Cannon CAV 4.2 Operator's Manual
CANNON® CAV® 4.2
Automated Dual-Bath Kinematic Viscometer
CAV® 4.2
P/N 68.0505
Operator’s Manual
Revision 2.0, February 5, 2016
ASTM D445
CAV® 4.2
CANNON Instrument Company®
Operator’s Manual
Revision 2.0, February 5, 2016
2139 High Tech Road
State College, PA 16803
CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Revision
Date
Details
Revision 1.0
June 12, 2015
Initial release
Revision 2.0
February 5, 2016
Add VISCPRO II operating instructions
Copyright
Copyright © 2016 CANNON Instrument Company®. All rights reserved.
Trademarks
CANNON® and the CANNON® logo are registered trademarks of CANNON Instrument
Company®.
Brookfield® is a registered trademark of Brookfield® Engineering Laboratories, Inc.
Watlow® is a registered trademark of Watlow® Electric Manufacturing Company.
Revision History
Contact
Address: CANNON Instrument Company®
2139 High Tech Road
State College PA 16803, USA
Phone: 1-814-353-8000; 1-800-676-6232
Fax: 1-814-353-8007
Website: http://www.cannoninstrument.com
Email:
Sales: sales@cannoninstrument.com
Service: service@cannoninstrument.com
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Contents
Overview........................................................................................................................... 1
Related documents ....................................................................................................................... 1
Specifications / Compliances ........................................................................................................ 2
Notes/Cautions/Warnings ............................................................................................................. 3
Safety precautions ........................................................................................................................ 3
Getting Started ................................................................................................................. 5
Unpack and inspect ...................................................................................................................... 5
Setup the CAV® 4.2 ...................................................................................................................... 8
Connect hoses ........................................................................................................................ 10
Fill baths .................................................................................................................................. 13
Connect cables ........................................................................................................................ 15
Set bath temperature (CAV 4.2 GUI) ........................................................................................... 16
Calibrate temperature (CAV 4.2 GUI) ........................................................................................... 17
Set vacuum and pressure (CAV 4.2 GUI) ..................................................................................... 19
Adjust the default wash settings (CAV 4.2 GUI) .......................................................................... 20
Run a wash (CAV 4.2 GUI) ........................................................................................................... 21
Train sensors (CAV 4.2 GUI) ........................................................................................................ 22
Run a sample test (CAV 4.2 GUI) ............................................................................................. 23
Review and export data (CAV 4.2 GUI) ........................................................................................ 24
Connecting with VISCPRO II ............................................................................................. 25
Connect equipment .................................................................................................................... 26
Install VISCPRO II ........................................................................................................................ 26
Set up network adapter .............................................................................................................. 28
Configure firewall rules ............................................................................................................... 30
Configure USB Power Settings ................................................................................................... 32
CAV Registry settings .................................................................................................................. 33
Operation ....................................................................................................................... 35
CAV 4.2 GUI .................................................................................................................................35
VISCPRO® II software interface .................................................................................................. 39
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Manage user accounts (VISCPRO II / CAV 4.2 GUI) ...................................................................... 41
Log in ...................................................................................................................................... 41
Change password .................................................................................................................... 42
Setup and edit user accounts .................................................................................................. 42
Logout .................................................................................................................................... 42
Connect VISCPRO II to the CAV® 4.2 .......................................................................................... 43
Set bath temperature (VISCPRO II) ............................................................................................. 43
Calibrate temperature (VISCPRO II) ............................................................................................ 44
Set vacuum and pressure (VISCPRO II) ........................................................................................ 44
Train sensors (VISCPRO II) .......................................................................................................... 45
Run a wash (VISCPRO II) ............................................................................................................. 45
Run a sample test (VISCPRO II) ................................................................................................... 46
View test results (VISCPRO II) ..................................................................................................... 49
Control preheaters ...................................................................................................................... 49
Control sample cup heaters ........................................................................................................ 50
Advanced Setup .............................................................................................................. 51
Calibrate viscometer tube (VISCPRO II) ...................................................................................... 51
Method/Test settings .................................................................................................................. 52
Print method settings ............................................................................................................. 52
Edit method settings ............................................................................................................... 53
Adjust Default Wash Settings ..................................................................................................... 56
Create a standard CAV Data Table analysis ................................................................................. 57
Maintenance and Service ................................................................................................. 59
Update CAV 4.2 software and firmware ...................................................................................... 59
Tools and materials required ................................................................................................... 59
To prepare the USB flash drive ................................................................................................ 59
To replace the UI updater ........................................................................................................ 60
To update the UI software....................................................................................................... 60
To update the controller firmware .......................................................................................... 60
To update the VISCPRO II software......................................................................................... 61
Change viscometer tube ............................................................................................................. 62
Replace power supply ................................................................................................................. 63
djust solvent dosing chamber sensors ...................................................................................... 64
A
Specifications.................................................................................................................. 65
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Warranty......................................................................................................................... 67
Products limited warranty .......................................................................................................... 67
Reagent and chemical warranty ................................................................................................. 67
Returning a product to CANNON® ............................................................................................. 68
Required information.............................................................................................................. 68
Hazardous materials ............................................................................................................... 68
Shipping notification .............................................................................................................. 68
Replacement Parts List..................................................................................................... 69
List of Figures
Figure 1 — Complete CAV® 4.2 System ............................................................................................ 8
Figure 2 — Tubing connections ....................................................................................................... 10
Figure 3 — Solvent inlets ................................................................................................................. 11
Figure 4 — Temperature baths ........................................................................................................ 13
Figure 5 — Temperature bath details .............................................................................................. 14
Figure 6 — Bath top (fill hole) .......................................................................................................... 15
Figure 7 — Main screen ................................................................................................................... 16
Figure 8 — Temperature settings screen ........................................................................................ 16
Figure 9 — Field entry screen .......................................................................................................... 16
Figure 10 — Thermometer access holes ........................................................................................... 17
Figure 11 — Temperature calibration screen ................................................................................... 18
Figure 12 — Bath screen .................................................................................................................. 19
Figure 13 — Services menu ............................................................................................................. 19
Figure 14 — Pressure/vacuum adjustment screen ........................................................................... 19
Figure 15 — Settings menu ............................................................................................................. 20
Figure 16 — Wash screen ................................................................................................................ 20
Figure 17 — Main screen (wash button)........................................................................................... 21
Figure 18 — Train screen ................................................................................................................. 22
Figure 19 — Methods screen ........................................................................................................... 23
Figure 20 — Field entry screen ........................................................................................................ 23
F
igure 21 — Closed network settings .............................................................................................. 25
Figure 22 — Network connections .................................................................................................. 28
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Figure 23 — Connection properties ................................................................................................. 28
Figure 24 — TCP/IP properties ........................................................................................................ 29
Figure 25 — Advanced settings ....................................................................................................... 29
Figure 26 — Main screen menu ....................................................................................................... 35
Figure 27 — Main screen ................................................................................................................. 37
Figure 28 — Bath screen ................................................................................................................. 38
Figure 29 – VISCPRO interface window .......................................................................................... 40
Figure 30 — Solvent dosing chamber .............................................................................................. 64
List of Tables
Table 1 — Related documents ........................................................................................................... 1
Table 2 — Specifications and compliances ........................................................................................ 2
Table 3 — Packing list (main components) ........................................................................................ 5
Table 4 — Packing list (installation) .................................................................................................. 6
Table 5 — Packing list (tools) ............................................................................................................ 6
Table 6 — Packing list (consumables) ............................................................................................... 7
Table 7 — Packing list (networking) .................................................................................................. 7
Table 8 — Packing list (spares) .......................................................................................................... 7
Table 9 — Tools and materials required ............................................................................................ 9
Table 10 — Silicone bath fluid selection .......................................................................................... 13
Table 11 — Tools and materials required ..........................................................................................17
Table 12 — Tools and materials required ........................................................................................ 19
Table 13 — Tools and materials required ......................................................................................... 21
Table 14 — Tools and materials required ........................................................................................ 22
Table 15 — Tools and materials required ......................................................................................... 23
Table 16 — Tools and materials required ........................................................................................ 26
Table 17 — VISCPRO II registry entries ............................................................................................ 27
Table 18 — CAV® 4.2 registry entries .............................................................................................. 33
able 19 — GUI screen details ......................................................................................................... 36
T
Table 20 — VISCPRO window details .............................................................................................. 39
Table 21 — Default user accounts ................................................................................................... 41
Table 22 — Preheater settings ........................................................................................................ 49
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Table 23 — Sample cup heater settings (may vary between instruments, this is a starting point) ... 50
Table 24 — Method Settings: Test ...................................................................................................53
Table 25 — Method Settings: Wash ................................................................................................ 54
Table 26 — Method Settings: Advanced ......................................................................................... 55
Table 27 — Method Settings: Drop Criteria ..................................................................................... 56
Table 28 — CAV data table fields ..................................................................................................... 57
Table 29 — Specifications ............................................................................................................... 65
Table 30 — CAV 4.2 replacement parts ........................................................................................... 69
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
viii
CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Title
Reference Number
Standard Test Method for Kinematic Viscosity of Transparent and
ASTM D445
Standard Specifications and Operating Instructions for Glass
ASTM D446
Petroleum products -- Transparent and opaque liquids --
ISO 3104
Glass capillary kinematic viscometers -- Specifications and
operating instructions
ISO 3105
Petroleum products -Transparent and opaque liquids -
viscosity
IP 71
Overview
The CANNON® CAV® 4.2 is an automated, high throughput, dual-bath kinematic viscometer
for ASTM D445. The CAV® 4.2 combines CANNON® quality and reliability with modern
design and unique features to enhance lab productivity, reduce costs, and improve data
quality.
Related documents
Table 1 — Related documents
Opaque Liquids (and Calculation of Dynamic Viscosity)
Capillary Kinematic Viscometers
Determination of kinematic viscosity and calculation of dynamic
viscosity
Determination of kinematic viscosity and calculation of dynamic
1
Overview CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Specifications / Compliances
Specifications
Details
Model
CAV® 4.2
Methodology
ASTM D445/D446, ISO 3104/3105, IP 71
Applications
Formulated oil analysis, hydraulic oil analysis, additive
heavy fuel testing, waxes/paraffin, crude oil testing, glycols
Dimensions (W × D × H)
36 cm × 66 cm × 72 cm (14.25 in × 26 in × 28.5 in)
Weight
63 kg (140 lb)
Operational temperature
20 °C to +100 °C (± 0.01 °C); without a TE bath cooler, the
Down to 15 °C (± 0.03 °C) with integrated TE bath cooler
Maximum throughput
24 tests per hour
Automated sample capacity
28 positions (2 × 14 positions)
Minimum sample/solvent
volume required
8 mL sample/15 mL solvent per test
Viscosity range
0.5 mm²/s to 10,000 mm2/s in 100-fold increments
are also available.
Timing resolution
0.01 seconds (timing accuracy to ± 0.001 seconds)
Power requirements
100 VAC, 50/60 Hz, 1200 W
230 VAC, 50/60 Hz, 1200 W
Operating conditions
15 °C to 30 °C, 10% to 75% relative humidity (non-
Compliance
CE Mark: EMC Directive (2004/108/EC); Low Voltage
Directive (2006/95/EC); ROHS
Table 2 — Specifications and compliances
analysis, marine fuel testing, base stock analysis, light and
range
minimum temperature is +5 °C above ambient temperature
Up to 150 °C (± 0.03 °C) with integrated high temperature
bath
(depending on viscometer tubes selected). Fast run tubes
115 VAC, 50/60 Hz, 1200 W
condensing), Installation Category II, Pollution Degree 2
2
CANNON® Overview
CAV® 4.2 Operator's Manual, Rev. 2.0
Notes/Cautions/Warnings
Notes, caution, and warnings are used in the manual to call an operator’s attention to
important details prior to performing a procedure or step. Read and follow these important
instructions. Failure to observe these instructions may void warranties, compromise operator
safety, and/or result in damage to the CAV® 4.2.
Notes provide more information about the content that follows.
Cautions alert the operator to conditions that may damage equipment.
Warnings alert the operator to conditions that may cause injury.
Safety precautions
Please observe the following general safety precautions for proper and safe operation of the
CAV® 4.2.
• Only qualified personnel should operate the CAV® 4.2.
• Make sure that you read and understand all operating instructions and safety
precautions listed in this manual before installing or operating your unit. If you have
questions regarding instrument operation or documentation, contact CANNON
Instrument Company.
• Do not deviate from the installation, operation, or maintenance procedures described in
this manual. Improper use of the CAV® 4.2 may result in a hazardous situation and may
void the manufacturer’s warranty.
• Handle and transport the unit with care. Sudden jolts or impacts may cause damage to
components.
• Observe all warning labels. Never remove warning labels.
3
Overview CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
~MAINS
• Never operate damaged or leaking equipment.
• Unless procedures specify otherwise, always turn off the unit and disconnect the mains
cable from the power source before performing service or maintenance procedures, or
before moving the unit.
• Refer all service and repairs to qualified personnel.
~MAINS
(O)
The
supply. The AC power input must match the electrical specifications of
the instrument.
Never operate the equipment with a damaged MAINS AC power cable.
Use only the manufacturer-supplied MAINS AC power cable. This cable
must be inserted into a receptacle with a protective earth ground.
The (O) symbol indicates the OFF position for the electrical switches for
your unit.
symbol indicates the connections for the AC power
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CANNON®
CAV® 4.2 Operator's Manual, Rev. 2.0
Description
Part Number
CAV® 4.2
68.0229
Sample carousel (2)
68.0049 for use with glass vials
68.0092 for use with metal vials
MAINS AC power cable
Varies by locale
Dostmann digital thermometer
61.5600
Thermometer probes (2)
61.5601
CAV® 4.2 Operator’s Manual
68.0505
Getting Started
This chapter covers all steps necessary to set up, calibrate, and run a sample on the CAV® 4.2.
Procedures are intended to be performed in the order written. These are basic, simplified
procedures that will familiarize an operator with the instrument. More detailed instructions
are provided in other chapters.
Unpack and inspect
Unpack and inspect the complete CANNON® CAV® 4.2 and all accessories as soon as they are
received.
Caution: Many components are fragile. Use caution when moving and
handling the CAV® 4.2 and accessories.
1. Carefully unpack the entire contents of the shipment.
2. Referring to the packaging list, verify that all materials were received.
3. Inspect materials for defects and shipping damage. Contact your CANNON
representative to resolve any issues.
Table 3 — Packing list (main components)
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CAV® 4.2 Operator's Manual, Rev. 2.0
Getting Started CANNON®
Description
Part Number
Solvent
1
⁄8" blue FEP tubing (25 ft)
81.2185
Brass tee fittings (2)
81.0007
Bottle caps for GL-38 bottles (4)
65.3201
20 micron filters (4)
65.0047
1
⁄2" white nylon tubing (15 ft)
62.1500.3
Brass elbow
68.0309
1
⁄2" white nylon elbows (2)
62.1500.2
1
⁄2" white nylon tees (2)
62.1500.4
Exhaust
6 mm blue FEP tubing (15 ft)
81.2102
Description
Part Number
1
⁄8" Allen wrench
27.1340
3
⁄16" Allen wrench
68.0464
T-wrench
81.2222
Glass funnel
81.3112
Rubber stoppers (3)
11.3115
Tubing cutter
81.1074
Yellow Tygon tubing (2 ft)
71.4.16
Table 4 — Packing list (installation)
Waste
Table 5 — Packing list (tools)
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CAV® 4.2 Operator's Manual, Rev. 2.0
CANNON® Getting Started
Description
Part Number
Sample test oils
varies
Glass vials (144 vials)
9717-V01: glass vials
Silicone bath fluid (2 L)
Varies by application
Description
Part Number
CAT cables, red (2)
61.3378
USB to Ethernet adapter
68.0496
8-port network switch
68.0495
USB cable
68.0508
USB flash drive
17.5121
Description
Part Number
6 A fuses (4)
28.0851
12 A fuses (4)
25.2455
Thermal fuse
68.0439
Hose fittings (2)
81.2101
Compression connectors (4)
81.2096
Brass 3⁄8" to 1⁄4" reducer fittings (2)
61.3566
O-rings (4)
61.3567
Table 6 — Packing list (consumables)
(optional) Metal sleeves (14)
68.0455: metal sleeves
Table 7 — Packing list (networking)
Table 8 — Packing list (spares)
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CAV® 4.2 Operator's Manual, Rev. 2.0
Getting Started CANNON®
Setup the CAV® 4.2
Initial setup of the CAV® 4.2 involves connecting the hoses and cables and filling the baths
with silicone bath fluid.
Figure 1 — Complete CAV® 4.2 System
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CAV® 4.2 Operator's Manual, Rev. 2.0
CANNON® Getting Started
Description
Hose connections
Complete CAV® 4.2
1⁄8" blue FEP tubing (25 ft)
MAINS AC power cable
1⁄2" white nylon tubing (15 ft)
Waste receiver
Bottle caps for GL-38 bottles (4)
Solvent
20 micron filters (4)
7
⁄8" wrench
3⁄16" Allen wrench
Glass funnel
Rubber stopper
Silicone bath fluid (2 L)
Tubing cutter
Glass or metal vials
Optional
Networking
Brass tee fittings (2)
CAT cables, red (2)
Brass elbow
USB to ethernet adapter
1⁄2" white elbows (2)
8-port network switch
1⁄2" white tees (2)
6 mm blue FEP tubing (15 ft)
Table 9 — Tools and materials required
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CAV® 4.2 Operator's Manual, Rev. 2.0
Getting Started CANNON®
Solvent inlets
Waste outlets
Exhaust ports
Connect hoses
Assemble the CAV® 4.2 on a secure, level surface with sufficient room behind the instrument
to maintain a clear airflow and allow for unimpeded connection of the solvent inlet and waste
outlet tubing.
Figure 2 — Tubing connections
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CAV® 4.2 Operator's Manual, Rev. 2.0
CANNON® Getting Started
Solvent inlet well
Solvent tubing
Inlet pipes with
connectors
B A A B
1. Place the CAV® 4.2 on a solid, level workbench. The workbench must be located near a
MAINS AC power connection capable of providing sufficient current (10 A at 115 V
AC) to
the CAV® 4.2. Depending on the materials tested, solvent used, and laboratory
regulations, the work area may also need to be equipped with a ventilation system.
2. Place the waste receiver beneath the CAV® 4.2. In order to promote proper drainage, the
top of the waste receiver must be lower than the waste outlets on the back of the
instrument.
3. Place the solvent bottles alongside or beneath the CAV® 4.2.
4. Measure and cut the
1
⁄8" blue FEP tubing to use as the solvent tubing. Each piece of
tubing must run from the solvent inlet well to the bottom of a solvent bottle.
5. Connect the solvent tubing to the CAV® 4.2:
a. Remove the cover plate from the solvent inlet well.
b. Thread the tubing through the solvent inlets on the back of the lid.
c. Unscrew the appropriate compression connector and slide it onto the tubing.
d. Slide the tubing onto the flared inlet pipe and hand tighten the compression
connector.
Figure 3 — Solvent inlets
compression
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CAV® 4.2 Operator's Manual, Rev. 2.0
Getting Started CANNON®
Note: Each piece of tubing must run from the middle of the CAV® 4.2
6. Insert the solvent tubing into the solvent bottle:
a. Thread the tubing through the bottle cap.
b. Screw a 20 micron filter onto the end of the tubing.
c. Screw the bottle cap onto the solvent bottle.
7. Repeat steps 4 through 6 for each piece of solvent tubing.
into the waste receiver. 1⁄2" white nylon elbows and tees are provided to
enable combining both waste tubes into one tube before entering the
waste receiver. A brass elbow is also provided to connect the waste
tubing to the waste receiver.
8. Measure and cut the
1
⁄2" white nylon tubing to use as the waste tubing.
Caution: Do not overtighten the waste outlet compression nut.
9. For each bath, connect the waste tubing to the CAV® 4.2:
a. Unscrew the brass compression nut from the waste outlet fitting.
b. Thread the tubing through the compression nut.
1
c. Slide the ferrule onto the tubing. Position it
⁄2" from the end of the tubing.
d. Insert the tubing into the outlet fitting until the ferrule is seated.
e. Tighten the compression nut by hand.
7
f. Using a
⁄8" wrench, tighten the compression nut to create a good seal.
10. Connect the waste tubing to the waste receiver.
11. Measure, cut, and install the 6 mm blue FEP tubing as exhaust tubing.
12
CAV® 4.2 Operator's Manual, Rev. 2.0
CANNON® Getting Started
Bath operating range
Recommended bath fluid viscosity
20 °C to 100 °C
10 cSt
101 °C to 150 °C
20 cSt
Left bath
Right bath
Display hood
Plumbing lid
Fill baths
Each temperature bath must be filled with Dow Corning 200 silicone fluid prior to operation.
The viscosity of the fluid depends upon the temperature of the bath during most operations:
Table 10 — Silicone bath fluid selection
Figure 4 — Temperature baths
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CAV® 4.2 Operator's Manual, Rev. 2.0
Getting Started CANNON®
Drain plug
Warning: Follow all lab policies regarding the safe handling and
disposal of all hazardous materials.
1. Open the plumbing lid.
2. Raise the display hood by pulling it forward, up, and then back in an arcing motion until
the hood rests on top of the frame. Once raised, the latches will keep the hood in
position.
3
3. Insert the
/16" Allen wrench into each drain plug access hole and verify that the drain
plug is closed (clockwise to close).
Cold fill level
access holes
Figure 5 — Temperature bath details
4. Insert the funnel into the thermometer hole in the top of the bath to be filled.
5. Slowly pour a small amount of silicone fluid into the bath. Check for leaks. Continue
filling until the bath fluid reaches the cold fill level (marked with a thin black/red line on
the glass), approximately 0.9 L.
6. Repeat steps 3 through 5 for the second bath.
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CAV® 4.2 Operator's Manual, Rev. 2.0
CANNON® Getting Started
Fill hole
Figure 6 — Bath top (fill hole)
Connect cables
1. Connect the MAINS AC power cord to the CAV® 4.2.
2. Plug the power cord into the MAINS AC outlet at the work station.
3. (optional) Connect the CAV® 4.2 to the network switch with one CAT cable.
4. (optional) Connect the network switch to the PC with a CAT cable and USB adapter.
15
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