Thank you for choosing this OHAUS product.
Please read the manual completely before using the STARTER 5000 bench pH meter to avoid
incorrect operation.
STARTER 5000 is a 0.001pH bench meter with a color touch-screen LCD. It’s a new generation of
intuitive and easy-to-use bench meters for reliable measurements.
A few of the many existing features are:
x Bi-lingual graphical user interface
x Auto, manual time endpoint which can assist users to freeze the stable reading value to
meet different customer requirements
x 8 buffer groups (US, EU, NIST and JJG) with 1 self-defined buffer
x IP54 water and dust protection
1.1 Definition of Signal Warnings and Symbols
Safety notes are marked with signal words and warning symbols. These show safety issues and
warnings. Ignoring the safety notes may lead to personal injury, damage to the instrument,
malfunctions and false results.
Signal Words
WARNING For a hazardous situation with medium risk, possibly resulting in
injuries or death if not avoided.
CAUTIONFor a hazardous situation with low risk, resulting in damage to the
device or the property or in loss of data, or injuries if not avoided.
Attention For important information about the product
CAUTION Read all safety warnings before installing, making connections, or
servicing this equipment. Failure to comply with these warnings could result in
x Verify that the AC adapter's input voltage range and the plug type are compatible with the
local AC power supply.
x Make sure that the power cord does not pose a potential obstacle or tripping hazard.
x Use the equipment only in dry locations.
x Dry off any liquid spills immediately. The instrument is not watertight.
x Use only approved accessories and peripherals.
x Operate the equipment only under ambient conditions specified in these instructions.
x Disconnect the equipment from the power supply when cleaning.
x Do not operate the equipment in hazardous or unstable environments.
x Service should only be performed by authorized personnel.
x I f the equipment is used in a manner not specified by the manufacturer, the protection
provided by the equipment may be impaired.
personal injury and/or property damage. Retain all instructions for future reference.
WARNING Do not use this instrument in an environment subject to explosion
hazards. The housing of the instrument is not gas tight (explosion hazard due to
spark formation, corrosion caused by the ingress of gases).
CAUTION When using chemicals and solvent s, comply with the instructions of the
producer and the general lab safety rules.
The model ST5000-B (basic package) has the following items:
In addition to ST5000-B content, the ST5000-F package also includes the following:
Each pH buffer powder should be dissolved in 250ml pure water or deionized water in a
volumetric flask. You also can order the bottled buffer solution from Ohaus.
More electrodes, solutions, accessories and spare parts, please contact Ohaus for more details.
After adjusting the tension knob to some extent, t he upper arm can be move up and down.
When the pH electrode is placed on the arm and calibration or measurement is being
performed, the storage bottle of pH electrode can be placed into the base hole for easy
storage:
2.3 Installing the power adapter
Insert the adapter plug into the power adapter slot.
CAUTION Only use an adapter plug that is compatible with the mains power
receptacle. Make sure that the adapter plug is fully seated in the power adapter slot
before plugging it into the mains power receptacle.
There are 2 sockets for the electrode. “pH” socket (BNC); “TEMP.” Socket (Cinch).
For ST350 3-in-1 electrode, connect both the BNC and Cinch socket. For 2 -in-1 pH electrodes
(e.g. ST230), only connect the BNC.
3 DISPLAY AND ICONS
3.1 Turn on the meter
STARTER 5000 is a color touch screen 0.001pH bench meter. It does not have any buttons.
After connecting with power, the meter will turn on, if meter in screen protection, you can tap the
screen to turn on the screen.
Note: If customer did not operate the meter for more than 6 hours, the meter will completely shut
off automatically. You cannot turn on the meter by tap ping the screen any more. You need to
reconnect power to turn on the meter.
Select the language and then press to enter the main interface.
Main Interface
Tap this area to enter the interface to set the endpoint mode. Available
modes are Auto, Manual and Time end
is
displayed.
Sensor ID:"
Tap this area to enter the interface to select, set or change the sensor ID.
The current sensor ID is displayed.
Cond:"
Tap this area to
sensor performance icon (judged by calibration data) is displayed.
and offset: ± (0
Electrode
or offset: ± (
) mV
Electrode condition is
acceptable
%
or offset: ± (
Electrode
not
good or needs cleaning
Calibration reminder icon
calibration from last calibration. When the time is reached, this icon will be displayed
and blink to remind that it is time to perform a calibration.
“Buffers:”
This area displays the current buffer group, tap this area to enter the interface to
select the buffer group.
Start icon. Tap this icon and the meter wil
iconwill blink. The start icon area will show the stop icon
Calibration icon. Tap this icon to start calibration.
Save icon. After saving the current measurement result (endpoint reached), this
icon color will change
, indicating that the reading has
already been saved and cannot be saved twice.
Output icon. Output
If “Shut off connection” is chosen in
icon
therwise the output icon will be displayed in the
same position.
Information, measure and calibrate tap area
The information area is also the shortcut to enter the setting interface:
point. The current endpoint mode
Sensor
There are 3 sensor condition icons:
Slope: more than 95%
-15) mV
condition is good
enter the sensor calibration data interface. The current
Slope: 90-95%
15-35
. Set the time you want the meter to alert you to do
The meter display will turn off automatically according to the time set in the menu System Setting
►Screen Protection ►LCD Auto-off. To turn on the screen again, tap the screen.(See 3.1)
A complete pH measurement process should follow the procedure:
a) Rinse the pH electrode and connect to meter
b) Prepare the buffer and calibrate the pH electrode
c) Prepare the sample
d) Conduct pH measurement of the sample
e) Record measurement data
f) Rinse the pH electrode and store
Prepare the pH electrode: the pH electrode should be rinsed with pure water before and after
usage. Check if the electrode is physically damaged. (Be careful with the glass bulb)
The pH electrode should be stored in the storage bottle. After the pH electrode has been put into
the sample or buffer solution, stir several seconds then wait 30 to 60 seconds for the signal to be
stable, and then press the button to operate (Calibration or measurement).
WARNING Do not operate the equipment in hazardous environments. The equipment
is not explosion protected.
CAUTION When using chemicals and solvents, comply with the instructions of the
chemical producer and the general lab safety rules.
4.1 Calibration
Buffer group
STARTER 5000 can perform 1-5 point calibrations for predefined buffer groups. For self-defined
buffer group, it can do 1-9 point calibration.
Before calibration, make sure the current buffer group is the group wanted.
When using a new pH electrode, a calibration should be performed before any m easurement. If a
pH electrode is not used for a few days, a calibration should be performed before next usage.
Calibration is to display the right pH value when the meter receive the mV value signal from the
pH electrode.
Slope: the linear coefficient between mV and pH acco rding to theoretical value (e.g. -
59.16mV/pH @ 25°C means 100% slope);
Offset: the mV value when the pH value is 7.00. (Theoretical value is 0 mV)
STARTER 5000 will give an electrode condition icon to show the performance of the pH electrode
according to the calibration data. Normally, if we get sad face icon after a proper calibration, you
may need to replace the pH electrode with a new one.
STARTER 5000 automatically corrects for the t emperature dependence of the buffer pH values.
E.g. for US standard buffer group "1.68, 4.01, 7.00, 10.01" reference the following table:
For example, with calibration buffer 10.01 at 15°C, the calibration result should be 10.12 pH.
Performing calibration
After rinsing the pH electrode, put the electrode into the first buffer, stir for 10s then press to
start the calibration. When in calibration, the signal icon blinks. When the endpoint has been
reached,
are now 3 options:
Quit the calibration and go back to main interface
Finish current point calibration, go to calibration result interface
Do the next point calibration
Note: During calibrating process, the ST5000 is always in Auto Endpoint Mode.
Note: The use of 3-in-1 pH electrode which include the temperature sensor or a separate
temperature electrode is recommended. When using the MTC mode, enter the correct
temperature value and keep all buffer and sample solutions at the set temperature.
appears while disappears and current point calibration is finished, There
Be sure the electrode has been calibrated before measurement. After rinsing,
Place the pH electrode in the sample.
Press
measurement is finished.
Note: If the signal is not stable all the time, it is recommended to use manual endpoint mode to
avoid bad repeatability.
to start the pH measurement, when the endpoint has been reached, the current
mV and Rel.mV measurement
Press to shift to or mode; follow the same procedure as for pH
measurement to perform mV or Rel.mV measurement.
If the meter is connected t o an ORP electrode, the mV result is the value of Oxidation-Reduction
Potential value; also called Redox value.
4.3 Temperature measurement
For better accuracy, we recommend to use either a built-in or a separate temperature electrode.
If a temperature electrode is used, ATC and the sample temperature are displayed.
If the meter does not detect a temperature electrode, it automatically switches to the manual
temperature compensation mode and MTC appears. MTC temperature should be set.
Note: STARTER 5000 accepts NTC 30 kΩ temperature sensor. For ATC (Auto Temperature
Compensation) or MTC (Manual Temperature Compensation), the Temperature Compensation
only corrects for the change in the output of the electrode, not for the change in the actual solution.
That means the meter corrects the signal (mV) from the pH electrodes t o get a more accurate pH
value according to the real temperature.
STARTER 5000 can print the measurement or calibration data through RS232. After the printer
(e.g. OHAUS SF-40A) is connected to the meter properly, make the following settings(See 5.1):
please order the connect cable for ST5000 (P/N 30059316) to connect SF40A and ST5000.
System Setting ► Output , select Printer
System Setting ► Baud Rate, select 9600.
The format for the print-out measurement is:
Date Time User SampleID
6-13-2015 14:20:22 User01 Sample02
SensorID Endpoint mode MTC/ATC
Sensor02 Manual ATC
Temperature Result
25.3°C 6.999pH
The format for the print-out calibration data is:
Calibration Data
SensorID Serial Number
Sensor02 14060012
Cal. Date Cal. Time ATC/MTC
01-01-2015 14:20:33 ATC
Buffers mV Offset Slope
4.00pH 176.94mV
7.00pH 0.05mV 0.05mV 98.22%
When performing continuous measurement, the format for the print-out calibration data is:
Timing Measure Record
System setting is used to set meter parameters, the meter information could also be f ound in it.
Please see section 3.4 for reference.
System setting ►Save Mode
Save mode has 2 options, one is Auto Save Endpoint Reading, another is Manual Save Endpoint
Reading. Auto Save Endpoint Reading means that when the measurement reac hes the endpoint
(auto, manual or time endpoint), the meter will save the endpoint reading automatically.
The Save icon
saved only once.
will change from black to light grey
; An endpoint reading can be
System Setting ►Output
When selecting shut off connection, the main interface will display the save icon, or
display the Output Icon
System Setting ► Restore Factor y Setup
Restoring the factory setup includes the following:
Auto Endpoint
In this mode, the meter will reach the endpoint and lock the reading according to the following
stability criteria automatically:
0.1pH resolution: the signal of the sensor input may not change by more than 0.3mV in 6
seconds.
0.01pH resolution: the signal of the sensor input may not change by more than 0.1mV in 6
seconds.
0.001pH resolution: the signal of the sensor input may not change by more than 0.03mV in 6
seconds.
Time Endpoint
In this mode, the user needs to input the endpoint time, e.g. 15 seconds. This means after starting
the measurement for 15s, the meter will reach the endpoint.
Manual Endpoint
In this mode, the user needs to decide when the signal reading is stable, then press the stop icon
to reach manual endpoint.
Measurement Setting ►GLP Measurement Mode
GLP mode requires each measurement to have the User ID and Sam ple ID. If there is no sample
ID or user ID, the meter will show the interface to let user input the required data.
Measurement Setting ►Co ntinuous Measure
During continuous measure, the user needs to input the time interval to get each reading result.
Below is the Graph of continuous measure.
The Y axis is pH value. The x axis is the Number of measurement result.
Before calibration, please make sure the current buffer group is correct for your buffer solutions.
User can select from the 8 predefined buffer groups.
User can also set self-defined buffer groups. The adjacent 2 calibration point difference should be
larger than 0.99pH.
Calibration Setting ►Calibration Reminder
Enter this setting to set the time, from the last calibration, after how many hours the meter should
remind to perform calibration again. The meter will show the calibration reminder icon
blink, to remind user to perform calibration.
and
5.4 Data Log
Tap Data to get into the Data log interface, including measurement data and calibration data.
You can delete all the measurement data here. The only way to delete calibration data is to
restore factory setup.
The data can be output to a USB Flash Drive (≤4GB).
When the input value/measurement result is out of range or calibration data is not good enough,
the meter will display error information.
If the error cannot be solved by the error message displayed, please contact Ohaus sales
representative for further assistance.
6.2 Meter maintenance
The STARTER 5000 series instruments do not require any maintenance other than occasional
wiping with a damp cloth.
Attention: Follow these safety precautions when cleaning the instrument
x Disconnect the instrument from the power supply
x Do not open the instrument
x Do not allow liquids to enter the instrument
Attention: The housing is made of acrylonitrile butadiene styrene (ABS). This material is attacked
by some organic solvents, such as toluene, xylene and methyl ethyl ketone (MEK). Any spillage
should be immediately wiped off.
6.3 Electrode maintenance
Make sure the electrode is filled with electrolyte solution. Always store the electrode according to
the electrode instruction manual and do not allow it to dry out.
If the electrode response becomes sluggish or the slope is not good enough, try the following:
o Soak the electrode in 0.1M HCl for more than 8 hours.
o For fat or oil contaminant, degrease the membrane with cotton wool soaked in either
acetone or a soap solution.
After electrode treatment, a new calibration should be performed. If the electrode slope is still not
good, the electrode might need to be replaced.
6.4 Information
Tap the Information icon to enter the information interface. Here the user can input related
information by tapping the area with "
" in the bottom left such as sensor purchase date, etc.
Page 21
EN-18 STARTER 5000 Bench pH Meter
Model
SSTARTER 5000
Measuring range
-2.000…20.000 pH
–
-30
Resolution
0.1/0.01/0.001 pH
1
0.1
Error limits
± 0.002 pH
±
± 0.1
Calibration
1-9 points
8 predefined buffer group+1 self-defined buffer group
Memory
1000 measurements
10*10 calibration data
Power supply
100-240V~0.3A input, 9V 1.12A output AC Adapter
Size/weight
Approximately 210 x 170 x 80 mm / 0.65 kg
Ship dimension/weight
Approximately 372 x 310 x 185 mm / 2.30 kg
Display
Touch screen liquid crystal with backlight
Input
BNC, impedance > 3 x 10e+12 Ω
Cinch, NTC 30 kΩ
Temperature-compensation
ATC & MTC
Housing
ABS
7 TECHNICAL DATA
7.1 Specifications
The technical data is valid under the following ambient conditions:
x Indoor use only
x Altitude: Up to 2000 m
x Specified Temperature range: 5°C to 40°C
x Humidity: maximum relative humidity 80 % for temperatures up t o 30°C decreasing linearly to
50% relative humidity at 40°C
x Mains supply voltage fluctuations: up to ±10% of the nominal voltage
x Installation category II
x Pollution degree: 2
x Operability is assured at ambient temperatures between 5°C to 40°C
This product conforms to the EMC Directive 2004/108/EC and the Low Voltage
Directive 2006/95/EC.
In conformance with the European Directive 2002/96/EC on Waste Electrical
and Electronic Equipment (WEEE) this device may not be disposed of in
domestic waste. This also applies to countries outside the EU, per their specific
requirements. The Batteries Directive 2006/66/EC introduces new
requirements from September 2008 on removability of batteries from waste
equipment in EU member States. To comply with this Directive, this device has
been designed for safe removal of the batteries at end-of-life by a waste
treatment facility. Please dispose of this product in accordance with local
regulations at the collecting point specified for electrical and electronic
equipment. If you have any questions, please contact the responsible authority
or the distributor from which you purchased this device. Should this device be
passed on to other parties (for private or professional use), the content of this
regulation must also be related.Thank you for your contribution to
environmental protection.
FCC Note: This equipment has been tested and found to comply with the limits for a Class
A digital device, pursuant to part 15 of the FCC Rules. These limits are designed to provide
reasonable protection against harmful interference when the equipment is operated in a
commercial environment. This equipment generates, uses, and can radiate radio frequency
energy and, if not installed and used in accordance with the instruction manual, may cause
harmful interference to radio communications. Operation of this equipment in a residential
area is likely to cause harmful interference in which case the user will be required to correct
the interference at his own expense.
Industry Canada Note
This Class A digital apparatus complies with Canadian ICES-001
ISO 9001 Registration
In 1994, OHAUS Corporation, USA, was awarded a certificate of registration to ISO 9001 by
Bureau Veritus Quality International (BVQI), confirming that the OHAUS quality
management system is compliant with the ISO 9001 standards requirements. On June 21,
2012, OHAUS Corporation, USA, was re-registered to the ISO 9001:2008 standard.
STARTER 5000 automatically correct for the temperature dependence of the buffer group pH value
given in the following tables. Please choose the buffer group you want before calibration.
Ohaus products are warranted against defects in materials and workmanship from the date of
delivery through the duration of the warranty period. During the warrant y period Ohaus will repair,
or, at its option, replace any component(s) that proves to be defective at no charge, provided that
the product is returned, freight prepaid, to Ohaus.
This warranty does not apply if the product has been damaged by accident or misuse, exposed to
radioactive or corrosive materials, has foreign material penetrating to the inside of the product, or
as a result of service or modification by other than Ohaus. In lieu of a properly returned warranty
registration card, the warranty period shall begin on the dat e of shipment t o the authorized dealer.
No other express or implied warranty is given by Ohaus Corporation. Ohaus Corporation shall not
be liable for any consequential damages.
As warranty legislation differs from state to state and country to country, please contact Ohaus or
your local Ohaus dealer for further details.