Hach-Lange DR 5000 User Manual
DOC022.52.00654
DR 5000
USER MANUAL
January 2008, Edition 3
© Hach-Lange GmbH, 2007–2008. All rights reserved. Printed in Germany.
2
Table of Contents
Section 1 Specifications ........................................................................................................................................ 7
Section 2 General Information .............................................................................................................................. 9
2.1 Safety information .............................................................................................................................................. 9
2.1.1 Use of hazard information ......................................................................................................................... 9
2.1.2 Precautionary labels ................................................................................................................................. 9
2.1.3 Class 1 LASER ....................................................................................................................................... 10
2.1.4 Chemical and Biological Safety .............................................................................................................. 10
2.1.5 Source Lamp Safety ............................................................................................................................... 10
2.2 Overview of product ......................................................................................................................................... 11
Section 3 Installation ........................................................................................................................................... 13
3.1 Unpack the instrument ..................................................................................................................................... 13
3.2 Operating environment .................................................................................................................................... 13
3.3 Connection ....................................................................................................................................................... 14
3.4 Cell compartment, Multi Cell Holder, 100 mm Cell Adapter (optional) ............................................................. 15
3.4.1 100 mm adapter (optional) ...................................................................................................................... 16
3.4.2 Installation Multi Cell Holder ................................................................................................................... 17
3.5 Beam path ........................................................................................................................................................ 18
Section 4 Start Up ................................................................................................................................................ 19
4.1 Power the instrument on and off ...................................................................................................................... 19
4.2 Language selection .......................................................................................................................................... 19
4.3 Self-Check ....................................................................................................................................................... 19
Section 5 Standard Operations ........................................................................................................................... 21
5.1 Overview .......................................................................................................................................................... 21
5.1.1 Tips for the use of the touch screen ........................................................................................................ 21
5.1.2 Use of the alphanumeric keypad ............................................................................................................ 21
5.1.3 Main Menu .............................................................................................................................................. 22
5.2 Instrument Setup mode .................................................................................................................................... 23
5.2.1 Operator ID ............................................................................................................................................. 23
5.2.2 Sample ID ............................................................................................................................................... 24
5.2.3 Date and time .......................................................................................................................................... 25
5.2.4 Display and sound preferences .............................................................................................................. 25
5.2.5 Lamp Control .......................................................................................................................................... 26
5.2.5.1 VIS-Lamp and UV-Lamp ............................................................................................................. 26
5.2.5.2 Effect caused by the lamp settings on the Measuring Mode ...................................................... 27
5.2.6 PC and printer ......................................................................................................................................... 29
5.2.6.1 Printer setup ............................................................................................................................... 29
5.2.6.2 Print data .................................................................................................................................... 31
5.2.6.3 HACH Data Trans ....................................................................................................................... 31
5.2.7 Password ................................................................................................................................................ 32
5.2.7.1 Password deactivation ................................................................................................................ 33
5.3 Store, recall, send and delete data .................................................................................................................. 35
5.3.1 The Data Log .......................................................................................................................................... 35
5.3.1.1 Auto/manual data storage ........................................................................................................... 35
5.3.1.2 Recall stored data from the data log ........................................................................................... 35
5.3.1.3 Send data from the data log ...........................................................................................
5.3.1.4 Delete stored data from the data log .......................................................................................... 37
5.3.2 Store, recall, send and delete data from wavelength scan and time course ........................................... 38
5.3.2.1 Data storage from wavelength scan or time course ................................................................... 38
5.3.2.2 Recall stored data from wavelength scan or time course ........................................................... 38
5.3.2.3 Send data from wavelength scan or time course ........................................................................ 39
5.3.2.4 Delete stored data from wavelength scan or time course ........................................................... 41
............ 36
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Table of Contents
5.4 Stored Programs .............................................................................................................................................. 42
5.4.1 Select a saved test/method; enter user-specific basic data .................................................................... 42
5.4.2 Stored program options .......................................................................................................................... 42
5.4.3 Use of program timers ............................................................................................................................ 44
5.4.4 Set the reading mode .............................................................................................................................. 44
5.4.4.1 Take single wavelength measurements (single reading) ............................................................ 45
5.4.4.2 Take single wavelength measurements (continuous readings) .................................................. 45
5.4.5 Set the dilution factor .............................................................................................................................. 46
5.4.6 Run a standard adjust ............................................................................................................................. 46
5.4.7 Set the chemical form ............................................................................................................................. 47
5.4.7.1 Change of the default setting of the chemical form .................................................................... 48
5.4.8 Run a reagent blank ................................................................................................................................ 48
5.4.9 Analysis of samples ................................................................................................................................ 49
5.4.10 Update/edit tests ................................................................................................................................... 50
5.4.10.1 Manual update of test data ....................................................................................................... 50
5.4.10.2 Program a new test ................................................................................................................... 51
5.4.11 Add stored programs to the favorite programs list ................................................................................ 51
5.5 Barcode Programs ........................................................................................................................................... 52
5.5.1 Complete a barcode 13 mm test/vial ...................................................................................................... 53
5.5.2 Select the measuring range .................................................................................................................... 53
5.5.3 Select the chemical evaluation form ....................................................................................................... 53
5.5.3.1 Change of the default setting of the chemical form .................................................................... 54
5.5.4 Basic test-specific and sample-specific data settings ............................................................................. 54
5.5.5 Sample blank .......................................................................................................................................... 55
5.5.6 Update/edit barcode tests ....................................................................................................................... 56
5.5.6.1 Manual update of a barcode test ................................................................................................ 56
5.5.6.2 Update an existing barcode test ................................................................................................. 59
5.5.6.3 Program a new test ..................................................................................................................... 60
5.5.7 Upgrade of the instrument software ........................................................................................................ 60
5.5.8 Program an own barcode-readable application with LCW 906 ............................................................... 61
5.5.8.1 Evaluation of barcode-readable application with LCW 906 ........................................................ 61
5.5.8.2 Edit/delete of barcode-readable application ............................................................................... 62
Section 6 Advanced Operations ......................................................................................................................... 65
6.1 User Programs ................................................................................................................................................. 65
6.1.1 Program a user method .......................................................................................................................... 65
6.1.1.1 Single wavelength settings ......................................................................................................... 67
6.1.1.2 Multi wavelength settings ............................................................................................................ 68
6.1.1.3 Calibration settings for single and multi wavelength mode ......................................................... 70
6.1.1.4 Store a user program .................................................................................................................. 74
6.1.1.5 Additional user-defined parameters and functions ..................................................................... 74
6.1.2 Free programming program type ............................................................................................................ 76
6.1.2.1 Measurement process ................................................................................................................ 76
6.1.2.2 Enter a new element of a measuring sequence ......................................................................... 77
6.1.2.3 Enter the calibration formula (evaluation formula) ...................................................................... 79
6.1.2.4 Enter variables ............................................................................................................................ 82
6.1.2.5 Save a free programming user program ..................................................................................... 82
6.1.3 Select a user program ............................................................................................................................. 82
6.1.4 Add, edit and delete user programs from the favorites list ...................................................................... 83
6.1.4.1 Add to Favorites .......................................................................................................................... 83
6.1.4.2 Edit .............................................................................................................................................. 84
6.1.4.3 Delete ......................................................................................................................................... 84
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Table of Contents
6.2 Favorite Programs ........................................................................................................................................... 85
6.2.1 Recall a favorite program ........................................................................................................................ 85
6.2.2 Delete a favorite program ....................................................................................................................... 85
6.3 Standard Addition – monitoring/checking results ............................................................................................. 86
6.3.1 Complete a standard addition ................................................................................................................. 87
6.4 Single Wavelength (absorbance, concentration and transmittance measurements) ....................................... 91
6.4.1 Set up single wavelength mode .............................................................................................................. 91
6.4.2 Take single wavelength measurements (single reading) ........................................................................ 93
6.4.3 Take single wavelength measurements (continuous readings) .............................................................. 93
6.5 Multi-Wavelength mode – measurements at more than one wavelength ........................................................ 94
6.5.1 Set the reading mode at different wavelengths ....................................................................................... 94
6.5.2 Complete a measurement in the multi wavelength mode ....................................................................... 97
6.6 Wavelength Scan mode – recording of absorbance and transmittance spectrums ......................................... 98
6.6.1 Set up the wavelength scan .................................................................................................................... 98
6.6.2 Wavelength scan reading ..................................................................................................................... 101
6.6.2.1 Navigation of the wavelength scan graph or a wavelength scan analysis ................................ 102
6.6.3 Work with reference scans .................................................................................................................... 103
6.7 Time course of absorbance/transmittance ..................................................................................................... 105
6.7.1 Time course setup parameters ............................................................................................................. 105
6.7.2 Time course scan reading ..................................................................................................................... 106
6.7.3 Analysis of time course data ................................................................................................................. 107
6.7.3.1 Navigation of a time scan or a time scan analysis .................................................................... 108
6.8 System checks ............................................................................................................................................... 109
6.8.1 Instrument information .......................................................................................................................... 109
6.8.2 Upgrade of the instrument software ...................................................................................................... 110
6.8.3 Optical checks ....................................................................................................................................... 110
6.8.3.1 Wavelength check .................................................................................................................... 111
6.8.3.2 Noise check .............................................................................................................................. 112
6.8.3.3 Stray light check ....................................................................................................................... 114
6.8.3.4 Absorbance check .................................................................................................................... 115
6.8.3.5 Drift check ................................................................................................................................. 116
6.8.3.6 Verification kit ........................................................................................................................... 117
6.8.4 Output checks ....................................................................................................................................... 119
6.8.5 Lamp history ......................................................................................................................................... 119
6.8.6 Factory service ...................................................................................................................................... 120
6.8.7 Service time .......................................................................................................................................... 120
6.8.8 Instrument Backup ................................................................................................................................ 121
Section 7 Maintenance ...................................................................................................................................... 125
7.1 Cleaning requirements ................................................................................................................................... 125
7.1.1 Spectrophotometer .......................................................................................................
7.1.2 Display .................................................................................................................................................. 125
7.1.3 Cuvettes/sample cells ........................................................................................................................... 125
7.2 Lamp replacement ......................................................................................................................................... 126
7.2.1 Tungsten lamp replacement ................................................................................................................. 126
7.2.2 Deuterium lamp (UV) replacement ....................................................................................................... 127
7.3 Fuse replacement .......................................................................................................................................... 128
7.4 Filter pad maintenance .................................................................................................................................. 129
7.4.1 Filter pad replacement .......................................................................................................................... 129
........................ 125
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Table of Contents
Section 8 Troubleshooting ................................................................................................................................ 131
Section 9 Replacement Parts ............................................................................................................................ 133
Section 10 Contact Information ........................................................................................................................ 135
Section 11 Warranty, liability and complaints ................................................................................................. 137
Index .................................................................................................................................................................... 139
6
Section 1 Specifications
Specifications are subject to change without notice.
Performance specifications
Operating mode Transmittance (%), Absorbance and Concentration
Source lamp Gas-filled Tungsten (visible) and Deuterium (UV)
Wavelength range 190–1100 nm
Wavelength accuracy ± 1 nm in Wavelength Range 200–900 nm
Wavelength reproducibility < 0.1 nm
Wavelength resolution 0.1 nm
Wavelength calibration Automatic
Wavelength selection Automatic, based on method selection
Scanning speed 900 nm/min 1 nm steps
Spectral bandwidth 2 nm
Photometric range ± 3.0 Abs in Wavelength Range 200–900 nm
Photometric accuracy
Photometric linearity
Stray light
Data storage 1000 measured values (result, date, time, sample ID, user ID)
5 mAbs at 0.0–0.5 Abs
1% at 0.50–2.0 Abs
< 0.5%–2 Abs
< = 1% at > 2 Abs
with neutral glass at 546 nm
KI-solution at 220 nm
> 3.3 Abs / < 0.05%
User programs 50
Physical and environmental specifications
Width 450 mm (17.7 in)
Height 200 mm (7.9 in)
Depth 500 mm (19.7 in)
Weight 15.5 kg (34.2 Ibs)
Operating requirements 10–40 °C (50–104 °F), max. 80% relative humidity (non-condensing)
Storage requirements –25–60 °C (–13–140 °F) max. 80% relative humidity (non-condensing)
Additional technical data
Mains connection 100–240 V~; 50/60 Hz; automatic changeover
Use only shielded cable with max. length of 3 m.
Interfaces
Water-resistant to
Enclosure
Safety class Safety class I
1 x USB type B
2 x USB type A
IP 31
7
Specifications
8
Section 2 General Information
2.1 Safety information
Please read this entire manual before unpacking, setting up or
operating this equipment. Pay attention to all danger, warning and
caution statements. Failure to do so could result in serious injury to
the operator or damage to the equipment.
Make sure that the protection provided by this equipment is not
impaired, do not use or install this equipment in any manner other
than that specified in this manual.
2.1.1 Use of hazard information
DANGER
Indicates a potentially or imminently hazardous situation
which, if not avoided, will result in death or serious injury.
WARNING
Indicates a potentially or imminently hazardous situation
which, if not avoided, could result in death or serious injury.
CAUTION
Indicates a potentially hazardous situation that may result in
minor or moderate injury.
2.1.2 Precautionary labels
This symbol, if noted on the instrument, references the instruction manual for operation and/or safety information.
This symbol, if noted on the instrument, indicates a hot surface.
Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after
12 August of 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC),
European electrical equipment users must now return old or end-of life equipment to the Producer for disposal at no
charge to the user.
Note: For return for recycling, please contact the equipment producer or supplier for instructions on how to return
end-of-life equipment, producer-supplied electrical accessories and all auxiliary items for proper disposal.
Important Note: Indicates a situation which, if not avoided, may
cause damage to the instrument. Information that requires special
emphasis.
Note: Information that supplements points in the main text.
Read all labels and tags attached to the instrument. Personal injury
or damage to the instrument could occur if not observed. A symbol,
if noted on the instrument, will be included with a danger or caution
statement in the manual.
LASER CLASS 1
This symbol indicates that the instrument contains a Class 1 LASER device.
Data: 0.3 mW; λ = 650 nm
9
General Information
2.1.3 Class 1 LASER
2.1.4 Chemical and Biological Safety
A Class 1 LASER is installed in this instrument. Class 1 LASERS
are products where the radiant power of the LASER beam
accessible (the accessible emission) is always below the Maximum
Permissible Exposure value. Therefore, for Class 1 LASERS the
output power is below the level at which it is believed eye damage
will occur. Exposure to the beam of a Class 1 LASER will not result
in eye injury. Class 1 LASERS may therefore be considered safe.
However, Class 1 LASER products may contain LASER systems of
a higher Class but there are adequate engineering control
measures to ensure that access to the beam is not reasonably
likely. Examples of such products include LASER printers and
compact disc players. CDRH assession number 0510555-02.
Data: 0.3 mW; wavelength = 650 nm
DANGER
Potential Chemical/ Biological Exposure Hazards. Handling
chemical samples, standards and reagents can be dangerous.
Users of this product are advised to familiarize themselves
with safety procedures and the correct use of chemicals, and
to carefully read all relevant Material Safety Data Sheets.
2.1.5 Source Lamp Safety
Normal operation of this instrument may involve the use of
hazardous chemicals or biologically harmful samples.
• The user must observe all cautionary information printed on the
original solution containers and safety data sheet prior to their
use.
• All waste solutions must be disposed in accordance with local
and national law.
• The type of protective equipment must be selected according to
the concentration and amount of the dangerous substance at
the specific workplace.
The source lamp operate at high temperatures.
• To avoid a possible electric shock, disconnect the instrument
from the power source before servicing the lamp. Make sure
that the instrument cannot be accidentally switched on again.
CAUTION
The UV lamp generates UV light.
Do not look directly at an operating lamp without wearing UV
protective eye glasses.
10
Important Note: To prevent a possible burn, allow the lamp to cool
at least 30 minutes before handling.
2.2 Overview of product
General Information
The DR 5000 Spectrophotometer is a complete scanning UV/VIS
spectrophotometer with a wavelength range of 190 to 1100 nm. The
instrument comes with a complete set of application programs and
multi-language support.
The DR 5000 Spectrophotometer contains the following application
modes: Stored Programs, User Programs, Favorite Programs,
Single Wavelength Mode, Multi-Wavelength Mode, Wavelength
Scanning Mode and Time Course Mode.
The DR 5000 is used for testing in visible and ultraviolet
wavelengths. A gas-filled tungsten lamp produces light in the visible
spectrum (320 to 1100 nm), and a deuterium lamp available
produces light in the ultraviolet spectrum (190 to 360 nm).
The DR 5000 Spectrophotometer provides digital readouts in direct
concentration units, absorbance, or percent transmittance.
When a user-generated or programmed method is selected, the
on-screen menus and prompts direct the user through the test.
This menu system also can be used to generate reports, statistical
evaluations of generated calibration curves, and to report
instrument diagnostic checks.
11
General Information
12
Section 3 Installation
3.1 Unpack the instrument
3.2 Operating environment
WARNING
Electrical and Fire Hazards. Use only the provided power
supply. Only qualified personnel should conduct the tasks
described in this section of the manual.
The DR 5000 Spectrophotometer comes packaged with the
following items:
• DR 5000 Spectrophotometer
• Mains power cable
• Multi Cell Holder
• DR 5000 User Manual
• CD-ROM containing the HACH and HACH LANGE procedures
Note: If any of these items are missing or damaged, contact the
manufacturer or a sales representative immediatly.
The following conditions are necessary to ensure correct
instrument operation and accurate results:
• Place the instrument firmly on an even surface. Do not push
any objects under the instrument.
• Maintain an ambient temperature of 10 to 40 ºC (50 to 104 ºF)
for proper instrument operation.
• The relative humidity should be less than 80%; moisture should
not condense on the instrument.
• Leave at least a 15 cm (6 in.) clearance at the top and on all
sides for air circulation to avoid overheating of electrical parts.
• Do not operate or store the instrument in extremely dusty,
damp or wet locations.
• Keep the surface of the instrument, the cell compartment and
all accessories clean and dry at all times. Splashes or spills on
and in the instrument should be cleaned up immediately (see
section 7.1 on page 125).
Important Note: Protect the instrument from temperature
extremes, including heaters, direct sunlight and other heat sources.
13
Installation
3.3 Connection
The DR 5000 has three USB interfaces as a standard feature,
located on the back of the instrument (Figure 1).
The USB Type A interfaces are used for communications with a
printer, USB memory stick or keyboard. A USB memory stick is
used to update instrument software.
The USB Type B interface is used for communications with a PC.
The optional Hach Data Trans software (see section 5.2.6.3 on
page 31) must be installed on the PC for this use.
A USB hub may be used to connect several accessories at a time.
Note: USB cables must not be longer than 3 meters (10 feet).
These USB interfaces enable data and graphics to be output to a
Printer and a PC and upgrade of instrument software (see
section 6.8.2 on page 110).
Figure 1 Interfaces
1 USB type A 4 Fuse
2 USB type B 5 Plug in power supply
3 On/Off switch
14
Installation
3.4 Cell compartment, Multi Cell Holder, 100 mm Cell Adapter (optional)
Figure 2 Cell compartment
1 Cell compartment 2 Cell compartment for 13 mm round cuvettes/vials only
The DR 5000 Spectrophotometer comes equipped with a Multi Cell
Holder (Figure 3 on page 16) which is the Standard Holder,
provided with each instrument. The Multi Cell Holder can
accommodate the following cell types:
• 10 mm square cells
• 20/50 mm rectangular cells
• 1“ round cells
• 1“ square cells
Only one cell type can be used for a measurement. On the top and
bottom of the Multi Cell Holder are a variety of openings to
accommodate different types of cells. Beside each opening is
printed the type of cell for which it is intended.
Optionally there is a 100 mm adapter available.
15
Installation
Figure 3 Multi Cell Holder (Top and Bottom)
1 10 mm square cell 4 1“ round cell
2 20 mm rectangular cell 5 1“ square cell
3 50 mm rectangular cell
3.4.1 100 mm adapter (optional)
1 100 mm rectangular cell
Figure 4 100 mm Cell Adapter
16
3.4.2 Installation Multi Cell Holder
Installation
Assembly of the Multi Cell Holder:
1. Open the cell compartment.
2. Identify the correct opening for the selected cell type in the
Multi Cell Holder.
3. Insert the Multi Cell Holder in the cell compartment in such a
way that the name of the selected cell type can be read directly
and the cell opening is at the front. Secure the holder with two
locking screws (Figure 5).
Figure 5 Installation Multi Cell Holder
17
Installation
3.5 Beam path
Figure 6 shows the beam path of the DR 5000:
Figure 6 Beam path
1 Deuterium lamp 10 Exit slit
2 Lamp selection mirror 11 Cell compartment
3 Tungsten lamp 12 Lens
4 Mirror 13 Round cuvette/vial compartment
5 Grating 14 Measurement element
6 Reference element 15 Monochromator
7 Mirror 16 Mirror
8 Splitter mirror 17 Mirror
9 Filter 18 Entrance slit
18
Section 4 Start Up
4.1 Power the instrument on and off
1. Plug in power supply.
2. Close the empty cell compartment.
3. Turn the instrument on by pressing the power switch on the
back.
Note: Do not turn the instrument off and on in rapid succession. Always
wait about 20 seconds before turning the instrument on again, otherwise
the electronic and mechanical systems will be damaged.
4.2 Language selection
The spectrophotometer software includes several language
options. The first time the instrument is turned on, the language
selection screen will appear.
1. Select the desired language.
4.3 Self-Check
2. Press OK to confirm the language selection. The self check will
start automatically.
Changing the language setting
The instrument functions in the selected language until the option is
changed.
1. While turning the instrument on, touch the screen at any point
until the list for selecting a language appears (about
30 seconds).
2. Select the required language.
3. Press OK to confirm. The test program subsequently starts
automatically.
Each time the instrument is powered up, a series of diagnostic tests
are performed automatically to ensure operation of major system
components.
This procedure, which takes approximately two minutes, checks the
system, lamp, filter adjustment, wavelength calibration and voltage.
Each test which functions correctly is confirmed with a check mark.
The Main Menu is displayed when power up diagnostics are
completed.
Note: Further error messages during self check, see Section 8 on page
131.
19
Start Up
20
Section 5 Standard Operations
5.1 Overview
5.1.1 Tips for the use of the touch screen
The entire screen is touch-activated. To make a selection, press the
screen with a fingernail, fingertip, pencil eraser or a stylus. Do not
press the screen with a sharp object, such as the tip of a ball
point pen.
• Do not place anything on top of the screen, to prevent damage
or scratching on the screen.
• Press keys, words or icons to select them.
• Use scroll bars to move up and down long lists very quickly.
Press and hold the scroll bar, then move up or down to move
through the list.
• Highlight an item from a list by pressing it once. When the item
has been successfully selected, it will be displayed as reversed
text (light text on a dark background).
5.1.2 Use of the alphanumeric keypad
This display is used to enter letters, numbers and symbols as
needed when programming the instrument. Unavailable options are
disabled (grayed out). The icons on the right and left of the screen
are described in Table 1.
The central keypad changes to reflect the chosen entry mode.
Press a key repeatedly until the desired character appears on the
screen. A space can be entered by using the underscore on the
YZ_ key.
Note: A USB keyboard (with US keyboard layout) or a USB Barcode
handset scanner can be used for input (see Section 9 on page 133).
Table 1 Alphanumeric keypad
Icon / key Description Function
ABC/abc Alphabetic
# % Symbols Punctuation, symbols and numerical sub- and superscripts may be entered.
123 Numeric For entering regular numbers.
CE Clear Entry Clear the entry.
Left Arrow Backspace
Right Arrow Advance
When entering alphabetic characters (ex. user-entered units), this key allows to
toggle between upper and lower case letters.
Moves back one position. This deletes the character previously entered in the new
position.
Moves to the next space in an entry when two adjacent characters occur on the
same key.
21
Standard Operations
5.1.3 Main Menu
Option Function
Stored programs are pre-programmed methods that make use of HACH reagents and LANGE
Stored Programs (HACH
LANGE Programs)
User Programs
cuvette tests and pipette tests.
The DR 5000 Procedures Manual contains illustrated, step-by-step procedures for analyses
using HACH programs. The working procedures for LANGE tests are included in the test packs.
User programs make "made to measure analysis" possible:
–Users can program methods they have developed themselves
–Existing HACH and LANGE methods can be stored as user programs. The LANGE tests can
then be modified to suit the user's requirements.
A variety of modes may be selected from the Main Menu. The
following table briefly describes each menu option.
Table 2 Main Menu options
Favorite Programs List of methods/tests created by the user to suit his own requirements.
Single wavelength measurements are:
Absorbance measurements: The light absorbed by the sample is measured in absorbance
units.
Single Wavelength
Multi Wavelength
Wavelength Scan
Time Course The time scan records the absorbance or % transmittance at a wavelength over a defined time.
System Checks
Recall Data Stored data can be recalled, filtered, sent and deleted.
Instrument Setup
Transmittance measurements (%): The percentage of the light that passes through the sample
and reaches the detector is measured.
Concentration measurements: A concentration factor can be entered to enable the measured
absorbance values to be converted into concentration values.
In the multi-wavelength mode, absorbance (Abs) or percentage transmittance (%T) is measured
at up to four wavelengths and absorbance differences and absorbance relationships are
calculated. Simple conversions into concentrations can also be carried out.
A wavelength scan shows how the light from a sample is absorbed over a defined wavelength
spectrum.This function can be used to determine the wavelength at which the maximum
absorbance value can be measured.The absorbance behavior is displayed graphically during the
scan.
The system checks menu offers a number of options, including optical checks, output checks,
lamp history, instrument update, service time and instrument backup.
In this mode, user-specific or method-specific settings can be entered: Operator-ID, Sample-ID,
Date & Time, Display & Sound, Lamp Control, PC & Printer, Password,
and Module Options.
22
5.2 Instrument Setup mode
Standard Operations
1. Select Instrument Setup in the Main Menu.
A selection of functions appears in order to configure the functions
of the instrument.
This display appears when the multi-cell holder is installed or the
13 mm round cuvette/vial compartment is used. If the imstrument
recognizes a Sipper module or a Peltier module the Carousel
Options key is replaced by Sipper Options or Peltier Options.
Optional modules for the DR5000:
• Carousel Holder (Sample Changer)
• Pour-Thru Cell module
• Sipper module
• Peltier module (Temperature control module)
Refer to the corresponding manuals/instruction sheets for more
information.
5.2.1 Operator ID
Use this option to enter up to 30 sets of operator initials (up to
5 characters each) into the instrument. This feature helps record
which operator measured each sample.
1. Press Operator ID in the Instrument Setup.
2. Press New to enter a new Operator ID.
3. Use the alphanumeric keypad to enter a new Operator ID.
4. Press OK to confirm.
5. The display shows the chosen Operator ID.
6. Press OK. The instrument will return to the Instrument Setup
screen and show the selected operator identifier.
7. The chosen Operator ID is activated.
Note: Press Delete to remove an Operator ID from the list.
Note: Alternatively, enter or change an Operator ID in measurement mode.
In the results screen, press Options>More>Instrument Setup or if an
Operator ID is already assigned, select the "Operator ID symbol
immediately in the results screen.
23
Standard Operations
5.2.2 Sample ID
Use this option to enter up to 30 Sample Identification tags (up to
13 characters each) into the instrument. Sample IDs can be used to
specify the sample location or other sample specific information.
1. Press Sample ID in the Instrument Setup.
2. Press New to enter a new Sample ID.
3. Use the alphanumeric keypad to enter a new Sample ID.
Note: If a USB Barcode handset scanner ( see Section 9 on page 133)
is connected, Sample IDs can also be scanned.
4. Press OK to confirm.
5. To number the Sample IDs sequentially (e.g. Inflow (01 etc.)),
select Add Number.
• Use the arrow keys to specify the first number of the
sequence.
• Use the key between the arrow keys to enter the first
number of the sequence using the alphanumeric keypad.
6. Press OK to return to "Instrument Setup".
24
7. The Sample ID is activated. Each Sample ID is automatically
numbered in ascending order after a measurement. The
number is shown in parentheses behind the Sample ID.
Note: To remove a Sample ID, highlight the ID and press Delete.
Standard Operations
There are two ways to enter or change a Sample ID in the
Measurement Mode:
Option 1
In the result display, press Options>More>Instrument Setup
Sample ID is already assigned, select the Sample ID symbol in the
result display.
Option 2
With an USB keyboard (with US keyboard layout) or a scanner a
Sample ID can be directly entered in the result display.
Note: This sample ID will not be added to the list
. If a
5.2.3 Date and time
1. Press Date & Time in the Instrument Setup.
2. The date and time are subdivided over a number of fields.
3. Press OK to confirm. The instrument will return to
5.2.4 Display and sound preferences
1. Press Display & Sound in the Instrument Setup.
The following options will be displayed:
• Display Contrast—Adjusts the display brightness to suit
Press the appropriate field and use the arrow keys to change
the value.
Instrument Setup.
lighting conditions.
• Screen touch—Activates//Deactivates a short beep each time
the screen is pressed (Default:off).
• Reading done—Activates/Deactivates a sound when a
reading is complete (Default: short beep every time a reading is
complete).
•Timer—Adjusts the length of the timer sound. Select Short or
Long. Long beeps are recommended for noisy environments.
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Standard Operations
5.2.5 Lamp Control
2. Select Long to change the number of audio signals.
Use the alphanumeric keypad to enter/specify the number of
audio signals (4–25).
Note: A high number of audio signals increases the duration of the
tones and a small number of audio signals reduces the duration of the
tones.
3. Press OK to confirm. The selected number of the audio signals
sounds as a corresponding acoustic signal.
4. Press OK to confirm. The instrument will return to
Instrument Setup.
The tungsten lamp produces light in the visible spectrum 320 to
1100 nm.
The deuterium lamp (UV-lamp) available produces light in the
ultraviolet spectrum 190 to 360 nm.
5.2.5.1 VIS-Lamp and UV-Lamp
In the overlap zone from 320 to 360 nm, either the deuterium lamp
(UV-lamp) or the tungsten lamp can be used for measurements.
The lifetime of the lamps is influenced
• by on-off operation and the length of time in use.
• Typical use is to turn the instrument on for the entire 8–10 hour
shift, and then off until the next day.
Note: In general, avoid on/off cycles of the lamp; this shortens the lamp’s
life span. For maximum life, turn the lamp off only if it will remain off for at
least 4–5 hours.
The lamp switches on automatically
• if a lamp is needed for the selected program
• if the instrument is operating inside the lamp’s spectrum
1. Press Lamp Control in the Instrument Setup.
2. Select On to switch on the VIS-Lamp and/or UV-Lamp.
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3. Select Save: in order to define a time interval for the burning
time of the VIS lamp and/or UV lamp.
4. Press the field below Save to select the lamp burning time.
Standard Operations
5. Select the length of time the lamp will be switched on.
Note: After this period of time the lamp automatically turns off, after no
measurement has been made outside the corresponding range (UV/VIS).
6. Touch OK to confirm.
7. To uc h UV Switch key to select the wavelength value between
320 nm and 360 nm, at which the instrument changes from the
visible to UV source.
8. Use the alphanumeric keypad to enter the maximum
wavelength for UV operation.
9. Touch OK to confirm and return to “Lamp Control“.
10. Touch OK to confirm and return to “Instrument Setup“.
Note: The selected program that requires a lamp has highest priority. If the
lamp in the Lamp Control was turned off, the lamp will be turned on
automatically if it is needed for the stored program.
5.2.5.2 Effect caused by the lamp settings on the Measuring Mode
UV-Lamp switches on manually. The icon ”UV Lamp“ appears in the
display and flashes.
The instrument will display ”Lamp Warmup...“. This takes about
3 minutes.
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Standard Operations
When the lamp is warmed up and ready, the UV icon stops flashing.
Note: If both lamps are On, the icon UV-VIS is displayed in the selected
Measurement Mode.
Note: Alternatively you can touch the UV- or VIS-Lamp icon on the
measurement screen to change the actual setting.
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5.2.6 PC and printer
USB Interfaces Description
USB (Type B)
USB (Type A)
This USB interface is only intended to connect the instrument to a PC (with installation of the
HACH Data Trans Software).
These USB ports can be used to connect a printer, a USB memory stick , a barcode scanner or a
keyboard.
Standard Operations
The instrument is provided with 3 USB interfaces, which are located
on the back of the instrument (see Figure 1 on page 14). These
interfaces can be used for exporting data and graphics to a printer,
updating data and for data communication to a personal computer.
These interfaces can be used for the connection of a USB stick, an
external USB keyboard or a USB Barcode handset scanner.
Note: A USB hub may be used to connect several accessories at a time.
A USB memory stick is used to upgrade data and software, see
section 6.8.2 on page 110.
Important Note: A screened USB cable must not be longer than
3m!
Table 3 USB connector
5.2.6.1 Printer setup
1. Press PC & Printer in the Instrument Setup.
A list with information about the connections opens.
For reasons of compatibility, the printer language must be
HP PCL 3.
2. Press Printer.
3. Press Setup to display the Printer Setup screen.
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Standard Operations
Printer Setup:
• Resolution: Print quality
• Paper: Paper size
Note: If an optional Thermal Printer is connected, the function "Auto Send"
on/off is available.
4. Select Auto-Send: On to send all measured data automatically
to the Thermal printer.
Note: The option Auto-Send is not available for any other printer (e.g. ink
jet printer).
5. Press Resolution to select the print quality.
Select between
• 100 dpi
• 150 dpi and
• 300 dpi
6. Press OK to confirm.
Note: Press OK again to return to the PC & Printer menu.
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