Fluke HART-5699F User manual

Page 1
Hart Scientific
5680/5682/5699
Metal Sheath Standard
Platinum Resistance Thermometer
User’s Guide
Rev. 5C1301
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Page 2
1 Before You Start . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.1 Symbols Used . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
1.2 Safety Information . . . . . . . . . . . . . . . . . . . . . . . . . . 2
1.2.1 WARNINGS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
1.2.2 CAUTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
1.3 Authorized Service Centers. . . . . . . . . . . . . . . . . . . . . . 3
2 Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
2.2 Application . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.3 Calibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.3.1 Calibration Intervals . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.4 Recalibration . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.5 Return Procedure . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
3 Specifications and Warranty . . . . . . . . . . . . . . . . . . . 9
3.1 Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
3.2 Construction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
3.3 Electrical Circuit . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
3.4 Warranty . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
4 Installation . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
4.1 Environmental Issues . . . . . . . . . . . . . . . . . . . . . . . . 11
4.2 Mounting . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
4.3 Lead Wire Identification. . . . . . . . . . . . . . . . . . . . . . . 11
5 SPRT Care and Handling Guidelines . . . . . . . . . . . . . . 13
5.1 SPRT Care. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
5.2 SPRT Handling Guidelines . . . . . . . . . . . . . . . . . . . . . 13
6 Operation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
6.1 General . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
6.2 Comparison Calibration of Other Instruments . . . . . . . . . . . 15
6.3 Immersion Requirements . . . . . . . . . . . . . . . . . . . . . . 15
6.4 Thermal EMF . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
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6.5 Measuring Current . . . . . . . . . . . . . . . . . . . . . . . . . 16
6.6 Cooling Rates at High Temperatures . . . . . . . . . . . . . . . . 16
7 Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
7.1 Case . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
8 Troubleshooting. . . . . . . . . . . . . . . . . . . . . . . . . . 21
8.1 Troubleshooting . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
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Page 4

Figures and Tables

Table 1 International Electrical Symbols . . . . . . . . . . . . . . . . . . . . . 1
Figure 1 5680/5682/5699 Metal Sheath Platinum Resistance Thermometer . . . . 5
Table 2 Specifications . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
Figure 2 Circuit Schematic . . . . . . . . . . . . . . . . . . . . . . . . . . . . 12
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1 Before You Start
1.1 Symbols Used
Table 1 lists the International Electrical Symbols. Some or all of these symbols may be used on the instrument or in this manual.
Tabl e 1 International Electrical Symbols
Symbol Description
AC (Alternating Current)
AC-DC
Battery
CE Complies with European Union Directives
1 Before You Start
Symbols Used
DC
Double Insulated
Electric Shock
Fuse
PE Ground
Hot Surface (Burn Hazard)
Read the User’s Manual (Important Information)
Off
On
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5680/5682/5689 SPRT
User’s Guide
Symbol Description
Canadian Standards Association
OVERVOLTAGE (Installation) CATEGORY II, Pollution Degree 2 per IEC1010-1 re fers to the level of Impulse Withstand Voltage protection provided. Equipment of OVERVOLTAGE CATEGORY II is energy-consuming equipment to be supplied from the fixed installation. Examples include household, office, and laboratory appliances.
C-TIC Australian EMC Mark
The European Waste Electrical and Electronic Equipment (WEEE) Directive (2002/96/EC) mark.
1.2 Safety Information
Use this instrument only as specified in this manual. Otherwise, the protection provided by the instrument may be impaired.
The following definitions apply to the terms “Warning” and “Caution”.
“WARNING” identifies conditions and actions that may pose hazards to the user.
“CAUTION” identifies conditions and actions that may damage the in­strument being used.
1.2.1
WARNINGS
To avoid personal injury, follow these guidelines.
DO NOT use this instrument to measure the temperature of any hazard ous live component.
DO NOT use this unit for any application other than calibration work.
DO NOT use this unit in environments other than those listed in the user’s manual.
Use of this instrument at high temperatures for extended periods of time can cause the handle to become hot.
Follow all safety guidelines listed in the user’s manual.
Calibration Equipment should only be used by Trained Personnel.
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-
1.2.2
CAUTIONS
To avoid possible damage to the instrument, follow these guidelines.
DO NOT remove the label from the handle. This cautions the user con
-
cerning the delicate nature of the instrument.
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1 Before You Start
Authorized Service Centers
Read Section entitled “SPRT Care and Handling Guidelines” before re-
moving the SPRT from the shipping box or case. Incorrect handling can damage the SPRT and void the warranty.
Keep the shipping container in case it is necessary to ship the SPRT. In-
correct packaging of the SPRT for shipment can cause irreparable dam­age.
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2 Introduction
2.1 General
The Hart Metal Sheath Standard Platinum Resistance Thermometer (SPRT) is designed to be an excellent primary standard interpolating instrument convert ing temperature to resistance. Hart Scientific offers three models (5680, 5682, and 5699). Models 5680 and 5682 metal sheath SPRTs cover the International Temperature Scale of 1990 (ITS-90) range from below the Triple Point of Ar gon (–189°C) to 480°C. The 5699 metal sheath SPRT covers the ITS-90 range from below the Triple Point of Argon (–189°C) to 661°C. The 5680 has a resis
tance of 25Ω at the triple point of water (0.01°C), the 5682 has a resistance of 100Ω at the triple point of water, and the 5699 has a resistance of 25.5Ω at the
triple point of water.
These metal sheath SPRTs are hand constructed at Hart Scientific by experts with years of SPRT manufacturing experience. Each SPRT is carefully an nealed at the appropriate temperatures and precisely tested for stability. The sensing element is fabricated using high purity platinum wire wound in a strain free design on a special frame. The 5680 and 5682 sensors are protected by a ceramic capsule. The 5699 sensor is protected by a platinum capsule. The sen­sors are pressure sealed with a special argon/oxygen mixed gas and fit with a terminal box handle with a strain relieved connection to the five wire cable. Gold plated spade lugs terminate the wires.
2 Introduction
General
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Figure 1 5680/5682/5699 Metal Sheath Platinum Resistance Thermometer
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5680/5682/5689 SPRT
User’s Guide
2.2 Application
Hart Scientific metal sheath SPRTs are classified as primary standards. A pri mary standard is defined in terms of transfer of the ITS-90 from a standards laboratory to a customer’s laboratory. Primary standards are calibrated in a standards lab using known intrinsic values.
2.3 Calibration
In order for any instrument to be used as a standard it must be calibrated. The SPRT may be purchased calibrated or non-calibrated. Hart has the capability to perform fixed-point or comparison calibrations traceable to NIST. They can be economically calibrated using the comparison method or any one of several fixed-point calibrations matching ITS-90 subranges.
2.3.1 Calibration Intervals
Accuracy required for the application and the condition of use dictate the cali­bration intervals. Calibration checks at the triple point of water should be ac­complished periodically and the results recorded. Once a written history of the SPRT is available, calibration intervals can be adjusted. The SPRT does not need to be recalibrated as long as the change in resistance does not exceed the owner’s specifications.
Depending on the user’s Quality Assurance requirements, the SPRT drift should be checked periodically at the Triple Point of Water (TPW). Section 8, Troubleshooting, provides information on drift with respect to mechanical shock and oxidation. If the R bration tolerances, a full recalibration should be scheduled.
cannot be restored after annealing to within cali-
tp
-
2.4 Recalibration
The recalibration of the SPRTs should be scheduled according to the user’s company Quality Assurance requirements. Normally, an SPRT is recalibrated annually. Unless the SPRT is used only over a limited range, calibration over the full range of the SPRT (–200°C to 480°C for the 5680 and 5682, and –200°C to 661°C for the 5699) is recommended. For information on recalibrating your SPRT, contact a Hart Scientific Authorized Service Center (see Section 1.3) for calibration options, an RMA number, and current pricing.
2.5 Return Procedure
Call an Authorized Service Center for an RMA number before shipping.
Extreme care must be taken in shipping a SPRT. Place the thermometer in its factory provided protective storage case. Be sure the case is latched securely. Place the protective case in the original manufacturer’s wooden shipping crate or wooden crate with similar dimensions (44 1/2 in. x 11 3/4 in. x 11 3/4 in.).
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2 Introduction
Return Procedure
Place soft insulation on all sides of the crate to cushion the SPRT against me chanical shocks. The cover of the crate should be attached with screws. Label ing as extremely fragile is recommended.
Whether the thermometer is returned for repair or warranty, please include a letter containing the following information
Description of the faulty operation and circumstances of failure.
Complete shipping instructions for the return of the thermometer to the
customer.
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3 Specifications and Warranty
3.1 Specifications
Tabl e 2 Specifications
5680 5682 5699
Temperature Range –200°C to 480°C –200°C to 661°C
Resistance Value at TPW
Specified Current 1 mA 1 mA or 0.5 mA 1mA
Resistance Ratio
Sensitivity
Stability <0.010°C/100 hours at 480°C
Repeatability < 2mK < 1mK
Diameter of Pt Sensor Wire
Lead Wires 5: four sensor wires plus grounding wire
Protective Sheath Inconel™600
Insulation Resistance
Ω
±0.5
25.5
W(234.3156K) W(302.9146K)
0.1
(typically < 0.005°C)
0.07 mm (0.003") 0.04 mm (0.0016") 0.07 mm (0.003")
Diameter: 6.35 mm (0.25") Length: 485 mm (19.1")
> 100M >1000M
Ω
1.11807
Ω
/°C 0.4Ω/°C 0.1Ω/°C
Ω
at 480°C
Ω
at 20°C
100Ω±1.0
0.844235
3 Specifications and Warranty
Ω
Specifications
25.5Ω±0.5
<8 mK per year max (typically 2–3 mK per year)
Inconel™600 Diameter: 5.56 mm ±0.13 mm (0.219" ±0.005") ±0.127 mm (0.005") Length: 482 mm (19")
> 100M >1000M
Ω
Ω
at 661°C
Ω
at 20°C
3.2 Construction
The Model 5680/5682 SPRTs cover the range from –200°C to 480°C and the Model 5699 SPRT covers the range from –200°C to 661°C. The sensor ele
­ments are crafted using high purity platinum wire wound in a strain free design on a specially designed support.
3.3 Electrical Circuit
The metal sheathed SPRTs are provided with a terminal box handle. The eight-foot cable has five polyethylene coated wires enclosed in a super-flex rubber jacket with a stainless steel spring strain relief. Gold plated spade lugs terminate the wires. The fifth wire is a ground wire which is connected to the Inconel sheath.
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5680/5682/5689 SPRT
User’s Guide
3.4 Warranty
Fluke Corporation, Hart Scientific Division (Hart) warrants this product to be free from defects in material and workmanship under normal use and service for a period as stated in our current product catalog from the date of shipment. This warranty extends only to the original purchaser and shall not apply to any product which, in Hart’s sole opinion, has been subject to misuse, alteration, abuse or abnormal conditions of operation or handling.
Software is warranted to operate in accordance with its programmed instruc tions on appropriate Hart products. It is not warranted to be error free.
Hart’s obligation under this warranty is limited to repair or replacement of a product which is returned to Hart within the warranty period and is determined, upon examination by Hart, to be defective. If Hart determines that the defect or malfunction has been caused by misuse, alteration, abuse or abnormal condi tions or operation or handling, Hart will repair the product and bill the pur chaser for the reasonable cost of repair.
To exercise this warranty, the purchaser must forward the product after calling or writing an Authorized Service Center for authorization. The Service Center assumes NO risk for in-transit damage.
THE FOREGOING WARRANTY IS PURCHASER’S SOLE AND EXCLU­SIVE REMEDY AND IS IN LIEU OF ALL OTHER WARRANTIES, EX­PRESS OR IMPLIED, INCLUDING BUT NOT LIMITED TO ANY IMPLIED WARRANTY OR MERCHANTABILITY, OR FITNESS FOR ANY PARTICULAR PURPOSE OR USE. HART SHALL NOT BE LIABLE FOR ANY SPECIAL, INDIRECT, INCIDENTAL, OR CONSEQUENTIAL DAM­AGES OR LOSS WHETHER IN CONTRACT, TORT, OR OTHERWISE.
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4 Installation
4.1 Environmental Issues
Primary standard equipment should be used in a calibration laboratory or other facility specifically designed for this purpose. Environmental requirements include:
Stable temperature and relative humidity <80%
Clean, draft-free area
Low noise level: low radio frequency, magnetic or electrical interference
Low vibration levels
4.2 Mounting
Most often temperature standards, primary and secondary, are used to calibrate other temperature-sensitive equipment.
The SPRT must be mounted carefully to avoid any damage to the sensor. If the fluid bath used does not have a lid designed for SPRT insertion, clamps should be used to ensure that the handle and cable are not immersed. Do not screw the clamps too tight. Over tightening will damage the sheath. If metal comparison blocks are used in the bath, maintain a close fit between the thermometer sheath and the well in the comparison block. However, allow for the thermal expansion of the thermometer sheath when determining block well tolerances.
4 Installation
Environmental Issues
4.3 Lead Wire Identification
The Model 5680/5682/5699 SPRTs are equipped with a five-wire cable. Four lead wires are used to cancel lead wire resistance. The fifth wire is a ground wire which is connected to the Inconel sheath. For best results, the readout de vice should be equipped to handle four-terminal resistors.
The lead wire colors are red, black, white, yellow, and green. Lead wire pairs, attached to each end of the sensor, are identified by heat shrink tubing. Red and black wires have red heat shrink tubing. Blue and white wires have black heat
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5680/5682/5689 SPRT
User’s Guide
shrink tubing. The green wire is the ground wire which should be connected to the ground. See Figure 2.
White
Red
BLACK RED
Yellow
to ground
R
x
connected to Inconel sheath
Black
GREEN
Figure 2 Circuit Schematic
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Page 15
5 SPRT Care and Handling Guidelines
5 SPRT Care and Handling Guidelines
5.1 SPRT Care
CAUTION: READ THIS SECTION BEFORE REMOVING THE SPRT
FROM THE SHIPPING BOX OR CASE
The 5680/5682/5699 Standard Platinum Resistance Thermometers (SPRTs) are extremely delicate instruments. Great care must be taken when handling the SPRT to maintain the calibration accuracy. Vibration or shock may cause the resistance to increase. A slight tap to the SPRT tip as it is removed from an in strument can cause a change in R SPRT will prolong the life expectancy. When not in use, the SPRT should be stored in the protective case provided by Hart Scientific.
5.2 SPRT Handling Guidelines
1.
DO keep the thermometer as clean as possible. Always remove any fluid from the sheath immediately after taking the thermometer from a bath.
2.
DO immerse the thermometer in the appropriate liquid for the tempera­ture range. If a dry block is used, the well diameter should allow the SPRT to comfortably slip in and out without excess movement. For best results, immerse the thermometer as deep as possible to avoid “stem ef­fect” (the temperature error caused by the conduction of heat away from the sensor). Do not submerge the handles.
3.
DO allow sufficient time for the thermometer to stabilize before making measurements allowing for the best accuracy.
4.
DO use the correct drive current with the thermometer to prevent error in temperature or resistance.
5.
DO anneal the thermometer at 480°C for the 5680 and 5682, and at 661°C for the 5699 when it has been subjected to mechanical or temper ature shock. The SPRT should also be annealed before calibration.
6.
DO use the protective case provided or other protection when the ther mometer is not in use.
7.
DON’T subject the thermometer to any physical shock or vibration.
8.
DON’T subject the thermometer to temperatures above the highest spec ified operating temperature.
9.
DON’T expose the thermometer’s handle or cables to extreme temperatures.
10.
DON’T submerge the handle or cable in liquids.
as high as 1 mK. Correct handling of the
tp
SPRT Care
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5680/5682/5689 SPRT
User’s Guide
Model 5699 only
11.
12.
DO anneal the SPRT after delivery or when using at a temperature higher than 600°C.
DON’T take the SPRT out directly when it has been at a temperature higher than 500°C. Allow the SPRT to cool to a temperature less than 500°C before removing it to room temperature. See Section 6.6 for more information.
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6 Operation
6 Operation
6.1 General
For best results, be familiar with the operation of the calibration bath or furnace and the read-out instrument. Be sure to follow the manufacturer’s instructions for the read-out instrument and the calibration bath or furnace.
6.2 Comparison Calibration of Other Instruments
General
The uniformity and stability of the bath and the degree of accuracy required de termine the number of temperature measurements necessary. However, to fol low “good” practice procedures, always measure the triple point of water (R after each temperature measurement. This provides the most accurate measure ment of the ratio:
Rt
()
=
()
Rtp
()
Wt
Equation 1: Resistance Ratio Equation
6.3 Immersion Requirements
Stem effect can cause measurement errors for any thermometer not immersed in the fluid at least 152 mm (6 inches). This error is due to heat lost or gained by the sensing element through the thermometer stem. In addition, heat losses occur due to radiation losses from the sensing element to the housing. How­ever, the effect of the shunt resistance is insignificant. Full immersion is recom mended in a furnace or freeze point cell.
The immersion depth for primary standards is dependent on several factors in cluding accuracy requirements and type of liquid. Therefore, we recommend a 203 mm (8 inch) minimum immersion depth.
The exact immersion depth required can be determined by performing a gradi ent test taking measurements approximately every 127 mm (0.5 inch) until there is a significant difference in readings. Allow the thermometer to stabilize at each new depth. Plot the results to see the stem effect.
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­)
tp
-
-
-
-
6.4 Thermal EMF
Two factors contribute to thermal EMF, chemical consistency and physical con sistency. Variations in chemical structure and discrepancies in crystal structure due to impurities can contribute to thermal EMF. These factors are minimized by annealing the full length of wire before construction of the SPRT.
Likewise, connection to extension lead wires and readout instruments can be a source of thermal EMF. The thermal EMF is caused by a difference in tempera
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Page 18
5680/5682/5689 SPRT
User’s Guide
ture between two connections. If the two connections are the same temperature, there will be little or no thermal EMF effects. However, if there is a substantial temperature difference between connections, the thermal EMF effects will be significant. Therefore, cover or insulate any exposed bridge or galvanometer terminals to lessen the source of error. The effects of thermal EMF can be can celed by using an AC bridge or a DC bridge with reversible current.
6.5 Measuring Current
Each SPRT has a specified drive current depending upon the particular sensor. The recommended currents are in the following table.
Errors caused by self-heating of the element need to be minimized. Allowing sufficient time for the SPRT to stabilize and the heat to be dispersed into the surrounding medium will provide the most accurate results.
The Model 5680/5682/5699 measurements are made at 1 mA and 1.4 mA. These measurements are then extrapolated to zero current. This can be done graphically by plotting i² vs. R and extrapolating to zero power or by using the following equation.
Model Resistance Drive Current
5680
5682
5699
25
100
25
Ω
Ω
Ω
1.0 mA
0.5 mA or 1.0 mA
1.0 mA
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16
iR R
−−()
RR
01
1221
=−
2
ii
221
where:
R
= Zero current resistance
0
R
= Resistance measured at current i
1
R2= Resistance measured at current i
1
2
Equation 2: Calculation of R0
6.6 Cooling Rates at High Temperatures
The equilibrium concentration of point defects in the pure platinum wire in crease exponentially to the increase in temperature. If a high cooling rate (i.e., removing a SPRT from a high temperature and cooling it to room temperature in less than a minute) occurs above 500°C, some of the point defects in the platinum wire become trapped in the crystalline structure causing a slight in crease in resistance. This slight increase in resistance can be reversed by an nealing the SPRT. To avoid this problem, slowly cool the SPRT at a rate of roughly 150°C/hour above 500°C before removing to room temperature. The
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Page 19
Cooling Rates at High Temperatures
6 Operation
SPRT can be safely removed from an instrument at 500°C or less and cooled to room temperature without concern for the cooling rate.
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7 Accessories
7.1 Case
The SPRTs are shipped in a protective case. The SPRT should be stored in this case when not in use. The SPRT should be shipped in this case when returning (see Section 2.5, Return Procedure).
7 Accessories
Case
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8 Troubleshooting
8.1 Troubleshooting
In the event that the probe appears to function abnormally, this section may help to find and solve the problem. Several possible problem conditions are de scribed along with likely causes and solutions. If a problem arises, please read this section carefully and attempt to understand and solve the problem. If the probe seems faulty or the problem cannot otherwise be solved, contact an Au thorized Service Center (see Section 1.3) for assistance. Be sure to have the model number and serial number of your probe available.
Problem Solution
Data changes
Data unstable
8 Troubleshooting
Troubleshooting
Slight mechanical shock can cause temperature errors
as much as 2mK. If this is observed, first measure and record the R and 5682) or 661° (5699 only) overnight. Measure the R
again. The annealing should decrease the Rtp. Re
tp
peat the annealing, R times. When the R the R
tp
rized Service Center. Oxidation of the platinum sensor may occur after pro-
longed use between 200 – 450°C. R crease. To reduce the effects of oxidation, anneal the SPRT at 480°C (5680 and 5682) or 661°C (5699 only) overnight (12 hours). Measure the R annealing, R nealing process should return R erances. If the R SPRT is usable. If the R ance, but it is stable, recalibrate the SPRT.
Severe mechanical shock can permanently damage the SPRT. If annealing the SPRT does not resolve the data change, contact an Authorized Service Center.
If the data is unstable at the Triple Point of Water (TPW), check the connection first. If this action does not fix the problem contact a Hart Scientific Authorized Ser vice Center. The SPRT may be damaged and need re pair.
If the data is unstable at high temperatures, it may be due to electrical noise in the system. Reduce the tem perature and observe the data. If it is stable, electrical noise is interfering with the measurements at high tem peratures. Check the grounding of the readout device and the heat source. A faulty ground on either device could interfere with high temperature measurements. A ground lead wire (the fifth wire) of the SPRT may help to reduce electrical noise interference. Be sure the ground lead wire is connected to an appropriate ground on the read-out device.
Next anneal the SPRT at 480°C (5680
tp.
measurement cycle several
tp
is stable, recalibrate the SPRT. If
does not stabilize, contact a Hart Scientific Autho-
tp
will show an in-
tp
again. Repeat the
measurement cycle several times This an-
tp
is within calibration tolerance, the
tp
is not within calibration toler
tp
tp
to within calibration tol-
tp
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5680/5682/5689 SPRT
User’s Guide
Problem Solution
Temperature readout different than expected, e.g. the heat source is set at 300°C, the SPRT measures 275°C
Measure the SPRT resistance at TPW.
If the resistance of the SPRT is less than the rated resis
tance, there may be a short in the sensor. Contact an Authorized Service Center.
If the resistance of the SPRT is only a few ohms, there
may be a short in the four lead-wires. Contact an Autho rized Service Center.
If the SPRT is open, the resistance will be “Out of Limits”
or in the kilo-ohm or mega-ohm range. Contact an Au thorized Service Center.
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