Sierra Top-Trak 820 Series, Top-Trak 820, Top-Trak 822S, Top-Trak 824, Top-Trak 820S Instruction Manual

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Sierra 820 Series

Top-Trak™ Mass Flow Meters

Models: 820, 820S, 822, 822S, 824, 824S, 826 and 827

Instruction Manual

Part Number IM-82

Revision H, November 2017

Page 2

Table of Contents Series 820 Instruction Manual

GLOBAL SUPPORT LOCATIONS: WE ARE HERE TO HELP!

CORPORATE HEADQUARTERS

5 Harris Court, Building L Monterey, CA 93940 Phone (831) 373-0200 (800) 866-0200 Fax (831) 373-4402

www.sierrainstruments.com

EUROPE HEADQUARTERS

Bijlmansweid 2 1934RE Egmond aan den Hoef The Netherlands Phone +31 72 5071400 Fax +31 72 5071401

ASIA HEADQUARTERS

Second Floor Building 5, Senpu Industrial Park 25 Hangdu Road Hangtou Town Pu Dong New District, Shanghai, P.R. China Postal Code 201316 Phone: + 8621 5879 8521 Fax: +8621 5879 8586

IMPORTANT CUSTOMER NOTICE: OXYGEN SERVICE

Sierra Instruments, Inc. is not liable for any damage or personal injury, whatsoever, resulting from the use of Sierra Instruments standard ma ss flow meters or controllers for oxygen gas. You are responsible for determining if this mass flow meter or controller is appropriate for your oxygen application. You are responsible for cleaning the mass flow meter or controller to the degree required for your oxygen flow application

No part of this publication may be copied or distributed, transmitted, transcribed, stored in a retrieval system, or translated into any human or computer language, in any form or by any me ans, electronic, mechanical, manual, or otherwise, or disclosed to third parties without the express written permission of Sierra Instruments. The information contained in this manual is subject to change without notice.

TRADEMARKS

Top-TrakTM and Cal-Bench TM is a Registered Trademark of Sierra Instruments, Inc. Other product and company names listed in this manual are tradem arks or trade names of their respective manufacturers.

Page 3

Series 820 Instruction Manual Table of Contents

Table of Contents

Chapter 1 Introduction

Introduction ......................................................................... 1-1

Using this Manual .............................................................. 1-1

Safety Information ............................................................. 1-2

Receipt of System Components ........................................ 1-2

Technical Assistance .......................................................... 1-2

Top Trak Features .................................................................... 1-3

The 820 Series Flow Sensing Principle ................................... 1-4

Chapter 2 Installation

Installation Overview ............................................................... 2-1

Installing the Transducer .......................................................... 2-2

Compression Fittings ......................................................... 2-2

VCO Fittings ................................................................. 2-2

VCR Fittings .................................................................. 2-3

All 1/2-inch Size Connections ........................................... 2-3

Wiring the Transducer ............................................................. 2-4

Standard 0-5 VDC Output Signal Wiring ......................... 2-5

Optional 4-20 mA Output Signal Wiring .......................... 2-5

Remote Display Installation ..................................................... 2-6

Chapter 3 Operation

Transducer Operation ...............................................................

Transducer Accuracy ......................................................... 3-1

Referencing the Transducer to Non-Standard Conditions .... 3-2

Transducer Over-Ranging ................................................. 3-2

Zero and Span Adjustments ............................................... 3-3

Totalizer Option ................................................................. 3-4

Chapter 4 Maintenance and Repair

Transducer Cleaning ................................................................ 4-1

Flow Path Cleaning Model 822/824 ........................................ 4-2

Inlet and Outlet Screens ..................................................... 4-2

Laminar Flow Element ...................................................... 4-3

Flow Path Cleaning Model 826/827 ........................................ 4-4

Laminar Flow Element ...................................................... 4-4

Flow Path Cleaning Model 822-S/824-S ................................ 4-5

Laminar Flow Element ...................................................... 4-5

Sensor Cleaning and Inspection ........................................ 4-8

Transducer Calibration ............................................................. 4-9

Transducer Troubleshooting .................................................... 4-11

Returning Equipment to the Factory ....................................... 4-13

3-1

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Table of Contents Series 820 Instruction Manual

Appendix A Conversion Formulas and Gas Tables Appendix B 822/824 Product Specifications Appendix C 822S/824S Product Specifications Appendix D 826/827 Product Specifications

List of Figures

1-1. Top-Trak Features (Typical) ........................................ 1-3

1-2. Flow Paths through the Transducer ............................. 1-4

1-3. Flow Measuring Principle ............................................ 1-4

2-1. Piping Requirements for 1/2-inch Size Connections .. 2-3

2-2. Transducer D-Connector Pin Assignments ................. 2-4

2-3. Standard 0-5 VDC Output Signal Wiring ................... 2-5

2-4. Single Transducer Current Loop Connection .............. 2-5

2-5. Multiple Transducer Current Loop Connections ........ 2-6

2-6. Mounting the Remote Display ..................................... 2-6

4-1. Model 822/824 Flow Components .............................. 4-2

4-2. Correct LFE Position ................................................... 4-3

4-3. Model 826/827 Flow Components ............................... 4-4

4-4. Low Flow Transducer LFE Cleaning .......................... 4-5

4-5. Medium Flow Transducer LFE Cleaning ................... 4-6

4-6. High Flow Transducer LFE Cleaning ......................... 4-7

4-7. Printed Circuit Board Component Locations .............. 4-11

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Series 820 Instruction Manual Table of Contents

Cautions

Caution!

Only qualified personnel should install the transducer.

Do not supply +DC power at the D-connector while using a

power supply at the power jack. Both supplies may be damaged.

Caution!

Operating a 12 VDC transducer at 24 VDC will cause equip-

ment damage.

Caution!

Only qualified personnel should perform transducer service, ca-

libration or troubleshooting procedures.

Caution!

When using toxic or corrosive gases, purge the unit thoroughly

with inert dry gas before disconnecting from the gas line.

Caution!

Printed circuit boards are sensitive to electrostatic discharge. To avoid damaging the board, follow these precautions to minimize the risk of damage:

 before handling the assembly, discharge your body by touching

a grounded, metal object

 handle all cards by their edges unless otherwise required  when possible, use grounded electrostatic discharge wrist

straps when handling sensitive components

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Page 7

Series 820 Instruction Manual Chapter 1 Introduction

Chapter 1 Introduction

This instruction manual covers the installation, operation and maintenance of Sierra’s 820 Series product line including the following Top-Trakª Models:

 822 Mass Flow Meter with display (nylon flow body)  824 Mass Flow Meter without display (nylon flow body)  826 Hi-Flow Meter with display (aluminum flow body)  827 Hi-Flow without display (aluminum flow body)  822-S Mass Flow Meter with display (stainless steel flow body)

 824-S Mass Flow Meter without display (stainless steel flow body)

Sierra’s Top-Trakª Mass Flow Meters are designed for precise measurement of gas mass flow. The 820 Series offers a broad range of sizes and process connections for flexibility and versatility. The primary standard calibration ensures starting point accuracy and NIST traceability. The meter’s 0-5 VDC or 4-20 mA output signal is provided for recording, data-logging or control. The optional display reads the mass flow rate directly in engineering units or percentage of full scale.

Using This Manual

This manual is organized into four chapters:

 Chapter 1 includes the introduction and theory of operation  Chapter 2 provides installation and wiring instructions  Chapter 3 describes transducer operation and features  Chapter 4 covers maintenance, calibration and troubleshooting

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Gas tables and conversion formulas are found in Appendix A. The product specifications and dimensional drawings are found in Appendix B.

Throughout this manual, we use the word

transducer

as a generic term to represent all models of Sierra’s 820 Series TopTrak Mass Flow Meters.

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Chapter 1 Introduction Series 820 Instruction Manual

Safety Information

Caution and warning statements are used throughout this book to draw your attention to important information.

Warning! Caution!

This statement appears with information that is important to protect people and equipment from damage. Pay very close attention to all warnings that apply to your application.

Receipt of System Components

When receiving a Sierra transducer, carefully check the outside packing carton for damage incurred in shipment. If the carton is damaged, notify the local carrier and submit a report to the factory or distributor. Remove the packing slip and check that all ordered components are present and match your specifications (as ordered). Make sure any spare parts or accessories are not discarded with the packing material. Do not return any equipment to the factory without first contacting Sierra Customer Service.

This statement appears with information that is important for protecting your equipme nt and performance. Read and follow all cautions that apply to your application.

Technical Assistance

If you encounter a problem with your transducer, review the configuration information for each step of the installation, operation and set up procedures. Verify that your settings and adjustments are consistent with factory recommendations. Refer to Chapter 4, Troubleshooting, for specific information and recommendations.

If the problem persists after following the troubleshooting procedures outlined in Chapter 4, contact Sierra Instruments by fax or by E-mail (see inside front cover). For urgent phone support you may call (800) 866-0200 or (831) 373-0200 between 8:00 a.m. and 5:00 p.m. PST. In Europe contact Sierra Instruments bv at +31 20

6145810. When contacting Technical Support, make sure to include this information:

 the flow range, serial number, Sierra order number and

model number (all marked on the transducer nameplate)

 the problem you are encountering and any corrective action

taken

 application information (gas, pressure, temperature, pipe

and fitting configuration)

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Series 820 Instruction Manual Chapter 1 Introduction

Top-Trak Features

Standard Top-Trak Mass Flow Meters require a 12 to 15 VDC external power source (24 VDC input power optional). The transducer’s 0 to 5 VDC output signal allows for flow recording, data-logging or control. A 4 to 20 mA output signal is optionally available. Input power and output signal connections are made via the 9-pin subtype D-connector located on the side of the transducer. An additional input power jack is located just below the D-connector. (It is important to connect input power at only one location.)

The transducer shown below is a typical example of a 822 Series Top-Trak Mass Flow Meter. Other models may vary slightly in their appearance but are operationally equivalent.

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Figure 1-1. Top-Trak Features (Typical)

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Chapter 1 Introduction Series 820 Instruction Manual

The 820 Series Flow Sensing Principle

The operating principle of Top-Trak transducers is based on heat transfer and the first law of thermodynamics. During operation process gas enters the instrument’s flow body and divides into two flow paths, one through the sensor tube, the other through the laminar flow element bypass. The laminar flow bypass generates a pressure drop, P1–P2, forcing a small fraction of the total flow to pass through the sensor tube (m1).

Figure 1-2. Flow Paths through the Transducer

Two resistance temperature detector (RTD) coils around the sensor tube direct a constant amount of heat (H) into the gas stream. In actual operation, the gas mass flow carries heat from the upstream coil to the downstream coil. The resulting temperature difference (?T) is detected by the RTD coils and gives the output signal. Since the molecules of the gas carry away the heat, the output signal is linearly proportional to gas mass flow.

Figure 1-3. Flow Measuring Principle

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Series 820 Instruction Manual Chapter 2 Installation

Chapter 2 Installation

Installation Overview

To ensure a successful installation, inlet and outlet tubing should be clean and free from burrs or rims caused by cutting prior to plumbing the transducer into the system. The protective caps covering the inlet/outlet fittings should not be removed until immediately prior to installation.

Before installing the transducer, verify the following:

1. Make sure the installation site meets the specific operating parameters recorded on the transducer’s nameplate. Each transducer is factoryconfigured for a specific gas and flow range. If the operating pressure is more than 50 psi (3.4 bar) away from the calibration pressure, it is advisable to return the unit to the factory for re-calibration. (Adjusting zero may be sufficient to remain within specification.)

2. Do not locate the transducer in areas subject to sudden temperature changes, moisture, drafts or near equipment radiating significant amounts of heat. Make sure to allow adequate space for cable connectors and wiring.

3. For 1/2-inch size inlet/outlet process connections on models 826 and 827 make sure the location meets the minimum number of recommended pipe diameters upstream and downstream of the transducer. A minimum of 5 inches (127 mm) upstream and 2-1/2 inches (64 mm) downstream is always recommended. (not necessary for other models)

4. Horizontal mounting is preferable. Vertical mounting is possible with best results achieved when the factory calibration is specifically performed for vertical mounting. In vertical positions zero shift will occur depending on the gas pressure at zero flow.

5. If the gas contains any particulate matter, install an in-line filter prior to the transducer. Recommended filter size: 15 micron for flows of 10 sccm to 30 slpm, 30 micron for above 30 slpm.

6. If a potential over-flow condition exists, insert a valve or critical orifice in the line to limit flow to approximately 25 percent above the full scale range of the meter.

7. Confirm that the transducer o-ring material is compatible with the gas to be measured.

8. For remote displays, confirm the supplied cable is of sufficient length to connect the components.

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Chapter 2 Installation Series 820 Instruction Manual

Installing the Transducer

Follow the installation instructions that apply to your transducer’s

Caution!

Only qualified personnel

should install the

transducer.

process connection. For all 1/2-inch size process connections, observe the piping recommendations given on page 2-3. Before operation, all plumbing should be checked carefully for leaks and the transducer purged with dry nitrogen.

Compression Fittings

1. Position the transducer with the flow direction arrow pointing downstream in the direction of flow.

2. Verify the position of the front and back ferrule. Insert the tubing into the fitting. Make sure that the tubing rests firmly on the shoulder of the fitting and that the nut is finger tight. (Do not mix or interchange parts of tube fittings made by different manufactur- ers.)

3. Hold the body steady with a backup wrench.

tighten the nut 1-1/4 turns from finger tight. For 1/8-inch, 1/4- inch and 3∕8-inch sizes, tighten only 3/4 turn from finger tight.

over-tighten!

4. Check the system’s entire flow path thoroughly for leaks. (Do not use liquid leak detectors, instead monitor pressure decay. Overexposing the transducer to leak detector fluid may damage the unit.)

For 1/2-inch size,

Do not

VCO Fittings

1. Position the transducer with the flow direction arrow pointing

2. Install new o-rings compatible with the gas to be used. (Do not mix

3. Hold the body steady with a backup wrench.

4. Check the system’s entire flow path thoroughly for leaks. (Do not use

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downstream in the direction of flow.

or interchange parts of tube fittings made by different manufacturers.)

Tighten the nut

finger tight and then 1/4 turn tighter with a wrench.

tighten!

Do not over-

liquid leak detectors, instead monitor pressure decay. Over- exposing the transducer to leak detector fluid may damage the unit.)

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Series 820 Instruction Manual Chapter 2 Installation

1/4 inch Female NPT Connections

1. Position the transducer with the flow direction arrow pointing in the direction of flow.

Use a good quality paste pipe thread sealant. Apply to pipe threads.

3. Tighten the pipe no more than 1 turn past hand-tight. Caution! Do not over-tighten. Damage to the instrument may result.

1/2-Inch Size NPT Connections

1. Install a section of straight pipe at least ten pipe diameters in length up-

stream of the transducer. Also, allow at least five pipe diameters downstream for accurate operation. DO NOT use reducers. If the preceeding components in the flow path create disturbances extend the upstream pipe length.

2. Position the transducer with the flow direction arrow pointing down-

stream in the direction of flow.

3. Tighten fittings until leak tight (refer to published standards for specific

recommendations).

(standard on nylon flow bodies

)

4. Check the system’s entire flow path thoroughly for leaks. (Do not use liq-

uid leak detectors, instead monitor pressure decay. Over-exposing the transducer to leak detector fluid may damage the unit.)

Figure 2-1 Piping Requirements for all 1/2-Inch Size Process Connections

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Page 14

Chapter 2 Installation Series 820 Instruction Manual

Caution!

Do not supply +DC powe

at the D-connector whil using a power supply a the power jack. Both sup-

plies may be damaged.

Caution!

Operating a 12 VDC trans-

ducer at 24 VDC will cause

equipment damage.

Wiring the Transducer

Standard Top-Trakrm transducers require a 12 to 15 VDC power supply (15 VDC nominal, 100 mA maximum). 24 VDC input power is optional. Transducers are connected to the power supply through

either

the dedicated DC power jack or through the 9-pin D-connector located on the side of the enclosure. Before powering the unit, check the transducer’s nameplate to confirm input power:

 PV1 = 12 to 15 VDC  PV2 = 24 VDC

Note: operating a 24 VDC transducer at 12 to 15 VDC will result in unreliable operation.

The transducer’s standard 0 to 5 VDC (4-20 mA optional) output sig- nal is available through the D-connector. The mating connector is in- cluded with the transducer. Connection details are given on the fol- lowing pages.

When the transducer is configured for a remote display, signal connections are made via the 9-pin connector. Input power connections are not included in the standard interface cable. Power connections for the display and the transducer are shared when the connector is wired for a remote display. Optionally the input power can be applied at the power jack (either 12 volts (PV 1) or 24 volts (PV2). Remote display mounting dimensions are given at the end of this chapter.

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Series 820 Instruction Manual Chapter 2 Installation

Figure 2-2. Transducer D-Connector Pin Assignments

Note: The power jack requires a plug that has a 2.5mm inner diameter and a 5mm outer diameter. The center is positive (+).

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Chapter 2 Installation Series 820 Instruction Manual

Standard 0-5 VDC Output Signal Wiring

The standard 0-5 VDC output signal flows from Pin 3 (0-5 VDC Out) through the load (1K Ohm minimum) to Pin 7 (Power Common). The figure below is a typical example of input power and output signal connections.

Figure 2-3. Standard 0-5 VDC Output Signal Wiring

Optional 4-20 mA Output Signal Wiring

The optional 4-20 mA output signal flows from Pin 9 (4-20 mA Out) through the load (50 to 500 Ohms maximum) to Pin 7 (Power Common). The figure below is a typical example of input power and output signal connections. (Multiple transducer current loop output connections are given on the next page.)

Figure 2-4. Single Transducer Current Loop Connection

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Series 820 Instruction Manual Chapter 2 Installation

Figure 2-5. Multiple Transducer Current Loop Connection

Remote Display Installation

Mount the remote display at a convenient location within reach of the supplied interface cable. The maximum cable length is 100 feet (30 m).

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Figure 2-6. Mounting the Remote Display

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Page 19

Series 820 Instruction Manual Chapter 3 Operation

Chapter 3 Operation

The output signal of the transducer is either 0-5 VDC (standard) or 4-20 mA (optional). The output signal is linear and proportional to the gas mass flow rate. For example, for a 0-5 VDC output signal,

5.00 VDC is the output signal for the full scale listed on the transducer’s nameplate, 2.50 VDC is for one-half of full scale, and 0.00 VDC is for zero flow. For a 4-20 mA output signal, 20.00 mA is the output signal for the full scale, 12.00 mA is for one-half of full scale, and 4.00 mA is for zero flow.

Transducer Operation

When the transducer is installed and the system has undergone a complete leak check:

1. Apply power. The output signal will be at a high level for the first 10 to 20 seconds while the sensor warms up to its normal operating temperature range. Assuming zero flow, the output signal will then drop to zero (or 4 mA, depending on output configuration). Allow at least thirty minutes of warm-up time.

2. For first-time start ups, perform an initial zero output check as described on page 3-3. After checking the initial zero setting, the transducer is ready to monitor the gas mass flow rate.

Transducer Accuracy

The standard accuracy of Top-Trak is ±1.5% of full scale. The ±1.5% of full scale accuracy means that the 0-5 VDC output signal is accurate to within ±.075 VDC. The 4-20 mA output is accurate to within ±0.24 mA.

For example, the output signal for zero flow can be as much as ±.075 VDC or +0.24 mA. If the transducer has an output signal at zero flow, as long as it is within either of these two ranges, it does not mean it is malfunctioning.

For transducers with a digital display, the accuracy is simply .015 times the full scale flow rate stated on the nameplate. For example, if the full scale is 10 slpm, the digital display will be accurate to ±0.15 slpm. The reading at zero flow may be as much as +0.15 slpm and still be within the stated accuracy specification.

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Chapter 3 Operation Series 820 Instruction Manual

Referencing the Transducer to Non-Standard Conditions

The gas flow rate output of your transducer is referenced to “normal” conditions of 21 °C (70°F) and 760 mm of mercury (1 atmosphere) unless otherwise specified on the certificate of calibration. Check the stated reference conditions of your transducer. If you are comparing your transducer’s output with another type of flow meter, different reference conditions could cause a discrepancy between the flow readings.

For example, the output reading of a Top-Trak will be approximately 7% lower when referenced to 0°C rather than 21°C. To find the flow rate referenced to other standard conditions or the actual temperature and pressure conditions in the pipe where your transducer is located, see Appendix A.

Transducer Over-Ranging

If the flow rate exceeds the full scale value listed on the transducer nameplate, the output signal and digital display (if so equipped) will read a higher value. The transducer is not calibrated for overranged flows and will probably be both non-linear and inaccurate. Over-range conditions are indicated by the display and/or output signal going to a level above the full scale range. When the overrange condition is removed, it may take several seconds for the

transducer to recover and resume normal operation.

If the supply voltage is only 12 VDC, the over-ranged reading may exceed the full scale value by 10% maximum. If the supply voltage is higher, as with the 24 VDC option, then the output can exceed the full scale by as much as 50%, or more. Digital displays cannot exceed 3-1/2 digits (1999). If the flow rate exceeds 1999, the rightmost digits will blank and only the left-hand “1” will appear on the display.

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Page 21

Series 820 Instruction Manual Chapter 3 Operation

Zero and Span Adjustments

The zero and span potentiometers are accessed through the ports marked on the side of the transducer. Normally, span adjustments are not made unless you are calibrating the transducer. The span adjustment should not be used unless you have a known, precise nonzero flow rate that you wish to match. Before making any zero adjustments, confirm that the system has reached its normal operating temperature and pressure and the transducer is mounted in its final position.

For transducers without the digital display:

1. Power the transducer and allow at least 30 minutes of warm up time before attempting any adjustments. Set gas flow to zero. Confirm that no flow exists.

2. Connect a digital multimeter to Pin 3 (0-5 Out) or, Pin 9 (4-20 Out) and Pin 7 (Power Common). Check the reading. If it does not indicate 0± .05 VDC, (or 4.0± .016mA) adjust the zero potentiometer.

Since the output signal does not indicate negative numbers, it is necessary to adjust down from a slightly positive reading. Begin by slowly rotating the zero pot clockwise until a positive reading is indicated. To complete the zero adjustment, slowly turn the pot counterclockwise until zero is achieved, or to the point where out- put quits changing (may be slightly above zero point in some cas- es) DO NOT ADJUST DOWNWARD BEYOND THIS POINT.

For transducers with the digital display:

1. Power the transducer and allow at least 30 minutes of warm up time before attempting any adjustments. Set gas flow to zero. Confirm that no flow exists.

2. Observe the reading on the digital display. If the reading is greater than 1.0% of full scale, adjust the zero potentiometer.

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Chapter 3 Operation Series 820 Instruction Manual

820 Totalizer Operation

The optional 820 totalizer is designed to provide a totalizer function within the digital display of the 820 series. It will display the flow rate, the total flow or both at once. If your instrument has this option, it is described below. Note the flow units and the totalizer units are pre-set at the factory and must be the same.

Screens:

The totalizer display has three screens which are accessed by pressing the button circled in the photo below:

Screen 1

(start-up screen shown in photo above): Flow units are

shown together with the actual flow

Screen 2 Screen 3

: Totalized flow in the same units as Screen 1 above

: Actual flow is shown together with the total flow

Totalizer:

A total of 8 digits can be shown by the totalizer ranging from .0000001 to 99999999. The decimal point will automatically shift position as the total increases. Upon reaching the maximum count (99999999), the totalizer will “roll-over”--be cleared and begin counting from zero again.

The totalizer may be cleared by going to screen 2 or 3 and then pressing the button for more then 5 seconds. The clearing of the totalizer can be observed on the screen.

The total count is saved in non-volatile memory every 5 minutes. If the unit is switched off within 5 minutes from power-up then no total will be saved and the previous total will be shown at the next power-up.

Caution:

happen that during power up the screen remains blank. If this occurs, please turn the unit off and then back on again

Due to the combination of the hardware/LCD, it may

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Page 23

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

Caution!

It is important that this

transducer be serviced

and/or calibrated by

qualified personnel.

Chapter 4 Maintenance and Repair

Top-Trakm transducers essentially require no scheduled maintenance other than periodic flow path cleaning if the gas is dirty. If an in-line filter is used, the filtering element should be periodically replaced or ultrasonically cleaned. CAUTION: If the laminar flow element is removed from any TopTrakm flow meter, re-calibration will be required to return the instrument to original accuracy.

Calibration of Sierra Instruments flow meters and controllers requires a calibrating standard of at least equal accuracy and preferably an order of magnitude better than the transducer, and a skilled factory technician familiar with the Top-Trak. It is recommended that Top-Trak meters be returned to the factory for annual evaluation and calibration.

Included in this chapter are general instructions for:

 Transducer Cleaning Instructions ............................... page 4-1

 Transducer Calibration ................................................ page 4-9

 Transducer Troubleshooting .................................... page 4-11

 Returning Equipment to the Factory ....................... page 4-12

Transducer Cleaning

Due to transducer design variations, separate cleaning instructions are given in this chapter for each of the following models:

 Model 822/824 with nylon flow body  Model 826/827 with aluminum flow body  Model 822-S/824-S with stainless steel flow body

When toxic or corrosive gases are used, the transducer must be thoroughly purged with inert dry gas before disconnecting from the gas line. Transducers used with toxic or corrosive gases SHOULD NOT BE returned to the factory since they constitute a safety hazard. Contact the factory with specific questions.

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Page 24

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

Flow Path Cleaning Model 822/824

Figure 4-1. Model 822/824 Flow Components

Caution!

When using toxic or cor rosive gases, purge the unit thoroughly with iner dry gas before disconnecting from the gas line.

Inlet and Outlet Screens

1. Remove the transducer from the system.

2. Remove inlet and outlet fittings.

3. Pull out the laminar flow element (LFE) holddowns.

4. Replace or clean the inlet and outlet screens.

5. Re-assemble components. When the transducer is installed in the system, leak test the connection.

6. To be within the original accuracy, calibrate the transducer (see page 4-9).

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Page 25

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

Laminar Flow Element

The laminar flow element (LFE) is a precision flow divider which

Caution!

the LFE from the meter will change your calibra- tion.

the LFE unless you are prepared to re-calibrate

Removing

Do not remove

the instrument.

diverts a preset amount of flow through the sensor tube. The particular LFE used depends on the gas and flow range of the instrument. To clean or inspect the LFE:

1. Remove the transducer from the system.

2. Remove the inlet and outlet fittings and inlet screen.

3. The LFE has a slightly tapered shape with the larger diameter on the upstream (inlet) side. To remove, use a blunt object which does not mar the flow channels to push the LFE from the outlet side to the inlet side. A 3/8-inch (9 mm) nut driver works well.

4. Clean the LFE using an alcohol-based solvent. Make sure to carefully clean all active flow channels in the LFE.

5. Re-install the LFE making sure to press it in the correct distance as shown below.

6. Re-assemble remaining components. When the transducer is installed in the system, leak test the connection. Re-zero the transducer (see Chapter 3).

7. Calibrate the instrument (see page 4-9).

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Figure 4-2. Correct LFE Position

Page 26

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

Flow Path Cleaning Model 826/827

Caution!

the LFE from the meter will change your calibra- tion.

the LFE unless you are

prepared to re-calibrate

Removing

Do not remove

the instrument

Laminar Flow Element

The laminar flow element (LFE) is a precision flow divider which diverts a preset amount of flow through the sensor tube. The particular LFE used depends on the gas and flow range of the instrument. To clean or inspect the LFE:

1. Remove the transducer from the system.

2. Remove the 6-32 hex nuts and washers. Remove the end caps. Note the position of the three (3) LFE elements.

3. To remove the LFE, use a blunt object which does not mar

the flow channels to push the LFE from the flow body.

4. Clean the LFE using a suitable solvent. Make sure to carefully clean all active flow channels in the LFE.

5. Re-install the LFE making sure to position it with both ends even with the transducer flow body.

6. Re-assemble remaining components. When the transducer is installed in the system, leak test the connection. Re-zero the transducer (see Chapter 3).

7. Perform a calibration (see page 4-9).

Figure 4-3. Model 826/827 Flow Components

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Page 27

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

Flow Path Cleaning Model 822-S/824-S

Caution!

the LFE from the meter will change your calibra- tion.

the LFE unless you are prepared to re-calibrate

Removing

Do not remove

the instrument

Laminar Flow Element

The laminar flow element (LFE) is a precision flow divider which diverts a preset amount of flow through the sensor tube. The LFE is made of precision machined 316 stainless steel. The particular LFE used depends on the gas and flow range of the instrument. Should the LFE require cleaning or inspection due to deposition, use the appropriate cleaning procedure which is specific to flow body size.

Figure 4-4. Low Flow Transducer LFE Cleaning

Low Flow Transducers:

The LFE is accessed by unscrewing the main inlet fitting and removing it from the flow body. The LFE is screwed into the inlet fitting, which has been specially machined for this purpose. To access the components:

1. Remove the transducer from the system.

2. The inlet filter screen is held in place in the inlet fitting by the

LFE. Disassemble by holding the fitting steady with a wrench and unscrewing the LFE with a medium flat-tipped screwdriver.

IM-82 4-

3. Remove the LFE assembly taking care not to bend the inlet screen. Inspect the sealing O-ring and replace if necessary. Inspect the inlet screen and replace if corroded or damaged. Light to medium particulate contamination can be cleaned by back washing with a suitable solvent. Air dry thoroughly.

Page 28

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

4. Inspect the LFE for damage and replace if necessary. Remember that removal or replacement of the LFE or inlet screen requires transducer re-calibration.

5. Re-assemble components. When the transducer is installed in the system, leak test the connection. Re-zero the transducer (see Chapter 3).

6. To be within the original accuracy, calibrate the transducer (see page 4-9).

Caution!

the LFE from the meter will change your calibra- tion.

the LFE unless you are prepared to re-calibrate

Removing

Do not remove

the instrument.

Figure 4-5. Medium Flow Transducer LFE Cleaning

Medium Flow Transducers:

In the medium flow body, the LFE assembly consists of the honeycomb laminar flow element, inlet screen, 0.63 inch long standoff, two ranging washers, 2-1Ú4 inch long 4-40 screw and 4-40 nut. Range changes in the honeycomb element are made with various diameter ranging washers. To access the components:

1. Remove the unit from the system.

2. Access the LFE by unscrewing the four 10-32 socket head cap screws from the inlet side of the flow body and remove the inlet end cap. (Note the position of the screws, one has a shorter length.)

4-6 IM-82

Page 29

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

4. Inspect the honeycomb element for damage and replace if necessary. Replacement of the LFE or inlet screen requires transducer re-calibration.

5. Re-assemble components. When the transducer is installed in the system, leak test the connection.

6. To be within the original accuracy, calibrate the transducer (see page 4-9).

Figure 4-6. High Flow Transducer LFE Cleaning

Caution!

the LFE from the meter will change your calibra- tion.

the LFE unless you are prepared to re-calibrate

Removing

Do not remove

the instrument

High Flow Transducers:

The high flow LFE is similar to the honeycomb element used in the medium flow body but larger in diameter. The high flow body consists of four parts: inlet tube, inlet cap, main flow body and end cap. The inlet tube is only removed to inspect and replace the sealing Oring between the inlet tube and inlet cap. To access the components:

1. Remove the unit from the system.

2. To remove the inlet screen, remove the four 1∕4-28 socket head cap screws on the inlet side of the flow body and separate the inlet cap from the main flow body.

3. Inspect the inlet screen for damage and corrosion and replace if necessary. Light to medium particulate contamination can be cleaned by back washing with a suitable solvent. Air dry thoroughly.

4. Inspect the sealing O-ring for damage and replace if necessary. The inlet screen is mounted with the fine mesh side facing the inlet.

IM-82 4-

5. To remove the LFE loosen and remove the four threaded rods holding the end cap to the main flow body. Separate the end cap from the main flow body and remove the LFE assembly. The LFE

Page 30

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

assembly consists of: 6-32 x 31∕8 inch long screw, a #6 washer, two ranging washers, honeycomb laminar flow element, LFE, spacer, inlet filter, and 6-32 nut.

6. Inspect the honeycomb element for damage and replace if necessary. Replacement of the LFE or inlet screen requires transducer re-calibration.

7. Re-assemble components. When the transducer is installed in the system, leak test the connection.

8. To be within the original accuracy, calibrate the transducer (see page 4-9).

Caution!

corrosive gases, purge the un it thoroughly with inert dry gas before disconnecting from the gas line.

When using toxic or

Sensor Cleaning and Inspection

Due to sensor design variations, the following sensor cleaning in-

structions are for Model 822-S/824-S

models must be returned to the factory.

Sensor cleaning is accomplished by simply rodding out the sensor with the Sensor Cleaning Stylette, part number “CKÓ available from Sierra. A 0.028 inch diameter piano wire may also be used.

To access the sensor for inspection or cleaning:

1. Remove the transducer from the system. Remove the two socket head access port plugs with a 1Ú4-inch Allen wrench. Visually inspect the sensing ports and sensor.

1. Use a hemostat or tweezers to push the cleaning wire into the downstream opening of the sensor tube. Do not force the cleaning wire, move it back and forth–DO NOT TWIST OR ROTATE.

only

. All other transducer

2. Flush the sensor tube with a

4-8 IM-82-E

non-residuous solvent compatible with the O-ring material. In cases where solids are deposited in sensor, units should be returned to factory for complete cleaning and re-calibration.

Page 31

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

3. Blow dry all parts with dry nitrogen and re-assemble. When the transducer is installed in the system, leak test the connection. Re-zero the transducer (see Chapter 3).

Transducer Calibration

Calibration of Sierra’s flow meters requires a calibration standard of at least four times the accuracy of the transducer. Sierra’s Cal-

Caution!

It is important that this

transducer be calibrated

only by qualified personnel.

Bench Automated Primary Calibration System is the preferred method of calibration and is used at the factory for all calibrations from 10 sccm up to 50 slpm. Most calibrations can be performed with a digital voltmeter (DVM) or multimeter with 0.25% accuracy and four digits, dry nitrogen and the K-factor tables included in this manual. Flow meters require a metering valve for setting a constant flow rate.

The following procedures are offered as guidelines for calibration. It is always best to return the transducer to the factory for calibration. Calibration checks and minor adjustments to the zero and full scale are made via the access ports in the enclosure. If the linearity needs adjustment (when installing a different bypass to change the range) skip Step 2 and Step 3. If linearity does not need adjustment, complete only Steps 1 through 3.

Step 1. Warm Up

Plug in the unit to be calibrated and allow at least 30 minutes warm up time before attempting any adjustments.

Step 2. Zero Adjust

Slide open the zero and span access doors. Connect a DVM or multimeter to the transducer output pins. Adjust the zero potentiometer for 0.0 volts (4 mA) at zero flow.

Step 3. Check Full Scale

Generate full scale flow using a metering valve in-line with the unit under test. Compare the indicated flow rate with the flow standard reading. If they agree to within ±10%, adjust the span potentiometer for exact agreement. If the readings do not agree within ±10%, attempt to determine the cause of disagreement. Possibilities are:

 leaks in the system or in the transducer  wrong or improper use of K-factor  wrong or improper correction for temperature and pressure  partially clogged or dirty sensor tube

IM-82 4-

Page 32

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

• replacement of components in the flow path do not exactly match the original parts

This completes transducer calibration. To adjust linearity, continue with Step 4.

Step 4. Adjusting Linearity (see Figure 4-7)

First gain access to the printed circuit board inside the enclosure:

1. For units with the digital display, carefully rotate the display until it hits the top plate. Slide the display’s two side panels up and remove. Move the display aside taking care not to damage the connecting cable.

2. Remove the two Phillips head screws from the top of the transducer enclosure. Remove the two Phillips head screws from the back of the transducer enclosure. Pull the enclosure panels off.

3. Orient the transducer with the component side of the circuit board facing you. Plug in the transducer and allow to warm up for at least 30 minutes.

Step 5. Zero Adjust

Connect a DVM to the transducer output pins. Adjust the zero potentiometer for 0.0 volts (4 mA) at zero flow.

Step 6. Calibrate 25%

Use the calibration standard to set a flow rate of 25% of full scale. Adjust the span potentiometer R21 for 1.25 volts (8 mA) at the output of the transducer.

Step 7. Calibrate 50%

Increase the flow rate to 50% of full scale. If the output is within +0.05 V (0.2 mA), no adjustment is necessary. If the output is beyond these limits, install a jumper block at J1 in the appropriate position (see Figure 4-7). Adjust R25 for the proper reading.

Step 8. Calibrate 75% and 100%

Set the flow to 75% of full scale. If the output is outside the limits set in Step 7, install a jumper block in J2 in the appropriate position. Adjust R27 for the correct reading. Repeat this procedure for 100% flow using R29. Repeat Steps 6 through 8 at least one more time.

4-10 IM-82

Page 33

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

Figure 4-7. Printed Circuit Board Component Locations

Transducer Troubleshooting

When you suspect that the transducer is not operating correctly, there are a few simple checks that can be made before taking the unit out of service:

1. Make certain that there are no leaks in the gas line.

2. Check that all cables are connected and are in good condition.

3. Verify that the power supply is in the correct range and properly connected to the transducer.

4. Double check connector pin outs when replacing another manufacturer’s transducer.

This information is provided to help locate the cause of a transducer failure. It is not intended to be an all inclusive repair guide. For most repairs, the unit should be returned to the factory for service.

IM-82 4-

Page 34

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

Problem

Possible Cause

Solution

No output No power

Inlet filter screen clogged Clogged sensor

PCB defective

Plug in power supply Clean or replace screen Return to factory for cleaning* Return to factory for repair

Unit will not zero

Gas leak Application requires high pressure and non-horizontal mounting PCB defective

Find and correct leaks Re-zero transducer (see Chapter 3)

Return to factory for repair

Reads full scale with no flow

Gas leak Liquid present in system Defective sensor

Find and correct leaks Check for liquid in flow path Return to factory for repai

Output too high Incorrect calibration or K-factor

Liquid present in system Defective sensor

Correct calibration/k-factor Check for liquid in flow path Return to factory for repair

Out of calibration Dirty or clogged sensor

Change in composition of gas Gas leak LFE dirty Inlet filter screen clogged Incorrect inlet conditions (1/2-inch size models)

PCB defective

*Model 822-S/824-S see sensor cleaning instructions

Return to factory for cleaning* See K-factory tables Find and correct leaks

Clean LFE Clean or replace screen Replumb transducer correctly (See Chapter 2) Return to factory for repair

4-12 IM-82

Page 35

Series 820 Instruction Manual Chapter 4 Maintenance and Repair

Returning Equipment to the Factory

Factory Calibration—All Models

Sierra Instruments maintains a fully-equipped calibration laboratory. All measuring and test equipment used in the calibration of Sierra transducers are traceable to NIST Standards. Sierra is ISO-9001 registered and conforms to the requirements of ANSI/NCSL-Z540 and ISO/IEC Guide 25.

Instructions for Returning Your Instrument for Service

The following information will help you return your instrument to Sierra Instruments' Factory Service Center and will ensure that your order is processed promptly. Prices may vary depending on the flow range, type of gas and operating pressure of your unit. To request a rough estimate of the pricing, contact your local Sierra Instruments distributor or contact one of our offices directly. A detailed quote will be provided following a full evaluation of your instrument.

Please follow these easy steps to return your instrument for factory service:

Caution!

Always fully neutralize any

toxic gas trapped in- side

the instrument before

removing it from the gas

line.

1. Obtain a Return Materials Authorization (RMA) number from the Sierra Instruments website at

http://www.sierrainstruments.com/rma/login.php

2. If you require service beyond calibration, but do not know which service(s) will be required, describe the symptoms as accurately as possible on the RMA form.

3. Pack your instrument carefully. Use the original packaging and

foam or bubble wrap (packing peanuts NOT recommended) and include a copy of the RMA form (complete with Sierra supplied RMA number) with the unit(s).

4. Ship the unit(s) to the following address:

Sierra Instruments, Inc. Attention: Factory Service Center 5 Harris Court, Building L Monterey, CA 93940 USA

IM-82 4-

Page 36

Chapter 4 Maintenance and Repair Series 820 Instruction Manual

CUSTOMER SERVICE AND SUPPORT INFORMATION:

Email Technical Support: Email Sales:

FACTORY USA (Monterey, California)

PHONE: 831-373-0200 FAX: 831-373-4402

EMAIL: service@sierrainstruments.com

European Sales & Service Center (Egmond a/d Hoef, Netherlands)

PHONE: +31 72 5071400 FAX: +31 72 5071401

EMAIL: service@sierra-instruments.nl

Asia Sales & Service Center (Shanghai, Peoples Republic of China)

PHONE: FAX: +86 21 5879 85861

sales@sierrainstruments.com

TOLL FREE: 800-866-0200

+ 86 21 5879 8521

SAFETY NOTE ABOUT PURGING

service@sierrainstruments.com

WARNING: When toxic or corrosive gases are used, purge unit thoroughly with inert dry gas before disconnecting from the gas line to prevent personnel from being injured when coming in contact with the instrument. If an instrument used with a toxic or corrosive gas is returned to the factory, a Material Safety Data Sheet (MSDS) must be enclosed & attached to the outside of the box to alert Sierra personnel of the potential hazard. Also, make sure the inlet & outlet are solidly plugged off.

4-14 IM-82

Page 37

Series 820 Instruction Manual Appendix A

Appendix A Conversion Formulas and Gas Tables

Conversion of Flow Rate to Other T and P Conditions

The flow rate of your transducer is referenced to certain “standard” conditions of temperature and pressure. Unless otherwise specified in your order, these standard conditions are 21 °C (70°F) and 760 mm of mercury (1 atmosphere). If you wish to convert to other “standard” conditions or to find the “actual” conditions in the pipe where your instrument is installed, use the following relationship:

Q2 = Q

( )1 = The standard conditions under which your instrument

was calibrated,

= The new standard conditions or the actual temperature

( )

and pressure conditions in the pipe,

= The gas mass flow rate referenced to the calibrated standard

conditions (sccm or slm),

(1)

= The gas mass flow rate referenced to the new standard or

actual conditions (sccm or slm—“S” means “standard,” accm or alm—“A” means “actual”),

P = Absolute pressure (kg/cm

or psia), and

T = Absolute temperature (°K or °R) (°K = °C + 273, °R = °F + 460).

Example 1: Changing “Standard” Conditions

If your transducer has a flow rate reading of 10.00 slm and was cali brated at standard conditions of 70°F (21°C) and 1 atmosphere (14.7 psia), and if you wish to convert this reading to standard conditions of 32°F (0°C) and 1 atmosphere, then you would use Equation (1) as follows:

14.7 460 + 32

Q2 = _________________ (10.0) = 9.28 slm

14.7 460 + 70

The flow rate referenced to 0°C will be approximately 7% lower than when referenced to standard conditions of 21 °C.

IM-82 A-1

Page 38

Appendix A Serie s 8 2 0 I nstruct i o n Manua l

Example 2: Finding the “Actual” Flow Rate

If the flow rate and calibrated standard conditions are as given in Example 1 and you wish to find the actual flow rate at 100°F and 30 psig, then you would use Equation (1) as follows:

14.7 460 + 100

Q2 = (10.00) = 3.47 lm

14.7 + 30 460 + 70

Calculating For a Single Gas

The following tables provide K-factors and thermodynamic properties of gases commonly used with mass flow meters and controllers. The purpose of these tables is two-fold:

1. Calibrating an “actual” gas with a reference gas. This is particularly useful if the actual gas is not a common gas or if it is toxic, flammable, corrosive, etc.

2. Interpreting the reading of a flow meter or flow controller which has been calibrated with a gas other than the actual gas.

In applying the tables, the following fundamental relationship is used:

Q1/Q2 = K1/K

(1)

Where:

Q = The volumetric flow rate of the gas referenced to normal

conditions of 0°C and 760 mm Hg (sccm or slm),

K = The K-factor defined in equation (6),

( ) 1 = Refers to the “actual” gas, and

( ) 2 = Refers to the “reference” gas.

The K-factor is derived from the first law of thermodynamics applied to the sensor tube, as described in Chapter 1:

H = µC

(2)

-2 IM-82

Page 39

Series 820 Instruction Manual Appendix A

Where:

= The constant amount of heat applied to the sensor tube,

= The mass flow rate of the gas (gm/min)

= The coefficient of specific heat of the gas (Cal/gm);

Cp is given in the Table (at 0°C),

= The temperature difference between the downstream and

upstream coils, and

= A correction factor for the molecular structure of the gas

given by the following table:

Number of Atoms in the Gas Molecule N

Monatomic 1.040

Diatomic 1.000

Triatomic 0.941

Polyatomic 0.880

The mass flow rate, µ, can also be written as:

µ = ρQ

Where:

= The gas mass density at standard conditions (g/l);

en in the tables (at 0°C, 760 mm Hg).

Furthermore, the temperature difference, ΔT, is proportional to the output voltage, E, of the mass flow meter, or

T = aE

where:

= a constant.

If we combine equations (3) and (4), insert them into equation (2), and solve for Q, we get

(4)

is giv-

Q = (bN/ρCp)

(3)

(5)

IM-82

where:

b = H/aE = a constant if the output voltage is constant.

-3

Page 40

Appendix A Serie s 8 2 0 I nstruct i o n Manua l

For our purposes, we want the ratio of the flow rate, Q1, for an actual gas to the flow rate of a reference gas, Q2, which will produce the same output voltage in a particular mass flow meter or controller. We get this by combining equations (1) and (5):

Q1/Q2 = K1/K2 = (N1/

ρ1Cp1)/(N2/

ρ2CP2) (6)

Please note that the constant b cancels out. Equation (6) is the fundamental relationship used in the accompanying tables. For convenience, the tables give “relative” K-factors, which are the ratios K1/K2, instead of the K-factors themselves. In the tables, the relative K-factor is K

actual

/KN2 where the reference gas is the commonly used gas, nitrogen (N2). The remaining columns give Cp and p, enabling you to calculate

directly using Equation (6). In some instances, K1/K

K1/K

from the tables may be different from that which you calculate directly. The value from the tables is preferred because in many cases it was obtained by experiment. Sierra calibrates every transducer with primary standards using the actual gas or a molecular equivalent reference gas. The calibration certificate accompanying the transducer cites the reference gas used.

Example 1:

A transducer is calibrated for nitrogen (N2), and the flow rate is 1000 sccm for a 5.000 VDC output signal. The flow rate for carbon dioxide at a 5.000 VDC output is:

CO2/QN2

CO2

= K

CO2

/K N2, or

= (0.74/1.000)1000 = 740 sccm

Example 2:

A transducer is calibrated for hydrogen (H2), and the flow rate is 100 sccm for a 5.000 VDC output signal. The flow rate for nitrous oxide (N2O) is found as follows:

N2O/QH2

N2O

Note that the K -factors relative to nitrogen must be used in each case.

Example 3:

= K

N2O

/K H2, or

= (0.71/1.01) 100 = 70.3 sccm

We want a transducer to be calibrated for use with dichlorosilane (SiH2Cl2) at a 100 sccm full scale flow. We wish to use the preferred reference gas Freon-14 (CF4). What flow of CF4 must we generate to do the calibration?

SiH2CL2 /QCF4

100/Q

CF4

= 100/0.869 = 115 sccm

= K

= 0.869

SiH2CL2

CF4

-4 IM-82

Page 41

Series 820 Instruction Manual Appendix A

Calculating Dual Gas Mixtures

Equation (6) is used for gas mixtures, but we must calculate for the mixture. The equivalent values of p, Cp, and N for a dual

gas mixture are given as follows: The equivalent gas density is:

P 󰇛ml / mT󰇜 P1 󰇛m2/mT󰇜 P2

Where:

M1m

( )1 = Refers to gas #1, and ( )2 = Refers to gas #2

The equivalent specific heat is:

Cp = F1C Where:

F F

m2=

󰇛m1 Pi󰇜/󰇛mTP󰇜

󰇛m2P2󰇜/󰇛mTP󰇜

Total mass flow rate (g/min).

+ F2Cp2

The equivalent value of N is:

N 󰇛Ml / mT󰇜 N1󰇛m2/mT󰇜 N2

The equivalency relationships for p, Cp, and N for mixtures of more than two gases have a form similar to the dual-gas relationship given above.

IMPORTANT NOTE ABOUT K-FACTORS: Please note that if you have a transducer calibrated for a gas such as methane and wish to use the K-factors to measure a gas such as air, that the inaccuracy of the measurement can range from ±5 to 10%. The use of K-factors is, at best, only a rough approximation and should not be used in applications that require a better than ±5 to 10% accuracy.

It should also be noted that certain gases, in similar “families,” will work exceptionally well with K-factors; however, those instances are only true when similar thermal properties of the gas are present.

IM-82

-5

Page 42

Series 820 Instruction Manual Appendix A

Actual Gas Symbol (Cal/g) (g/l) @

Chemical K-factor

Relative

Cp Density Elastomer* Nylon

O-ring* Valve Compatible

0°C

Seat

Corrosive

Gas

Limited

Warranty

Acetylene C2H2 0.58 0.4036 1.162

Air 1 0.24 1.293

Viton® Viton®

Allene (Propadiene) C3H4 0.43 0.352 1.787 KR

Ammonia NH3 0.73 0.492 0.76 NEO KR

Argon Ar 1.45 0.1244 1.782

Arsine AsH3 0.67 0.1167 3.478

Viton® Viton®

Viton®

Boron Trichloride BCl3 0.41 0.1279 5.227 KR KR

Boron Trifluoride BF3 0.51 0.1778 3.025

Boron Tribromide Br3 0.38 0.0647 11.18

Bromine Br2 0.81 0.0539 7.13

Bromine Pentafluoride BrF5 0.26 0.1369 7.803

Bromine Trifluoride BrF3 0.38 0.1161 6.108

Viton®

Viton® Viton®

Viton®

KR NO

Bromotrifloromethane CBrF3 0.37 0.1113 6.644 Viton® Viton®

(Freon-13 B1)

1,3-Butadiene C4H6 0.32 0.3514 2.413

Butane C4H10 0.26 0.4007 2.593

1-Butane C4H8 0.3 0.3648 2.503

2-Butane C4H8 CIS 0.324 0.336 2.503

2-Butane C

4H8

TRANS

0.291 0.374 2.503

Carbon Dioxide CO2 0.74 0.2016 1.964

Carbon Disulfide CS2 0.6 0.1428 3.397

Carbon Monoxide CO 1 0.2488 1.25

Carbon Tetrachloride CCl4 0.31 0.1655 6.86

Viton® Viton®

Viton®

KR NO

Carbon Tetra fluoride CF4 0.42 0.1654 3.926 Viton® Viton®

(Freon-14)

Carbonyl Fluoride COF2 0.54 0.171 2.945

Carbonyl Sulfide COS 0.66 0.1651 2.68

Chlorine CL2 0.86 0.114 3.163

Chlorine Trifluoride CIF3 0.4 0.165 4.125

Viton® Viton®

Viton®

KR NO

Chlorodifluoromethane CHClF2 0.46 0.1544 3.858 Viton® KR

(Freon-22)

Chloroform CHCI3 0.39 0.1309 5.326

Viton®

Chloropentafluoroethane C2CIF5 0.24 0.164 6.892 Viton® KR

(Freon-115)

Chlorotrifluromethane CCIF3 0.38 0.153 4.66 Viton® KR

(Freon-13)

* If no O-ring material is specified then O-ring to be used is Viton

YES

Page 43

Actual Gas Symbol (Cal/g) (g/l) @

Chemical K-factor

Relative

Cyanogen C2N2 0.61 0.2613 2.322

Cp Density Elastomer* Nylon

O-ring Valve Compatible

0°C

Seat

Viton®

Cyanogen Chloride CICN 0.61 0.1739 2.742 KR KR

Cychlopropane C3H5 0.46 0.3177 1.877

Deuterium D2 1 0.1722 1.799

Diborane B2H6 0.44 0.508 1.235

Dibromodifluoromethane CBr2F2 0.19 0.15 ATEX

Dibromethane 0.47 0.075 7.76

Viton®

Dichlorodifluoromethane CCI2F2 0.35 0.1432 5.395 Viton® KR

(Freon-12)

Dichlorofluoromethane CHCl2F 0.42 0.14 4.952 Viton® KR

(Freon-21)

Dichloromethylsilane (CH

Dichlorosilane SiH2Cl2 0.4 0.15 4.506

SiCl2 0.25 0.1882 5.758

3) 2

Viton®

Dichlorotetrafluoroethane C2Cl2F4 0.22 0.1604 7.626 Viton® KR

(Freon-114)

1,1-Difluoroethylene C2H2F2 0.43 0.224 2.857 Viton® KR

(Freon-1132A)

Dimethylamine (CH3) 2NH 0.37 0.366 2.011

Dimethyl Ether (CH3) 2O 0.39 0.3414 2.055

2,2-Dimethylpropane C3H12 0.22 0.3914 3.219

Ethane C2H6 0.5 0.4097 1.342

Ethanol C2H6O 0.39 0.3395 2.055

EthylAcetylene C4H6 0.32 0.3513 2.413

Ethyl Chloride C2H5CI 0.39 0.244 2.879

Ethylene C2H4 0.6

~.358

1.251

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Ethylene Oxide C2H4O 0.52 0.268 1.965 KR KR

Fluorine F2 0.98 0.1873 1.695

Fluoroform (Freon-23) CHF3 0.5 0.176 3.127

Freon-11 CCI3F 0.33 0.1357 6.129

Freon-12 CCI2F2 0.35 0.1432 5.395

Freon-13 CCIF3 0.38 0.153 4.66

Freon-13 B1 CFrF3 0.37 0.1113 6.644

Freon-14 CF4 0.42 0.1654 3.926

Freon-21 CHCI2F 0.42 0.14 4.952

Freon-22 CHCIF2 0.46 0.1544 3.858

Freon-113 CCI

FCCIF2 0.2 0.161 8.36

Freon-114 C2Cl2F4 0.22 0.16 7.626

Freon-115 C2ClF5 0.24 0.164 6.892

Viton®

Viton® Viton®

Viton®

KR NO

Freon-C318 C4F8 0.17 0.185 8.397 NEO NEO NO

Corrosive

Gas

Limited

Warranty

800 Only

YES

Page 44

Page 45

Actual Gas Symbol (Cal/g) (g/l) @

Germane GeH4 0.57 0.1404 3.418

Germanium Tetrachloride

Helium He 1.454 1.241 0.1786

Hexafluoroethane C2F6 0.24 0.1834 6.157 Viton® KR NO

(Freon-116)

Hexane C6H14 0.18 0.3968 3.845

Hydrogen H2 1.01 3.419 0.0899

Hydrogen Bromide HBr 1 0.0861 3.61

Hydrogen Chloride HCl 1 0.1912 1.627 KR KR

Hydrogen Cyanide HCN 1.07 0.3171 1.206

Hydrogen Fluoride HF 1 0.3479 0.893 KR KR

Hydrogen Iodide HI 1 0.0545 5.707

Hydrogen Selenide H2Se 0.79 0.1025 3.613

Hydrogen Sulfide H2S 0.8 0.2397 1.52 NEO KR

Iodine Pentafluoride IF5 0.25 0.1108 9.9

Isobutane CH(CH3)3 0.27 0.3872

Isobutylene C4H8 0.29 0.3701 2.503

Krypton Kr 1.453 0.0593 3.739

Methane CH4 0.72 0.5328 0.715

Methanol CH3OH 0.58 0.3274 1.429

Methyl Acetylene C3H4 0.43 0.3547 1.787

Methyl Bromide CH3Br 0.58 0.1106 4.236

Methyl Chloride CH3Cl 0.1926 2.253

Methyl Fluoride CH3F 0.68 0.3221 1.518

Methyl Mercaptan CH3SH 0.52 0.2459 2.146

Methyl Trichlorosilane (CH3) SiCl3 0.25 0.164 6.669

Chemical K-factor

Relative

GeCL4 0.27 0.1071 9.565

Cp Density Elastomer* Nylon

O-ring Valve Compatible

0°C

Seat

2.593

Viton® Viton®

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Viton®

Corrosive

Gas

Limited

Warranty

YES

Molybdenum Hexafluoride

Monoethylamine C2H5NH2 0.35 0.387 2.011

Monomethylamine CH3NH2 0.51 0.4343 1.386

Neon NE 1.46 0.245 0.9

Nitric Oxide NO 0.99 0.2328 1.339

Nitrogen N2 1 0.2485 1.25

Nitrogen Dioxide NO2 0.74 0.1933 2.052 KR KR NO

Nitrogen Trifluoride NF3 0.48 0.1797 3.168

Nitrosyl Chloride NOCl 0.61 0.1632 2.92

Nitrous Oxide N2O 0.71 0.2088 1.964

Octafluorocyclobutane C4F8 0.17 0.185 8.397 Viton® KR

(Freon-C318)

Oxygen Difluoride OF2 0.63 0.1917 2.406

Oxygen O2 1 0.2193 1.427

Ozone O3 0.446 0.3 2.144

MoF6 0.21 0.1373 9.366

Viton®

Viton® Viton®

Viton®

Viton® Viton®

YES

Page 46

Actual Gas Symbol (Cal/g) (g/l) @

Pentaborane B5H9 0.26 0.38 2.816

Pentane C5HI2 0.21 0.398 3.219

Perchloryl Fluoride CIO3F 0.39 0.1514 4.571

Perfluoropropane C3F8 0.174 0.197 8.388

Phosgene COCl2 0.44 0.1394 4.418

Phosphine PH3 0.76 0.2374 1.517

Phosphorous Oxychloride POCl3 0.36 0.1324 6.843

Phosphorous Pentafluoride PH5 0.3 0.161 5.62

Phosphorous Trichloride PCl5 0.3 0.125 6.127

Propane C3H8 0.36 0.3885 1.967

Propylene C3H6 0.41 0.3541 1.877

Silane SiH4 0.6 0.3189 1.433

Silicon Tetrachloride SiCl4 0.28 0.127 7.58

Silicon Tetrafluoride SiF4 0.35 0.1691 4.643

Sulfur Dioxide SO2 0.69 0.1488 2.858

Sulfur Hexafluoride SF6 0.26 0.1592 6.516

Sulfuryl Fluoride SO2F2 0.39 0.1543 4.562

Teos 0.09

Tetrafluorahydrazine N2F4 0.32 0.182 4.64

Trichlorofluormethane CCl3F 0.33 0.1357 6.129 Viton® KR

(Freon-11)

Trichlorisilane SiHCl3 0.33 0.138 6.043

1,1,2-Trichloro-1,2,2 CCl

Trifluorethane (Freon-113)

Trisobutyl Aluminum (C4H9)Al 0.061 0.508 8.848

Titanium Tetrachloride TiCl4 0.27 0.12 8.465

Trichloro Ethylene C2HCl3 0.32 0.163 5.95

Trimethylamine (CH3)3N 0.28 0.371 2.639

Tungsten Hexasfuoride WF6 0.25 0.081 13.28 KR Teflon

Uranium Hexafluoride UF6 0.2 0.0888 15.7

Vinyl Bromide CH2CHBr 0.46 0.1241 4.772

Vinyl Chloride CH2CHCl 0.48 0.12054 2.788

Xenon Xe 1.44 0.0378 5.858

Chemical K-factor

Relative

FCClF2 0.2 0.161 8.36

Cp Density Elastomer* Nylon

O-ring Valve Compatible

0°C

Seat

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Viton®

KR KR

Viton®

Viton® Viton®

Viton®

Viton® Viton®

Corrosive

Gas

Limited

Warranty

YES

Page 47

Series 820 Instruction Manual Appendix B

Appendix B 822/824 Product Specifications

Page 48

Page 49

Series 820 Instruction Manual Appendix C

Appendix C 822S/824S Product Specifications

Page 50

Page 51

Page 52

Series 820 Instruction Manual Appendix D

Appendix D 826/827 Product Specifications

Page 53

Page 54