Agilent Technologies 8860 Site Preparation Manual

Agilent 8860 Gas Chromatograph
Site Preparation Guide
Notices
CAUTION
WARNING
© Agilent Technologies, Inc. 2019
No part of this manual may be reproduced in any form or by any means (including electronic storage and retrieval or translation into a foreign language) without prior agreement and written consent from Agilent Technologies, Inc. as governed by United States and international copyright laws.
Manual Part Number
G2790-90012
Edition
First edition, January 2019
Printed in USA
Agilent Technologies, Inc. 2850 Centerville Road Wilmington, DE 19808-1610 USA
安捷伦科技 (上海)有限公司 上海市浦东新区外高桥保税区 英伦路 412 号 联系电话:(800)820 3278
Warranty
The material contained in this document is provided “as is,” and is subject to being changed, without notice, in future editions. Further, to the maximum extent permitted by applicable law, Agilent disclaims all warranties, either express or implied, with regard to this manual and any information contained herein, including but not limited to the implied warranties of merchantability and fitness for a particular purpose. Agilent shall not be liable for errors or for incidental or consequential damages in connection with the furnishing, use, or performance of this document or of any information contained herein. Should Agilent and the user have a separate written agreement with warranty terms covering the material in this document that conflict with these terms, the warranty terms in the separate agreement shall control.
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Safety Notices
A CAUTION notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly performed or adhered to, could result in damage to the product or loss of important data. Do not proceed beyond a CAUTION notice until the indicated conditions are fully understood and met.
A WARNING notice denotes a hazard. It calls attention to an operating procedure, practice, or the like that, if not correctly performed or adhered to, could result in personal injury or death. Do not proceed beyond a WARNING notice until the indicated conditions are fully understood and met.
Site Preparation Guide

Contents

1 Agilent 8860 GC Site Preparation
Site Preparation Checklist 6
Bench Preparation 7
Maximum Length of Cables and Hoses 10
2 GC Installation Kits
Installation Kits 14
3 Dimensions and Weights
Dimensions and Weight 18
Foreline Pump Requirements for Systems Including an MSD 20
ALS Dimensions and Weight 21
4 Environmental Conditions
Environmental Conditions 24
Heat Dissipation 25
ALS Environmental Conditions 26
5 Exhaust Venting
Exhaust Venting 28
Venting hot air 28 Venting other gases 29 Exhaust vent fittings 30
6 GC System Power Requirements
Power Requirements 32
USA fast heating oven, 240 V 34 Canadian installation 34 Common instrument power cord plugs 34
ALS Power Requirements 38
7 Gas Selection and Plumbing
Gas and Reagent Selection 40
Hydrogen Carrier Gas 42 Gas and Reagent Purity 42
Site Preparation Guide 3
Gas Supplies 43 GC/MS Gas Requirements 45 Performance verification 48
Gas Plumbing 49
Supply tubing for most carrier and detector gases 50 Supply tubing for hydrogen gas 50 Two-stage pressure regulators 51 Pressure regulator-gas supply tubing connections 51 Filters and traps 52
A LAN Requirements
Site LAN Network 56
4 Site Preparation Guide

1 Agilent 8860 GC Site Preparation

Site Preparation Checklist 6
Bench Preparation 7
Maximum Length of Cables and Hoses 10
This guide outlines the site requirements for GC, GC/MS, and automatic liquid sampler (ALS) installation. Site requirements include the necessary space, electrical supplies, gas supplies, operating supplies and consumables required to successfully install the GC and related instruments and systems.
The site must meet the requirements specified in this guide before beginning installation.
Refer to the Agilent Web site at www.agilent.com for the most up-to-date listing of GC, GC/MS, and ALS supplies and consumables.
Site Preparation Guide 5
1 Agilent 8860 GC Site Preparation

Site Preparation Checklist

Site Preparation Checklist
For typical system requirements for system installation, see the diagrams on page 8 through
page 9.
Use the following checklist to ensure that the site is properly prepared for GC system installation.
1 Ensure that the appropriate installation hardware has been acquired.
See “Installation Kits” on page 14.
2 Ensure that the location in which the GC system is being installed meets the
requirements for environmental conditions. See “Environmental Conditions” on page 24. Also see “Heat Dissipation” on page 25.
3 Prepare bench space for the GC system. Ensure that the bench has the size and
weight capacity to accommodate the GC and associated components. See “Bench
Preparation” on page 7. Also see “Dimensions and Weight” on page 18.
4 Ensure that system components are oriented so that they can be connected
properly. See “Maximum Length of Cables and Hoses” on page 10.
5 If the system being installed includes an MSD, ensure that the bench allows for
proper installation and connection of the foreline pump. See “Foreline Pump
Requirements for Systems Including an MSD” on page 20.
6 Ensure that appropriate venting is provided for the GC system. See “Exhaust
Venting” on page 28.
7 Ensure that a dedicated power circuit is available for each device in the system.
See “Power Requirements” on page 32.
8 Ensure that appropriate gas and reagent supplies are provided for the GC system.
See “Gas and Reagent Selection” on page 40.
9 Ensure that appropriate gas plumbing is provided for the GC system. See “Gas
Plumbing” on page 49.
10 If the GC system being installed includes a data system, ensure that the PC meets
the requirements necessary to properly support the GC system. For more information, see the site prep guide for your data system.
11 If the GC being installed is to be connected to a site LAN, ensure that the appropriate
cabling is available. See “Site LAN Network” on page 56.
6 Site Preparation Guide
1 Agilent 8860 GC Site Preparation

Bench Preparation

Bench Preparation
When planning a bench layout:
Consider component dimensions, weights, and space requirements. See “Dimensions and
Weight” on page 18.
Consider the lengths of cables and hoses for connection of components. See “Maximum
Length of Cables and Hoses” on page 10.
For systems that include an MS, consider foreline pump requirements. See “Foreline
Pump Requirements for Systems Including an MSD” on page 20.
Allow space for operational access.
Note that the 7200 Q-TOF requires 48 cm (1.6 ft) of space in front to allow for the RIS
probe extraction tool handle when installed.
Note that some repairs to the GC/MS, or to the GC itself, will require access to the back of the instrument(s).
Examples are provided here for systems including a GC with an ALS, computer and printer. Most examples also include an MS.
See several example layouts below.
Site Preparation Guide 7
1 Agilent 8860 GC Site Preparation
Typical GC System - 8860 GC with computer and printer.
Total weight: ~84 kg (186 lb)
Maximum power consumption: ~3,250 VA (11,090 btu/hr)
78 cm (31-in.)
without heat
deflector
65 cm (26-in.)
with heat
deflector
Leave 30 cm (12-in.)
open space for
operational access
Use isolated circuits with
dedicated grounds for GC
and MSD.
Application
Gas
*
* Use 1/8-in. Swagelok gas connections
Purity
Supply
Pressure
(psi)
† 1 psi = 6.89 kPa
Carrier Helium
Hydrogen
Nitrogen
99.9995
99.9995
99.9995
50 - 80
50 - 80
50 - 80
Detectors
TCD Helium 99.9995 50 - 80
FID, NPD,
FPD, TCD
Hydrogen 99.9995 50 - 80
ECD, FID,
FPD, NPD,
TCD
Nitrogen 99.9995 50 - 80
FID, NPD,
FPD
Air Zero
grade
50 - 80
80 cm
(32-in.)
(without
ALS)
100 cm (40-in.)
(with ALS)
~2.35 m (7.7 ft.)
~86 cm (34-in.) ~56 cm (22-in.) ~56 cm (22-in.)~44 cm (17.3-in.)
Bench Preparation
8 Site Preparation Guide
1 Agilent 8860 GC Site Preparation
Typical GC/MS System - 8860 GC, 5977 MSD, with computer and
printer.
Total weight: ~123 kg (271 lb)
Maximum power consumption: ~4,350 VA (14,843 btu/hr)
78 cm (31-in.)
without heat
deflector
65 cm (26-in.)
with heat
deflector
If bench backs up to
wall, drill 1.5-in. hole
for foreline pump
hose.
Leave 30 cm (12-in.) open
space for operational
access
Use isolated circuits with
dedicated grounds for GC
and MSD.
Place foreline pump on floor or
on vibration reducing bench.
Application
Gas
*
* Use 1/8-in. Swagelok gas connections
Purity
Supply
Pressure
(psi)
† 1 psi = 6.89 kPa
Carrier Helium
Hydrogen
Nitrogen
99.9995
99.9995
99.9995
50 - 80
50 - 80
50 - 80
Detectors
TCD Helium 99.9995 50 - 80
FID, NPD,
FPD, TCD
Hydrogen 99.9995 50 - 80
ECD, FID,
FPD, NPD,
TCD
Nitrogen 99.9995 50 - 80
FID, NPD,
FPD
Air Zero
grade
50 - 80
80 cm
(32-in.)
(without
ALS)
100 cm (40-in.)
(with ALS)
~2.35 m (7.7 ft.)
~86 cm (34-in.) ~56 cm (22-in.) ~56 cm (22-in.)~44 cm (17.3-in.)
Bench Preparation
Site Preparation Guide 9
1 Agilent 8860 GC Site Preparation
CAUTION

Maximum Length of Cables and Hoses

Maximum Length of Cables and Hoses
The distance between system modules may be limited by some of the cabling and the vent or vacuum hoses.
Table 1 Cable and hose lengths
Item Length
Remote cable 2 m (6.6 ft)
LAN cable 10 m (32.8 ft)
Power cords 2 m (6.6 ft)
Vacuum hose 1.3 m (4.24 ft)
Foreline pump power cord 2 m (6.6 ft)
7697A Headspace Sampler transfer line 99 cm (39-in.)
G1888 Headspace Sampler transfer line 80 cm (31.5-in.)
The supporting surface for the 7200/7250 Q-TOF GC/MS system should be kept relatively vibration free. Do not put the rough pump on your laboratory bench with the 7200/7250 Q-TOF GC/MS due to the vibration that the pump creates. Vibration can lead to a loss of mass accuracy and resolution.
10 Site Preparation Guide

2 GC Installation Kits

Installation Kits 14
This section provides details for available installation hardware.
Refer to the Agilent Web site at www.agilent.com for the most up-to-date listing of GC, GC/MS, and ALS supplies and consumables.
Site Preparation Guide 13
2 GC Installation Kits
NOTE

Installation Kits

Installation Kits
Installation kits are not supplied with the GC. If you did not order the GC with the factory plumbing option (305), Agilent highly recommends the following kits in Table 2.
Agilent recommends purchasing the installation kit(s) that provides parts useful for GC
installation. (Tab le 2 lists the appropriate installation kits.)
In addition to these installation kits, fittings and reducers are required to convert gas cylinder regulator fittings (for example, 1/4-inch male NPT) to the 1/8-inch female Swagelok fittings needed to connect gases to the instrument. These fittings are not included with the GC or with the installation kits. See “Gas Plumbing” on page 49 for details.
Table 2 Installation kits
Kit Part number Contents
Recom mended for GCs wit h FID, NPD, F PD:
GC Supply Gas Installation Kit with Gas Purifiers See Figure 1.
Recommended for GCs with TCD/ECD, MS, and MSD:
19199N Includes Gas Clean Filter system kit
CP736530 (with 1 oxygen, 1 moisture, and 2 charcoal filters), 1/8-inch brass nuts and ferrules, copper tubing, 1/8-inch brass tees, tubing cutter, 1/8-inch brass caps, universal external split vent trap with replacement cartridges, and 1/8-inch ball valve.
GC Supply Gas Installation Kit See Figure 2.
Gas Clean carrier gas filter kit, 1/8-inch See Figure 3.
19199M Includes 1/8-inch brass nuts and
ferrules (20), copper tubing, 1/8-inch brass tees, tubing cutter, 1/8-inch brass caps, 7-mm nut driver, T-10 Torx driver, T-20 Torx driver, 4 open-end wrenches, and 1/8-inch ball valve
CP17974
14 Site Preparation Guide
2 GC Installation Kits
Installation Kits
Figure 1. GC Supply Gas Installation Kit with Gas Purifiers 19199N
Figure 2. GC Supply Gas Installation Kit 19199M
Figure 3. Gas Clean carrier gas filter kit, 1/8-inch CP17974
Site Preparation Guide 15
2 GC Installation Kits
Installation Kits
16 Site Preparation Guide

3 Dimensions and Weights

Dimensions and Weight 18
Foreline Pump Requirements for Systems Including an MSD 20
ALS Dimensions and Weight 21
This section lists the dimensions of the GC, GC/MS, and automatic liquid samplers (ALS).
Site Preparation Guide 17
3 Dimensions and Weights

Dimensions and Weight

Dimensions and Weight
1 Ensure that you can accommodate the shipping pallets when you take delivery.
See Table 3.
2 Prepare laboratory bench space before the system arrives. Make sure the prepared area is
clean, clear, and level. Pay special attention to the total height requirements. Avoid bench space with overhanging shelves. See Table 4 .
Table 3 Pal let d i mens ions and weights
Product Height Width Depth Weight
GC
8860 Series GC shipping pallet
With third side detector (side mount)
MS
7200/7250 Q-TOF MS 96 cm (38-inch) 130 cm (51-inch) 91 cm (36-inch) 175 kg (385 lb)
7200 Flight Tube 66 cm (26-inch) 66 cm (26-inch) 147 cm (58-inch) 36.4 kg (80 lb)
7250 Flight Tube 66 cm (26-inch) 206 cm (81-inch) 81 cm (32-inch) 87 kg (191 lb)
76 cm (30-inch) 76 cm (30-inch)
86 cm (34-inch) 87 cm (34-inch)
103 cm (40.5-inch) 108 cm (42.5-inch)
N/A
Table 4 Instrument dimensions, weights, and required clearances
Product Height Width Depth Weight
GC
8860 Series GC
With third side detector (side mount)
GC operational /oven access Requires
GC rear ventilation / maintenance
clearance
MSD
5975 Series MSD
Diffusion pump 41 cm (16-inch) 30 cm (12-inch) 54 cm (22-inch) 39 kg (85 lb)
Standard turbo pump 41 cm (16-inch) 30 cm (12-inch) 54 cm (22-inch) 39 kg (85 lb)
Foreline pump
Standard Oil-free
GC/MS operational and maintenance access
5977 Series MSD
Diffusion pump 41 cm (16-inch) 30 cm (12-inch) 54 cm (22-inch) 39 kg (85 lb)
50 cm (19.2-inch) 50 cm (19.2-inch)
21 cm (8-inch) 19 cm (7.5-inch)
59 cm (23-inch) 68 cm (27-inch)
54 cm (21-inch) 54 cm (21-inch)
50 kg (112 lb) 57 kg (125.4 lb)
30 cm (12-inch) open space above GC.
Requires
Requires wall to dissipate hot air and allow for routine maintenance.
13 cm (5-inch) 32 cm (13-inch)
Requires 30 cm (1 ft) to the left of the unit.
27 cm (10.7-inch) open space in front of GC.
25 cm (10-inch) clearance between back of instrument and
31 cm (12-inch) 28 cm (11-inch)
11 kg (23.1 lb) 16 kg (35.2 lb)
Performance turbo pump 41 cm (16-inch) 30 cm (12-inch) 54 cm (22-inch) 41 kg (90 lb)
18 Site Preparation Guide
3 Dimensions and Weights
Dimensions and Weight
Table 4 Instrument dimensions, weights, and required clearances (continued)
Product Height Width Depth Weight
Foreline pump
Standard Oil-free (MVP-070) Oil-free (IDP3)
21 cm (8-inch) 19 cm (7.5-inch) 18 cm (7-inch)
13 cm (5-inch) 32 cm (13-inch) 35 cm (14-incn)
31 cm (12-inch) 28 cm (11-inch) 14 cm (6-inch)
11 kg (23.1 lb) 16 kg (35.2 lb) 10 kg (21 lb)
GC/MS operational and maintenance access
MS
7000 and 7010 Triple Quad MS
EI Mainframe 47 cm (18.5-inch) 35 cm (14-inch) 86 cm (34-inch) 59 kg (130 lb)
EI/CI Mainframe 47 cm (18.5-inch) 35 cm (14-inch) 86 cm (34-inch) 63.5 kg (140 lb)
Foreline pump 28 cm (11-inch) 18 cm (7-inch) 35 cm (14-inch) 21.5 kg (47.3 lb)
GC/MS operational and maintenance
access
7200 Q-TOF MS
Mainframe 133 cm (52.5-inch) 90 cm (34.5-inch) 100 cm (39.5-inch) 138 kg (305 lb)
Foreline pump 28 cm (11-inch) 18 cm (7-inch) 35 cm (14-inch) 21.5 kg (47.3 lb)
7250 Q-TOF MS
Mainframe 190 cm (74.8-inch) 90 cm (34.5-inch) 100 cm (39.5-inch) 138 kg (350 lb)
Foreline pump DS202 28 cm (11-inch) 18 cm (7-inch) 35 cm (14-inch) 21.5 kg (47.3 lb)
Foreline pump IDP-15 36.4 cm (14.3-inch) 33.3 cm (13.1-inch) 48.5 cm (19.1-inch) 45.5 kg (100 lb)
GC/Q-TOF operational and maintenance
access
Headspace sampler (HS)
7697A Headspace sampler
111 vial model 12 vial model
GC with 7697A Headspace sampler Requires 69 cm (27-inch) to the right of the GC (G4557A), or 64 cm
G1888 Headspace sampler 56 cm (22-inch) 46 cm (18.1-inch) 64 cm (25-inch) 46.3 kg (102 lb)
ALS
80 cm (32-inch) 61 cm (24-inch)
Requires 30 cm (1 ft) to the left of the unit.
Requires 30 cm (1 ft) to the left of the unit.
Requires 40 cm (16-inch) clearance on both sides of the unit. Requires 30 cm (12-inch) clearance behind the unit.
69 cm (27-inch) 64 cm (25-inch)
(25-inch) to the right of the GC (G4556A).
70 cm (27.5-inch) 69 cm (27-inch)
46 kg (101 lb)
38.2 kg (84 lb)
GC with 7693A ALS injector Requires 50 cm (19.5-inch) above the GC 3.9 kg (8.6 lb) each
GC with 7693A ALS tray Requires 43 cm (16.8-inch) left of the GC
Requires 4.2 cm (1.7-inch) in front of GC
GC with 7650A ALS injector Requires 50 cm (19.5-inch) above the GC 3.9 kg (8.6 lb) each
GC with CTC PAL Autosampler Requires 76.6 cm (30.2-inch) above the GC and
65 to 98 cm (25.6 to 38.6-inch) to the right of the GC, depending on configuration
6.8 kg (15 lb) each
Site Preparation Guide 19
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