Riccione, 14 I-20156 Milano Tel. +39 02 39 23 14-1 Fax +39 02 39 23 14-39 info@hach-lange.it www.hach-lange.it
HACH LANGE S.R.O.
Lešanská 2a/1176 CZ-141 00 Praha 4 Tel. +420 272 12 45 45 Fax +420 272 12 45 46 info@hach-lange.cz www.hach-lange.cz
HACH LANGE
8, Kr. Sarafov str. BG-1164 Sofia Tel. +359 (0)2 963 44 54 Fax +359 (0)2 866 15 26 info@hach-lange.bg www.hach-lange.bg
HACH LANGE S.L.U.
Edif. Arteaga Centrum C/Larrauri, 1C- 2ª Pl. E-48160 Derio/Vizcaya Tel. +34 94 657 33 88 Fax +34 94 657 33 97 info@hach-lange.es www.hach-lange.es
HACH LANGE S.R.O.
Roľnícka 21 SK-831 07 Bratislava – Vaj nory
Tel. +421 (0)2 4820 9091 Fax +421 (0)2 4820 9093 info@hach-lange.sk www.hach-lange.sk
HACH LANGE SU ANALİZ SİSTEMLERİ LTD. ŞTİ.
Hilal Mah. 75. Sokak Arman Plaza No: 9/A TR-06550 Çankaya/ANKARA Tel. +90 (0)312 440 98 98 Fax +90 (0)312 442 11 01 bilgi@hach-lange.com.tr www.hach-lange.com.tr
29
Contact information
HACH LANGE D.O.O.
Fajfarjeva 15 SI-1230 Domžale Tel. +386 (0)59 051 000 Fax +386 (0)59 051 010 info@hach-lange.si www.hach-lange.si
HACH LANGE MAROC SARLAU
Villa 14 – Rue 2 Casa Plaisance Quartier Racine Extension MA-Casablanca 20000 Tél. +212 (0)522 97 95 75 Fax +212 (0)522 36 89 34 info-maroc@hach-lange.com www.hach-lange.ma
ΗΑCH LANGE E.Π.Ε.
Αυλίδος 27 GR-115 27 Αθήνα Τηλ . +30 210 7777038 Fax +30 210 7777976 info@hach-lange.gr www.hach-lange.gr
HACH LANGE E.P.E.
27, Avlidos str GR-115 27 Athens Tel. +30 210 7777038 Fax +30 210 7777976 info@hach-lange.gr www.hach-lange.gr
HACH LANGE D.O.O.
Ivana Severa bb 42 000 Varaždin Tel. +385 (0) 42 305 086 Fax +385 (0) 42 305 087 info@hach-lange.hr www.hach-lange.hr
30

Section 9 Warranty and Liability

The manufacturer warrants that the product supplied is free of material and manufacturing defects and undertakes the obligation to repair or replace any defective parts at zero cost.
The warranty runs for 24 months. If a maintenance contract is taken out within 6 months of purchase, the warranty period is extended to 60 months.
With the exclusion of the further claims, the supplier is liable for defects including the lack of assured properties as follows: all those parts that, within the warranty period calculated from the day of the transfer of risk, can be demonstrated to have become unusable or that can only be used with significant limitations due to a situation present prior to the transfer of risk, in particular due to incorrect design, poor materials or inadequate finish will be improved or replaced, at the supplier's discretion. The identification of such defects must be reported to the supplier in writing without delay, but no later than 7 days after the identification of the fault. If the customer fails to notify the supplier, the product is considered approved despite the defect. Further liability for any direct or indirect damages is not accepted.
If instrument-specific maintenance and servicing work defined by the supplier is to be performed within the warranty period by the customer (maintenance) or by the supplier (servicing) and these requirements are not met, claims for damages due to the failure to comply with the requirements are rendered void.
Any further claims, in particular claims for consequential damages cannot be made.
Consumables and damage caused by improper handling, poor installation or incorrect use are excluded from this clause.
The process instruments of the manufacturer are of proven reliability in many applications and are therefore often used in automatic control loops to provide the most economical possible operation of the related process.
To avoid or limit consequential damage, it is therefore recommended to design the control loop such that a malfunction in an instrument results in an automatic change over to the backup control system. This establishes the most secure operating condition for the environment and for the process.
31
Warranty and Liability
32

Appendix A Modbus register

Table 1 Sensor Modbus registers
Register# Data type Length R/W Description
40001 Unsigned integer 1 R Reserved 40002 Float 2 R Measurement value as PAH, unit PPB 40004 Float 2 R Measurement value as PAH, unit PPM 40006 Float 2 R Measurement value as OIL, unit PPB 40008 Float 2 R Measurement value as OIL, unit PPM 40016 String 6 R Serial number 40022 String 8 R/W Name of location 40030 Unsigned integer 1 R/W Choose the parameter, 47=PAH, 48=OIL
40031 Unsigned integer 1 R/W
40040 Float 2 R/W Offset for calibration 40042 Float 2 R/W Factor for calibration 40050 Unsigned integer 1 R/W Logging interval from 5 sec to 1800 sec 40051 Unsigned integer 1 R/W Measuring interval from 1 sec to 300 sec
40052 Unsigned integer 1 R/W
40055 Unsigned integer 1 R/W Set output mode for calibration 40056 Unsigned integer 1 R/W Set output mode for service 40057 Float 2 R Version of application file 40059 Float 2 R The entry is for the application file 40061 Float 2 R Version of the probe 40063 Unsigned integer 1 R The entry is for the device driver file 40064 Unsigned integer 1 R The entry is for the device driver file 40065 Unsigned integer 1 R The entry is for the device driver file
40066 Integer 1
40067 Integer 1 R
40068 Unsigned integer 2 R Operating hours of analyzer
R
Measurement units 38=ppb, 39= g/L, 2=ppm, 0=mg/L
Amplification for the low/high range probe,
AUTO,
0= 1= 0.01 to 50/500 PPB, 2= 0.01 to 500/5000 PPB
Days left until exchanging lamp, negative values show that exchange is overdue
Days left until maintenance, negative values show that service is overdue
33
Modbus register
34
Index
A
Areas of application ................................................... 8
C
Calibration .................................................................. 5
Chain mount kit ........................................................ 13
D
Data logger .............................................................. 17
Dimensions ................................................................ 6
E
Error messages ........................................................ 25
F
Flow cell ................................................................... 15
Function test .............................................................. 9
I
Inspection interval ...................................................... 6
Measurement accuracy .............................................. 5
Measuring method ..................................................... 5
Measuring principle .................................................... 8
Measuring range ........................................................ 5
Modbus register ....................................................... 33
P
Precautionary labels ................................................... 7
Pressure range ........................................................... 5
Product contents ........................................................ 8
R
Reproducibility ............................................................ 5
Response time ........................................................... 5
S
Safety information ...................................................... 7
Safety sleeve ............................................................ 11
Specifications ............................................................. 5
System configuration ................................................ 17
M
Maintenance schedule ............................................. 23
W
Warnings .................................................................. 25
Wearing parts ........................................................... 25
35
Index
36
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