Teledyne 9110AH User Manual

INSTRUCTION MANUAL

MODEL 9110AH

NITROGEN OXIDES ANALYZER

SERIAL NO. _______________

TELEDYNE ANALYTICAL INSTRUMENTS

16830 CHESTNUT STREET

CITY OF INDUSTRY, CA 91749-1020

TOLL-FREE: 888-789-8168

FAX: 626-961-2538

TEL: 626-934-1500

WEB SITE: www.teledyne-ai.com

01620

REV. F

TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

SAFETY MESSAGES

Your safety and the safety of others is very important. We have provided many important safety messages in this manual. Please read these messages carefully.

A safety message alerts you to potential hazards that could hurt you or others. Each safety message is associated with a safety alert symbol. These symbols are found in the manual and inside the instrument. The definition of these symbols is described below:

GENERAL WARNING/CAUTION: Refer to the instructions for details on the specific danger.

CAUTION: Hot Surface Warning

CAUTION: Electrical Shock Hazard

Technician Symbol: All operations marked with this symbol are to be performed by qualified maintenance personnel only.

Electrical Ground: This symbol inside the instrument marks the central safety grounding point for the instrument.

CAUTION

The analyzer should only be used for the purpose

and in the manner described in this manual.

If you use the analyzer in a manner other than that for which

it was intended, unpredictable behavior could ensue with

possible hazardous consequences.

TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

TABLE OF CONTENTS

SAFETY MESSAGES..................................................................................II

TABLE OF CONTENTS.............................................................................III

LIST OF FIGURES................................................................................... VII

LIST OF TABLES ................................................................................... VIII

1 HOW TO USE THIS MANUAL...............................................................1-1

2 GETTING STARTED.............................................................................2-1

2.1 UNPACKING ...........................................................................................................................2-1

2.2 ELECTRICAL AND PNEUMATIC CONNECTIONS .........................................................................2-1

2.3 INITIAL OPERATION.................................................................................................................2-6

3 SPECIFICATIONS, WARRANTY...........................................................3-1

3.1 SPECIFICATIONS.....................................................................................................................3-1

3.2 WARRANTY............................................................................................................................3-2

4 THE M9110AH NOX ANALYZER ...........................................................4-1

4.1 PRINCIPLE OF OPERATION......................................................................................................4-1

4.2 OPERATION SUMMARY...........................................................................................................4-4

4.2.1 Sensor Module, Reaction Cell, Detector....................................................................4-4

4.2.2 Pneumatic Sensor Board.............................................................................................4-4

4.2.3 Computer Hardware and Software .............................................................................4-5

4.2.4 V/F Board......................................................................................................................4-5

4.2.5 Front Panel...................................................................................................................4-5

4.2.6 Power Supply Module...................................................................................................4-7

4.2.7 Pump, Valves, Pneumatic System...............................................................................4-7

4.2.8 Ozone Generator...................................................................................................... 4-10

4.2.9 NO2 - NO Converter ................................................................................................. 4-10

5 SOFTWARE FEATURES.......................................................................5-1

5.1 INDEX TO FRONT PANEL MENUS............................................................................................5-1

5.1.1 Sample Menu................................................................................................................5-4

5.1.2 Set-Up Menu................................................................................................................5-5

5.2 SAMPLE MODE.......................................................................................................................5-9

5.2.1 Test Functions..............................................................................................................5-9

5.2.2 CAL, CALS, CALZ, Calibration Functions............................................................... 5-13

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5.3 SET-UP MODE ...................................................................................................................5-15

5.3.1 Configuration Information (CFG) ............................................................................. 5-15

5.3.2 Automatic Calibration (AutoCal)............................................................................... 5-15

5.3.3 Data Acquisition System (DAS) ............................................................................... 5-16

5.3.4 Range Menu.............................................................................................................. 5-18

5.3.5 Password Enable ......................................................................................................5-21

5.3.6 Time of Day Clock.....................................................................................................5-21

5.3.7 Diagnostic Mode ....................................................................................................... 5-21

5.3.8 Communications Menu............................................................................................. 5-21

5.3.9 Variables Menu (VARS) ...........................................................................................5-22

5.4 M9110AH OPERATING MODES.......................................................................................... 5-22

5.4.1 NO/NOx/NO2 Switching Mode ..................................................................................5-23

5.4.2 NOx Only Mode.......................................................................................................... 5-24

5.4.3 NO Only Mode........................................................................................................... 5-24

5.5 4-20 MA CURRENT LOOP................................................................................................... 5-24

5.6 STATUS OUTPUT................................................................................................................ 5-25

5.7 RS-232 INTERFACE........................................................................................................... 5-25

5.7.1 Setting up the RS-232 Interface............................................................................... 5-26

5.7.2 Command Summary..................................................................................................5-29

5.7.3 TEST Commands and Messages............................................................................ 5-33

5.7.4 WARNING Commands and Messages................................................................... 5-34

5.7.5 CALIBRATION Commands and Messages............................................................ 5-35

5.7.6 DIAGNOSTIC Commands and Messages.............................................................. 5-36

5.7.7 DAS Commands and Messages.............................................................................. 5-37

5.7.8 VARIABLES Commands and Messages................................................................. 5-39

6 OPTIONAL HARDWARE AND SOFTWARE..........................................6-1

6.1 RACK MOUNT OPTIONS.........................................................................................................6-1

6.2 ZERO/SPAN VALVES OPTION..................................................................................................6-2

6.2.1 Autocal - Setup Zero/Span Valves..............................................................................6-2

6.3 ISOLATED 4-20 MA CURRENT LOOP OPTION.........................................................................6-4

6.4 MOLYBDENUM CONVERTER OPTION......................................................................................6-5

6.5 EXTERNAL DESICCANT CANISTER OPTION.............................................................................6-5

6.6 ALTERNATE BYPASS FLOW ORIFICE OPTION..........................................................................6-5

6.7 EXTERNAL CONVERTER OPTION............................................................................................6-5

7 CALIBRATION AND ZERO/SPAN CHECKS.........................................7-1

7.1 MANUAL ZERO/SPAN CHECK OR CAL WITH ZERO/SPAN GAS IN THE SAMPLE PORT ...............7-3

7.2 MANUAL ZERO/SPAN CHECK WITH ZERO/SPAN VALVES OPTION ............................................7-6

7.3 DYNAMIC ZERO/SPAN CALIBRATION USING AUTOCAL ............................................................7-7

7.4 USE OF ZERO/SPAN VALVES WITH REMOTE CONTACT CLOSURE...........................................7-8

7.5 NO ONLY MODE CALIBRATION ..............................................................................................7-9

7.6 NO

ONLY MODE CALIBRATION .............................................................................................7-9

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7.7 CALIBRATION REQUIREMENTS FOR AUTORANGE OR REMOTE RANGE....................................7-9

7.8 CALIBRATION REQUIREMENTS FOR INDEPENDENT RANGE................................................... 7-10

7.9 CALIBRATION QUALITY ........................................................................................................ 7-10

7.10 CONVERTER EFFICIENCY COMPENSATION ........................................................................7-11

7.11 RECOMMENDATIONS FOR CEM APPLICATIONS ................................................................. 7-12

7.11.1 Calibration Gasses................................................................................................. 7-12

7.11.2 Calibration Frequency.............................................................................................7-13

7.11.3 Converter Efficiency............................................................................................... 7-13

8 MAINTENANCE ....................................................................................8-1

8.1 MAINTENANCE SCHEDULE......................................................................................................8-1

8.2 REPLACING THE SAMPLE PARTICULATE FILTER ......................................................................8-2

8.3 REPLACING THE CONVERTER.................................................................................................8-4

8.4 CLEANING THE REACTION CELL .............................................................................................8-6

8.5 PNEUMATIC LINE INSPECTION ............................................................................................. 8-10

8.6 LEAK CHECK PROCEDURE .................................................................................................. 8-13

8.7 LIGHT LEAK CHECK PROCEDURE........................................................................................ 8-13

8.8 PROM REPLACEMENT PROCEDURE.....................................................................................8-14

9 TROUBLESHOOTING AND ADJUSTMENTS .......................................9-1

9.1 OPERATION VERIFICATION - DIAGNOSTIC TECHNIQUES...........................................................9-3

9.1.1 Fault Diagnosis with TEST Variables..........................................................................9-3

9.1.2 Fault Diagnosis with WARNING Messages...............................................................9-8

9.1.3 Fault Diagnosis using DIAGNOSTIC Mode ............................................................9-10

9.1.4 M9110AH Internal Variables.................................................................................... 9-17

9.1.5 Test Channel Analog Output..................................................................................... 9-19

9.1.6 Factory Calibration Procedure................................................................................. 9-20

9.2 PERFORMANCE PROBLEMS................................................................................................. 9-24

9.2.1 AC Power Check....................................................................................................... 9-24

9.2.2 Flow Check................................................................................................................ 9-25

9.2.3 No Response to Sample Gas .................................................................................. 9-25

9.2.4 Negative Output......................................................................................................... 9-26

9.2.5 Excessive Noise....................................................................................................... 9-26

9.2.6 Unstable Span........................................................................................................... 9-27

9.2.7 Unstable Zero............................................................................................................ 9-28

9.2.8 Inability to Span......................................................................................................... 9-28

9.2.9 Inability to Zero.......................................................................................................... 9-28

9.2.10 Non-Linear Response............................................................................................ 9-29

9.2.11 Slow Response....................................................................................................... 9-30

9.2.12 Analog Output Doesn't Agree With Display Concentration.................................. 9-30

9.3 SUBSYSTEM TROUBLESHOOTING AND ADJUSTMENTS......................................................... 9-31

9.3.1 Computer, Display, Keyboard................................................................................... 9-31

9.3.2 RS-232 Communications ......................................................................................... 9-34

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9.3.3 Voltage/Frequency (V/F) Board............................................................................... 9-37

9.3.4 Status/Temp Board................................................................................................... 9-43

9.3.5 Power Supply Module................................................................................................ 9-45

9.3.6 Ozone Generator...................................................................................................... 9-49

9.3.7 Flow/Pressure Sensor.............................................................................................. 9-53

9.3.8 NOx Sensor Module .................................................................................................. 9-58

9.3.9 Z/S Valves .................................................................................................................9-63

9.3.10 Pneumatic System.................................................................................................. 9-64

10 M9110AH SPARE PARTS LIST.........................................................10-1

APPENDIX A ELECTRICAL SCHEMATICS............................................ A-1

TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

LIST OF FIGURES

FIGURE 2-1: REMOVAL OF SHIPPING SCREWS & CHECK FOR CORRECT POWER.............................2-3

FIGURE 2-2: REAR PANEL...............................................................................................................2-4

FIGURE 2-3: INLET AND EXHAUST VENTING RECOMMENDATIONS....................................................2-5

FIGURE 2-4: FRONT PANEL..........................................................................................................2-10

FIGURE 2-5: ASSEMBLY LAYOUT.................................................................................................. 2-12

FIGURE 4-1: BLOCK DIAGRAM.........................................................................................................4-3

FIGURE 4-2: EXTERNAL PUMP PACK...............................................................................................4-9

FIGURE 5-1: SAMPLE MENU TREE ..................................................................................................5-2

FIGURE 5-2: SETUP MENU TREE ....................................................................................................5-3

FIGURE 8-1: REPLACING THE PARTICULATE FILTER ........................................................................8-3

FIGURE 8-2: CONVERTER ASSEMBLY..............................................................................................8-5

FIGURE 8-3: REACTION CELL ASSEMBLY ........................................................................................8-8

FIGURE 8-4: SAMPLE/BYPASS FLOW CONTROL ASSEMBLY.............................................................8-9

FIGURE 8-5: PNEUMATIC DIAGRAM............................................................................................... 8-11

FIGURE 8-6: PNEUMATIC DIAGRAM WITH ZERO/SPAN VALVES...................................................... 8-12

FIGURE 9-1: SPAN CALIBRATION VOLTAGE................................................................................... 9-23

FIGURE 9-2: CPU BOARD JUMPER SETTINGS ............................................................................. 9-33

FIGURE 9-3: RS-232 PIN ASSIGNMENTS..................................................................................... 9-35

FIGURE 9-4: V/F BOARD JUMPER SETTINGS................................................................................ 9-42

FIGURE 9-5: POWER SUPPLY MODULE LAYOUT........................................................................... 9-47

FIGURE 9-6: ELECTRICAL BLOCK DIAGRAM .................................................................................. 9-48

FIGURE 9-7: OZONE GENERATOR SUBSYSTEM............................................................................ 9-52

FIGURE 9-8: FLOW/PRESSURE SENSOR ...................................................................................... 9-55

FIGURE 9-9: NO FIGURE 9-10: NO

FIGURE 9-11: PMT COOLER SUBSYSTEM ................................................................................... 9-60

FIGURE 9-12: HIGH VOLTAGE POWER SUPPLY ............................................................................ 9-62

SENSOR MODULE ............................................................................................ 9-56

SENSOR MODULE.......................................................................................... 9-57

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

LIST OF TABLES

TABLE 2-1: FINAL TEST AND CALIBRATION VALUES....................................................................... 2-13

TABLE 2-1: FINAL TEST AND CALIBRATION VALUES (CONTINUED)................................................. 2-14

TABLE 4-1: SAMPLING MODES OF THE M9110AH ..........................................................................4-1

TABLE 4-2: FRONT PANEL STATUS LED'S......................................................................................4-6

TABLE 4-3: OZONE GENERATOR START-UP TIMING ..................................................................... 4-10

TABLE 5-1: M9110AH SAMPLE MENU STRUCTURE .......................................................................5-4

TABLE 5-2: M9110AH SETUP MENU .............................................................................................5-5

TABLE 5-2: M9110AH SETUP MENU (CONTINUED).......................................................................5-6

TABLE 5-3: M9110AH SETUP MENU .............................................................................................5-7

TABLE 5-4: M9110AH SETUP MENU .............................................................................................5-8

TABLE 5-5: DAS DATA CHANNEL EDITING................................................................................... 5-17

TABLE 5-6: CALIBRATE, SETUP PASSWORDS............................................................................... 5-21

TABLE 5-7: M9110AH OPERATING MODES................................................................................. 5-23

TABLE 5-8: STATUS OUTPUT PIN ASSIGNMENTS......................................................................... 5-25

TABLE 5-9: RS-232 PORT SETUP - FRONT PANEL......................................................................5-26

TABLE 5-10: RS-232 SWITCHING FROM TERMINAL MODE TO COMPUTER MODE........................ 5-28

TABLE 5-11: RS-232 TERMINAL MODE EDITING KEYS.................................................................5-28

TABLE 5-12: RS-232 COMMAND SUMMARY ................................................................................ 5-30

TABLE 5-13: RS-232 COMMAND SUMMARY ................................................................................ 5-31

TABLE 5-14: RS-232 INTERFACE COMMAND TYPES....................................................................5-32

TABLE 5-15: RS-232 TEST MESSAGES....................................................................................... 5-33

TABLE 5-16: RS-232 WARNING MESSAGES................................................................................ 5-34

TABLE 5-17: RS-232 CALIBRATION MESSAGES........................................................................... 5-35

TABLE 5-18: RS-232 CALIBRATION COMMANDS.......................................................................... 5-36

TABLE 5-19: RS-232 DIAGNOSTIC COMMAND SUMMARY ............................................................5-37

TABLE 6-1: ZERO/SPAN VALVE OPERATION ....................................................................................6-2

TABLE 6-2: SETUP AUTOMATIC ZERO/SPAN CHECKING OR CALIBRATION........................................6-3

TABLE 6-3: ACTION OF MODE FIELD IN AUTOCAL..........................................................................6-4

TABLE 7-1: TYPES OF ZERO/SPAN CHECK AND CALIBRATION..........................................................7-2

TABLE 7-2: MANUAL ZERO CALIBRATION PROCEDURE - ZERO GAS THRU SAMPLE PORT................7-3

TABLE 7-3: ENTER EXPECTED SPAN GAS CONCENTRATIONS PROCEDURE.....................................7-4

TABLE 7-4: MANUAL SPAN CALIBRATION PROCEDURE - SPAN GAS THRU SAMPLE PORT.................7-5

TABLE 7-5: MANUAL ZERO CHECK PROCEDURE - Z/S VALVES........................................................7-6

TABLE 7-6: MANUAL SPAN CHECK PROCEDURE - Z/S VALVES........................................................7-7

TABLE 7-7: Z/S VALVE MODES WITH REMOTE CONTACT CLOSURE................................................7-8

TABLE 7-8: CALIBRATION REQUIREMENTS FOR AUTORANGE OR REMOTE RANGE........................ 7-10

TABLE 7-9: CALIBRATION QUALITY CHECK ................................................................................... 7-11

TABLE 7-10: CONVERTER EFFICIENCY - AUTOMATIC CALCULATION .............................................7-12

TABLE 8-1: PREVENTATIVE MAINTENANCE SCHEDULE.....................................................................8-1

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TABLE 9-1: TEST FUNCTIONS.........................................................................................................9-4

TABLE 9-1: TEST FUNCTIONS (CONTINUED)...................................................................................9-5

TABLE 9-1: TEST FUNCTIONS (CONTINUED)...................................................................................9-6

TABLE 9-1: TEST FUNCTIONS (CONTINUED)...................................................................................9-7

TABLE 9-2: FRONT PANEL WARNING MESSAGES ............................................................................9-9

TABLE 9-2: FRONT PANEL WARNING MESSAGES (CONTINUED)................................................... 9-10

TABLE 9-3: SUMMARY OF DIAGNOSTIC MODES ............................................................................ 9-11

TABLE 9-4: DIAGNOSTIC MODE - SIGNAL I/O................................................................................ 9-12

TABLE 9-4: DIAGNOSTIC MODE - SIGNAL I/O (CONTINUED).......................................................... 9-13

TABLE 9-4: DIAGNOSTIC MODE - SIGNAL I/O (CONTINUED).......................................................... 9-14

TABLE 9-4: DIAGNOSTIC MODE - SIGNAL I/O (CONTINUED).......................................................... 9-15

TABLE 9-5: MODEL 9110AH VARIABLES...................................................................................... 9-18

TABLE 9-6: TEST CHANNEL READINGS.........................................................................................9-19

TABLE 9-6: TEST CHANNEL READINGS (CONTINUED)...................................................................9-20

TABLE 9-7: MOTHERBOARD JUMPER SETTINGS........................................................................... 9-39

TABLE 9-1: V/F BOARD SWITCH SETTINGS.................................................................................. 9-39

TABLE 9-8: POWER SUPPLY MODULE SUBASSEMBLIES................................................................ 9-46

TABLE 9-9: POWER SUPPLY MODULE LED OPERATION............................................................... 9-49

TABLE 9-10: OZONE GENERATOR CONTROL CONDITIONS........................................................... 9-50

TABLE 10-1: TELEDYNE M9110AH SPARE PARTS LIST........................................................... 10-1

TABLE 10-1: TELEDYNE M9110AH SPARE PARTS LIST (CONTINUED).....................................10-2

TABLE 10-1: TELEDYNE M9110AH SPARE PARTS LIST (CONTINUED).....................................10-3

TABLE 10-2: TELEDYNE MODEL 9110AH EXPENDABLES KIT ................................................ 10-4

TABLE 10-3: TELEDYNE MODEL 9110AH LEVEL 1 SPARES KIT WITH MINI-HICON CONVERTER

............................................................................................................................................. 10-5

TABLE 10-4: TELEDYNE MODEL 9110AH LEVEL 1 SPARES KIT WITH MOLYBDENUM

CONVERTER.......................................................................................................................... 10-6

TABLE A-1: ELECTRICAL SCHEMATICS ........................................................................................... A-1

TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

1 HOW TO USE THIS MANUAL

The Model 9110AH has been designed to produce accurate data, be serviceable, reliable and easy to use. The M9110AH's microprocessor continually checks operating parameters such as temperature, flow, and critical voltages. The instruments design uses top mounted, modular components with captive screws to facilitate repair and ease of access. If you encounter any difficulty refer to the Troubleshooting Section 9 - General Hints.

We recognize that the need for information from this manual changes as time passes. When the instrument first arrives, it is necessary to get it up and running quickly and verify its correct operation. As time passes, more detailed information is often required on special configurations, calibration alternatives and other operational details. Finally there is the need for periodic maintenance and to quickly troubleshoot problems to assure maximum reliability and data integrity.

To address these needs, we have created three indexes to the information inside. They are: Table of Contents: Outlines the contents of the manual in the order the information is presented. This is a good

overview of the topics covered in the manual. There is also a list of Tables and a list of Figures. Index to M9110AH Front Panel Menus: The Menu Index briefly describes the front panel menus and refers you to other sections of the

manual that have a detailed explanation of each menu selection. Troubleshooting Section 9: The Troubleshooting Section allows you to diagnose and repair the instrument based on

variables in the TEST menu, the results of DIAGNOSTIC tests, and performance faults such as excessive noise or drift. The troubleshooting section also explains the operation, adjustment, diagnosis and testing of each instrument subsystem.

If you are unpacking the instrument for the first time, please refer to Getting Started in Section 2.

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

2 GETTING STARTED

2.1 Unpacking

CAUTION

Your safety and the safety of others is very important. We

have provided many important safety messages in this manual.

Please read these messages carefully.

To avoid personal injury, always use two persons to

lift and carry the Model 9110AH.

1. Before operation it is necessary to remove the shipping hold-down screws. Remove the instrument cover, then remove 2 screws as shown in Figure 2-1.

2. Also check for internal shipping damage, and generally inspect the interior of the instrument to make sure all circuit boards and other components are in good shape.

3. Please check the voltage and frequency label on the serial number tag on the rear panel. Compare that to your local power before plugging in the Instrument.

2.2 Electrical and Pneumatic Connections

1. Refer to Figure 2-2 to locate the rear panel electrical and pneumatic connections.

2. Attach the pump to the “Exhaust Out” port on the instrument rear panel. The exhaust from the pump should also be vented to atmospheric pressure.

3. Attach the sample inlet line to the sample inlet port. For initial testing, sample gas can be calibration gas or stack gas. The pressure of the sample gas at the inlet port should be at ambient pressure and constant. See Figure 2-3.

4. If desired, attach the analog output connections to a strip chart recorder and/or datalogger. Refer to Figure 9-4 - Analog Output Voltage Ranges - for switch settings. Factory default setting is 0-5 VDC.

5. Connect the power cord to the correct voltage line, then turn to Section 2.3 Initial Operation.

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electrical subassemblies.

WARNING

Analyzer Exhaust – O3 Scrubber – Pump Pack

Danger – Analyzer exhaust contains ozone.

Ozone scrubber must always be present between

analyzer exhaust and pump.

Vent pump exhaust to well ventilated area at atmosphere

pressure FIRE or EXPLOSION HAZARD.

WARNING

Lethal voltages present inside case.

Do not operate with cover off during normal operation.

Before operation check for correct

input voltage and frequency.

Do not operate without proper chassis grounding.

Do not defeat the ground wire on power plug. Turn off analyzer power before disconnecting

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Figure 2-1: Removal of Shipping Screws & Check for Correct Power

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Figure 2-2: Rear Panel

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Figure 2-3: Inlet and Exhaust Venting Recommendations

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

2.3 Initial Operation

1. Turn on the instrument power.

2. The display should immediately light, showing the computer’s memory configuration, then the instrument type - M9110AH. If you are unfamiliar with the M9110AH, we recommend that you read the overview Section 4 before proceeding. A diagram of the software menu trees is in Figure 5-1 and Figure 5-2.

3. The M9110AH requires about 30 minutes for all internal components to come to temperature. During this time the ozone generator power is OFF until the membrane dryer has time to purge itself, therefore there will be no response from the instrument, even if span gas is coming in the sample port. Many warning conditions are not displayed during this time, even though temperatures and other conditions are out of specification. All warning messages are enabled after 30 minutes of operation.

4. While waiting for instrument temperatures to stabilize, you can check for correct operation by using some of the M9110AH's diagnostic and test features.

5. Examine the TEST functions by comparing the values listed in Table 2-1 to those in the display. Remember that as the instrument warms up the values may not have reached their final values yet. If you would like to know more about the meaning and utility of each TEST function refer to Table 9-1. Also, now is a good time to verify that the instrument was shipped with the options you ordered. Table 2-1 also contains the list of options. Section 6 covers setting up the options.

6. Electric Test and Optic Test both generate simulated signals in the M9110AH.

A. Electric Test checks the electronics of the PMT signal path. To operate Electric Test from

the front panel:

1) Scroll the TEST function to PMT.

2) Press SETUP-MORE-DIAG, then press ENTR to accept the default password. Scroll to Electric Test and press ENTR to turn it on. Instrument responses should come to the values indicated in Table 2-1. To turn off this test press EXIT. For more information on the circuitry being tested refer to the Troubleshooting Section 9.1.3.2.

B. Optic Test is an "end to end" test of the analyzer HVPS-PMT-detector-electronics-

computer. It simulates a signal by turning on a LED in the Sensor Module. To operate Optic Test from the front panel:

1) Scroll the TEST function to PMT.

2) Press SETUP-MORE-DIAG, then press ENTR to accept the default password. Scroll to Optic Test and press ENTR to turn on optic test. Instrument response should come up to the values indicated in Table 2-1. To turn off this test press EXIT. To return to the SAMPLE mode press EXIT until SAMPLE is displayed in the upper left display. For more information about OT operation see Section 9.1.3.3.

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7. When the instrument is warmed up, re-check the TEST functions against Table 2-1. All of the readings should compare closely with those in the table. If they do not see Section 9.1.1. The next task is to calibrate the analyzer. There are several ways to do a calibration, they are summarized in Table 7-1. For a preliminary checkout we recommend calibration with span gas coming in through the sample port. The procedure is:

Step 1 - Set the range, then enter the expected NOx and NO span gas concentrations:

Step Number Action Comment

1. Press CAL-CONC-NOX

2. Press ENTR ENTR stores the expected NOx span value. The internal

3. Press CAL-CONC-NO

4. Press ENTR ENTR stores the expected NO span value. The internal

5. Press EXIT Returns instrument to SAMPLE mode.

6. Press SETUP-RNGEMODE-SNGL

7. Press SETUP-RNGESET

This key sequence causes the M9110AH to prompt for the expected span concentration. Enter the span value by pressing the key under each digit until the expected value is set.

formulas are adjusted to compute this number when span gas concentration is input into the instrument.

In the same CAL-CONC sub menu press the NO button and enter the expected NO span value. As before this value will be used in the internal formulas to compute the NO concentration value.

formulas are adjusted to compute this number when span gas concentration is input into the instrument.

If necessary, you may want to change ranges. Normally the instrument is shipped in single range mode set at 100 ppm. We recommend doing the initial checkout on the 100 ppm range.

After SETUP-RNGE-SET, enter 100 and press ENTR. The instrument will now be in the 100 ppm range.

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Step 2 - Calibrate the instrument:

Zero/Span Calibration Procedure

Step Number Action Comment

1. Input Zero gas Allow Zero gas to enter the sample port on the rear of the

instrument.

2. Press CAL The M9110AH enters the calibrate mode from sample mode.

3. Wait 10 min Wait for reading to stabilize at the zero value. If you wait less

than 10 minutes the final zero value may drift.

4. Press ZERO The ZERO button will be displayed.

5. Press ENTR Pressing ENTR actually changes the equations and zeros the

instrument.

6. Press EXIT, input Span gas

7. Wait 10 min Wait for reading to stabilize at the span value.

8. Press SPAN The SPAN button should be displayed. If there is no SPAN

9. Press ENTR Pressing ENTR actually changes the equations so that the

10. Press EXIT Pressing EXIT returns the instrument to SAMPLE mode.

M9110AH returns to the CAL menu. Now switch gas streams to span gas.

button check the Troubleshooting Section 9.2.8 for instructions on how to proceed. In certain circumstances at low span gas concentrations both the ZERO and SPAN buttons will appear.

concentration displayed is the same as the expected span concentration you entered above, thus spanning the instrument.

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Step 3 - Review Quality of calibration:

Calibration Quality Check Procedure

Step Number Action Comment

1. Scroll the TEST function menu until the NOx SLOPE is displayed.

2. Scroll the TEST function menu until the NO SLOPE is displayed.

4. Scroll the TEST function menu until the NOx OFFS is displayed.

5. Scroll the TEST function menu until the NO OFFS is displayed.

The SLOPE value for NOx should be 1.0  0.3. If the value is not in this range, check Section 7.1 or 9. If the SLOPE value is in the acceptable range the instrument will perform optimally.

The SLOPE value for NO should be 1.0  0.3. If the value is not in this range, check Section 7.1 or 9. If the SLOPE is in the acceptable range the instrument will perform optimally.

NOTE: The NO and NOx slopes should be equal within  0.3.

The M9110AH will display the OFFSET parameter for the NOx equation. This number should be near zero. A value of

0.0 50 indicates calibration in the optimal range. If the OFFSET value is outside this range, check Section 7.1 or 9.1 for procedures to correct the OFFSET value to near zero.

The Instrument will now display the NO OFFSET value. It should also have a value near zero (0.0 50).

Step 4 - The M9110AH is now ready to measure sample gas.

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Figure 2-4: Front Panel

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Figure 2-5: Assembly Layout

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Table 2-1: Final Test and Calibration Values

TEST Values

RANGE ppm 5-5000 5.3.4 NOISE ppm 0.0 - 0.2 9.1.1, Table 9-1, 9.2.5 SAMP FLW cc/min 300  50 (Default)

OZONE FL cc/min 250  15 9.3.6 PMT mV 0-5000 9.3.8

AUTOZERO mV -10 to +50 4.1 HVPS V 400 - 700 constant 9.3.8.5 DCPS mV 2500  200 9.3.5

RCELL TEMP BLOCK TEMP BOX TEMP

PMT TEMP CONV TEMP

Observed Value

Units Nominal Range Reference Section

9.3.7, Table 9-1

550  50 (Optional)

C 50  2 9.3.8.2

C 50  2 9.3.4.1

C 8-48 9.3.4.1

C 7  1 9.3.8.4

C 700  10 (Std)

315  5 (Moly)

9.3.4.1

RCEL PRES IN-Hg-A 2 - 10 constant 9.3.7 SAMP PRES IN-Hg-A 25 - 30 constant 9.3.7

Electric Test &Optic Test

Electric Test

PMT Volts mV 2000  200 9.1.3.2 NO Conc ppm 250  25 9.1.3.2 NOx Conc ppm 250  25 9.1.3.2

OPTIC TEST

PMT Volts mV 100  20 9.1.3.3 NO Conc ppm 12.5  2 9.1.3.3 NOx Conc ppm 12.5  2 9.1.3.3

(table continued)

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

Table 2-1: Final Test and Calibration Values (Continued)

Parameter

NO Span Conc ppm 0.5 - 5000 Table 7-3 NOx Span Conc ppm 0.5 - 5000 Table 7-3 NO Slope - 1.0  0.3 7.1, 7.9

NOx Slope - 1.0  0.3 7.1 NO Offset mV  25 7.1, 7.2 NOx Offset mV  25 7.1, 7.2 Conv Efficiency % 0.75 - 1.10 7.10, 5.2.2.6

Noise at Zero ppm 0.0 - 0.2 Table 9-1 Noise At Span ppm 0.1 - 0.5 Table 9-1

Sample Flow cc/min 50 20 9.3.7, Figure 9-8 Bypass Flow cc/min 250 (Std)

Ozone Flow cc/min 250  15 9.3.7, Figure 9-8

Factory Installed Options Option Installed

Observed Value

Units Nominal Range Reference Section

Measured Flows

Figure 8-4

500 (Optional)

Power Voltage/Frequency Rack Mount, w/ Slides Rack Mount, w/ Ears Only Rack Mount, External Pump w/o Slides Stainless Zero/Span Valves 4-20 mA Current Loop Output, Isolated Bypass flow 500 cc/min Molybdenum Converter Desiccant Canister - O3 generator

PROM # Serial # Date Technician

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

INTENTIONALLY BLANK

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

3 SPECIFICATIONS, WARRANTY

3.1 Specifications

Operating Modes Ranges In 1 ppm increments from 5 ppm to 5,000 ppm

Noise at zero 0.02 ppm RMS Noise at span <0.2% of reading RMS above 20 ppm Detection Limit(Note 1) 0.04 ppm RMS Zero Drift (Note 2) <0.2% full scale/24 hours Zero Drift (Note 2) <0.4% full scale/7 days Span Drift (Note 2) <1% FS/24 hours Lag Time Switching Mode 20 sec (Note 3)

mode

Response Time Switching Mode 95% in < 40 sec (Note 3)

mode

Sample Flow Rate 290 10 cc/min (Including bypass) Linearity 1% of full scale

Precision 0.5% of reading Temperature Range 5-40o C Humidity 0-95% RH non-condensing Temp Coefficient < 0.1% per o C Voltage Coefficient < 0.1% per V Dimensions HxWxD 7"x17"x23.6" (18 cm x 43 cm x 61 cm) Weight, Analyzer 43 lbs (20 kg) Weight, Pump Pack 16 lbs (7 kg) Power, Analyzer 100 V~ 50/60 Hz, 120 V~ 60 Hz, 220 V~ 50 Hz, 240 V~ 50 Hz, 200 watts Power, Analyzer Power, Ext Pump 110 V~ 60 Hz, 220 V~ 50 Hz, 240 V~ 50 Hz, 295 watts Power, Ext Pump Environmental Installation Category (Over-voltage Category) II Pollution Degree 2 Analog Resolution 1 part in 2048 of selected voltage or current range Recorder Output 0-100 mV, 0-1, 5, 10v, bipolar Current Loop Option 4-20ma isolated Status 12 Status Outputs from opto-isolator Measurement Units ppm, mg/m3

230 V~ 50 Hz, 2.5A

NO/NOx switching mode, NO only mode, NOx only mode Single range, independent ranges or autoranging

4 sec (Note 3)

95% in < 10 sec (Note 3)

1. Defined as twice the zero noise level.

2. At constant temperature and voltage.

3. Lag & response times longer for external converter option.

4. Electrical ratings for CE Mark compliance.

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TELEDYNE Model 9110AH NOX Analyzer Operator Manual, 01620, Rev. F

3.2 Warranty

WARRANTY POLICY (02024c)

Prior to shipment, TELEDYNE equipment is thoroughly inspected and tested. Should equipment failure occur, TELEDYNE assures its customers that prompt service and support will be available.

COVERAGE

After the warranty period and throughout the equipment lifetime, TELEDYNE stands ready to provide on-site or in-plant service at reasonable rates similar to those of other manufacturers in the industry. All maintenance and the first level of field troubleshooting is to be performed by the customer.

NON-TELEDYNE MANUFACTURED EQUIPMENT

Equipment provided but not manufactured by TELEDYNE is warranted and will be repaired to the extent and according to the current terms and conditions of the respective equipment manufacturers warranty.

GENERAL

TELEDYNE warrants each Product manufactured by TELEDYNE to be free from defects in material and workmanship under normal use and service for a period of one year from the date of delivery. All replacement parts and repairs are warranted for 90 days after the purchase.

If a Product fails to conform to its specifications within the warranty period, TELEDYNE shall correct such defect by, in TELEDYNE's discretion, repairing or replacing such defective Product or refunding the purchase price of such Product.

The warranties set forth in this section shall be of no force or effect with respect to any Product: (i) that has been altered or subjected to misuse, negligence or accident, or (ii) that has been used in any manner other than in accordance with the instruction provided by TELEDYNE or (iii) not properly maintained.

THE WARRANTIES SET FORTH IN THIS SECTION AND THE REMEDIES THEREFORE ARE EXCLUSIVE AND IN LIEU OF ANY IMPLIED WARRANTIES OF MERCHANTABILITY, FITNESS FOR PARTICULAR PURPOSE OR OTHER WARRANTY OF QUALITY, WHETHER EXPRESSED OR IMPLIED. THE REMEDIES SET FORTH IN THIS SECTION ARE THE EXCLUSIVE REMEDIES FOR BREACH OF ANY WARRANTY CONTAINED HEREIN. TELEDYNE SHALL NOT BE LIABLE FOR ANY INCIDENTAL OR CONSEQUENTIAL DAMAGES ARISING OUT OF OR RELATED TO THIS AGREEMENT OF TELEDYNE'S PERFORMANCE HEREUNDER, WHETHER FOR BREACH OF WARRANTY OR OTHERWISE.

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Teledyne 9110AH User Manual

Specifications and Main Features

Frequently Asked Questions

User Manual