SKC Limited Universal Pump Step User Manual

www.skcltd.com
Step by Step Guide
An Introduction to Air Sampling
Universal Pump
Contents
The Universal Air Sampling Pump ......................................................................................................................1
The I.O.M. Sampler ...........................................................................................................................................2
Inhalable Dust Sampling using the I.O.M. Sampler .............................................................................................3
Respirable Dust Sampling using the Cyclone Sampler .......................................................................................6
Gas & Vapour Sampling using Sorbent Tubes ..................................................................................................10
Gas & Vapour Sampling using Impingers .........................................................................................................13
Bag Sampling using the Universal Pump .........................................................................................................15
Duct Sampling for Volatile Organic Compounds ...............................................................................................16
The Sample Train .............................................................................................................................................17
Sample Train Check List .................................................................................................................................. 17
A helping hand from the experts
This guide is designed as an introduction to the basic principles of air sampling methods. The advice in this guide deals with the setting up of equipment only.
Advice notes relating to specific sampling methods can be obtained from the HSE (www.hse.gov.uk) and these will give you a good understanding of the approach you should take to sampling in your particular industry.
As an expert in the field of air sampling, SKC believe in supporting customers every step of the way, so in addition to the Step By Step guides there is a range of training seminars available to help you get the best from your sampling equipment.
If you are new to air sampling, our one day seminar 'A Practical Course in Air Monitoring' will give you the help you need to get started.
The course includes both theoretical and practical sessions in the use of air sampling equipment. An experienced practitioner will offer valuable input on sampling strategy and will assist with instrument configuration and calibration. You will soon have everything you need to formulate a professional monitoring programme.
Contact SKC Limited customer services today for details on courses and available dates:
T: +44 (0) 1258 480188
E: info@skcltd.com
W: www.skcltd.com
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The Universal Air Sampling Pump
LCD display Air inlet hosetail
Keypad
Keypad cover
Keypad cover screw
Flow adjust screw
Exhaust port cover
On/off switch
Inlet filter housing
Inlet filter
Inlet filter O ring
Filter housing screws
Accessory mounting screws
Flow indicator*
*The flow indicator is for use only to identify changing flow conditions during sampling, such as a reduction in flow caused by a crimped tube. It must not be used to calibrate the sample flow rate.
Low flow mode screw cover
Belt clip
Charging jack socket
Cover over low flow regulator
Battery pack
Battery pack screws
Model depicted - 224-PCTX8
Features vary by model
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The I.O.M. Sampler*
IMPORTANT
The I.O.M. cassette and filter paper combined must be pre and post weighed together for an
accurate inhalable result
The I.O.M. sampler is designed and closely adheres to the definition for inhalable dust given in EN481
I.O.M. - what does it stand for? The "Institute of Occupational Medicine". Based in Edinburgh, researchers at the Institute developed this sampler to overcome some of the difficulties encountered with other sampling devices. It is less prone to the effects of air movement around it than others and utilises a cassette rather than just a filter paper. There is a very good reason for the cassette system being adopted. One of the problems with other devices using a filter paper alone is loss of sample on the walls of the sampler itself. The dust which coats the walls of the sampler is not normally included in the results, hence under sampling is a possibility. With the I.O.M. sampler this problem is overcome by using a cassette with the filter inside. It is important that when a sample is taken the cassette and filter paper are pre and post weighed as a single unit. By doing this all the dust on both the filter paper and on the internal walls of the cassette are included.
†Foam plug only required for respirable sampling
*Not required on stainless steel I.O.M. sampler
The diagram below shows the component parts of the sampler and how they are put together.
To fit a filter unscrew the front plate. The cassette, comprising the inlet spout and filter support grid can now be removed by pulling forward gently. The two halves of the cassette clip together and can be separated with gentle pressure. Once separated a filter can be placed in the support grid. Snap the inlet spout into the support grid making sure it is seated down properly. The cassette is replaced into the body of the sampler and the front plate screwed on firmly so that all of the O ring seals are compressed, thus ensuring there are no leaks.
For further information on the I.O.M. sampler see :­1986 paper, “New Personal Sampler For Airborne Total Dust In The Workplace” by D Mark / J Vincent. Ref: Annals Occupational Hygiene No. 30 Pages 89-102.
Spring
Clip
O Ring*
Support
Grid
Cassette
Cap
Front Plate
O Rings
Foam Plug†
Cassette
Inlet
Spout
Filter
Cassette
Dust Sampling - Inhalable and Respirable
The I.O.M. sampler can also be used for respirable dust sampling by inserting a foam plug into the inlet spout part of the cassette. The foam plug size selects some of the dust that is drawn though it and allows
Foam Plug Cassette Inlet Spout
the correct type of dust to be collected on the filter. It is also possible to measure both the inhalable and respirable dust fractions in one sample using the foam plug and I.O.M. cassette.
Sampler
Body
Rear view of front
plate showing
O ring positions
Sealing Cap
Ref: Report IR/EXM/99/06 produced by the Health and Safety Laboratory (UK). Available on the HSE web site. *Manufactured under license from the Institute of Occupational Medicine TM 2043339E.
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Inhalable Dust Sampling using the I.O.M. Sampler
For information on using the I.O.M. sampler for respirable dust fractions
please contact SKC customer support on +44 (0) 1258 480188
Inhalable dust is taken to mean any solid particle which by its small size can be carried in an airflow or remains airborne. It includes the thoracic and respirable dust fractions. The inhalable dust fraction size is defined in the standard EN481. More information is also given in SKC’s Basic Step By Step Guide (224-G1).
You will need :-
• Universal sample pump (fully charged)
• I.O.M. sampler
• A length of flexible tubing
• Two filter papers from the same box or batch
• Flow calibration device capable of measuring 2
litre/min, such as the Defender primary calibrator or a rotameter
• ‘Calidaptor’ calibration adaptor for the I.O.M.
sampler
• Toolkit to adjust the pump flow rate
3
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The correct flow rate for the I.O.M. sampler is 2.0 litre/min
1. Mount one of the filter papers into the I.O.M. cassette. Place the cassette into the sampler body and screw on the front cover.
2. Connect the I.O.M. sampler with filter paper fitted, to the inlet hosetail of the sample pump using the flexible tubing. The inlet hosetail on the Universal is mounted on the right hand side of the pump.
3. To set the flow rate required, in this case 2.0 litre/minute, a flow calibration device such as a Defender primary calibrator or a rotameter, and a ‘calidaptor’ should be used. Make sure the flow calibrator is capable of measuring the required flow rate. There are two types of float used in rotameters. To read them correctly depends on the type. To read a ball type rotameter correctly take the reading at the centre of the ball. To read a float type rotameter correctly take the reading at the top edge of the float. The float of a float
NOTE: MDHS 14/3 states that a primary standard such as the Defender should be used for flow calibration in favour of rotameters.
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Inhalable Dust Sampling using the I.O.M. Sampler
type rotameter is usually marked with a number of dots. The dots give indication that the float is spinning in the airflow, thus showing that it is not touching the walls of the rotameter tube which could affect the accuracy of the reading. Note that the rotameter must be placed onto a flat, level surface to ensure that the float does not touch the sides of the rotameter tube.
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Ball Type Float Type
Read Here Read Here
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4. The I.O.M. sampler with filter fitted is placed onto the foam sealing pad on the top of the calidaptor. Secure the I.O.M. sampler to the calidaptor using the finger screw, ensuring a good seal of the front face of the I.O.M. sampler to the foam pad. The hosetail fitting supplied with the calidaptor is screwed into the hole in the bottom of the calidaptor. The calidaptor hosetail is connected to the hosetail on the Defender primary calibrator marked ‘Suction’, with the length of tubing supplied with the calidaptor. Turn on the Defender primary calibrator and set it to take continuous flow readings.
with the calidaptor to connect the calidaptor to the rotameter. Fit the I.O.M. sampler to the calidaptor and secure with the finger screw.
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6. The pump flow rate is adjusted using the smallest bladed screwdriver attachment of the toolkit supplied with the pump. Unscrew and remove the keypad cover from the pump and switch on the pump using the on/off switch. Use the screwdriver tool to turn the adjustment screw labelled ‘FLOW ADJ’. As the screw is turned the flow reading on the flow calibrator should increase or decrease. If this does not happen check the system for leaks or blockages. One common cause of lack of flow is by using the separation papers (usually coloured blue) sometimes found in boxes of filters, instead of the filters themselves (usually white). Once the flow is set to the required level of 2.0 litre/min, switch the sample pump off.
7. Remove the I.O.M. sampler from the calidaptor and then remove the filter cassette from the sampler. Remove the filter paper from the cassette, and ensure that the cassette inlet spout and support grid are clean and free of contamination. Fit the second filter paper into
5. If using a rotameter to set the flow rate, the calidaptor is designed to screw directly into the inlet in the top of SKC rotameters. Unscrew the hosetail fitting supplied with the rotameter, and screw the calidaptor into the threaded hole in the top of the rotameter, fastening tightly to ensure a good seal. If using a non-SKC rotameter, use the hosetail fitting and length of tubing supplied
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the cassette. Pre-weigh the filter and cassette, and then fit the cassette back into the I.O.M. sampler. Check the flow once again with the pre­weighed filter and cassette in place and make any final adjustments needed to bring the flow to the required level. It is advisable to do this as quickly as possible to minimise the chance of collecting anything that may affect the final
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