The calibrator or the micro calibration bath described
in the operating instructions has been designed and
manufactured using state-of-the-art technology.
All components are subject to stringent quality and
environmental criteria during production. Our management
systems are certified to ISO 9001 and ISO 14001.
■
These operating instructions contain important information
on handling the instrument. Working safely requires that all
safety instructions and work instructions are observed.
■
Observe the relevant local accident prevention regulations
and general safety regulations for the instrument’s range
of use.
■
The operating instructions are part of the product and
must be kept in the immediate vicinity of the instrument
and readily accessible to skilled personnel at any time.
Pass the operating instructions onto the next operator or
owner of the instrument.
■
Skilled personnel must have carefully read and
understood the operating instructions prior to beginning
any work.
■
The general terms and conditions contained in the sales
documentation shall apply.
■
Subject to technical modifications.
■
Factory calibrations / DKD/DAkkS calibrations are carried
out in accordance with international standards.
The calibrator or micro calibration bath is a portable unit, for
service functions and also for industrial and laboratory tasks.
The temperature calibrators and micro calibration baths
from WIKA are provided for the calibration of thermometers,
temperature switches/thermostats, resistance thermometers
EN
and thermocouples. The operational safety of the delivered
instruments is only assured if the equipment is employed for
its intended use (verification of temperature sensors). The
given limit values should never be exceeded (see chapter
12 “Specifications”).
The appropriate instrument should be selected depending on
the application; it should be connected correctly, tests carried
out and all components serviced.
The instrument is manufactured in different versions. The
individual version for any single unit can be found on the
nameplate on the calibrator/micro calibration bath.
2.3 Scope of delivery
The calibrators/micro calibration baths are delivered in
special protective packaging. The packaging must be set
aside so that the calibrator or the micro calibration bath can
be sent safely back to the manufacturer for recalibration or
repair.
Scope of delivery for the model CTD9100 dry-well
temperature calibrator
■
Calibrator
■
Insert replacement tools
■
Standard bored insert
■
Power cord
■
Calibration certificate
■
Operating instructions
Scope of delivery for the model CTB9100 micro
calibration bath
■
Micro calibration bath
■
Transport cover
■
Sensor basket
■
Magnetic stirrer
■
Magnetic lifter
■
Power cord
■
Calibration certificate
■
Operating instructions
Scope of delivery for the model CTM9100 multi-function
calibrator
■
Multi-function calibrator
■
Insert replacement tools (standard and surface)
■
Standard bored insert
■
Transport cover
■
Sensor basket
■
Magnetic stirrer
■
Magnetic lifter
■
Infrared insert
■
Surface insert
■
External reference sensor
■
Power cord
■
Calibration certificate
■
Operating instructions
Cross-check scope of delivery with delivery note.
3. Safety
3.1 Explanation of symbols
DANGER!
... indicates a directly dangerous situation
resulting in serious injury or death, if not avoided.
WARNING!
... indicates a potentially dangerous situation
that can result in serious injury or death, if not
avoided.
CAUTION!
... indicates a potentially dangerous situation
that can result in light injuries or damage to
equipment or the environment, if not avoided.
... identifies hazards caused by electric power.
Should the safety instructions not be observed,
there is a risk of serious or fatal injury.
WARNING!
... indicates a potentially dangerous situation that
can result in burns, caused by hot surfaces or
liquids, if not avoided.
Information
... points out useful tips, recommendations
and information for efficient and trouble-free
operation.
11263911.05 03/2019 EN/DE/IT
3. Safety
3.2 Intended use
The calibrator or micro calibration bath is a portable unit, for
service functions and also for industrial and laboratory tasks.
The temperature calibrators and micro calibration baths
from WIKA are provided for the calibration of thermometers,
temperature switches/thermostats, resistance thermometers
and thermocouples.
This instrument is not permitted to be used in hazardous
areas!
The instrument has been designed and built solely for
the intended use described here, and may only be used
accordingly.
The technical specifications contained in these operating
instructions must be observed. Improper handling or
operation of the instrument outside of its technical
specifications requires the instrument to be taken out of
service immediately and inspected by an authorised WIKA
service engineer.
Handle electronic precision measuring instruments with
the required care (protect from humidity, impacts, strong
magnetic fields, static electricity and extreme temperatures,
do not insert any objects into the instrument or its openings).
Plugs and sockets must be protected from contamination.
The manufacturer shall not be liable for claims of any type
based on operation contrary to the intended use.
3.3 Improper use
WARNING!
Injuries through improper use
Improper use of the instrument can lead to
hazardous situations and injuries.
▶
Refrain from unauthorised modifications to
the instrument.
▶
Do not use the instrument within hazardous
areas.
▶
Only ever use the supplied mains cable.
Any use beyond or different to the intended use is considered
as improper use.
Special hazards
DANGER!
Danger of death caused by electric current
Upon contact with live parts, there is a direct
danger of death.
▶
The instrument may only be installed and
mounted by skilled personnel.
▶
Before replacing the fuse, cleaning,
maintenance/servicing and in the event of
danger, the calibrator or the micro calibration
bath must be disconnected by unplugging the
mains cable from the power supply outlet.
▶
The mains socket must be freely accessible
at all times!
Thermal fuse
For safety, the calibrator or the micro calibration
bath is fitted with an independently-operating
temperature fuse, which cuts out the heater
power supply if the temperature inside the
enclosure is too high. Once the metal block and
the liquid bath have cooled down, send in the
calibrator or the micro calibration bath to WIKA
for examination.
The calibrator and the micro calibration bath
have been designed as measuring and control
instruments. With any operation of the calibrator/
micro calibration bath not expressly provided
for in these operating instructions, additional
protective measures must be taken.
Since a malfunction of the calibrator/micro
calibration bath can cause personal injury or
damage to property, the equipment must be
protected by additional electro-mechanical
safeguards.
3.4 Safety instructions for using calibration liquids
Calibration liquid, water
Only use distilled water, otherwise the calibrator
tank can become strongly scaled and soiled.
Collect spilled liquids immediately and dispose
of them properly.
Wear the requisite protective equipment (see
chapter 3.6 “Personal protective equipment”).
▶
Observe the information in the material safety
data sheet for the corresponding medium.
▶
Before working with silicone oil, read the
material data safety sheet. The current
material safety data sheet can be found at
www.wika.de on the respective product page.
▶
Only use the silicone oil included within
the scope of supply or specified in these
operating instructions.
▶
When working with silicone oil, sufficient
ventilation should be ensured in the room
since it can give off pollutants.
▶
Since silicone oil is hygroscopic, after use,
always close the calibration bath using the
transport cover.
▶
Before transporting with silicone oil, allow the
calibrator or micro calibration bath to cool. The
transport cover is fitted with a safety valve. If
the micro calibration bath is closed when it is
still warm, excessive pressure can build up.
In order to avoid overpressuring, which could
lead to damage to the liquid bath, the safety
valve is activated at a pressure of approx.
2.5 bar [36 psi]. This can lead to hot vapour
escaping.
WARNING!
Risk of burns!
Touching the hot metal block or micro calibration
bath, the hot bath liquids or the test item can
lead to acute burns.
▶
Before transporting or touching the metal
block/liquid bath, make sure that it has cooled
down sufficiently.
3.5 Personnel qualification
WARNING!
Risk of injury should qualification be
insufficient!
Improper handling can result in considerable
injury and damage to equipment.
The activities described in these operating
instructions may only be carried out by skilled
personnel who have the qualifications described
below.
Skilled personnel
Skilled personnel, authorised by the operator, are understood
to be personnel who, based on their technical training,
knowledge of measurement and control technology and
on their experience and knowledge of country-specific
regulations, current standards and directives, are capable
of carrying out the work described and independently
recognising potential hazards.
Special operating conditions require further appropriate
knowledge, e.g. of aggressive media.
3.6 Personal protective equipment
The personal protective equipment is designed to protect the
skilled personnel from hazards that could impair their safety
or health during work. When carrying out the various tasks
on and with the instrument, the skilled personnel must wear
personal protective equipment.
Follow the instructions, displayed in the work area,
regarding personal protective equipment!
The required personal protective equipment must be
provided by the operating company.
Wear safety goggles!
Protect eyes from flying particles and liquid
splashes.
Collect spilled liquids immediately and dispose
of them properly.
Wear safety goggles!
Do not allow silicone oil to come into contact with
the eyes.
Wear protective gloves!
Protect hands from friction, abrasion, cuts or
deep injuries and also from contact with hot
surfaces and aggressive media.
The calibrator and micro calibration bath consist of a robust,
grey-blue-painted steel enclosure, with a carrying handle on
top.
The rear part of the enclosure includes a metal block or
liquid bath with an opening for the test item, accessible from
the top.
The metal block/liquid bath incorporate the heating or cooling
elements and the temperature sensor for determining the
reference temperature.
The metal block and the liquid bath are thermally insulated.
The front part contains the complete electronic unit for
controlling the reference temperature.
Solid state relays (SSR) are used to control the heating and
cooling elements.
On the front panel is the controller, which is fitted with a
7-segment LED (2 rows of 4 digits) for the reference and set
temperature.
The micro calibration bath has an additional knob for
controlling the stirring speed.
Temperature calibrator, model CTD9100-165Temperature calibrator, model CTD9100-650
Multi-function calibrator, model CTM9100-150Micro calibration bath, model CTB9100-165
4.2 Isometric views of the CTD9100 series dry-well temperature calibrators
1
Front and top of the model CTD9100
On the top of the dry-well temperature calibrator, you will find
3
2
the dry well access opening for inserting the inserts.
■
CTD9100-COOL: Ø 28 x 150 mm [Ø 1.10 x 5.91 in]
■
CTD9100-165:Ø 28 x 150 mm [Ø 1.10 x 5.91 in]
■
CTD9100-165-X: Ø 60 x 150 mm [Ø 2.36 x 5.91 in]
■
CTD9100-450:Ø 60 x 150 mm [Ø 2.36 x 5.91 in]
■
CTD9100-650:Ø 28 x 150 mm [Ø 1.10 x 5.91 in]
EN
The controller, with display and controls, is located on the
front of the calibrator.
Rear of the instrument
On the rear of the equipment is the product label with the key
information about the particular model.
■
CTD9100-COOL: -55 ... +200 °C [-67 ... +392 °F]
■
CTD9100-165:-35 ... +165 °C [-31 ... +329 °F]
■
CTD9100-450:40 ... 450 °C [104 ... 842 °F]
■
CTD9100-650:40 ... 650 °C [104 ... 1.202 °F]
1
The correct mains voltage and frequency is also given.
■
AC 100 ... 240 V, 50 ... 60 Hz
■
AC 115 V, 50 ... 60 Hz
■
AC 230 V, 50 ... 60 Hz
8
11263911.05 03/2019 EN/DE/IT
4
Furthermore, the individual serial number
(e.g. S/N 550 33 44) as well as the mains voltage and the
5
fuse rating is given.
You will also find the connector for the RS-485 interface here.
Underside of the instrument
On the underside of the instrument are the mains connection
socket and the power switch with its fuse-holder.
These are located in the centre, at the front. Furthermore,
depending on the model, there are one or two air intakes
located on the underside of the instrument.
The air intakes must not be obstructed in any way.
4.3 Isometric views of the CTB9100 series micro calibration baths
EN
1
3
2
9
On the top of the micro calibration bath are the block opening
for filling Ø 60 x 150 mm [Ø 2.36 x 5.91 in].
The controller, with display and controls, is located on the
front of the calibrator.
Rear of the instrument
On the rear of the equipment is the product label with the key
information about the particular model.
Furthermore, the individual serial number
(e.g. S/N 550 33 44) as well as the mains voltage and the
fuse rating is given.
You will also find the connector for the RS-485 interface here.
Underside of the instrument
On the underside of the instrument are the mains connection
socket and the power switch with its fuse-holder.
Front and top of the model CTB9100
1
These are located in the centre, at the front. Furthermore,
depending on the model, there are one or two air intakes
located on the underside of the instrument.
The air intakes must not be obstructed in any way.
4.4 Isometric views of the model CTM9100-150 multi-function calibrator
Front and top of the model CTM9100-150
1
3
11
On the top of the multi-function calibrator, you will find the dry
well access opening for inserting the different inserts or filling
Ø 60 x 150 mm [Ø 2.36 x 5.91 in].
EN
10
The controller, with display and control elements, is located
2
9
on the front of the calibrator. In addition, the control elements
for the external reference are placed on the front.
Rear of the instrument
On the rear of the equipment is the product label with the key
information about the particular model.
Furthermore, the individual serial number
(e.g. S/N 550 33 44) as well as the mains voltage and the
fuse rating is given.
You will also find the connector for the RS-485 interface here.
Underside of the instrument
1
On the underside of the instrument are the mains connection
socket and the power switch with its fuse-holder.
These are located in the centre, at the front. Furthermore,
there are two air intakes located on the underside of the
instrument.
The air intakes must not be obstructed in any way.
The instruments are fitted with an RS-485 communications
interface. Via this interface one can connect to a PC, level
converter or a network.
The software protocol used is a MODBUS-RTU protocol,
which is used in may monitoring programs available on the
market.
The transmission speed (baud rate) is factory set to 9,600
baud. Upon request, other data transmission rates are
possible.
The 5-pin socket has two pins, A and B, that you connect to
the corresponding connections on the PC, level converter or
network.
Plan view of the 5-pin panel socket
4.7 Interface protocol
The interface protocol is available on request for delivery as a
specific additional document.
4.8 Protective earth monitoring
The calibrator is fitted with a protective earth
monitor to keep a check on the base isolation
of the heater. The monitoring unit works
independently of the normal controls and
switches off the heating power supply as soon as
the calibrator no longer has a connection to the
protective earth system of the isolation.
Once reconnected to the protective earth
system, the monitoring unit automatically
switches the power supply back on to the
heating circuit.
EN
To connect to a PC, the RS-485 signal must be externally
converted to an RS-232 or USB signal. The appropriate
converter, including drivers, is available as an option.
The computer records all operational data and allows
programming of all calibrator configuration parameters.
The minimum requirements for operation with a USB
converter are:
■
IBM compatible PC
■
Installed operating system, Microsoft® Windows® 98 SE,
ME, 2000, XP (Home or Prof.) or 7
■
A USB interface (USB 1.1 or USB 2.0)
A network connection enables the connection of up to 32
calibrators/micro-baths on the same network.
To connect to a network, some factory setting is required. For
this, please contact the supplier or WIKA directly.
For access to the programming via the keypad
while the serial interface is communicating, the
message “buSy” appears on the display, and
therefore indicates that it is in an “occupied”
state.
4. Design and function / 5. Transport, packaging and storage
5. Transport, packaging and storage
5.1 Transport
Check the calibrator or the micro calibration bath for any
damage that may have been caused by transport.
EN
Obvious damage must be reported immediately.
CAUTION!
Damage through improper transport
With improper transport, a high level of damage
to property can occur.
▶
When unloading packed goods upon delivery
as well as during internal transport, proceed
carefully and observe the symbols on the
packaging.
▶
With internal transport, observe the
instructions in chapter 5.2 “Packaging and
storage”.
If the instrument is transported from a cold into a warm
environment, the formation of condensation may result
in instrument malfunction. Before putting it back into
operation, wait for the instrument temperature and the room
temperature to equalise.
5.2 Packaging and storage
Do not remove packaging until just before mounting.
Keep the packaging as it will provide optimum protection
during transport (e.g. change in installation site, sending for
repair).
Permissible conditions at the place of storage:
■
Storage temperature: -10 ... +60 °C [14 ... 140 °F]
■
Humidity: 30 ... 95 % relative humidity (no condensation)
Avoid exposure to the following factors:
■
Direct sunlight or proximity to hot objects
■
Mechanical vibration, mechanical shock (putting it down
hard)
Store the calibrator or the micro calibration bath in its original
packaging in a location that fulfils the conditions listed above.
6. Commissioning, operation
Personnel: Skilled personnel
Protective equipment: Protective gloves and safety goggles
Only use original parts (see chapter 13 “Accessories”).
WARNING!
Physical injuries and damage to property
and the environment caused by hazardous
media
Upon contact with hazardous media (e.g.
oxygen, acetylene, flammable or toxic
substances), harmful media (e.g. corrosive,
toxic, carcinogenic, radioactive), and also with
refrigeration plants and compressors, there is
a danger of physical injuries and damage to
property and the environment.
Should a failure occur, aggressive media and/
or with high temperature may be present at the
instrument.
▶
For these media, in addition to all standard
regulations, the appropriate existing codes or
regulations must also be followed.
▶
Wear the requisite protective equipment (see
chapter 3.6 “Personal protective equipment”).
6.1 Operating position
The operating position of the calibrator or the micro
calibration bath is in the vertical orientation, since this
guarantees an optimal temperature distribution in the metal
block or liquid bath.
Voltage supply
DANGER!
Danger to life caused by electric current
Upon contact with live parts, there is a direct
danger to life.
▶
Only ever use the supplied mains cable.
The voltage supply of the instrument is made via the power
cable. This is included in the scope of delivery.
In order to achieve the greatest possible accuracy, the use
of exactly matched inserts is necessary. For this, diameter of
the specimen must be accurately determined. The bore for
the insert is obtained by adding +0.5 mm [+0.02 in].
Inserts
Following use, the inserts should be removed
using the replacement tools and then the sleeve
and block should be cleaned. This prevents the
sleeves becoming jammed in the heating block.
Recommended calibration liquids for the different
temperature ranges:
Water as a calibration liquid
■
Only use distilled or demineralised water, otherwise the
calibrator tank can become strongly scaled and soiled.
Silicone oil as a calibration liquid
■
Only use the silicone oil recommended here.
■
When working with silicone oil, sufficient ventilation should
be ensured in the room since it can give off pollutants.
■
Since silicone oil is hygroscopic, after use, always close
the calibration bath using the transport cover.
Only use clean calibration liquids. The
checking of temperature sensors and other
temperature measuring devices may lead to the
contamination of the calibration liquid. These
contaminants, through the rotational movement
of the magnetic stirrer, may cause an abrasive
effect on the bottom tank.
Wear safety goggles!
Do not allow silicone oil to come into contact with
the eyes.
EN
6.3 Preparation of the micro calibration bath
In order to achieve the highest possible accuracy for a
micro calibration bath, it should be filled with an appropriate
calibration liquid.
6.3.1 Properties of the calibration liquid
Different calibration liquids, due to their specific properties,
deliver varying calibration results. A compensation to the
calibration liquid used in each case should, if necessary, be
■
Clean the tank
■
Before calibration, clean the sensors
■
Replace the worn magnetic stirrer
■
Replace the contaminated, cloudy calibration liquid
Wear protective gloves!
Protect hands from friction, abrasion, cuts or
deep injuries and also from contact with hot
surfaces and aggressive media.
performed by the manufacturer at the factory.
MediumCalibration rangeFlash point
Distilled water5 ... 90 °C [51 ... 194 °F]none
Dow Corning 200 Fluid with 5 CS-40 ... +123 °C [-40 ... +253 °F]133 °C [271 °F]
Dow Corning 200 Fluid with 10 CS-35 ... +155 °C [-31 ... +311 °F]163 °C [325 °F]
Dow Corning 200 Fluid with 20 CS7 ... 220 °C [45 ... 428 °F]232 °C [450 °F]
Dow Corning 200 Fluid with 50 CS25 ... 270 °C [77 ... 518 °F]280 °C [536 °F]
Following maximum filling heights are recommended:
EN
Calibrator modelmax. filling height
CTB9100-165 / CTM9100-150130 mm [5.12 in]
CTB9100-165 / CTM9100-150
with removable insert
CTB9100-225123 mm [4.84 in]
CTB9100-225 with removable insert105 mm [4.13 in]
CTB9100-225-X115 mm [4.53 in]
CTB9100-225-X with removable insert95 mm [3.74 in]
Following points should be observed at the maximum
filling heights:
■
Measured from the bottom of the sensor basket
■
Non loaded tank
■
WIKA standard filling liquid
■
Pre-filling ex-works with the optimal height
110 mm [4.33 in]
The magnetic stirrer is a
consumable.
Liquid bath
6.3.4 Insert for liquids
The insert for liquids consists of:
■
Insert with leak-proof cover
■
Sensor basket
■
Magnetic stirrer and lifter
■
Replacement tools
The transport cover is fitted with a safety valve.
If the micro calibration bath is closed when it is
still warm, excessive pressure can build up. In
order to avoid overpressuring, which could lead
to damage to the liquid bath, the safety valve
is activated at a pressure of approx. 2.5 bar
[36 psi]. This can lead to hot vapour escaping.
6.3.3 Operation of the magnetic stirrer
The greatest possible homogeneity is achieved by the
agitation of the calibration liquid via a magnetic stirrer.
Set the stirring speed to the maximum possible. Turning the
wheel upwards will increase the speed, turning it downwards
slows down the stirring speed.
Front of the controller with stirrer-speed dial
Insert for liquids
WARNING!
Risk of burns!
Hot liquids can lead to acute burns
▶
The insert for liquids must only be removed if
the calibrator is used at room temperature.
▶
The fill level must be matched the relevant
medium and the temperature.
If the insert for liquids is ordered with a new
model CTB9100 micro calibration bath or a new
model CTM9100 multi-function calibrator, the
instrument will have been matched to the insert
for liquids.
Should the insert for liquids be ordered
afterwards, a re-adjustment of the instrument at
the customer’s will be needed.
The operation of the calibrator with the surface insert is
suited to a simple and the most accurate calibration possible
of surface probes.
Fit the insert, which is hollow and long from the bottom, into
the block using a special replacement tool.
The sleeve also has three bores (1 x 3 mm, 1 x 3.1 mm and
1 x 4 mm [1 x 0.12 in, 1 x 0.12 in and 1 x 0.16 in]) directly
under the surface, so that the correct surface temperature
can be controlled at all times.
Following use, the inserts should be removed using the
specific replacement tools and then the sleeve and block
should be cleaned. This prevents the sleeves becoming
jammed in the heating block.
The calibration of surface thermometers is very
difficult and not fully defined. Thermometers
mounted on surfaces dissipate heat from
the surface and create a cold zone on the
surface being measured. In the multi-function
calibrators, the calibration temperature is created
in a specially designed surface insert and an
external reference thermometer measures the
temperature directly under the surface. The
reference thermometer also determines the
temperature of the cold zone through integration
of the temperature along the sensitive length of
the reference thermometer and thus provides
a true temperature calibration of surface
temperature sensors.
6.5 Infrared insert (only CTM9100-150)
The operation of the calibrator with the infrared insert is
suited to a quick and simple calibration of non-contact
thermometers.
Fit the hollow and specially-designed insert into the
block using a special replacement tool. The sleeve also
has two bores in the edge (1 x 3.5 mm and 1 x 4.5 mm
[1 x 0.14 in and 1 x 0.18 in]) for the accurate monitoring of the
temperature.
The design and surface finish of the sleeve is important, in
order that a defined emissivity of 1 is achieved.
Following use, the inserts should be removed using the
specific replacement tools and then the sleeve and block
should be cleaned. This prevents the sleeves becoming
jammed in the heating block.
With temperatures of < 0 °C [< 32 °F] and higher
air humidity, ice or dew can form in the insert.
This can falsify the calibration. By capping the
measurement opening, the ice or dew formation
can be strongly reduced.
■
Leave the measurement opening closed as
long as possible
■
Open the measurement opening for a short
while for the measurement
■
Remove any ice or dew present by heating
EN
The sleeve is designed so that the supplied
external reference provides the best possible
result, since the depth of the bore is adjusted
to the sensitive length. If a separate external
reference is used for comparison calibration,
ensure that the sensitive length is known and it
lies in the centre of the calibration surface.
To test temperature sensors, connect a separate
temperature-measuring instrument to the test item. By
comparing the temperature displayed on the external
measuring instrument with the reference temperature,
there is evidence of the status of the test item. This ensured
EN
that the test item requires a short time until it reaches the
temperature of the metal block or liquid bath.
There is no possibility for calibrating earthed
thermocouples, since the heating block is
earthed and this would therefore lead to false
measurement results.
6.7 Start-up procedure
If the calibrator is not used for a long time, because of the
materials used (magnesium oxide), moisture can penetrate
the heating elements.
Following transport or storage of the calibrator in moist
environments, the heating elements must be taken to higher
temperatures slowly.
During the drying process,it should be assumed that the
calibrator has not yet reached the required insulation voltage
for protection class I. The start-up set point is T
[248 °F] with a holding time of T
= 15 min.
n
= 120 °C
anf
Once the set temperature has been reached, through short
switch impulses, the radiated heating energy from the metal
block or liquid bath is delivered, so that the temperature
within remains constant.
Reference and set temperature display
6.10 Control of the reference temperature
The red LED OUT 1 indicates that the heater is turned on.
6.8 Switching on the calibrator/micro calibration bath
1. Connect to the mains using the mains connector supplied.
2. Switch on the mains switch.
The controller will be initialised.
The upper PV display will show tEst.
In the lower SV display, the version number (e.g. rL 2.2) will
be shown.
After approx. 5 secs, the initialisation will be complete and
the calibration mode will automatically be displayed.
The built-in heating or cooling elements will temper the metal
block automatically from room temperature to the controller’s
set temperature.
6.9 Reference and set temperature display
Upper PV display:
The red 4-digit, 7-segment display shows the current
temperature of the metal block or liquid bath.
Lower SV display:
The green, 4-digit, 7-segment display shows the current set
temperature of the metal block or the liquid bath.
Display with LED OUT 1
During the heating phase a steady light indicates that heating
energy is being supplied. A flashing LED indicates that the
reference temperature (set temperature) has almost been
reached and therefore the heating energy is only being
supplied in short bursts.
Control achieved via PID algorithm
To ensure good temperature stability, the cycle time of the
controller is set low and the control output is usually raised.
7. Operating elements of the calibrator/micro calibration bath
7. Operating elements of the calibrator/micro calibration bath
There are three modes available for operation
Calibration mode
In this standard operating state the calibration of test items
can be made.
Set-point mode
In this mode, the set temperature is entered.
Main menu
In this mode, all settings, such as specifying the desired
temperature or setting the control parameters are made.
7.1 Selection of the operating modes for the
CTM9100-150
To operate the multi-function calibrator in the desired mode
of operation, first specify the correct linearisation for the
controller. In the main menu (via the [P] button) select the
desired function using the arrow keys.
LIOperates as a micro calibration bath
DB Operates as a dry block
IrOperates as an infrared black body source
SU Operates as a surface temperature calibrator
Select the liquid used depending upon the desired calibration
temperature.
Dry-block operating mode
1. Cleaning the tank (if needed)
2. Inserting the insert (aluminium)
3. Set the speed of the magnetic stirrer to “0”.
4. In order to ensure the correct linearisation, set DB in the
controller. For this, press the [P] button for approx. 5 secs.
and confirm the appropriate setting in the main menu with
[P].
5. Set the switch to the left of the controller to external
reference. Connect the delivered external reference in to
the socket provided and slide into the appropriate bore in
the insert.
The insert has several bores into which the thermometer
probes being calibrated and the external reference, for
comparative calibration, can be inserted. The block is either
heated or cooled to the desired calibration temperature.
Once a stable temperature has been reached, the
temperature probes to be calibrated can be compared with
the reference thermometer.
EN
The desired function is accepted using the [P] button.
On the main screen, the desired linearisation (LI, DB, Ir or
SU) is displayed in the PV line every 5 secs.
7.2 Method of operation in calibration mode within
individual operating modes
Micro calibration bath operating mode (possible with or
without insert for liquids)
1. Insert the magnetic stirrer and sensor basket.
2. Fill the micro calibration bath (see chapter 6.3.2 “Filling
the micro calibration bath”).
3. Set the speed of the magnetic stirrer, in order to achieve
the best homogeneity possible.
4. In order to ensure the correct linearisation, set LI in the
controller. For this, press the [P] button for approx. 5 secs.
and confirm the appropriate setting in the main menu with
[P].
5. Set the switch to the left of the controller to internal
reference.
Angled thermometers, large-diameter thermometers or
thermometers with special designs cannot be calibrated
with a dry-well calibrator. For this reason the multi-function
calibrator also has the possibility to function as a stirred liquid
bath. The liquid is circulated using a magnetic stirrer and thus
provides very good temperature distribution within the bath.
11263911.05 03/2019 EN/DE/IT
Infrared operating mode
1. Cleaning the tank (if needed)
2. Insert the insert (hollow, ceramic coated)
3. Set the speed of the magnetic stirrer to “0”.
4. In order to ensure the correct linearisation, set Ir in the
controller. For this, press the [P] button for approx. 5 secs.
and confirm the appropriate setting in the main menu with
[P].
5. Set the switch to the left of the controller to external
reference. Connect the delivered external reference into
the socket provided and slide it into into the appropriate
bore on the outer edge of the insert.
The measuring spot of the pyrometer being calibrated must
be smaller than the diameter of the infrared insert.
Surface operating mode
1. Cleaning the tank (if needed)
2. Insert the insert (hollow, fitted with a collar at the top)
3. Set the speed of the magnetic stirrer to “0”.
4. In order to ensure the correct linearisation, set SU in the
controller. For this, press the [P] button for approx. 5 secs.
and confirm the appropriate setting in the main menu with
[P].
5. Set the switch to the left of the controller to external
reference. Connect the delivered external reference in to
the socket provided and slide into the appropriate bore
directly under the surface of the insert.
7. Operating elements of the calibrator/micro calibration bath
The calibration of surface thermometers is very difficult
and not fully defined. Thermometers mounted on surfaces
dissipate heat from the surface and create a cold zone on
the surface being measured. In the multi-function calibrator,
the calibration temperature is created in a specially designed
surface insert and an external reference thermometer
EN
measures the temperature directly under the surface. The
reference thermometer also determines the temperature
of the cold zone through integration of the temperature
along the sensitive length of the reference thermometer
and thus provides a true temperature calibration of surface
temperature sensors.
The sleeve is designed so that the supplied external
reference provides the best possible result, since the depth
of the bore is adjusted to the sensitive length. If a separate
external reference is used for comparison calibration, ensure
that the sensitive length is known and it lies in the centre of
the calibration surface.
7.3 Calibration (calibration mode)
As soon as the calibrator or micro calibration bath is switched
on, following the initialisation, it defaults to calibration mode.
On the upper PV display, the current reference temperature
is indicated.
On the lower SV display is the set temperature.
The LED OUT 1 signals the status of the outputs for the
heating control:
■
If the LED OUT 1 is on, the temperature will increase.
■
If the LED OUT 1 is not on, the heating is switched off.
a) Heating instrument
The LED OUT 2 signals the status of the outputs for the fan
control:
■
If LED OUT 2 is on, the fan is running at higher speed.
■
If LED OUT 2 is not on, the fan is running at lower speed.
b) Heating and cooling instrument
The LED OUT 2 signals the status of the outputs for the
cooling control:
■
If the LED OUT 2 is on, the temperature will decrease.
■
If the LED OUT 2 is not on, the cooling is switched off.
Two possibilities for setting the set temperature
Either a temporary set temperature is set (see chapter
7.3 “Calibration (calibration mode)”) or a fixed set
temperature (see chapter 7.4 “Setting a temporary set
temperature (set-point mode)”) is stored in the main menu.
7.4 Setting a temporary set temperature (set-point
mode)
In this operating state, a stored set temperature is temporarily
changed.
1. Press button [P] briefly.
On the upper PV display, the currently active set value
memory is displayed, e.g. SP2 (set point 2).
On the lower SV display is the corresponding set
temperature.
2. By pressing button [▲] the set temperature is increased.
By pressing button [▼] the set temperature is reduced.
3. By pressing button [P] again, the new set point is
accepted.
Display in HEATING calibration mode
Temporary set temperature setting
The LED OUT 2 signals the status of the outputs for the fan/
cooling control.
By pressing button [▲] or [▼] the value is
increased or decreased by 0.01 °C [0.01 °F].
If the keys are held down for at least 1 sec.,
however, the value increases or decreases more
rapidly, and after 2 secs. even faster, so that the
desired value can be reached very quickly.
If, in set-point mode, no button has been
pressed for approx. 15 secs., an automatic return
to calibration mode occurs.
7. Operating elements of the calibrator/micro calibration bath
7.5.1 Menu structure, parameter levels
As shown in the menu structure, via OPEr, the groups and
parameter levels are accessible, in which the settings can
then be made.
EN
Calibration mode
approx. 5 secs.
Set-point mode
Main menu
Return to another level
If, in the main menu, no button has been pressed for
approx. 15 secs., an automatic return to one level above in
calibration mode occurs.
A return can be made by pressing button [▲] or [▼].
7. Operating elements of the calibrator/micro calibration bath
7.5.2 Switching off automatic control
For certain tasks, it is advantageous to switch off control (e.g.
to make settings on the calibrator or micro calibration bath).
In calibration mode, press button [P] for approx. 5 secs., this
opens the main menu.
The upper PV display will show OPEr.
In the lower SV display, the LED SET will blink.
Display in main menu
Press button [▲] or [▼] until OFF is displayed.
7.5.3 Switching on automatic control
The control is switched off when the following display is
shown:
On the upper PV display, the current reference temperature
and OFF are indicated alternately.
On the lower SV display, the currently-selected set
temperature is displayed.
Display with setting Control OFF
The control is switched back on by pressing button [P] for
approx. 5 secs., this opens the main menu.
The upper PV display will show ’rEG.
In the lower SV display, the LED SET will blink.
EN
Control OFF menu
Confirm with button [P].
On the upper PV display, the current reference temperature
and OFF are indicated alternately.
On the lower SV display, the currently-selected set
temperature is displayed.
Display with setting Control OFF
The control is now switched off and the reference
temperature will fall steadily, unless it is
corrected.
Display ‘rEG
Confirm switching the control on by pressing button [P].
Control is now activated. The calibrator or micro
calibration bath will default to calibration mode
and the set temperature will be reached.
7. Operating elements of the calibrator/micro calibration bath
7.5.4 Switching on manual control
Switch off the automatic control of the calibrator or micro
calibration bath, and reach the required temperature with
manual control.
Press button [P] for approx. 5 secs., this opens the main
menu.
EN
The upper PV display will show OPEr.
In the lower SV display, the LED SET will blink.
Display in main menu
Press button [▲] or [▼] until OPLO is displayed.
The upper PV display will show OPLO.
In the lower SV display, the LED SET will blink.
By pressing button [▲], the output power is increased.
By pressing button [▼], the output power is decreased.
By pressing button [▲] or [▼] the value is
increased or decreased by 0.1 %. If the keys are
held down for at least 1 sec., however, the value
increases or decreases more rapidly, and after
2 secs. even faster, so that the desired value can
be reached very quickly.
7.5.5 Switching off manual control
The manual control is switched on if the following display is
shown:
On the upper PV display, the current reference temperature
is indicated.
On the lower SV display, an H and the current set output
power in % is displayed.
Manual control OPLO menu
Confirm by pressing the button [P].
On the upper PV display, the current reference temperature
is indicated.
On the lower SV display, an H and the current set output
power in % is displayed.
Display with setting manual control OPLO
Display with setting manual control OPLO
The manual control is switched back off by pressing button
[P] for approx. 5 secs., this opens the main menu.
The upper PV display will show ’rEG.
In the lower SV display, the LED SET will blink.
Display in main menu
Confirm switching the automatic control on by pressing
button [P].
7. Operating elements of the calibrator/micro calibration bath
7.5.6 Setting and storing fixed set temperatures
In order to store the set temperature in the calibrator or micro
calibration bath, the appropriate set-point memory must be
opened.
In calibration mode, press button [P] for approx. 5 secs.,
this opens the main menu.
The upper PV display will show OPEr.
In the lower SV display, the LED SET will blink.
Operator menu OPEr
If button [P] is pressed again, this opens the groups level.
The upper PV display will show OPEr.
In the lower SV display, ’SP is shown and additionally LED SET will blink.
Select one of the four set-point memories SP1, SP2, SP3 or
SP4 using button [▲] or [▼].
By pressing button [P] the corresponding set-point memory
will then be opened.
In the upper PV display, the selected set-point memory e.g.
SP3 will blink.
On the lower SV display, the corresponding currentlyselected set temperature is displayed.
Input in set-point memory SP3
By pressing button [▲], the set temperature is increased.
By pressing button [▼], the set temperature is decreased.
By pressing button [▲] or [▼] the value is
increased or decreased by 0.01 °C [0.01 °F].
If the keys are held down for at least 1 sec.,
however, the value increases or decreases more
rapidly, and after 2 secs. even faster, so that the
desired value can be reached very quickly.
EN
’SP Group
If button [P] is pressed again, this opens the parameter
level.
The upper PV display will show ’SP.
In the lower SV display, the set-point memory SP1 and
additionally LED SET will blink.
Parameter for set-point memory SP1
By pressing button [P], the newly-set temperature is
accepted.
The set-point memory is left and the screen returns to the
parameter level.
To return to calibration mode, press button [▲] or [▼] for a
long time.
If no button has been pressed for approx.
15 secs., an automatic return to one level above
in calibration mode occurs.
7. Operating elements of the calibrator/micro calibration bath
7.5.7 Recalling the stored set temperatures
The set temperature can be called up from calibration mode.
Press button [U] for approx. 2 secs. The current set-point
memory will be opened.
On the upper PV display, the current reference temperature
is indicated.
EN
On the lower SV display, the set-point memory (SP1,
SP2, SP3 or SP4) is shown for 2 secs., and then the
corresponding currently-selected set temperature is
displayed.
It initially displays the set-point memory (SP1, SP2, SP3 or
SP4).
Then it displays the stored set temperature.
A simple temperature profile can be generated.
After switching on the calibrator or micro calibration bath, the
temperature profile will run automatically.
Ramp control and temperature profile
Heating gradient, SLor
The heating gradient, SLor, is active if the reference
temperature is lower than the set temperature.
Each calibrator model has a maximum heating output, and
thus only settings < than this heating power make sense and
actually increase the time taken to achieve a set temperature.
Display on calling the set temperature
In order to retrieve a different stored set point, press button
[U] again.
The selected temperature value will be immediately adopted
and approached.
7.5.8 Setting the ramp control and a temperature
profile
Using the ramp control, the time can be defined over
which the target temperature is achieved. This time may be
shorter or longer than that which the calibrator or the micro
calibration bath would normally require.
By changing the set temperature or turning on the calibrator
or micro calibration bath, it is automatically determined which
of the gradients to use (heating gradient, SLor, or cooling
gradient, SLoF).
In the calibrator or in the micro calibration bath, the dwell
time, dur.t, can be programmed so that the set temperature
reached is automatically switched from the set-point memory
SP1 to the set temperature in set-point memory SP2 after a
predetermined time.
7. Operating elements of the calibrator/micro calibration bath
Cooling gradient SLoF
The cooling gradient, SLoF, is active if the reference
temperature is higher than the set temperature.
Only settings that are under the heating power of the
calibrator have an effect on the cooling gradient.
with distilled water
CTM9100-150 as calibrator< 4 °C/min [< 7 °F/min]
CTM9100-150 as infrared calibrator< 4 °C/min [< 7 °F/min]
CTM9100-150 as surface calibrator< 4 °C/min [< 7 °F/min]
Calibrator model
< 6 °C/min [< 11 °F/min]
< 4 °C/min [< 7 °F/min]
Setting for SLoF
(heating)
CTD9100-450 / CTD9100-650
up to 300 °C [572 °F]
300 °C to 100 °C [572 °F to 212 °F]
CTB9100-225 with silicone oil 20 CS
200 °C to 50 °C [392 °F to 122 °F]
50 °C to 30 °C [122 °F to 86 °F]
CTB9100-225 with distilled water
90 °C to 50 °C [194 °F to 122 °F]
50 °C to 30 °C [122 °F to 86 °F]
< 10 °C/min [< 18 °F/min]
< 5 °C/min [< 9 °F/min]
< 4 °C/min [< 7 °F/min]
< 0,5 °C/min [< 1 °F/min]
< 2 °C/min [< 4 °F/min]
< 0,5 °C/min [< 1 °F/min]
The heating and cooling gradients and the dwell time can
be set via the parameter level, ’rEG. This is achieved by
pressing button P for approx. 5 secs., this opens the main
menu.
The upper PV display will show OPEr.
In the lower SV display, the LED SET will blink.
Operator menu OPEr
If button [P] is pressed again, this opens the groups level.
The upper PV display will show OPEr.
In the lower SV display, ’SP is shown and additionally LED SET will blink.
EN
The dwell time, dur.t, is active when the set temperature,
SP1, has been reached. Subsequently, the calibrator or micro
calibration bath automatically switches to set temperature
SP2.
If settings have been made for these three
parameters, the calibrator or the micro
calibration bath will not use the new values until
you either change the set temperature or until the
calibrator or the micro calibration bath has been
turned off and then on again.
Another approach would be to switch the
automatic control off before the parameter
change (see chapter 7.5.2 “Switching off
automatic control”), and then turning it back
on (see chapter 7.5.3 “Switching on automatic
control”).
’SP group
Select the group, 'rEG, by pressing button [▼].
The upper PV display will show OPEr.
In the lower SV display, ’rEG is shown and additionally LED
7. Operating elements of the calibrator/micro calibration bath
If button [P] is pressed again, this opens the parameter
level.
The upper PV display will show ‘rEG.
In the lower SV display, SLor will blink.
EN
Parameter for heating gradient, SLor
7.5.8.1 Setting the heating gradient
The heating gradient, SLor, is active if the reference
temperature is lower than the set temperature.
The setting range stretches from 99.99 °C/min to 0.00 °C/min
[99.99 °F/min to 0.00 °F/min].
The function is deactivated if SLor = InF (in no
Function) is set.
You are at the parameter level (as described in chapter
7.5.1 “Menu structure, parameter levels”).
The upper PV display will show ‘rEG.
In the lower SV display, SLor will blink.
By pressing button [▲], the heating gradient, SLor, will be
increased.
By pressing button [▼], the heating gradient, SLor, will be
decreased.
By pressing button [▲] or [▼] the value is
increased or decreased by 0.1. If the keys are
held down for at least 1 sec., however, the value
increases or decreases more rapidly, and after
2 secs. even faster, so that the desired value can
be reached very quickly.
By pressing button [P], the newly-set heating gradient, SLor,
is accepted.
The display returns to the parameter level and the other
parameters can be set.
If no button has been pressed for approx.
15 secs., an automatic return to one level above
in calibration mode occurs.
After the setting has been made, the calibrator
or the micro calibration bath will not use the
new values until you either change the set
temperature or the calibrator or the micro
calibration bath has been turned off and then on
again.
7.5.8.2 Setting the cooling gradient
The cooling gradient, SLoF, is active if the reference
temperature is higher than the set temperature.
The setting range stretches from 99.99 °C/min to 0.00 °C/min
[99.99 °F/min to 0.00 °F/min].
The function is deactivated if SLoF = InF (in no
Function) is set.
Parameter for heating gradient, SLor
Press button [P].
On the upper PV display, SLor will blink.
On the lower SV display, the corresponding currently-