Thermo Sorvall T3 User manual

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Sorvall T3/G3
User’s Manual
Analyze Detect Measure Control
TM
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Sorvall T3/G3
User’s Manual
T3/G3
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Carefully read this manual before operating your instrument.
The validity of the guarantee is subject to the observation of the instructions and precautions described in this document.
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Thermo Fisher Scientific
MANUAL NUMBER
REV ECR/ECN DATE DESCRIPTION BY
a 11290098 02/07 Initial release
Preface
T3/G3 i
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ii T3/G3 Thermo Fisher Scientific
Packing List
75002385 T3 230V 50/60 Hz 75002386 T3 120V 60 Hz 75002396 T3 100V 50/60 Hz
75002387 RT3 230V 50/60 Hz 75002388 RT3 120V 60 Hz 75002397 RT3 100V 50 Hz 75002399 RT3 100V 60 Hz
75003432 G3 230V 50/60 Hz 75003431 G3 120V 60 Hz 75003428 G3 100V 50/60 Hz
75003434 RG3 230V 50/60 Hz 75003433 RG3 120V 60 Hz 75003429 RG3 100V 50 Hz 75003444 RG3 100V 60 Hz
Item number Quantity Check
Centrifuge
11290098 User manual 1
CE Declaration of compliance 1
Manual lid opening instructions 1
Imbalance protection instructions 1
64227001 Mains cord 1
26227005 Toolbox:
11210935 • Rotor removal tool 1
85241084 • Emergency unlooking tool 1
86000897 • 12 and 13 mm wrench 1
For missing parts call your nearest Thermo representative
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T3/G3 iiiThermo Fisher Scientific
WEEE Compliance
WEEE Compliance. This products is required to comply with the
European Union’s Waste Electrical & Electronic Equipment (WEEE) Directive 2002/96EC. It is marked with the following symbol. Thermo Fisher Scientific has contracted with one or more recycling/disposal companies in each EU Member State, and this products should be dis­posed of or recycling through them. Further information on Thermo Fisher Scientific’s compliance with these Directives, the recyclers in your country, and information on Thermo Fisher Scientific products which may assist the detection of substances subject to the RoHS Directive are available at www.thermo.com/WEEERoHS
WEEE Konformittät. Dieses Produkt muss die EU Waste Electrical & Electronic Equipment (WEEE) Richtlinie 2002/96ECerfüllen. Das Produkt ist durch folgendes Symbol gekennzeichnet. Thermo Fisher Scientific hat Vereinbarungen getroffen mit Verwertungs­/Entsorgungsanlagen in allen EU-Mitgliederstaaten und dieses Produkt muss durch diese Firmen widerverwetet oder entsorgt werden. Mehr Informationen über die Einhaltung dieser Anweisungen durch Thermo Fisher Scientific, die Verwerter und Hinweise die Ihnen nützlich sein können, die Thermo Fisher Scientific Produkte zu identizfizieren, die unter diese RoHS Anweisung fallen, finden Sie unter
www.thermo.com/WEEERoHS
Conformità WEEE. Questo prodotto deve rispondere alla direttiva dell’Unione Europea 2002/96EC in merito ai Rifiuti degli Apparecchi Elettrici ed Elettronici (WEEE). È marcato col seguente simbolo. Thermo Fisher Scientific ha stipulato contratti con una o diverse società di riciclaggio/smaltimento in ognuno degli Stati Membri Europei. Questo prodotto verrà smaltito o riciclato tramite queste medesime. Ulteriori informazioni sulla conformità di Thermo Fisher Scientific con queste Direttive, l’elenco delle ditte di riciclaggio nel Vostro paese e informazioni sui prodotti Thermo che possono essere utili alla rilevazione di sostanze soggette alla Direttiva RoHS sono disponibili sul sito www.thermo.com/WEEERoHS
WEEE Conformidad. Este producto requiere cumplir con la Directiva 2002/96EC WEEE (residuos de quipos electricos y electronicos). Este producto esta marcado con el simbolo WEEE, como se describe. En cada Estado Miembro de la Union Europea (EU), Thermo Fisher Scientific ha contratado con diversas companias para disponer y/o re­ciclar los residuos de equipos electricos y electronicos. Existe informa­tion adictional acerca de la conformidad de Thermo Fisher Scientific con esta Directiva, incluyendo los nombres de las diversas companias
Great Britain
Deutschland
Italia
Espana
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iv T3/G3 Thermo Fisher Scientific
WEEE Compliance
autorizadas para disponer/recyclar nuestros productos. Adicionalmente suministramos informacion acerca de los productos de Thermo Fisher Scientific que puedes asistir en la deteccion de substancian mensionades en la directiva RoHS, explicado en www.thermo.com/WEEERoHS
Conformité WEEE. Ce produit doit être conforme à la directive euro­péenne (2002/96EC) des Déchets d’Equipements Electriques et Electroniques (DEEE). Il est marqué par le symbole suivant. Thermo Fisher Scientific s’est associé avec une ou plusieurs compagnies de recy­clage dans chaque état membre de l’union européenne et ce produit devrait être collecté ou recyclé par celles-ci. Davantage d’informations sur la conformité de Thermo Fisher Scientific à ces directives, les recy­cleurs dans votre pays et les informations sur les produits Thermo Fisher Scientific qui peuvent aider la détection des substances sujettes à la directive RoHS sont disponibles sur www.thermo.com/WEEERoHS
France
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T3/G3 vThermo Fisher Scientific
Declaration of compliance
We, Thermo Electron Industries S.A.S., Z.I. d’Aze Bellitourne 53200 CHATEAU-GONTIER, France, declare that the instrument defined here below complies with the following European directives:
Nous, Thermo Electron Industries S.A.S., Z.I. d’Aze Bellitourne 53200 CHATEAU-GONTIER, France, déclarons que le matériel désigné ci­après est conforme aux directives européennes suivantes:
Wir, Thermo Electron Industries S.A.S. , Z.I. d'Aze Bellitourne 53200, CHATEAU-GONTIER, France, erklären dass das hier beschriebene Gerät sich in Übereinstimmung mit folgenden europäischen Richtlinien befindet:
Nostros, Thermo Electron Industries S.A.S., Z.I. d’Aze Bellitourne 53200 CHATEAU-GONTIER, France, declaramos que el instrumento bajo descrito está fabricado según las especificaciones establecidas por las siguientes normas europeas:
Nós, Thermo Electron Industries S.A.S., Z.I. d’Aze Bellitourne 53200 CHATEAU-GONTIER, France, declaramos que o instrumento aqui apresentado está de acordo com as normas européias abaixo listadas:
Noi, Thermo Electron Industries S.A.S., Z.I. d’Aze Bellitourne 53200 CHATEAU-GONTIER, France, dichiariamo che lo strumento sotto descritto è conforme alle seguenti Direttive europee:
Machinery: 98 / 37 / CEE
Low voltage: 72 / 23 / CEE - 93 / 68 CEE
EMC: 89 / 336 CEE - 92 / 31 CEE - 93 / 68 CEE
Safety standard: EN 61010-1 - EN 61010-2-020
Declaration of compliance
Declaration de conformite
Konformitätserklärung
Declaración de conformidad
Declaraçao de conformidade
Dichiarazione di conformità
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vi T3/G3 Thermo Fisher Scientific
Guarantee Terms
Thermo guarantees that this unit is free from defects in materials and workmanship when it leaves the factory, and will replace or repair the unit if it proves defective in normal use or during service for a period of ONE YEAR from the delivery.
This guarantee is invalid if the unit is incorrectly used, poorly serviced or neglected, mis-used or accidentally damaged.
There is no explicit guarantee other than as stated above.
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T3/G3 viiThermo Fisher Scientific
For further information, assistance or service
United States of America
Tel.: +1 888 213 17 90 Tel.: +1 866 984 37 66
Canada or Latin America
Tel.: +1 866 213 17 90 Fax: +1 866 984 37 66
China (Shanghai)
Tel.: +86 21 68 65 45 88 Fax: +86 21 6445 7907, +86 21 6445 7830
India (Mumbai)
Tel.: +91 22 5542 9494 Fax: +91 22 5542 9495
Japan
Tel.: +81 454 53 9220 Fax:+ 81 454 53 9222
Other Asia-Pacific Countries
Tel.: +852 28 85 46 13
Austria
Tel.: +43 (1) 80 14 00
France
Tel.: +33 1 69 18 77 77 +33 2 28 03 20 00
Belgium
Tel.: +32 24 82 30 30
Germany
Tel.: +49 61 84 90 69 40 Fax: +49 61 03 40 81 012
Finland
Tel.: +35 89 32 91 00
Italy
Tel.: +39 02 95 05 91
Netherlands
Tel.: +31 7 65 71 44 40
Russia/Cis
Tel.: +7 09 52 25 11 15
Spain and Portugal
Tel.: +34 9 32 23 31 54
Switzerland
Tel.: +41 (1) 4 54 12 12
United Kingdom and Ireland
Tel.: +44 87 06 09 92 03
Other Europe, Middle East, or Africa
Tel.: +49 61 8490 6940 Tel.: +33 2 2803 2000
In Other Countries:
Contact your local THERMO products distributor or agent.
E-mail Technical Service Representative for products at:
techsupport.led.asheville@thermo.com
Visit our web site at: www.thermo.com
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viii T3/G3 Thermo Fisher Scientific
Contents
Use and Function........................................................................................1-1
User Manual......................................................................................1-1
Warning Symbols ..............................................................................1-1
Description ......................................................................................1-1
Refrigeration and Heating Systems....................................................1-2
Drive System ....................................................................................1-3
Safety Interlock System ....................................................................1-3
Imbalance Detection System ............................................................1-3
Relative Centrifugal Force ................................................................1-4
Specifications ............................................................................................2-1
Dimensions and Weight....................................................................2-1
Centrifugation Specifications ............................................................2-1
Electrical Specifications ....................................................................2-2
Installation ..................................................................................................3-1
Environmental Conditions................................................................3-1
Unpacking ........................................................................................3-1
Positioning........................................................................................3-2
Mains Supply ....................................................................................3-2
Lid Opening and Rotor Checking ....................................................3-3
Manual Lid unlocking Procedure ......................................................3-3
Performance and Accessories ............................................................3-5
TTH751 Swing-out Rotor - Cat. N°: 11210936 ..............................3-5
Angle Rotors ....................................................................................3-8
Instructions for Use....................................................................................4-1
Controls and Indicators ....................................................................4-1
Display Screens ................................................................................4-2
Control Panel Functions ..................................................................4-2
Control Panel Indicators ..................................................................4-3
Description of Certain Events with Respect to the Control System ....4-4
Preparing the First Run of the Day ..................................................4-6
Sample Loading ................................................................................4-6
Chapter 1
Chapter 2
Chapter 3
Chapter 4
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T3/G3 ixThermo Fisher Scientific
Contents
Hazards, Precautions and Limitations of Use ......................................5-1
IEC 1010-2-020................................................................................5-1
Cautions............................................................................................5-1
Speed Control ..................................................................................5-2
Operational Limitations ....................................................................5-2
Aerosol Risks ....................................................................................5-2
Service and Maintenance ........................................................................6-1
Periodic Cleaning..............................................................................6-1
Contamination Hazards ....................................................................6-1
Disinfection ......................................................................................6-2
Radioactive Decontamination ..........................................................6-2
Power Supply Circuit Breaker............................................................6-3
Rotor Removal..................................................................................6-3
Trunnion Lubrication........................................................................6-3
Chemical Compatibility Table for Rotors, Tubes and Accessories......6-4
Disposal of Product....................................................................................7-1
Chapter 5
Chapter 6
Chapter 7
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Chapter 1 Use and Function
The user manual is part of the centrifuge, and contains important information for your safety and for the best use of the equipment
Always keep the manual close to the appliance and in a safe place, so that it is always available. Thermo strongly recommends that all users read this manual carefully.
The following symbols are provided to help the operator take advantage of the protection afforded by the equipment and to warn of potential danger.
On the main switch, allows centrifuge to operate. L
On the main switch, disconnects the centrifuge from the main power supply. L
Only authorized personnel can touch the parts close to this symbol and, in any case, only after switching off the main power supply.
Coming in contact with high voltages could cause severe injuries.
L
In this manual, this symbol means that you will find important information for safety, which if unobserved could result in damage to the appliance and/or harm to the operator. L
In this manual, this symbol means that you will find important information about minimizing biological risk: if unobserved the result could be harm to the operator. L
The T3/G3 centrifuges are designed for laboratory use.
They will separate the components of fluids into layers of varying density by subjecting them to high forces.
Centrifugal force provided by the centrifuge can also be used to drive solvents and low molecular weight solutes through the membrane of a filtering device. Retained macrosolutes will therefore be found above the membrane.
User Manual
Warning Symbols
Description
T3/G3 1-1Thermo Fisher Scientific
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Chapter 1
Use and Function
1-2 T3/G3 Thermo Fisher Scientific
Relative Centrifugal Force (RCF) generated by a rotor is directly proportional to its sedimentation useful radius and to the value of its speed squared.
A control system permits the user, through an extremely intuitive control panel, to set and control the speed, the g-force, the temperature (on the thermostated and refrigerated versions) and the run time, as well as to view different messages and warnings.
The T3/G3 Rare ventilated unit. A permanent air circulation reduces the heat level in the bowl.
However the temperature in the bowl can reach 10 °C above the ambient temperature after hours of continuous operation.
The T3/G3 Rare equipped with a powerful refrigeration system that allows samples to be processed at low temperature. The refrigerant, R134a, is free of CFC (Chloro-Fluoro-Carbons) in accordance with the Montreal Protocol directions for preservation of the ozone layer in the atmosphere.
The actual temperature in the bowl is continuously displayed on the front panel of the centrifuge. Under certain conditions (high speed, long duration runs) the sample temperature can be higher than the bowl temperature on the display. In this case, the user may compensate manually after empirical determination of the temperature differential.
The lid should remain closed when the refrigeration system is in use to avoid condensation.
The centrifuge has a rubber hose that allows condensation to be drained from the bowl. The drain hose exits at the back of the machine. Near the drain hose you can find the following label:
To remove condensation, please follow this procedure:
Switch off the centrifuge and disconnect the power.
Put a small basin under the hose.
Unplug the hose.
Refrigeration and
Heating Systems
Condensation drain on
refrigerated units
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Chapter 1
Use and Function
Drain the centrifuge bowl.
Insert the plug back into the hose.
Attention Do not remove the plug from the drain hose during centrifugation. L
A three phase brushless motor drives the rotating equipment. The rotor is contained in a sealed, armor plated centrifugation chamber.
The brushless motor requires no maintenance. A control system ensures the correct drive speed, which is continuously monitored.
The T3/G3 centrifuge series are equipped with an interlock system that assures two basic safety features:
The run cannot be started if the lid is not correctly closed.
The centrifuge lid cannot be opened if the rotor is running.
The centrifuge will not operate until the lid is closed and latched in place.
The lid remains latched until the rotor stops spinning. The lid access lamp indicates when the rotor has stopped: consequently the handle on the right hand side of the centrifuge can be used to open the lid.
If a power failure occurs, access to the samples in the centrifuge is possible via a manual lid opening procedure (see appropriate paragraph). For this operation a special tool (supplied with the centrifuge) is required.
Bypass the interlock system only under emergency conditions as the rotor could still be rotating.
The T3/G3 centrifuge series are equipped with a load imbalance detector.
In case of excessive imbalance, the load imbalance indicator LED is illuminated and the brake is applied immediately. The rotor will be decelerated to rest in few seconds.
As soon as the motor stops, open the centrifuge and redistribute the samples to produce an equal weight on diametrically opposite sides.
If the message persists, despite your efforts to balance the load, call your Thermo Service representative.
Drive System
Safety Interlock
System
Imbalance Detection
System
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Chapter 1
Use and Function
1-4 T3/G3 Thermo Fisher Scientific
Relative Centrifugal
Force
Note Imbalance tolerance depends upon the rotor in use. The
centrifuge will tolerate 15 gr. of imbalance with the TTH751 rotor equipped with standard buckets. Carefully balance the sample load to avoid actuating the imbalance detection system. If the protection has not been removed from the imbalance detection device during installation, the centrifuge will consider this as an imbalance situation and will not operate.
Relative Centrifugal Force (RCF), at the circumference of a rotor and bucket combination, is directly proportional to the speed (r.p.m.) and radius of the rotor. Therefore, a greater r.p.m. and/or a larger radius produces a greater RCF and improved faster separation of substances. The centrifuge control system carries out and displays the results of all calculations related to speed, radius and RCF.
Note : The value introduced for the radius can be adjusted to allow for position within the tube such as at a boundary. Maximum radii are quoted in the specifications tables. Use of improper radius will adjust the speed setting, automatically applying the wrong RCF.
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T3/G3 2-1Thermo Fisher Scientific
Chapter 2 Specifications
Dimensions and Weight
T3 G3 RT3 RG3
Product Dimensions
Height - lid open (cm / in) 92/ 36.2 134/ 58.8 92/ 36.2 134/ 58.8
Height - lid closed (cm / in) 42/ 16.5 86/ 33.8 42/ 16.5 86/ 33.8
Width (cm / in) 58/ 22.8 58/ 22.8 85/ 33.5 58/ 22.8
Depth (cm / in) 66/ 26.0 66/ 26.0 66/ 26.0 66/ 26.0
Weight unpacked (kg / lb.) 80/176 95/209 106/233 115/253
Packing
Height (cm / in) 50/ 19.7 99/ 38.9 50/ 19.7 99/ 38.9
Width (cm / in) 70/ 27.6 68/ 26.7 97/ 38.2 68/ 26.7
Depth (cm / in) 67/ 26.4 78/ 30.7 67/ 26.4 78/ 30.7
Weight packed (kg / lb.) 91/201 120/264 116/256 145/319
Centrifugation Specifications
T3/G3 RT3/RG3
Max capacity Swing-out (4x750 mL) 3000 mL (4x750 mL) 3000 mL
Fixed Angle (8x100 mL) (8x100 mL)
Max density 1200 kg/m3 1200 kg/m3
Max load 3.6 kg 3.6 kg
Max speed Swing-out 4000 rpm 4500 rpm
Fixed Angle 7800 rpm 8000 rpm
Max RCF Swing-out 3810 x g 4822 x g
Fixed Angle 9115 x g 9588 x g
Max noise < 66 dBA < 62 dBA
T3/G3 RT3/RG3
Microprocessor control yes yes
Programs (direct recall) 5 5
Speed set/display Range 500 - 7800 500 - 8000
Step 10 rpm at less than 1000 rpm 10 rpm at less than 1000 rpm
100 rpm at above 1000 rpm 100 rpm at above 1000 rpm
Accuracy ± 20 rpm (display) ± 20 rpm (display)
RCF set/display Range 20 - 9200 20 - 9600
Step 1 x g 1 x g
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2-2 T3/G3 Thermo Fisher Scientific
Chapter 2
Specifications
T3/G3 RT3/RG3
Accuracy ± 1 x g ± 1 x g
Timer set/display 30 s - 99 min + continuous 30 s - 99 min + continuous
Temperature set/display - -9°C to +40°C -9°C to +60°C
Acceleration rates 5 5
Braking rates 5 + inertial 5 + inertial
Drive system direct direct
Brushless induction motor yes yes
Electrical specifications
T3/G3 RT3/RG3
Nominal operating voltage 230V 230 V ±10% 230 V ±10%
120V 120 V ±10% 120 V ±10%
Power requirements (maximum) 1200 W 1500 W
Heat output (maximum) 3750 BTU / h 4435 BTU / h
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T3/G3 3-1Thermo Fisher Scientific
Environmental
Conditions
Unpacking
Chapter 3 Installation
General conditions accepted for centrifuge transport and storage are:
Ambient temperature -20°C to +50°C.
Relative humidity up to 90%.
General conditions accepted for operating the centrifuge safely are:
Indoor use.
Temperature: 5 °C to 40 °C.
Maximum relative humidity of 85%.
Maximum altitude: 2000 m
Installation category: II
Polution degree: 2
Due to the weight of the machine, all lifting and transporting must be carried out using proper handling equipment (i.e. fork lift trolley) that complies with current regulations, and by people having undergone the necessary training.
Thermo strongly recommends that all operators comply with the local laws and regulations on safety and health in the workplace. The machine must be supported from underneath. If it has to be transported without its pallet, for example on a staircase, professional handling assistance is required. L
Unpack the centrifuge, carefully removing any possible accessories and the material supplied for ordinary operations and maintenance.
Check the contents of the package using the packing list provided above.
Keep the packaging until the centrifuge has been tested and found fully functional.
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3-2 T3/G3 Thermo Fisher Scientific
Chapter 3
Installation
Positioning
Benchtop Units
Floor standing units
Main Supply
Lid Opening and
Rotor Checking
The machine must be installed in a dust and corrosion free room.
Leave a 30 cm / 12 in. space free on each side of and behind the machine for safety reasons, proper ventilation and maximum cooling performances. L
Place the centrifuge on a bench top, which must be rigid, horizontal and sufficiently strong to support the centrifuge’s weight and small vibrations.
Place the centrifuge on a horizontal floor.
Check mains and frequency: they must correspond to the values shown on the instrument identification label.
For your safety, check that mains wiring is effectively grounded. Thermo declines all responsibility for any damages due to non­grounding of the machine. L
Remember that in order to respect the electrical safety standards related to protection against indirect contact, the supply of power to the instrument must be via a power socket fitted with a protection device ensuring automatic cut-off in the case of an insulation fault. A supply fitted with a circuit breaker of the correct rating complies with this requirement.
Ensure that the centrifuge has been switched ON. Pull the handle on the centrifuge right side towards the front of the unit : the lid is automatically unlocked and opens.
In the case of a mains power outage, opening of the lid is prevented by the lid lock safety device. It is recommended to wait for the mains power to be switched back on so that this safety device enables the lid to be unlocked (refer to 3.6 for manual lid opening).
Carefully clean the inside of the centrifugation chamber removing any packing residues. In fact, due to air turbulence, solid particles accidentally left in the centrifugation chamber create excessive wear of the chamber itself and of the outer rotating equipment surface. L
To install the rotor:
Check that the motor shaft and rotor are clean
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T3/G3 3-3Thermo Fisher Scientific
Chapter 3
Installation
Manual Lid Unlocking
Procedure
Put the rotor on the motor shaft
Secure the rotor on the shaft by turning the hexagonal nut counter­clockwise (with the supplied tool)
Verify that the rotor cannot be removed by trying to pull it (gently) off the shaft.
In case you are using a swing-out rotor:
Gently grease the trunnions
Put the buckets on the trunnions after verifying that the weight of the buckets is identical (the weight is engraved on the bottom of each bucket).
In the event of mains non-availability or power failure, opening of the lid is prevented by the lid locking safety device. It is recommended that the user waits for the mains to be switched back on so that this safety device enables the lid to be unlocked.
Manual lid unlocking must only be done by someone informed of the possible danger and of the necessary precautions.
Rotating parts are a risk as they could come in contact with the user or be ejected. There is particularly high risk of injury if:
The user attempts to manually stop the rotor
Any object falls inside the centrifugation chamber while the rotor is running. L
Manual lid unlocking may be necessary under a very limited number of conditions, such as the urgent recovery of critical samples that could be damaged if left in the centrifuge rotor.
In this case the lid can be opened by using the special tool supplied with the centrifuge.
Always set the power switch to the OFF position before performing this manual procedure, even in the case of a mains power outage. L
Should the emergency occur due to power failure during centrifugation wait at least 10 minutes for the end of the rotor rotation. In spite of the absence of noise, the rotor could still be rotating when you need to open the lid manually. Upon opening, lift the lid by hand and observe the rotor (be careful in this operation): if it is still rotating, close the lid and wait.
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3-4 T3/G3
Thermo Fisher Scientific
Chapter 3
Installation
The protection sticker must be replaced after it has been pierced (item N° 85241772).
Figure 1. Insert the unlocking tool horizontally into the hole on the right hand side of the instrument.
Figure 2. While pressing up with your finger, to press down with the unlocking tool, pull the lid lever toward you:
the lid opens upwards.
!
En cas de nécessité, pour le déverrouillage manuel du couvercle,
attendre 10 min. ou l’arrêt du rotor avant d’utiliser l’outil
spécifique fourni à cet effet.
Cette étiquette, après avoir été percée, doit être
changée. If it is necessary to open the lid manually, wait 10 min. or until the rotor has stopped rotating, before using the lid opening tool provided. This label must be changed once it has been pierced.
Percer ici avec l'outil
Pierce here
with tool
85241772
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T3/G3 3-5Thermo Fisher Scientific
Chapter 3
Installation
Performance and Accessories
TTH 751 - Swing-out Rotor - Cat. N°: 11210936
• 4500 rpm /4822 x g
• For 4-750 mL bottles
• Up to 148-5 mL tubes
• Up to 16 standard microplates
• Certified sealed accessories are available
11174154 Standard buckets (4) Inserts: see table
81005750 750 ml bottles (6)
85240471 Cushion (4) - for 750 ml bottles
11174218 Sealed buckets (4) Inserts: see table
81005750 750 ml bottles (6)
85240471 Cushion (4) - for 750 ml bottles
11175372 Bucket - for CORNING 250 ml conical bottles
11175378 Sealed bucket - for 250 ml conical bottles
11175370 Bucket - for Nalgene 500 ml flat
11175371 Adapters (4) - for 250 ml conical bottle in 11175370
11210823 Microplate carriers (4)
11174207 Rubber cushion - for flexible microtiter plates
11174223 Sealed microplate carriers (4)
11174207 Rubber cushion - for flexible microtiter plates
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3-6 T3/G3 Thermo Fisher Scientific
Chapter 3
Installation
Inserts Available for the Following Buckets
- 11174154 Standard buckets (4)
- 11174218 Sealed buckets (4)
T3/G3 RT3/RG3
Cat. N° Color of insert Insert Rotor Max Tube Max* Tube Max Max Max Max Max
(set of 4) or type Capacity Capacity Ø [mm] tube height volume Radius Speed RCF Speed RCF
[mm] [mL] [mm] [rpm] [x g] [rpm] [x g]
11174201 Black / light blue 30 120 11.5 40 1.5 / 2 160 4000 2862 4500 3622
11174206 Black / coral 12 48 16.5 40 4 chlamydia 184 4000 3291 4500 4166
vials
11174205 Black / beige 9 36 18 40 4 chlamydia 184 4000 3291 4500 4166
vials
11174157 Black / grey 37 148 12.5 100 5 ria 172 4000 3077 4500 3894
11174193 Black / grey decanting - 12.5 - 5 decant 172 4000 3077 4500 3894
11174158 Black / light blue 30 120 13.5 100 6 rnd/flat 172 4000 3077 4500 3894
11210821 Black 21 108 13.5 107 10 vac 172 4000 3077 4500 3894
11174208 Black / orange 12 48 16.5 125 10 flat 184 4000 3291 4500 4166
11174188 Beige 12 36 18 120 10 flat 172 4000 3077 4500 3894
11174161 Brown 7 28 17.7 134 15 vac 185 4000 3309 4500 4188
11177573 Black 12 unsealed 48 18 122 15 con 188 4000 3363 4500 4256
1175781 Black 10 40 18 122 15 con 188 4000 3363 4500 4256
11174190 Orange 12 48 16.5 125 15 184 4000 3291 4500 4166
11174163 Coral 12 48 22.2 108 20 177 4000 3166 4500 4007
11174186 Dark red 7 28 30 115 25 flat 172 4000 3077 4500 3894
11174164 Dark red 7 28 30 115 50 rnd 182 4000 3256 4500 4120
11174529 Black 7 unsealed 28 30 116 50 con 185 4000 3309 4500 4188
11177572 Black 5 20 30 116 50 con - 4000 3363 4500 4256
11174199 Light blue 4 16 30 120 50 flat 172 4000 3077 4500 3894
11210560 Light blue 7 28 28 30 177 4000 3166 4500 4007
11174165 Dark blue 4 16 35 120 50 185 4000 3309 4500 4188
rnd/skirted
11174166 Dark green 2 8 45 118 100 185 4000 3309 4500 4188
11174167 Turquoise 1 4 63 134 250 flat 185 4000 3309 4500 4188
flacon con
11174192 Navy blue 1 4 80.5 125 450 rnd 185 4000 3309 4500 4188
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T3/G3 3-7Thermo Fisher Scientific
Chapter 3
Installation
Inserts Available for the 11175370 Bucket - for Nalgene 500 ml Flat:
T3/G3 RT3/RG3
Cat. N° Color of insert Insert Rotor Max Tube Max* Tube Max Max Max Max Max
(set of 4) or type Capacity Capacity Ø [mm] tube height volume Radius Speed RCF Speed RCF
[mm] [mL] [mm] [rpm] [x g] [rpm] [x g]
11175371 - 1 4 - - 250 con 208 4000 3721 4500 4709
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3-8 T3/G3 Thermo Fisher Scientific
Chapter 3
Installation
Angle rotor
• 8 tubes 100 mL
• 8000 rpm / 9588 x g
• 35° angle
Cat. No. Insert capacity Max tube Ø (mm) Accessory description
64662300 1 16.5 Set of 8 adaptors for 10 mL vac tubes
Angle rotor
• 10x50 mL tubes Ø 34mm
• L min/max 97/115mm
• 8000 rpm / 9302 x g
• 35° angle
• conical bottom
CD 100 - Angle Rotor
Cat. N°: 11210937
CD 50c - Angle Rotors
Cat. N°: 11210938
Page 29
Chapter 4 Instructions for Use
Controls and Indicators
All the controls are located on the front panel. The front panel is an intuitive interface: no previous operational knowledge is necessary; every parameter can be set by pressing the cursor key (or rotating the knob) from the minimum to the maximum and viceversa. All parameters can be accessed and changed both during operation and while the machine is at rest.
T3/G3 4-1Thermo Fisher Scientific
Buttons
1 - 4 Program Keys 5 Pre Cooling 6 Speed/RCF Toggle 7 Time/Radius Toggle 8 Acceleration rate set 9 Deceleration rate set 10 Stop Run 11 Pulse Run 12 Start Run 13 Temperature set (R only)
Display Screens
15 Display: speed/RCF 16 Display: time/raduis 17 Display: accel./decel. rates/temp. (R mod.)
LED Lights
1a Program 1 Indicator 2a Program 2 Indicator 3a Program 3 Indicator 4a Program 4 Indicator 5a Program Precooling Indicator 8a Acceleration Indicator 9a Deceleration Indicator 14 Lid Opening allowed Indicator 18 Speed Indicator 19 RCF Indicator 20 Time Indicator 21 Radius Input Indicator
1 1a 2 2a 15 18 16 20 8a 9a 17 11 14
3 3a 4 4a 6 19 7 21 8 9 13 5a 5 12 10
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4-2 T3/G3 Thermo Fisher Scientific
Chapter 4
Instructions for Use
Display Screens
Screen Description
Screen (15) This screen displays the set speed (rpm) or RCF (x g) for the given program when the centrifuge is
at rest, depending on which parameter is selected During a run, this screen displays actual speed
or RCF.
Screen (16) This screen displays either the set run time or the centrifugal radius when the centrifuge is at rest,
depending on which parameter is selected.
During a run, this display shows only time remaining (timed runs) or time elapsed (during
deceleration, ‘hold’ runs and ‘pulse’ runs).
Screen (17) This screen displays either the acceleration or the deceleration profile selected for the given
program. The value of the acceleration profile is displayed either during acceleration or when the
acceleration set button (8) is pressed. The value of the deceleration profile is displayed either
during deceleration or when the deceleration set button (9) is pressed.
Screen (17) on the R units This screen displays either the acceleration or the deceleration profile selected for the given
program. The value of the acceleration profile is displayed either during acceleration or when the
acceleration set button (8) is pressed. The value of the deceleration profile is displayed either
during deceleration or when the deceleration set button (9) is pressed.
In addition, it shows the temperature in the bowl of the centrifuge. When the centrifuge is at rest, the
set bowl temperature is displayed (°C). During a run, the actual bowl temperature is displayed (°C).
Control Panel Functions
Function Keystroke sequence and description
Start cycle Press the start button (12).
Stop cycle, immediate Press the stop button (10)
Pulse Press the pulse button (11) and hold. The centrifuge will accelerate the rotor to the speed setting of
the active program. When the button is released, the rotor will be decelerated to rest.
Set speed When the LED next to ‘RPM’ (18) is illuminated, the upper display shows speed values. To
increase/decrease the speed values, press on the corresponding up/down arrows.
Set RCF When the LED next to ‘G’ (19) is illuminated, the upper display shows RCF values. To
increase/decrease the RCF values, press on the corresponding up/down arrows.
When using RCF as a control/display value, make sure the correct centrifugal radius is entered into
the control system (see below). If an incorrect radius value is in the control system, the RCF value
displayed will not be accurate.
Set run time When the LED next to ‘TIME’ (20) is illuminated, the middle display shows time values. To
increase/decrease the run time values, press on the corresponding up/down arrows.
Set centrifugal radius When the LED next to ‘RADIUS’ (21) is illuminated, the middle display shows the value of the cen-
trifugal radius in millimeters. To increase/decrease the centrifugal radius, press on the correspon-
ding up/down arrows. This parameter can only be viewed and set while the centrifuge is at rest.
It is essential that this value be correct for the RCF control/display function to be accurate. The cor-
rect value of the centrifugal radius depends on the combination of rotor/buckets/adapters being
used.
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T3/G3 4-3Thermo Fisher Scientific
Chapter 4
Instructions for Use
Function Keystroke sequence and description
Set acceleration profile When the button (8) is pressed, the lower display (17) shows the number corresponding to the
acceleration profile currently registered (1 to 5 : 5 being the fastest).
To change the value, press the corresponding up/down arrows.
Set deceleration profile When the button (9) is pressed, the lower display (17) shows the number corresponding to the
deceleration profile currently registered
(0= The rotor, from 2000 rpm, will coast to a stop.
1 to 5: 5 being the fastest).
To change the value, press the corresponding up/down arrows.
Set temperature (R only) To increase/decrease the temperature set values, press on the corresponding up/down arrows.
To pre-program the centrifuge There are five available memory locations for pre-programmed protocols. Each corresponds to one
of the five memory buttons (1-5).
To enter/save a program into one of the locations, press the memory button corresponding to the
desired program position. The corresponding LED (1a-5a) will be illuminated. While the LED is illu-
minated, enter the desired parameter values. These values are automatically saved in memory.
To lock a program To lock a program, press and hold the corresponding button for several seconds until the correspon-
ding LED begins to flash. Release the button, and the program is locked. Parameters of the program
cannot be changed.
To unlock a program To unlock a program (when a program is locked, the associated LED flashes), press and hold the
corresponding button for several seconds until the associated LED stops flashing. Release the but-
ton, and the program is unlocked.
Precooling program Select the Precooling program pressing button 5, the LED 5a will light on.
Only temperature setting is required, Speed and Time are defined by the software according to the
rotor in use. Press button 12 to start the precooling program. When the rotor reach the selected
temperature, the 5a LED will blink in combination with acoustic signal.
Press button 10 to exit.
NOTE: The precooling program can not be locked. Use empty rotor without lid.
Control Panel Indicators
Indicator Description
When the lid interlock indicator LED (14) is illuminated, the lid interlock is not active. The lid can be
opened. The indicator will only be illuminated when the rotor is at rest and it is safe to open the lid.
When the lid interlock indicator LED is not illuminated, the lid cannot be opened. The rotor is still in
motion. This feature is in accordance with international safety standards.
Page 32
When the start button is pressed, the centrifuge will begin to accelerate the rotor. At this point the run timer will start and the middle display will begin to show remaining run time. The upper display will show either actual speed or actual maximum RCF values, whichever is currently selected. The lower display shows the given acceleration profile, and the LED corresponding to the acceleration button is illuminated.
During acceleration, the centrifuge automatically detects the rotor type and, therefore, its maximum allowed speed. If the operator sets a speed exceeding this, the centrifuge stops acceleration when the maximum allowed speed is reached, ensuring the operator’s safety. The display will blink and an audible alarm will invite the operator to correct the speed setting to a proper value.
During the run, the upper display will show either actual speed or actual maximum RCF values, whichever is currently selected. The middle display will show either remaining time (timed run) or elapsed time (‘hold’ and ‘pulse’ runs). During a run, the middle display will always show time. The user cannot change the display to show the given ‘radius’ value during a run. Most set parameters can be changed during a run when the selected program is not locked. Set speed can be changed by selecting speed as the control parameter for the upper display, then by pushing the up or down arrow, or turning the knob. Set run time can be changed by pressing the up or down arrow corresponding to the middle display. Set deceleration profile can be changed by first selecting the deceleration profile (pushing the ‘B’ button) and then using the up/down arrows, or turning the knob.
When the stop button is pressed (or when the run timer reaches zero), the centrifuge will begin to decelerate the rotor. At this point the run timer will stop and the middle display will begin to show elapsed braking time. The upper display will show either actual speed or actual maximum RCF values, whichever is currently selected. The lower display shows the given deceleration profile, and the LED corresponding to the acceleration button is illuminated.
At the end of a run, after the rotor has been decelerated to rest, the centrifuge will produce an audible ‘beep’ and the middle display will show the word ‘End’. Pressing any button or opening the lid will bring the displays back to their normal ‘at rest’ configuration (display of set parameters).
Description of Certain
Events with Respect
to the Control System
Start and acceleration phase
Set error
During the run
Stop and braking
(deceleration) phase
End of run
4-4 T3/G3 Thermo Fisher Scientific
Chapter 4
Instructions for Use
Page 33
T3/G3 4-5Thermo Fisher Scientific
Chapter 4
Instructions for Use
Error Codes
Origin
Incorrect speed measurement
Power was interrupted during a run.
Speed > 0 RPM at power ON
Lid open at start
Lid open in running mode
Imbalance.
Motor Over­temperature OR Lid lock error
Chamber Over­Temperature The unit displays this code if the measured temperature exceeds 50°C, at any time during the run. Electronic failure
State of the centrifuge
The rotor will brake to a stop. Lid opening is impossible till speed is zero and a 4 minutes- timeout is expired
At power off the rotor will coast to a stop.
The rotor will coast to a stop.
The centrifuge doesn‘t start if the lid isn’t properly closed
The rotor will brake to a stop.
The rotor will brake to a stop.
The rotor will brake to a stop.
The rotor will brake to a stop. Refrigeration Failure (Refrigerated only)
All controls are disabled
User’s action
Wait for rotor to stop. Wait for the 4 minutes timeout. To erase the message, open the lid, turn the power switch off and turn the power switch on Press any keyboard button to erase this message. Note: if Error 01 has been detected and not cleared, as above described, the alarm reset is possible only after a safety time of 30 minutes Wait for rotor to stop. Press any keyboard button to erase this message. Press any keyboard button to erase this message. Close the lid and press “START“ Wait for the centrifuge to stop. Press any keyboard button to erase this message. Wait for the centrifuge to stop. Press any keyboard button to erase this message. Verify that a balanced load is installed. Inspect the rotor and rearrange the tubes, or add additional tubes with fluid to balance the rotor. Wait for the centrifuge to stop. Press any keyboard button to erase this message. Wait for motor cooling down. Wait for the centrifuge to stop. Press any keyboard button to erase this message. Verify the operating condition.
To erase the message turn the power switch off and turn the power switch on
Error code 01
03
04
CLOSE Lid
06
IMBAL
08
09
11
Note All error indications can be cleared by turn the power switch off
and turn the power switch on. If error code reappears and the cause of the problem can’t be removed contact your local Thermo Service representative L
Page 34
Before installation, the rotor should be thoroughly inspected for evidence of corrosion or other damage and for cleanliness.
Chemical and stress corrosion of metallic parts will eventually lead to disruption of the rotor with potential severe damage to the centrifuge.
Particles stuck inside the pockets can cause breakage of tubes and lead to major imbalance and / or loss of sample and contamination.
The central hole of the rotor and the drive spindle should also be clean and undamaged. These parts should be wiped clean before each use.
The centrifuge also should be observed to verify proper appearance of screws, lid hooks, latches and for evidence of corrosion.
In case of problems contact your Thermo Service representative, because any deviation from the above mentioned advice may have serious consequences for the safety of the appliance and of the operators. L
Normal use of the centrifuge could require the manipulation of biohazards. Users and service personnel must have specific training for each substance they use, according to the “Laboratory Biosafety Manual” from the World Health Organization. L
The contents of each rotor pocket including sample, tube, cap and adapter (where used) must be of the same weight as the one diametrically opposite.
Imbalance of the rotor may cause major damage to the rotor and centrifuge. L
Do not attempt to introduce liquids into rotor pockets or into tubes already in the pockets.
Distribute the load correctly. Loads should be inserted two by two, samples of equal weight, at 180 degrees from the rotation axis and at equal distance (radius) from the center of rotation (see pictures).
When using fixed angle rotor, weight deviation between the tubes must not exceed ±5 grams.
Preparing the First
Run of the Day
Sample Loading
4-6 T3/G3 Thermo Fisher Scientific
Chapter 4
Instructions for Use
Page 35
T3/G3 4-7Thermo Fisher Scientific
Chapter 4
Instructions for Use
When using a swing-out rotor, the samples are placed in plastic inserts. The load must be statically and dynamically balanced:
Static balancing consists of balancing the weight of the 2 inserts which are in opposite locations in the rotor (±15 to 20 grams).
Dynamic balancing consists of placing the tubes in each insert symmetrically according to the axis of the trunnions.
If less than the maximum complement of samples is loaded, the tubes must be placed in opposite pockets.
An odd number of tubes requires an additional blank, water-filled tube of identical total weight to balance.
Significant vibrations can damage the accessories, the unit and the samples. Most vibration is caused by incorrect loading of the tubes. For
Incorrect
Correct
Incorrect
Dynamic Balancing : Correct
Page 36
this reason, the centrifuge is equipped with an imbalance detector.
In case of excessive imbalance, the load imbalance indicator LED is illuminated and the brake is applied immediately. The rotor will be decelerated to rest in few seconds.
As soon as the motor stops, open the centrifuge and redistribute the samples to produce an equal weight on diametrically opposite sides.
Also remember that the pins must be softly lubricated. Inadaquate lubrication of the pins may cause incorrect swinging of the buckets resulting in imbalance phenomen. See chapter 6.6 for details.
If the message persists, despite your efforts to balance the load, call your Thermo Service representative.
4-8 T3/G3 Thermo Fisher Scientific
Chapter 4
Instructions for Use
Page 37
T3/G3 5-1Thermo Fisher Scientific
IEC 1010-2-020
Cautions
Chapter 5 Hazards, Precautions and
Limitations of Use
This centrifuge conforms to the IEC 1010-2-020 international standard, which specifies particular safety requirements for laboratory centrifuges.
According to the standard warnings, the operator must respect the following precautions:
Mark a boundary area of 30 cm around the centrifuge.
No person or hazardous material can stay within this boundary longer than necessary for operational reasons, while the centrifuge is operating.
An emergency switch for disconnection of the mains, in case of malfunction, has to be available and familiar to all the persons operating the centrifuge. This switch has to be remote from the laboratory centrifuge, preferably outside the room in which the centrifuge is located, or adjacent to the exit from that room.
Moving or shifting the machine during centrifugation is dangerous.
Using the centrifuge with rotating equipment showing evidence of corrosion and wear marks, manipulating and/or tampering with the electronic and mechanical parts are dangerous operations.
Never try to bypass the lid lock safety while the rotor is spinning.
Do not try to open the lid until the display returns to the stand-by mode.
Only use a correctly grounded power source.
Use only rotors and accessories designed for use in these centrifuges. L
Pay special attention to the following:
Installation of the unit: proper ventilation, leveling of the centrifuge, rigidity and stability of the support.
Page 38
Rotor installation: verify that the rotor is locked in position before use.
Cleaning of the accessories and of the rotor chamber is particularly necessary when corrosive products are present in the samples (saline, acids, bases).
Load balancing.
IF ANY DANGEROUS EVENT OCCURS, KEEP YOURSELF FAR AWAY FROM THE INSTRUMENT AND SWITCH OFF THE MAIN POWER SOURCE
A view port located on the lid allows the measurement of the actual speed by a phototachometer.
Once a year, check for correct r.p.m. readout and speed control setting which should be within 100 r.p.m. of the actual.
The T3/G3 series of centrifuges and their associated rotors offer a high level of RCF performance. In some cases the maximum possible RCF will exceed the one sustainable by the sample container.
The rotor RCF performance displayed is the maximum available in the rotor pockets. Depending on the sample containers or on other application needs, the maximum RCF which must be used is to be determined by the operator.
The centrifuge is not explosion proof.
Using this centrifuge with explosive samples is entirely at the user’s own risk. Do not under any circumstances use the centrifuge in an explosive environment. L
Due to the action of the turbulence created in the bowl, a centrifuge is an aerosol generator.
A ventilated centrifuge (like the T3/G3 exhausts, into the room, air which has passed through its bowl. Thus the risk of the spread of aerosols is significant in a ventilated centrifuge.
In the case of samples presenting a biological or chemical risk, the operator must take suitable precautions to prevent or reduce this risk.
Speed Control
Operational
Limitations
Aerosol Risks
5-2 T3/G3 Thermo Fisher Scientific
Chapter 5
Hazard, Precautions and Limitations of Use
Page 39
T3/G3 5-3Thermo Fisher Scientific
Chapter 5
Hazard, Precautions and Limitations of Use
Thermo recommends the use of sealed buckets, which are certified for bio-containment through worldwide recognized testing procedures performed in recognized external laboratories. L
Aerosols are produced naturally when using uncapped tubes or bottles. They are also produced when a container deforms or breaks provoking a small or large sample leak.
We draw your attention to the use of tubes in angle rotors. Even if the liquid level does not touch the cap when in a static state, it could do so during centrifugation and leak. You should therefore follow the instructions of the tube supplier concerning the fill level and sealing of the tube.
Once a biological risk is known or suspected, samples should be placed in a sealed container. Should such containers not be available, sealed accessories should be used, such as angle rotors with sealed lids.
When aerosols are created in a centrifuge bowl, they persist in the air for a period of 3-5 minutes after the rotor stops moving. Indeed, the action of opening the lid itself causes the dispersion of aerosols into the environment.
When an elevated risk of aerosols or of breakage is perceived the accessories should be handled using gloves and opened in an environment ensuring the protection of the operator (safety cabinet, glove chamber, wearing a mask ...), even if they are apparently sealed. L
Duration of aerosol presence
Page 40
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T3/G3 6-1Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Chapter 6 Service and Maintenance
All cleaning operations should be performed with the centrifuge disconnected from the power outlet. L
No daily cleaning is required, except in the case of accidental tube breakage, or when there is a large amount of spillage in the bowl.
Clean the bowl and the accessories with a cotton wool pad dipped in 70% alcohol.
Never use metallic brushes to clean accessories.
After cleaning the accessories, rinse them in running water, preferably distilled water.
Dry the rotor with a soft absorbent non-woven cloth or tissue. Drying may be finished off with a warm air jet (e.g. a hair dryer).
Make sure that the pockets are well dried.
Ideally, spray with Anti-Corrosion Spray (Cat N° 11175399)
Store unused buckets upside down on a non-metallic grid to allow free passage of air.
The centrifuge is likely to be used in medical research where hazardous substances, including radioactive chemicals, are frequently found.
ALWAYS USE THE APPROPRIATE DECONTAMINATION PROCEDURES WHEN THE ROTOR IS EXPOSED TO THESE CHEMICALS. L
Examples of commonly used techniques are outlined below. The information is given as a guideline only.
It is the responsibility of the owner to use the most suitable procedure. If decontamination procedures require the use of warming (i.e. autoclave) the rotating equipment should always be completely disassembled before being subjected to heat and after external chemical cleaning.
Seals should be decontaminated with the method most suitable for them.
Periodic Cleaning
Daily
Weekly
Contamination
Hazards
Page 42
6-2 T3/G3 Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Disinfection
Radioactive
Decontamination
Alcohol (70% ethanol or isopropanol) applied for 10 minutes is ideal for bacteria and viruses.
Autoclave for 20 minutes at 120°C to destroy micro-organisms.
Polypropylene components are autoclaveable.
Rotor lids must be disassembled from rotor bodies. ‘O’ rings, autoclaved separately, should be replaced when deformed.
Any part which has been subjected to temperatures above 130 °C must be discarded.
Hypochlorite “bleach” used at 0.1% concentration with 10 minutes immersion is effective against bacteria, spores and viruses but, as an oxidizing agent, is corrosive to metal alloys and must be thoroughly rinsed off of metal parts and the parts dried. It should never be used if there is surface damage to the rotor.
Formalin (37% formaldehyde in water) in contact for 10 minutes has a similar effect to chlorine bleaches.
Rotors should be thoroughly rinsed under running water for 5 minutes to remove all traces of formalin then dried completely.
Formaldehyde is toxic. L
Gluteraldehyde 2%, sold under many brand names such as Cidex and Glutarex, requires total immersion for 10 minutes to ensure sterility. Thorough rinsing and drying is essential to protect users.
Gluteraldehyde builds up to a toxic level in the fatty tissues of the body. Phenols are very corrosive and should never be used. L
We recommend that all radioactive contamination be referred to your Radioactivity Safety Officer.
Rotors may be decontaminated by a mixture of equal volumes of:
Distilled water,
SDS diluted to 10%,
Ethanol diluted to 70%.
The rotor should then be rinsed with ethanol followed by distilled water and then dried completely.
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T3/G3 6-3Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Thermo makes no claims as to the effectiveness of proprietary brands of decontaminating solutions.
If the main circuit breaker of the centrifuge cuts off the power to the instrument, do not attempt to switch it on before a Thermo Service representative has checked over the unit.
This operation is necessary to allow the buckets to swing freely. Clean the trunnions regularly with a dry wipe (as well as the part of the bucket that rotates on the trunnions). Then, put a very small quantity of grease on the curved face of the trunnion. Do not apply too much grease because it will eventually coat the bowl of the centrifuge as centrifugal force pulls the grease from the trunnions.
If the centrifuge is having imbalance problems, try this operation before calling Thermo service. In many cases, imbalance problems arise due to the fact that poorly maintained bucket-trunnion interfaces prevent the buckets from swinging freely. L
Power Supply Circuit
Breaker
Trunnion Lubrification
Page 44
6-4 T3/G3 Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Chemical Compatibility Table for Rotors, Tubes and Accessories
S = Satisfactory AL = Aluminum BN = Buna N D = Discoloration but OK CAB = Cellulose acetate butyrate CN = Cellulose Nitrate P = Pure chemical OK DL = Delrin KY = Kynar M = Moderate resistance NO = Noryl NY = Nylon U = Unsatisfactory PA = Polyallomer (= PPCO) PC = Polycarbonate X = Explosion risk !!! PE = Polyethylene PP = Polypropylene O = No information
PPCO=Polypropylene Copolymer PS = Polysulfone d = Less resistance if T > 50°C SS = Stainless steel TF = Teflon t = Unsatisfactory if T >50°C TZ = Tefzel TI = Titanium
VA = Viton A
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Acetaldehyde S U U U O O O O M U M M O S S M S U Acetamide O O O O O O O O S U S S S O O O O O Acetic Acid (5%) S M S S M S S S S S S D S S S S S M Acetic Acid (20 %) S O O O O O O O S M S S S O O O O O Acetic Acid (60%) S U U U U S S M S U M D S S S S S U Acetic Acid (80 %) S O O O O O O O S U St S M O O O O O Acetic Acid (Glacial) S U U U U S O O S U M D M S S S S U Acetic Anhydride S O O O O O O O Sd U U Sd U O O O O O Acetone S U U U M M O U S U S M U S S M S U Acetonitrile O O O O O O O O Mt U S Mt U O O O O O Acetylene S O O O O O O O S O S S U O O O O O Adipic Acid O O O O O O O O S S St S S O O O O O Alanine S O O O O O O O S S U S U O O O O O Allyl Alcohol O O U O S O O U O S S S O O S S S O Aluminum Chloride O O S S O S O S S S S S O U S S S O Aluminum Fluoride O O O O O S O S S U S S O O S O S O Aluminum Hydroxide S O O O O O O O S Mt Sd S S O O O O O Aluminum Nitrate M O O O O O O O S O O S O O O O O O Aluminum Sulphate S O O O O O O O Sd O S Sd O O O O O O Amino Acids S O O O O O O O S S S S S O O O O O Ammonia S O O O O O O O S U S S Sd O O O O O Ammonium Acetate O O O O O O O O S S S S O O S S S O Ammonium Carbonate S U S S O S O S S U SSSSS SSO Ammonium Chloride M O O O O O O O St O St St O O O O O O Ammonium Hydroxide (10%) O S U O O O O S D U S D S S S S S S Ammonium Hydroxide (conc) O U U O O O O S D U S D O S S S S U Ammonium Oxalate O O O O O O O O Sd S S Sd S O O O O O Ammonium Phosphate U O O O O O O O S M S S O O O O O O Ammonium Sulphate S S O O U O O S S S S S O S S S S O Ammonium Sulphide O O O O O S O O S U O S O O S O O O n-Amyl Acetate S O O O O O O O Sd U Sd Sd U O O O O O Amyl Alcohol S M U O S O O S S S S S O O S S S M Amyl Chloride S O O O O O O O U U UUUOOOOO Aniline S O O O O S O O U O S M O O S S S O
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T3/G3 6-5Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Aqua Regia U U U O U O O O U U UUOOSSSM Barium Chloride U O O O O O O O S O S S O O O O O O Barium Hydroxide U O O O O O O O S O S S O O O O O O Barium Sulphate S O O O O O O O S O St S O O O O O O Benzaldehyde S O O O O O O O Sd Mt S Sd M O O O O O Benzene S U P O M O O S U U U U U S S S S S Benzoic Acid, Sat St O O O O O O O Sd Sd S Sd M O O O O O Benzyl Acetate O O O O O O O O Sd Mt S Sd U O O O O O Benzyl Alcohol S U U O M O O U U U UUOOS SSS Boric Acid U O O O O O O O S U Sd S U O O O O O Bromine U O O O O O O O U Mt UUUOOOOO Bromobenzene U O O O O O O O U U UUUOOOOO Bromoform U O O O O O O O U U UUUOOOOO Butadiene S O O O O O O O U U UUUOO OOO Butane S O O O O O O O O O OOOOO OOO n-Butanol S S U O S O O U O M S S M O S S S S n-Butyl Acetate S O O O O O O O S U S S U O O O O O Butylene S O O O O O O O O O S O O O O O O O Butyl Chloride O O O O O O O O U U UUUOOOOO Butyric Acid S O O O O O O O U Mt U U S O O O O O Caesium Acetate M O O O O O O O S S S S S O S S O O Caesium Bromide M O O O O O O O S S S S S O S S O O Caesium Chloride M O S S O O O O S S SSSSSSSO Caesium Formiate M O O O O O O O S S S S S O S S O O Caesium Iodide M O O O O O O O S S S S S O S S O O Caesium Sulphate M O O O O O O O S S S S S O S S O O Caesium Trifluoracetate M O M U O O O O S S S S S M S O O O Calcium Carbonate U O O O O O O O S O St S O O O O O O Calcium Chloride M S S O S O O S S M O D S S S O S S Calcium Hypochlorite M U O O M S O S S M S S S U S O S S Calcium Sulphate M O O O O O O O S O St S O O O O O O Carbazole O O O O O O O O S U S S U O O O O O Carbon Sulphide S O O O O O O O U U UUUOOOOO Carbon Tetrachloride X U S S M S O S U U U U S M S S S S Cedarwood Essence O O O O O O O O U St U U M O O O O O Chlorine, dry M O O O O O O O St Sd St St O O O O O O Chlorine, moist U O O O O O O O Mt Sd St Mt O O O O O O Chloroacetic Acid U O O O O O O O Sd Mt S Sd U O O O O O p-Chloroacetophenone O O O O O O O O S U S S U O O O O O Chlorobenzene O O U U O S O O U U UUOOSOSO Chloroform X U M S M S O U U U U U U S S M S S Chlorosulphonic M O O O O O O O M O M M O O O O O O Chromic Acid (5 %) U O O O O O O O S M S S U O O O O O Chromic Acid (10%) M U U U U S S O S M S S U U S S S S Chromic Acid (50%) U U U S U S O O D U S S U U S S M S Cinnamon Essence O O O O O O O O U St U U M O O O O O Citric Acid (10%) S S S O M S S M S S SSSSSSSS Copper Nitrate U O O O O O O O S O S S O O O O O O
Page 46
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Copper Sulphate U O O O O O O O S O St S O O O O O O Croesol S O O O O S O U S U S S O O S M S O Cyclohexane S O O O O O O O Mt Sd Mt Mt U O O O O O Cyclohexanol S O U O O O O S S M S S O O S O S O Cyclohexanone O O O O O O O O Mt U UUUUOOOO Cyclopentane O O O O O O O O Mt U UUUUOOOO Decane O O O O O O O O Mt Mt Mt Mt Sd O O O O O Dextran Sulphate M O O O O O O O S S S S S O S S O O Diacetone S O U O O O O O S O S S O O S O S O Diacetone Alcohol S O O O O O O O S O S S O O O O O O o-Dichlorobenzene O O O O O O O O Mt U Mt Mt U O O O O O p-Dichlorobenzene O O O O O O O O Mt U Mt Mt U O O O O O Dichloroethane O U U U S O S S U U UUOOSSSS Dichlorophenol O O O O O O O O U U UUUOO OOO Diethylamine S O O O O O O O St U U St Sd O O O O O Diethyl Benzene O O O O O O O O U Mt UUUOOOOO Diethylene Glycol S S S S S S O U S S S S S O S S S S Diethylene Glycol Ethyl Ether O O O O O O O O S Mt S S M O O O O O Diethyl Ether S O O O O O O O U U OUOOOOOO Diethyl Ketone S O U U M O O U U U M M O O S M S O Dimethylacetamide O O O O O O O O S U St S U O O O O O Dimethylformamide S O O O O O O O S U S S O O S M S O Dimethylsulphoxide S O O O O O O O S U O S O S S M S O Dioxane S U U O M S O O M U M M O O S S S U Diphenyloxide S O O O O O O O U O OUOOO OOO Dipropylene Glycol O O O O O O O O S Sd S S S O O O O O Distilled Water S S S S S O S S S S SSSSSSSS Ethanol (50%) S S S S M S S U S M SSSSSSSS Ethanol (95%) S S U U M S S U S U SSSSSSSS Ethyl Acetate M U U U M S O U M U S U U O S S S U Ethyl Benzene O O O O O O O O Mt U St Mt U O O O O O Ethyl Benzoate O O O O O O O O Sd M S Sd U O O O O O Ethyl Butyrate O O O O O O O O St U St St U O O O O O Ethyl Chloride S O O O O O O O St U St St U O O O O O Ethylene Chloride S O O O O O O O St U St St U O O O O O Ethylene Glycol S S S S S S O U S S S S S O S S S S Ethylene Oxide O O O O O O O O M Mt M M S O O O O O Ethyl Ether S O U U O O O O M U M M O O S M S O Ethyl Lactate O O O O O O O O O S St S S M O O O O Ethyl Malonate O O O O O O O O O S Mt S S M O O O O Fatty Acids S O O O O O O O Sd Sd Sd Sd S O O O O O Ferric Chloride U S O O M S S S S O S S O U S S S S Ferric Nitrate M O O O O O O O S O St S M O O O O O Ferric Sulphate S O O O O O O O S O S S O O O O O O Ficoll Paque M O O O O O O O S S S S S O S S O O Fluorine S O O O O O O O Mt Sd St Mt U O O O O O Fluorhydric Acid (10%) U U M M U S O S S M S S S U S S U O Fluorhydric Acid (50%) U U U U U S O O S U S S M U S S U M
6-6 T3/G3 Thermo Fisher Scientific
Chapter 6
Service and Maintenance
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T3/G3 6-7Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Formaldehyde (20%) S O O O O O O O S Sd S S Sd O O O O O Formaldehyde (40%) M M O S O S S S S S S D S S S S S S Formaldehyde (50%) S O O O O O O O S Sd S S Sd O O O O O Formic Acid (100%) S M U O U S S U S M S S O U S S S U Freon TF U O O O O O O O Sd Sd Sd Sd Sd O O O O O Fuel Oil O O O O O O O O Sd Sd Mt Sd Sd O O O O O Glucose S O O O O O O O S O S S O O O O O O Glutaraldehyde O O O O O O O O Sd Sd S Sd Sd O O O O O Glycerine S O O O O O O O S S S S S O O O O O Glycerol S O O S O S S O S S SSSSSSSO Heptane S O O O O O O O M O S M O O O O O O Hexane S O O O O O O O S O M S O O O O O O Hydrazine O O O O O O O O U U UUUOOOOO Hydrochloric Acid (5%) U O O O O O O O S S S S S O O O O O Hydrochloric Acid (37 %) U O O O O O O O Sd U S Sd S O O O O O Hydrochloric Acid (50%) U U U U U S S O M U S M O U S S S M Hydrochloric Acid (conc). U U U O U O O O S U O S O U S S S O Hydrofluoric Acid (10%) U U M M U S O S S M S S S U S S U O Hydrofluoric Acid (50%) U U U U U S O O S U S S M U S S U M Hydrogen Peroxide (3%) S M S S S O S S S S S D S S S S S S Hydrogen Peroxide (100%) S U S S U O S O S S S D S S S S U M Iodine, Crystals S O O O O O O O Mt U U Mt U O O O O O Isobutyl Alcohol O M U O S O O U S S S S O O S S S S Isopropyl Alcohol U M U U S O S U S M S S M O S S S S Isopropylbenzene O O O O O O O O Mt U Mt Mt U O O O O O Kerosene S O O O O O O O Sd S Mt Sd St O O O O O Lactic Acid (20%) O S O O O O S O S S SSSSS SSS Lactic Acid (100%) O S O O O O O O S S S S O S S S S S Lead Acetate (aq.) U O O O O O O O S S St S O O O O O O Lemon Essence U O O O O O O O O O OOOOO OOO Lime, (conc). M O O O O O O O S U S S S O O O O O Magnesium Chloride M O O O O O O O S S S S S O S S O O Magnesium Hydroxide U O U O O S S O S U S S O O S O S O Magnesium Nitrate M O O O O O O O S O Sd S O O O O O O Magnesium Sulphate S O O O O O O O S O St S O O O O O O Manganese Salts M O S O O O O O S O S S O O S O S O Mercury O O O O O O O O S U S S S O O O O O Methanol (100%) S S U U M S O U S M S D S S S S S U Methyl Acetate S O O O O O O O M U M M U O O O O O Methyl Alcohol (100%) S S U U M S O U S M S D S S S S S U Methyl Butyl Ketone O O O O O O O O U O OOOOO OOO Methyl Ethyl Ketone S U U U M M O U S U S S U O S M S U Methyl Isobutyl Ketone St O O O O O O O S U S S U O O O O O Methyl Isopropyl Ketone O O O O O O O O U U S U U O O O O O Methylene Chloride X U U U S S O U U U M U U S S S S M Mineral Oil O O O O O O O O Mt U Mt Mt Mt O O O O O Nickel Chloride U O O O O O O O S O St S O O O O O O Nickel Salts M S S O O O O S S S S S O S S S S S
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6-8 T3/G3 Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Nickel Sulphate U O O O O O O O S S St S O O O O O O Nitric Acid (10%) M U S S U S S M D S S S S D S S S S Nitric Acid (20%) U O O O O O O O S Sd S S St O O O O O Nitric Acid (50%) M U M M U S S M D M M M O D S S S S Nitric Acid (95%) M U U O U O O U M U U M U S S S S S Nitric Acid (conc.) St O O O O O O O U U Mt U U O O O O O Nitrobenzene O O O O O O O O U U UUUOOOOO Octane O O O O O O O O S Sd S S Sd O O O O O Octyl Alcohol S O O O O O O O O O S O O O O O O O Oleic Acid S U S S S S O S S S SSSSSSSM Orange Essence S O O O O O O O Mt M Mt Mt M O O O O O Oxalic Acid M M S S O S O S S S SSSSSSMS Oxygenated Water (20%) S O O O O O O O S S S S S O O O O O Oxygenated Water (50%) S O O O O O O O S S S S S O O O O O Oxygenated Water (90%) S O O O O O O O S S S S S O O O O O Ozone O O O O O O O O Sd Sd S Sd S O O O O O Paraffin S O O O O O O O S O S S O O O O O O Pentane S O O O O O O O U O UUOOO OOO Perchlorethylene S O O O O O O O U U UUUOOOOO Perchloric Acid X O O O O O O O St U St St U O O O O O Perchloric Acid (10%) U O O O U S O O S U M M O U S S S S Perchloric Acid (70%) X O O O O O O O M U M M U O S S O O Petrol S O O O O O O O St M St St M O O O O O Phenol (5%) S U O O U S O U M U S M U S S S U S Phenol (50%) U O O O O O O O U U UUUOSMOO Phenol, crystals U O O O O O O O St U St St U O O O O O Phenol, liquid U O O O O O O O U U UUUOOOOO Phenyl Ethyl Alcohol O O U O O O O S S O S S O O S O S O Phosphoric Acid (10%) O M S S U S S O S S SSSSSSOS Phosphoric Acid (conc.) O U M M U S O O S U S S S M S S M S Picric Acid S O O O O O O O U U UUUOO OOO Pine Oil O O O O O O O O Sd St St Sd M O O O O O Potash, conc. U O O O O O O O S U S S S O O O O O Potassium Bromide U O O O O O O O S S S S O O O O O O Potassium Carbonate M O S S O S S S S U S S O S S S S O Potassium Chlorate M O S S O S S S S S S S O S S O S O Potassium Chloride U O O O O O O O S S S S S O S S O O Potassium Hydroxide (5%) U M S M U O O S S U SSSSSSMS Potassium Hydroxide (conc.) U M U U U O O O S U S S O S S S U M Potassium Nitrate S O O O O O O O S O S S O O O O O O Potassium Permanganate S O O O O O O O S S S S D O S S O O Propane Gas S O O O O O O O U St U U M O O O O O Propionic Acid O O O O O O O O Sd U M Sd S O O O O O Propyl Alcohol S O O O O O O O S O St S O O O O O O Propylene Glycol S O O O O O O O S Sd S S S O O O O O Propylene Oxide O O O O O O O O S St S S S O O O O O Pyridine U O O O O O O O M U S M O O O O O O Resorcinol, Sat’d., Sol O O O O O O O O S Sd S S U O O O O O
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T3/G3 6-9Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Rubidium Bromide M O O O O O O O S S O S O O O O O O Saccharose U O O O O O O O S S S S S O O O O O Salycylic Acid, Sat O O O O O O O O S Sd S S S O O O O O Serum S O O O O O O O S S S S S O S S O O Silver Acetate O O O O O O O O S Sd S S S O O O O O Silver Nitrate U O O O O O O O S S S S S O S S O O Sodium Acetate S O O O O O O O S Sd S S S O O O O O Sodium Bisulphate M O S S O S S S S S S S O S S O S O Sodium Borate M O O O O O O O S S Sd S O O O O O O Sodium Bromide U O O O O O O O S S O S O O O O O O Sodium Carbonate (2%) M S S S S S S S S S S D O S S S S S Sodium Chloride (10%) S S S S S O O S S S SSSSS SMS Sodium Chloride (Sat’d.) S S O O S O O S S O S S O S S S S S Sodium Hydroxide (>1%) U M S S U S O S S U SSSSSSSS Sodium Hydroxide (10%) U M U U U S O S S U SSSSSSSS Sodium Hydroxide (conc.) U M U U U O O O M U S M O S S S M U Sodium Hypochlorite (5%) M M S S U S S S D S S S S M S S S S Sodium Iodide M O O O O O O O S S O S O O O O O O Sodium Nitrate S O O O O O O O S O Sd S O O O O O O Sodium Sulfate S O O O O O O O Sd O Sd Sd O O O O O O Sodium Sulphide S S S O O S O S S U S S O S S S M S Stearic Acid S O O O O O O O S Sd S S S O O O O O Sulphuric Acid (10%) M U S S U S S S S M S S S U S S S S Sulphuric Acid (20%) U O O O O O O O Sd Sd S Sd S O O O O O Sulphuric Acid (50%) U U U U U S S U S S S S S U S S M S Sulphuric Acid (conc.) U U U U U S O U D U M D U M S S U S Sulphuric Anhydride, dry or moist S O O O O O O O S Sd S S S O O O O O Tetrachloroethane M O O O O O O O M O O M O O O O O O Tetrachlorethylene O O O O O O O O U O S U O O O O O O Tannic Acid M O O O O O O O S O Sd S O O O O O O Tartaric Acid M O O O O O O O S Sd S S S O O O O O Tetrahydrofuran S O O O O O O O U U UUUOS SOO Thionyl Chloride O O O O O O O O U U UUUOO OOO Toluene S U P S M S O U U U U U U S S S M M Trichlorethylene S U O O O S O U U U UUUUSSMS Trichloroacetic Acid U O O O O O O O Mt Mt Mt Mt S O O O O O 1,2,4 - Trichlorobenzen O O O O O O O O U U UUUOO OOO Trichloroethane S U S O M S O S U U U U M O S S S S Triethylamine O O O O O O O O U O OUOOO OOO Triethylene Glycol O O O O O O O O S Sd S S S O O O O O Tris Buffer (neutral) S O O O O O O O S S S S S O S S O O Trisodium Phosphate O O S O M O O S S O S S O O S S S S Triton X-100 S O O O O O O O S S S S S O S M O O Turpentine S O O O O O O O Sd Mt St Sd U O O O O O Undecyl Alcohol O O O O O O O O Sd Sd St Sd M O O O O O Urea M O S S S O O S S S SSSSS SSO Urine O O S O S O O S S S S S O O S S S O Vinylidene chloride O O O O O O O O U U UUUOO OOO
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6-10 T3/G3 Thermo Fisher Scientific
Chapter 6
Service and Maintenance
Material AL BN CAB CN DL KY NO NY PA PC PE PP PS SS TF TZ TI VA
Chemical PPCO
Xylene S U P O M S O U U U U U U S S S S S Zinc Chloride M S S O O O O S S S S S S M S S S S Zinc Hydrosulphite U O O O O O O O O O OOOOOOOO Zinc Sulphate U O O O O O O O Sd O S Sd O O O O O O
* This table is intended as a guide only because of the difficulty in quantifying, cross-checking and monitoring the results under different conditions of temperature, pressure and purity relating to the solvents and samples dissolved therein. It is strongly recommended that you carry out your own trials, particularly before protracted work periods.
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T3/G3 7-1Thermo Fisher Scientific
Chapter 7 Disposal of Product
The following disposal recommendations are valid for the machine (or its accessories) at the end of its useful life, or the parts that be disposed f because they are worn out or degraded during use.
Prior to disposal, the machine and accessories must be decontaminated. In this respect the user is required to submit the enclosed decontamination certificate, completed and signed, to the company or persons who are in charge of disposal.
The elements of the product that may become noxius during the life of the product are the folowing:
Electric batteries and accumulators situated in the front panel of the machine among the other electrical and electronic componenets,
Oil in the compressor of the refrigeration systems,
Refrigerant
Disposal of these elements must be in accordance with applicable regulations and recommendations defined by the relevant regulatory bodies. In additions, these elements must be disposed of differently based on the different noxious substances they contain (possibly by a specialized disposal company).
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I-1 T3/G3 Thermo Fisher Scientific
Certificate of Decontamination and Cleaning
Read carefully the instructions below before sending an instrument, or parts of it, to Thermo Service Dept. or to any Authorized Technical Assistance Service. L
Mr / Mrs (name) .................................................................... Establishment ............................
Department ......................................................................................................................................
Address ................................................................................... Post / Zip code ............................
City ......................................................................................... State / Country ..........................
Declares the cleaning and decontamination of the following:
Product type .................................................................................................... Serial N° ............
Rotor ................................................................................................................ Serial N° ............
Rotor ................................................................................................................ Serial N° ............
Accessory - Description................................................................................... Serial N° ............
Accessory - Description................................................................................... Serial N° ............
Nature of contamination
..........................................................................................................................................................
..........................................................................................................................................................
Decontamination Procedure used
..........................................................................................................................................................
..........................................................................................................................................................
Decontamination certified by:
Mr / Mrs ................................................................................ Institution ..................................
Date ........................................................................................ Signature ....................................
When an instrument, or parts of it, requires servicing by Thermo personnel, the following procedure must be accomplished to ensure personnel safety:
Clean the instrument and proceed to its decontamination from any kind of dangerous products.
Compile this Decontamination Certificate with all the information required.
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T3/G3 I-2Thermo Fisher Scientific
Certificate of Decontamination and Cleaning
Attach this Certificate to the instrument (or part) before sending it to Thermo Service or other authorized technical service.
Thermo personnel will not accept to work on instruments deprived of this Decontamination Certificate. If an instrument is received at our Service facilities and, in our opinion, is a radioactive or biological hazard, the item will be refused and resent to the Customer. Disposition costs will be borne by the sender. Instructions for decontamination and cleaning are explained in the User Manual. Additional certificates are available from your local technical or Customer Service representative. In the event these certificates are not available, a written statement certifying that the instrument or part has been properly decontaminated and outlining the procedures used will be acceptable.
For your convenience, use a copy of this page
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P/N 11290098-a
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