Sartorius arium pro Operating Manual

Operating Manual
arium® pro
Water Purification System
85032-536-35
3
arium® pro Operating Manual
3
Contents
Contents
User Information ..............................................4
About These Instructions
.....................................4
Applications Advice | Technical Support
....................4
Safety Information
............................................5
Intended Usage
................................................6
1. Product Description
.....................................7
1.1 Flow Diagram for arium® pro .......................8
1.2 Electrical Connections ..............................8
1.3 arium® Exchange Interface .........................9
1.4 Tubing Connections ................................9
2. Unpacking and Installation
............................10
2.1 Unpacking .........................................10
2.2 Bench Mounting ..................................11
2.3 Wall Mounting ....................................12
3. Operating Concept
.....................................14
3.1 Display .............................................14
3.2 Operation in the Operating Mode. . . . . . . . . . . . . . . . .15
3.3 Navigation in the Menus ..........................17
4. Initial Startup
..........................................19
4.1 System Startup ....................................19
4.2 Setting the Language .............................19
4.3 Setting the Date and Time ........................20
4.4 Setting Measurement Unit ........................20
4.5 Purification Component Installation ..............20
4.6 System Rinsing ....................................22
4.7 Inserting Final Filter ...............................23
4.8 Rinsing the Final Filter ............................23
5. Operation
...............................................24
5.1 Operating Mode ...................................24
5.2 Dispensing Ultrapure Water .......................24
5.2.1 Manual Dispensing ........................25
5.2.2 Time-controlled Dispensing ...............26
5.2.3 Ultrapure Water Dispensing Through the
Sampling Tubing ...........................27
6. System Menu
...........................................28
6.1 Menu Tree .........................................28
6.2 Save Data ..........................................29
6.2.1 Parameter Selection .......................29
6.2.2 Single-item Save ...........................30
6.2.3 Save Interval ...............................30
6.2.4 Save When Dispensing .....................30
6.3 Settings ............................................31
6.3.1 Displayed Values ...........................31
6.3.2 Limit Values ................................32
6.3.3 ECO Mode ..................................32
6.3.4 Date | Time ................................33
6.3.5 Language ..................................33
6.3.6 Acoustic Signals ...........................33
6.3.7 Display .....................................34
6.3.8 PIN .........................................34
6.3.9 Resetting to Default .......................34
6.4 System Status .....................................34
6.4.1 Device ......................................34
6.4.2 Measured Values ...........................35
6.4.3 Timer .......................................35
6.4.4 Service .....................................35
6.4.5 Warnings ...................................35
7. Care and Maintenance
.................................36
7.1 Replacing Cartridges ..............................36
7.2 Depressurization ...................................40
7.3 Changing the Sterile Final Filter ..................42
7.4 Replacing Electrical Fuses .........................43
8. Malfunctions
...........................................44
8.1 Warning Messages ................................44
9. Disposal
.................................................45
10. Technical Specifications
...............................47
11. Accessories and Replacement Parts
...................48
12. EC Declaration of Conformity
.........................49
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arium® pro Operating Manual
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User Information
User Information
Warning | Danger Symbols
These notes identify hazards which have a high probability of resulting in death or serious physical injury if not avoided.
These notes identify hazards that can result in moderate or mild injuries if not avoided.
These notes identify hazards associated with the risk of material damage.
Explanation of Symbols
This symbol identifies useful information and tips.
The following symbols are used in these instructions:
t Indicates required steps.
y Describes what happens after you have performed a particular step.
− Texts that use this mark are lists
About These Instructions
t Please read these instructions carefully and completely before putting the
equipment into operation for the first time. Observe the safety instructions.
t These instructions are an important part of the product. Keep these instructions in
a safe place. If you give the device to others to use, give them these instructions too.
t If these instructions are lost, please contact Sartorius for a replacement or
download the latest manual from our website: www.sartorius.com
Applications Advice | Technical Support
Contact addresses for application advice and our technical support can be found online at: www.sartorius.com
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arium® pro Operating Manual
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Safety Information
Safety Information
Please read the following safety information thoroughly and follow the instructions exactly. This information is designed to ensure your safety and will prevent damage to your arium® pro system.
Danger of electric shock!
− To plug in your arium
®
pro system, use a properly grounded electrical outlet with
a voltage of 100 – 240 V, 50 – 60 Hz.
− Do not place your arium
®
pro system on top of electrical equipment. Routine
maintenance of the arium® pro system may involve water spillage.
Danger of injury from fire or explosion!
− Do not use your arium
®
pro system in the vicinity of highly flammable or
combustible materials as it contains components that may ignite such materials.
− The arium
®
pro system is to be operated with water only. Sanitizing and cleaning
agents should only be used according to the instructions given in this manual.
Danger of injury to eyes and skin!
− Avoid splashing sanitizing agents on clothing, eyes or skin (wear protective clothing).
− Make sure that all tubing connections are sealed tightly to avoid the liquid cleaning agent leaking.
− Carefully follow the manufacturer’s safety instructions included on the liquid cleaning agent containers and filter cartridges.
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arium® pro Operating Manual
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Safety Information
Danger of irreversible damage to arium® pro system components!
− Be sure to replace defective fuses with those of the same type and rating.
− Make sure that the outlet tubing is directed to an open drain.
− Protect against frost.
− Never connect peripheral devices to the device interfaces unless they have been recommended by Sartorius. This will prevent damage to your arium
®
pro.
− Never unplug any cables from your arium
®
pro when it is running as this can
cause malfunctions.
Intended Usage
The arium
®
pro water purification system is designed to provide ultrapure water for the laboratory from water pretreated by distillation, deionization or reverse osmosis. To make sure that these units work properly, only use the filter media and equipment listed in this operating manual. Any other use beyond this is considered improper use.
− The arium
®
pro system may only be operated by trained personnel.
− Only operate your arium® pro system with original accessories or replacement parts. If you modify this water purification system independently, the performance and operating safety of the system are no longer guaranteed. This can also endanger the safety of the operator.
− If you encounter any problems with your system, please contact your local Sartorius Service Center.
− Please take all pertinent precautions to prevent accidents and observe the generally valid technical and occupational safety rules and regulations.
− Use only materials recommended by Sartorius (such as cartridges, replacement parts and sanitizing agents).
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arium® pro Operating Manual
Product Description
1. Product Description
3
2
1
arium
®
pro front view
1. Display and control panel
2. Sampling with sterile final filter
3. Door
The arium
®
pro system was designed to provide ASTM, NCCLS, ISO and USP-grade water. Multi-stage purification methods purify pretreated water into ultrapure water by distillation, deionization or reverse osmosis. This involves the use of purification processes based on mixed-bed resins, activated carbon, and sterile filtration.
As the flow diagram on the next page shows, the feed water is pumped through two ultrapure water cartridges connected in series. At the outlet of the second cartridge, a conductivity-measuring cell performs permanent monitoring of the ultrapure water quality (LFP).
To guarantee ultrapure water of consistent and high quality, the ultrapure water purification system is constructed like a circulation ring. If no water is dispensed, the water circulates through the ultrapure water cartridges. The last purification step before dispensing is to run the water through a sterile final filter.
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arium® pro Operating Manual
Product Description
1.1 Flow Diagram for arium® pro
Speisewasser- eingang
Pumpe
Kartusche 1 Kartusche 2
Produktwasser
Endfilter 0,2 µm
Leitfähigkeitsmessung LFP (Produktwasser)
1.2 Electrical Connections
1 2 3 4 5 6 7 8 9 10
Electrical connections, side view right
1. SD card recorder | scanner (only available for arium
®
pro DI, UF, UV, VF)
2. Ethernet connection (for Sartorius Service personnel only)
3. Display port for connecting the dispenser unit (only available for arium
®
pro DI, UF, UV, VF )
4. RS-232 serial interface with a 9-pin sub-D port for connecting a printer (Sartorius YDP30)
5. arium
®
Exchange interface
6. Connection for optional level sensors (only available for arium
®
pro DI, UF, UV, VF )
7. Connection for optional foot switch (only available for arium
®
pro DI, UF, UV, VF)
8. Fuse drawer
9. Power switch
10. Mains connection
Feed water input
Conductivity measurement LFP (product water)
Product water
Final filter
0.2 μm
Pump
Cartridge 1 Cartridge 2
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arium® pro Operating Manual
Product Description
1.3 arium® Exchange Interface
The arium® Exchange interface enables communication with an arium® advance system. When such a cable is connected, the arium® bagtank (< 2 liters) will stop dispensing water if the fill level of the arium® pro system falls below the minimum. This is to prevent any malfunction of the arium® pro system.
Use the Firewire cable delivered with the arium
®
pro system for device communica­tion when supplying the arium® advance from a bagtank. To guarantee proper functioning, first switch on the arium® advance and then the arium® pro system.
A bagtank with an integrated pump must be used when supplying the arium
®
pro system from a bagtank, otherwise this could lead to malfunctioning. A bagtank 20 can be used without a pump as well, as long as it is positioned at the same height or higher than the arium® pro system.
1.4 Tubing Connections
Tubing connectors, side view right
1. Feed water supply
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arium® pro Operating Manual
Unpacking and Installation
2. Unpacking and Installation
We recommend that you have the set-up and initial startup of your arium® pro system carried out by a qualified Sartorius service technician.
2.1 Unpacking
Remove your arium
®
pro system from its packaging. You will find the accessories inside the arium® pro housing and in the top cover of the box. The equipment supplied includes the following:
Part description Qty.
arium
®
pro system (with pre-installed display | dispenser unit) 1
Feed water tubing with quick-fit adapter, PE, a” outer diameter, length 2.40 m
1
Timed dispense tubing, PVDF, ¼” outer diameter, length 2.40 m with adapter for the final filter and adapter for connection to the dispenser unit
1
Power cable 1 Operating instructions 1 arium
®
Quality Assurance Certificate 1
Wall mounting bracket for arium (on models used as wall-mounted systems)
1
Tubing adapter for feed water with ½” internal thread and a” outer diameter
1
Two-part tubing adapter for feed water with G ¾” internal thread and a” outer diameter
1
The cartridges are not included in the equipment supplied with your arium
®
pro
system.
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arium® pro Operating Manual
Unpacking and Installation
2.2 Bench Mounting
Danger of electric shock!
Do not place your arium
®
pro system on top of electrical equipment. Water may spill
when using the system.
Danger of fire or explosion!
Do not use your arium
®
pro system in the vicinity of highly flammable or combustible
materials as it contains components that may ignite such materials.
arium® pro as a Benchtop System
− Place the arium
®
pro system on a flat surface.
− When selecting a place of installation for your arium
®
advance system, you must ensure that a feed water supply, a 100–240 V electric socket and an atmospherically vented drain are available.
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arium® pro Operating Manual
Unpacking and Installation
2.3 Wall Mounting
The arium
®
pro system is optionally supplied with a wall bracket to enable you to attach the system securely to the wall so that it occupies a minimum amount of space. A clear wall area of at least 63 + 63 cm is required.
The wall bracket and the required screws for wall installation are not part of the regular equipment supplied.
arium® pro as a wall-mounted system
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arium® pro Operating Manual
Unpacking and Installation
Back panel of the arium® pro system unit’s wall mounting bracket and wall rail on models used as wall-mounted systems.
The assembly of the two wall brackets and wall rail, (included in delivery), is suitable for a load of 100 kg (220 lbs) and is only intended for the arium
®
pro system (including water). Do not put any additional load on the arium® pro system. When mounting the unit on a wall, make sure that the mounting surface and fasteners selected are capable of supporting a minimum of 100 kg (220 lbs). Inadequate support and | or fasteners may result in injury to the operator and damage to the equipment.
When selecting a place of installation for your arium
®
system, you must ensure that a feed water supply, a 100–240 V electric socket and an atmospherically vented drain are available.
− Use the pre-drilled slotted holes in the wall rail to mount it onto the wall.
− Fasten the wall rail to the wall using suitable screws and dowels (ensure that it is horizontally aligned).
− Mount the arium
®
pro system by hooking it into the wall mounting bracket.
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arium® pro Operating Manual
Operating Concept
3. Operating Concept
Operate your arium® using the control panel and the display. The control panel features four function keys and a continuously variable slider. The keys are described in the figure below. The display shows system information and menu items. The figure depicts the display in the operating mode your arium® system will be in after initial startup.
Eco/Home
1
2
3
SliderRML
11:43 01.01.15
0.055 µS/cm c
Menu Care
3.1 Display
As illustrated in the figure above, the display is divided into the following three main areas.
Header (1)
When your arium
®
is in the operating mode, the header displays the current time and current date. When navigating through menu items, the open menu item and the menu level are displayed.
Working Environment (2)
When your arium
®
is in the operating mode, the working environment displays the following information:
− The current conductivity of the product water (when the display is activated without compensated conductivity; if activated, the current water temperature is displayed as well)
− The flow diagram of the arium
®
pro system
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arium® pro Operating Manual
Operating Concept
The flow diagram represents the ultrapure water cartridges. When a cartridge change is due, they start blinking and a warning message appears.
If your arium® pro system is not in the operating mode, the working environment of the display shows the current menu item.
Footer (3)
The footer displays the current key function assignment for the keys L, M and R.
3.2 Operation in the Operating Mode
The keys L, M, R and Eco/Home and the slider are available for operation in the operating mode.
“Menu” Key (L)
You can use this key to switch to the system menu. Information on the system menu can be found in Chapter “6. Menu”.
“Care” Key (M)
You can use this key to switch to the care section. Information on the care menu can be found in Chapter “7. Care”.
“Dispense” Key (R)
You can use this key to switch directly to controlled water dispensing. Here you have the option to select between timed dispense or volume-controlled dispensing. Further information can be found in Chapter “5.2 Dispensing Ultrapure Water”.
Slider
Use the slider to start manual water dispensing. Further information can be found in Chapter “5.2 Dispensing Ultrapure Water”.
“Eco/Home” Key
The Eco/Home key is used to activate the “Eco mode”. In the Eco mode, the ultrapure water in your arium
®
pro system is recirculated every hour for 15 minutes. The purpose of this is to guarantee high water quality even during longer periods of inoperation.
To access the Eco mode, press and hold the Eco/Home key for 3 seconds. To exit an active Eco mode, press the Eco key once more. The picture on the left shows the active Eco mode.
Eco/Home
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arium® pro Operating Manual
Operating Concept
Your arium® pro system also features an automatic ECO mode. This automatic ECO mode is activated by default and returns the system to the Eco mode after the Eco time has elapsed. The Eco time starts after the last entry into the system. It can be configured in the System menu (see Chapter “6.3.3 ECO Mode”, page 32).
Key Locking Function
The arium
®
pro system has a key locking function. When the key locking function is active, it is not possible to dispense water. All other functions (measurement, expiry of ECO time, print interval and error and warning messages) continue to run in the background. When the automatic ECO time has elapsed, the device enters ECO mode and automatically removes the key lock so that the device is once again ready for operation upon leaving ECO mode. If a warning or an error appears while the key lock is activated, the device will likewise automatically cancel the key lock and display the corresponding message.
To activate the key lock, simultaneously press the Eco/Home key and the “Dispense” key (R). Use the same key combination to deactivate the key locking function.
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