Thermo Fisher Scientific pH 560 User Manual

Alpha pH 560
pH Controller
pH/mV/ºC meter
Preface
This manual serves to explain the use of the Thermo Scientific Alpha pH 560 Controller. The manual functions in
two ways, firstly as a step by step guide to help the user operate the instrument. Secondly, it serves as a handy reference guide. This instruction manual is written to cover many anticipated applications of the Alpha pH 560 Controller. If you have doubts in the use of the instrument, please do not hesitate to contact the nearest Authorised Distributor.
The information presented in this manual is subject to change without notice as improvements are made, and does not represent a commitment on part of Thermo Fisher Scientific.
Thermo Fisher Scientific cannot accept any responsibility for damage or malfunction of the unit due to improper use of the instrument.
Copyright ©2006 All rights reserved. Thermo Fisher Scientific Pte Ltd.
Thermo Scientific Alpha pH 560
Contents
Chapter 1
Chapter 2
Introduction .....................................................................................................1
Before You Begin ..............................................................................1
Intended Use..................................................................................... 1
Safety Instructions............................................................................. 1
Taking Out of Service .......................................................................2
Correct Disposal of the Unit ............................................................. 2
Getting Started................................................................................................ 3
Description of Instrument.................................................................3
Measurement and Control System ....................................................4
Connection Terminals ......................................................................4
Connectors:................................................................................. 4
Switching Between PT100 & PT1000 Temperature Sensors .........5
Remove Back Cover ....................................................................5
Remove Back PCBA ...................................................................5
Set Jumper J7.............................................................................. 6
Connecting pH/ORP Electrode ........................................................ 7
Connection Terminals ......................................................................7
Connecting Temperature Probe ..................................................7
Connect Potential Matching Pin (PMP) ..................................... 7
Installation ........................................................................................8
Mechanical Dimensions .................................................................8
Wall Mount ................................................................................... 9
Panel Mount ..................................................................................9
Display & Keypad........................................................................... 11
Display Overview......................................................................... 11
Mode Indicators........................................................................... 11
Status Annunciators .....................................................................12
Units of Measurement Indicators ................................................ 12
Key Functions................................................................................. 13
Chapter 3
Chapter 4
Thermo Scientific Alpha pH 560
Operation........................................................................................................14
Measurement Mode ........................................................................ 14
Menu Overview ..............................................................................15
Calibration Mode..........................................................................................16
Preparing the Controller & Electrode for Calibration .....................16
Entering pH/ORP Calibration Mode.............................................. 16
pH Calibration................................................................................ 17
For USA Standard Buffer
1-Point Calibration: ..................................................................17
2-Point Calibration: ..................................................................18
.............................................................17
For NIST Buffer ..........................................................................20
1-Point Calibration: ..................................................................20
2-Point Calibration: ..................................................................20
ORP Calibration............................................................................. 22
Temperature Calibration.................................................................23
Chapter 5
Chapter 6
Chapter 7
Chapter 8
Chapter 9
Setup Mode ................................................................................................... 24
Temperature Settings ...................................................................... 26
Configuration Settings ................................................................. 32
Technical Specifications ........................................................................... 36
List of Accessories ...................................................................................... 38
Troubleshooting ........................................................................................... 40
General Information .................................................................................... 41
Appendices ................................................................................................... 42
pH Buffer Values at Various Temperatures .................................. 42
Graphical Representation of the Function of Hysteresis ............... 43
General Instructions Concerning Controller Settings...................43
Abbreviations Used in LCD......................................................... 44
Thermo Fisher Scientific iii
Chapter 1

Introduction

Before You
Begin

Intended Use

Thank you for purchasing the Alpha pH 560 Controller.
The construction of the pH 560 Controller employs leading edge tech­nology and complies with safety regulations currently in force. Notwithstanding this, improper use could lead to hazards for the user or a third-party, and/or adverse effects on the plant or other equipment. Therefore, the operating instructions must be read and understood by the persons involved before working with the pH Controller.
The instruction manual must always be stored close at hand, in a place accessible to all people working with the pH Controller.
If you have questions, which are not or insufficiently answered in this instruction manual, please contact your authorized supplier. They will be glad to assist you.
Alpha pH 560 Controllers are intended solely for pH or ORP and temperature measurement, as described in this instruction manual.
Any other use, or use not mentioned here, that is incompatible with the technical specifications is deemed inappropriate. The operator is solely responsible for any damage arising from such use.
Other prerequisites for appropriate use include:
Comply with the instructions, notes and requirements set out in
this instruction manual.
Comply with all local safety regulations concerning safety at
work.
Comply with all information and warnings in the
documentation dealing with the products used together with the pH Controller (housings, sensors, etc.).
Comply with local environmental and operational conditions.
Safety
Instructions
Thermo Scientific Alpha pH 560 1
The Alpha pH 560 Controller should be installed and operated
only by personnel familiar with the instrument and who are qualified for such work.
A defective pH Controller must neither be installed nor put
into service.
The Alpha pH 560 must only be operated under the specified
operating conditions (see Page 36).
The Alpha pH 560 must not be repaired by the customer.
No modifications to the Alpha pH 560 are allowed. The
manufacturer/supplier accepts no responsibility for damage
caused by unauthorized modifications. The risk is borne entirely
by the user.
Taking Out of
Service
Correct Disposal
of the Unit
First disconnect the unit from the power supply and then undo
all electrical connections.
Remove the unit from the wall / panel.
When the Alpha pH 560 Controller is permanently taken out of service, obey the local environmental regulations for correct disposal or send the instrument to your local distributor, they will take care of proper disposal.
2 Thermo Scientific Alpha pH 560
Chapter 2

Getting Started

Description of
Instrument
The Thermo Scientific Alpha pH 560 Controller is used for measuring pH and temperature values. The pH values can be measured using industrial combination pH sensors. The temperature values can be measured using 3-wire Pt100 / Pt1000 sensors. The Controller can be used for applications such as water treatment and controlling, galvanic-decontamination, chemical processing, food processing, clean or wastewater control and neutralization processes.
The pH Controller has many user-friendly and safety features which include:
Push-button keypad for calibration and setup
Built-in non-volatile memory to ensure that calibration
and other information are not erased if power supply fails
Menu-driven program that simplifies setup
1 or 2 point calibration with selectable USA or NIST
standard pH buffer set
Automatic temperature compensation (ATC)
Manual temperature compensation setting without the
ATC probe, with independent setting for calibration and process temperature
High resolution ADC for precise measurement
Large dual display LCD for easy reading with clear
multiple annunciators, operational mode indicators and error indicators.
Two switching contacts as set-point relays
Limit (on/off) control mode
Separately adjustable high and low set-point hysteresis
(dead bands) to prevent chattering of relays around the set points
0 to 2000 seconds time delay adjustment on all relays –
minimizes false alarms
Backlight LCD display
Thermo Scientific Alpha pH 560 3
Measurement
and Control
System
A typical measurement system consists of:
A pH process Controller
A pH sensor with integrated or separate Pt100/Pt1000
temperature sensor
An appropriate measurement cable
An immersion, flow or process assembly
A final control element such as pump or valve
Connection
Terminals
Connectors:

Figure 2–1. Measurement and Control System

Remove the screws from the four corners at the back of the pH Controller. Remove the back cover. The connectors are exposed on the back PCBA as shown in the diagram below.
J11 – 24V DC power
J8 – 9V DC power
J9 – Relay connections
J10 – pH electrode & Temperature probe connections (wiring has
to be done in the detachable connector
4 Thermo Scientific Alpha pH 560
Switching Between
PT100 & PT1000
Temperature
Sensors
Remove Back Cover
Remove Back PCBA
Figure 2–2. Outer Side of Back PCBA
The Controller supports both Pt100 & Pt1000 (2-wire or 3-wire) temperature sensors. The default factory setting is Pt100. If you need to use Pt1000 temperature sensor, you have to change the jumper setting (J7) as described below.
Remove screws from the four corners at the back of the pH Controller. Remove the back cover.
Remove the screw located center of the back PCBA. Detach the back PCBA from the Controller. Turn over the back PCBA. Locate J7 jumper on the inner side of the back PCBA as shown in the figure below.
Thermo Scientific Alpha pH 560 5
Set Jumper J7
Figure 2–3. Inner Side of Back PCBA
Set the J7 jumper to required sensor (Pt100 or Pt1000) type.
6 Thermo Scientific Alpha pH 560
Connecting
pH/ORP
Electrode
1. If the pH/ORP electrode has a BNC connector, remove the BNC
connector from the cable.
NOTE: Oakton Instruments offers an optional ‘BNC to Spade Lug adapter’ (Order code: 05994-90) that can be used with pH/ORP electrode without removing the BNC connector.
2. Strip the insulation of the cable so that the bare wires are exposed
enough for connection as shown in diagram below.
Figure 2–4. pH/ORP Electrode Cable
NOTE: Make sure to strip inner black layer (screen) to expose the clear sheath.
3. Connect pH sensing wire to Pin 1 of J10 connector
4. Connect pH reference wire to Pin 2 of J10 connector
Connection
Terminals
Connecting Temperature
Probe
Connect Potential
Matching Pin (PMP)
For Automatic Temperature Compensated (ATC) pH readings, a 100Ω Pt RTD temperature probe (2-wire or 3-wire) can be connected to the Controller.
3-Wire Probe:
1. Connect PT100 compensate wire to Pin 5 of J10 connector
2. Connect PT100 sense wire to Pin 6 of J10 connector
3. Connect PT100 GND wire to Pin 7 of J10 connector
2-Wire Probe:
1. Short Pin 5 & 6 of J10 connector using a small piece of wire.
2. Connect PT100 sense wire to Pin 6 of J10 connector
3. Connect PT100 GND wire to Pin 7 of J10 connector
If using a pH electrode with a PMP, connect the additional wire (PMP) from the pH electrode to Pin 8 of J10 connector. This liquid electrical reference wire is only used when the pH Controller is configured to ‘Symmetrical mode of operation’. Refer page 14 for details on symmetrical mode of operation.
Thermo Scientific Alpha pH 560 7

Installation

Mechanical
Dimensions
Figure 2–5. Frontal View
Figure 2–6. Side View
8 Thermo Scientific Alpha pH 560
W
all Mount
Figure 2–7.
Panel Mount
Figure 2–8.
Thermo Scientific Alpha pH 560 9
Figure 2–9.
10 Thermo Scientific Alpha pH 560
Display &
Keypad
Display Overview
The Liquid Crystal Display (LCD) of Alpha pH 560 Controller has two alpha-numerical displays (Upper and a Lower).
Upper display: Measured pH, mV or relative mV value are
displayed when the Controller is in normal operation (measurement) mode.
Lower display: Measured temperature value is displayed when the
Controller is in normal operation (measurement) mode. In pH Calibration mode, standard pH buffer values are displayed here: while measured mV values are displayed in the ORP Calibration mode.
The two displays indicate function names, options & settings in Setup mode. Refer page 24 for more details.
The LCD also consists of various mode indicators, status annunciators and unit of measurement indicators.
Mode Indicators
Figure 2–10. LCD Display
MEAS
SETUP CAL
Measurement mode; blinks in Symmetric mode (Refer Page 14 )
Setup mode (Refer Page 24)
Calibration mode (Refer Page16)
Thermo Scientific Alpha pH 560 11
Loading...
+ 36 hidden pages