Turns On or Off display and fan. On returns with last screen. (All modes)
When pressed, selects Test Library screen.
When pressed, returns to current test, or cycles through several display screens.
12
4
5
6
7
8
9
10
11
12
When pressed, brings up analyzer Setup menu.
When pressed, either starts or stops the drying process.
When pressed, travels up through menu options, selects alphanumeric
characters.
When pressed, travels to the left through displays.
When pressed, travels to the right through displays.
When pressed, travels down through menu options, selects alphanumeric
characters.
When pressed, accepts selection/input (Select mode) or sends Print command
(Run mode).
When pressed, performs Tare function. (Pressing during a test has no effect.)
Leveling feet Used to level the Moisture Analyzer.
MB45 5
1.Getting to know your Moisture Analyzer
This section provides you with essential information on your MB45 Moisture Analyzer. Please read
through the section carefully even if you have previous experience with OHAUS Moisture Analyzers and
be sure to familiarize yourself with the safety notes.
1.1 Introduction
Thank you for deciding to purchase a MB45 Halogen Moisture Analyzer from Ohaus. Behind your
instrument stands OHAUS, a leading manufacturer of precision Moisture Analyzers, Balances, Scales and
Indicators. An Aftermarket Department with trained instrument technicians is dedicated to provide you
with the fastest service possible in the event your instrument requires servicing. OHAUS also has a
Customer Service Department to answer any inquiries regarding applications and accessories.
To ensure you make full use of the possibilities offered by your Moisture Analyzer, please read the
manual completely before installation and operation.
1.2 Overview of the Moisture Analyzer
The Moisture Analyzer offers a high level of operating convenience and useful functions to make accurate
measurements.
The Moisture Analyzer has the following features:
— Up to twice as fast as IR Moisture Analyzers.
— Fully programmable with front panel controls.
— Extremely rugged and chemically resistant construction.
— Ergonomic operating controls and a large, easily readable display.
— Easy to follow menus for simplified operation.
— Built-in functions for manual, automatic timing, printing intervals, and custom units.
— Built-in selectable drying profiles.
— Able to set step heating levels to accommodate a variety of sample types.
— Built-in library stores up to 50 samples complete with setup parameters and statistics.
— Built-in RS232 communication interface.
— Any of five languages (English, Spanish, French, German, Italian) are selectable on the display.
— Display contains all test data during drying process.
— A variety of accessories includes disposable pan liners, calibration mass, temperature calibration
kit, interface communication cables, printer, and a security device.
1.3 What is a Moisture Analyzer?
The Ohaus Halogen Moisture Analyzer can be used to determine the moisture content of practically any
substance. The instrument operates on the thermogravimetric principle: At the start of the measurement,
the Moisture Analyzer determines the weight of the sample; the sample is then quickly heated by the
integral halogen dryer unit and moisture vaporizes. During the drying operation, the instrument
continuously determines the weight of the sample and displays the result. On completion of drying, result
is displayed as % moisture content, % solids, weight or % regain.
6 MB45
1.3 What is a Moisture Analyzer? (cont.)
Of particular importance in practice is the rate of heating. In comparison with conventional infrared
heating or the drying oven method, for example, the halogen dryer of your instrument needs a shorter
time to reach its maximum heating power. It also allows the use of high temperatures; an additional
factor in shortening the drying time. Response times for the control of production are shorter resulting in
increased productivity.
All parameters of a measurement (drying temperature, drying time, etc.) can be pre-selected. The
Moisture Analyzer offers many other possibilities. A few of these are listed here:
— The integrated database for drying procedures stores the settings for your samples.
— The drying characteristics can be matched to the type of sample.
— You can choose between various types of result displays at any time.
— Your settings and measurement results can be recorded and stored.
— Built-in battery backup stores valuable data during a power failure.
Even though the Moisture Analyzer contains many functions, operation remains simple. The three button
controls on the front panel: Test Menu, Display and Setup allows entry into a variety of displays which
includes a test library where previous samples are recorded along with the test parameters so that a
similar sample can be run without the need to enter all new data. There are additional displays which
indicate the test ID number, selected temperature, actual temperature, time, initial weight and moisture
content in percent, solids in percent, grams or custom unit, % regain and a graphical display which
illustrates the time and percentage.
Your Moisture Analyzer conforms with all common standards and directives. It supports standard
procedures, work techniques and records as required by GLP (Good Laboratory Practices) and SOP
(Standard Operating Procedure). We recommend the use of the OHAUS AS-142 Printer. Your Moisture
Analyzer has a CE declaration of conformity and OHAUS is registered to ISO 9001 - Quality Management
System.
MB45 7
1.4 Safety is first
Your Moisture Analyzer employs state of the art technology and meets the latest
demands regarding instrument safety. Improper operation can endanger personnel
and can cause property damage. For safe and dependable operation, please comply
with the following instructions:
— The Moisture Analyzer is used for determination of the moisture in samples.
Please use the instrument exclusively for this purpose. Any other type of use can
endanger personnel and damage the instrument or other property.
— The Moisture Analyzer must not be operated in a hazardous environment and only
under ambient conditions specified in these instructions.
— The Moisture Analyzer may be operated only by trained personnel who are
familiar with the properties of the samples used and with the handling of the
instrument.
— Your Moisture Analyzer is supplied with a 3-pin power cable with an equipment
grounding conductor. Only extension cables which meet the relevant standards
and also have an equipment grounding conductor may be used. Intentional
disconnection of the equipment grounding conductor is prohibited.
The Halogen Moisture Analyzer works with heat!
— Ensure sufficient free space around the instrument to avoid heat accumulation
and overheating (approximately 1 m free space above the instrument).
—Never place flammable materials on, below or next to the instrument as the area
around the dryer unit warms up.
—Exercise caution when removing the sample. The sample itself, the sample
chamber and any sample containers may still be very hot.
— During operation, you should never open the dryer unit as the ring-shaped
heating element or its protective glass can reach 400°C! If you have to open the
dryer unit on occasion, disconnect the instrument from the power supply and wait
until the dryer unit has cooled down completely.
8 MB45
1.4 Safety is first (Cont.)
Certain samples require special care!
With certain types of samples, there is a possibility of danger to personnel or damage
to property through:
Fire or explosion:
— Flammable or explosive substances;
— Substances containing solvents;
— Substances which release flammable or explosive vapors when heated. With
such samples, work at a drying temperature that is low enough to prevent the
formation of flames or an explosion and wear protective goggles. Should there be
any uncertainty regarding the flammability of a sample, always work with a small
sample (maximum. 1 gram). In such cases, never leave the instrument
unattended! In cases of doubt, perform a careful risk analysis.
Poisoning, burning:
— Substances which contain toxic or caustic components. Such substances may be
dried only in a fume hood.
Corrosion:
— Substances which release corrosive vapors when heated (e.g. acids). In the case
of such substances, we advise you to work with small amounts of samples as
the vapor can condense on cooler housing parts and cause corrosion. Please
note that the user always takes responsibility and assumes liability for damage
caused by use of the types of samples mentioned above!
— Never make any modifications or constructional alterations to the instrument and
use only original spare parts and optional equipment from Ohaus Corporation.
— Your Moisture Analyzer is a rugged, precision instrument – but you should still
treat it carefully; it will then provide you with many years of trouble-free operation.
— Please comply with all notes and instructions in these operating instructions.
Keep the instructions in a safe place where they are immediately at hand if any
points are unclear.
APPLICATION DISCLAIMER:
— Moisture determination applications must be optimized and validated by the user
according to local regulations. Application specific data provided by Ohaus is
provided for reference purposes only. Ohaus waives all liability for applications
based on this data.
MB45 9
1.5 What you should know about these instructions
These instructions guide you step by step through the operation of your Moisture Analyzer. Section 2
provides detailed installation instructions. Section 3 allows you to perform a simple measurement.
Section 4 explains the menu operation. Section 5 explains how to set the analyzer up. Section 6 covers
the configuring and operation of the analyzer. Section 7 explains the use of the built-in library. Section 8
explains how to obtain the best results. Section 9 details printing operations. Section 10 covers
maintenance. A1 is an appendix with application samples.
The following graphic orientation aids represent certain functions, notices and controls. These graphic
aids are not meant to be step by step operational procedures but simply a guide.
This hand symbol indicates pressing a button.
This representation symbolizes the current display of your Moisture
Analyzer.
This symbol indicates additional information and instructions which
facilitate your handling of the Moisture Analyzer and contribute to proper
and economical use.
This symbol indicates safety and hazard instructions which must be
complied with. Nonconformance with such instructions can lead to
personal injuries to the user, damage to the Moisture Analyzer or other
tangible assets or to malfunctions.
10 MB45
2. Installation
In this section, you will learn how you unpack and install your new Moisture Analyzer and prepare it for
operation. On completion of the steps described in this section, your Moisture Analyzer is ready for
operation.
2.1 Unpacking and checking the standard equipment
Open the package and remove the instrument and the accessories. Check the completeness of the
delivery.
The following accessories are part of the standard equipment of your new Moisture Analyzer.
— 1 Box, Aluminum sample pans
— 1 Pan support
— 1 Specimen sample (circular, absorbent cellulose disk)
— 1 Draft shield element
— 1 Heat shield
— 1 Power cable
— 1 Set of operating instructions
— 1 Warranty card
Remove packing material from the instrument.
Check the instrument for transport damage. Immediately inform your Ohaus dealer if you have
complaints or parts are missing.
Store all parts of the packaging. This packaging guarantees the best possible protection for the transport
of your instrument.
MB45 11
2.2 Selecting the Location
The Moisture Analyzer should always be used in an environment which is free from excessive air
currents, corrosives, vibration, and temperature or humidity extremes. These factors will affect displayed
weight readings.
DO NOT install the Moisture Analyzer:
• Next to open windows or doors causing drafts
or rapid temperature changes.
• Near air conditioning or heat vents.
• Near vibrating, rotating or reciprocating
equipment.
• Near magnetic fields or equipment that
generate magnetic fields.
• On an unlevel work surface.
• In confined areas, allow sufficient space
around the instrument for ease of operation
and keep away from radiating heat sources.
2.3 Installing the Heat Shield, Draft Shield and Pan Support
Lift the cover straight up and Install the heat shield in the base
Pan Support
Draft Shield
Heat Shield
of the heating chamber.
Install the draft shield element (only one position possible) on
top of the heat shield.
Install the pan support into postion. Turn the pan support until it
engages. In the locked position, the rear arm of the pan support
points directly towards the rear of the analyzer.
12 MB45
2.4 Leveling the Moisture Analyzer
Exact horizontal positioning and stable installation are prerequisites for repeatable results. To
compensate for small irregularities or inclinations at the location, the instrument can be leveled.
Adjust the leveling feet at the rear of the Moisture Analyzer
until the air bubble in the indicator is centered. The level
indicator is located under the cover towards the rear of
the Moisture Analyzer.
NOTE: The instrument should be leveled each time its
location is changed.
Leveling
Indicator
Leveling
Foot
2.5Connecting to a Power Supply
Check to ensure the voltage identification label on the Moisture Analyzer matches
your local line voltage. If this is not the case, do not connect the Moisture Analyzer to
the power supply, contact your responsible OHAUS dealer.
The halogen dryer unit is designed to operate at a specific line voltage
(120 V ac or 240 V ac). The dryer unit is installed at the factory and is matched to
the particular line voltage of the country of destination.
Connection to a line voltage that is too high can lead to burning out the halogen
heater, whereas, a supply voltage that is too low will prolong the drying process and
the instrument may not operate properly.
MB45 13
2.5 Connecting to a Power Supply (cont)
Connect the power cord supplied to the three pin connector located at the
rear of the Moisture Analyzer and to a power source. The Moisture
Analyzer becomes operational as soon as power is applied. The display
will remain off until the On/Off button is pressed.
Allow the Moisture Analyzer to warm up for at least 30 minutes to enable it to
adapt itself to the ambient conditions. If the Moisture Analyzer has been stored in a
very cold environment before installation, it may require several hours for it to
stabilize.
WARNING:
If the power cable supplied is not long enough, use only a proper 3-pin extension
cable with an equipment grounding connector.
2.6 Switching the Moisture Analyzer on and off
Your Moisture Analyzer is on at all times when connected to a power source. The display can be turned
on or off.
TEST ID:
TEMP/TIME:
TARG. WGT:
CLOSE
COVER
-DEFAULT-
100°C / 10:00
1.000 G
0.000
* GRAMS
To switch the Moisture Analyzer on, press the On/Off button. An internal
diagnostic test is performed; the display lights and the logo and product
name appears followed by the initial display.
To switch the Moisture Analyzer off, press the On/Off button. After the
analyzer has been switched off, it is in the standby mode. If you wish to
perform a test, press the On/Off button again.
As your Moisture Analyzer needs no warm-up time when in the standby
mode and is immediately ready for testing samples, we advise you to
switch the display off by use of the On/Off button and not to disconnect it
from the power supply. This also ensures that the Moisture Analyzer is
always in thermal equilibrium.
14 MB45
3. Making a simple measurement
With your Moisture Analyzer powered on, you are ready to operate for the first time and perform a simple
measurement. For this simple test, you will enter the Test Menu and enable the test. By doing this test,
you will become familiar with the instrument and the various displays.
Included with your Moisture Analyzer is a specimen sample for your first measurement. This sample is
an absorbent glass fiber pad. During your first measurement, the instrument operates with the factory
settings.
If the display is not visible and the unit is plugged into a power source,
press the On/Off button.
TEST ID:
TEMP/TIME:
TARG. WGT:
CLEAR
PAN
PRESS
TARE
-DEFAULT-
100°C / 10:00
1.000 G
0.000
* GRAMS
The display indicates the parameters for DEFAULT settings. Follow the
instructions on the lower left side of the display.
NOTE: If the unit has been operated, the default test settings may
have changed. If required, see Section 6 to reset the test
parameters.
For this simple test, the default settings are:
Drying temperature is set to: 100°CProfile is set to: standard Switch Off is set to: timed 10:00 minutes
Display is set to: % moist Print interval is set to: OFF Target weight is set to: 1 grams
Save is set to: NO
Open the cover on the Moisture Analyzer.
Clear the pan.
Place the empty sample pan in the pan handler (this is possible
without tilting the sample pan if you insert this in the pan handler from
the side directly below the round flange). Place the pan handler in the
sample chamber. Ensure that the tongue of the pan handler fits exactly
in the slot of the draft shield element. The sample pan must lie flat in
the pan handler.
Note: It is advisable for you to work with the pan handler at all times.
The pan handler is ergonomic, safe and provides protection against
possible burns due to a hot sample pan.
Place the specimen sample in the sample pan (glass fiber pad).
Press the Tare button.
This sets the Moisture Analyzer to zero. A new display now appears
with instructions.
MB45 15
3. Making a simple measurement (cont)
TEST ID:
TEMP/TIME:
TARG. WGT:
SAMPLE
<.500G
-DEFAULT-
100°C / 10:00
1.000 G
0.000
* GRAMS
Wet the specimen sample with a 0.5 to 1 gram of water.
NOTE: Minimum sample size must be greater than 0.5 gram.
TEST ID:
TEMP/TIME:
TARG. WGT:
CLOSE
COVER
-DEFAULT-
100°C / 10:00
1.000 G
0.930
* GRAMS
Close the cover.
Starting the test
Press the Start/Stop button. The Moisture Analyzer starts the
drying and measurement process.
C
-DEFAULT-
100°C / 10:00
0.930 GRAMS
4.04
* %MOISTURE
Drying and measurement
You are now able to follow the progress of the drying cycle on the
display. This first display comes up automatically when the test
was started.
TEST ID:
TEMP/TIME:
INITIAL WT:
70
08:11
Observing the test progress
There are six displays available when the Moisture Analyzer is running a test. The Display button on the
front panel when pressed repeatedly accesses each of the six displays during the run mode of the
Analyzer and cycles though each display in the order shown below.
The displays indicate the Test ID, Temperature/Time, Initial Weight, actual temperature, elapsed time
duration of the test, either moisture, solids, grams, percent regain, a graph representing the actual test
progress and statistics at the end of the test.
16 MB45
Observing the test progress (cont)
Press the Display button repeatedly to view the progress of the sample test with different displays.
The test automatically stops at the end of 10:00 minutes. If you want to end the test sooner, press the
START/STOP button.
Press×Display
Press
Display
Ö
TEST ID:
TEMP/TIME:
INITIAL WT:
100 C
08:11
Press
Display
Õ
Congratulations! You have just performed your first measurement with your
moisture analyzer.
-DEFAULT-
100°C / 10:00
0.930 GRAMS
0.00
* %SOLIDS
Press
Display
Ö
PressØDisplay
Press
Display
Õ
Carefully remove the sample pan handler from the drying area.
Warning: As the pan and sample may still be hot, you should let these cool
down before removing the pan from the pan handler!
To remove the sample pan from the pan handler, lift the pan slightly from
below and pull it sideways out of the pan handler (if you no longer need the
sample and pan, you can simply tilt the pan handler until the pan slides out).
The last display from the test remains on the screen until you press the Tare
button. Press the Tare button. This sets the Moisture Analyzer to zero.
The display returns to the first test display, ready to repeat the test.
If you want to get out of the test mode, simply press any other button on the unit.
Continue to review the rest of this manual and become familiar with the menus.
MB45 17
4. The menus
4.1 What are the menus?
There are two sets of menus used in the Moisture Analyzer. One is the Setup menu which is activated by
the Setup button. This menu permits calibration, adding custom units, language selection, beeper
volume settings, time and date format, communication settings and print criteria. The Test menu is
activated by the Test Menu button. This menu permits setting up new test parameters which includes test
temperatures, ID, profiling, timed information, type of display, print intervals, editing and running the test.
A test library is also included which holds data for up to 50 tests which can be recalled and run at any
time. The contents of each menu are shown below.
SETUP TEST MENU
⎯ Lockout
⎯ Weight Calibration
⎯ Temperature Calibration
⎯ Language
English, Deutsch, Español, Francais,
Italiano
⎯ Beeper
− Low, High, Off
⎯ Time-Date
− Date Format, Set Date
− Time Format, Set Time
⎯ RS232
− Baud Rate
1200, 2400, 4800, 9600, 19,200
− Parity
Odd, Even, None
− Data Bits
7, 8
− Stop Bits
1, 2
− Handshake
None, XON-XOFF, RTS-CTS
⎯ Print
− Print On/Off
− GLP On/Off
⎯ Display
− Contrast
− Brightness
⎯ Factory Reset
Test Library
⎯ 01
⎯ Load Test
⎯ Edit Test
⎯ Delete Test
⎯ 02
⎯ Load Test
⎯ Edit Test
⎯ Delete Test
⎯ 03
⎯ Load Test
⎯ Edit Test
⎯ Delete Test
y
y
y
⎯ 50
⎯ Load Test
⎯ Edit Test
⎯ Delete Test
⎯ Edit Test
⎯ Test Parameters
⎯ Test ID:
⎯ Profile:
⎯ Dry Temp:
⎯ Switch Off:
⎯ Result:
⎯ Custom
⎯ Target Wt:
⎯ Print Int:
⎯ Save Test:
− Standard
− Fast
− Ramp
− Step
− Timed-Switch Off
− Man.-Use Start/Stop
− AFREE – Wt
loss/time
− A90 - <
− A60 - <
− A30 - <
− % Moisture
− Custom Units
− Grams
− % Regain
− % Solids
− Factor, Exponent, LSD
− Off, 1, 3, 5, 10, 30
− 1, 2, 5 Min.
1MG in 90 sec.
1MG in 60 sec.
1MG in 30 sec.
Sec
18 MB45
4.2 Menu operation
In this section you will learn how to work with the menus. Information regarding the individual menu
options and available settings can be found in the following sections.
How to select the test menu
Pressing the Test Menu button accesses the Test Library menu. The Test
Library contains up to 50 tests. All tests which were previously entered
can be recalled and the parameters for the recalled test when selected will
be repeated.
How to exit the test menu without making changes
Press the Display button.
How to select the setup menu
Pressing the Setup button will give you access to the Analyzer Setup
ANALYZER SETUP
LOCK OUT
WEIGHT CAL
TEMP CAL
LANGUAGE
BEEPER
TIME-DATE
menu.
How to exit the setup menu without making changes
Press the Display button.
or
TEST PARAMETERS
TEST ID:
PROFILE:
DRY TEMP:
SWITCH OFF:
RESULT:
CUSTOM:
071000A
STANDARD
100C
TIME 10M
MOISTURE%
OFF
How to select the menu options
Press either the up or down arrow buttons and scroll to the desired option.
Each time the arrow
option. Each time the
button is pressed, the menu advances to the next
arrow button is pressed, the menu returns to the
previous menu option. When scrolling past the last item, the screen
displays the next item.
How to enter the menu option
Press the Enter button when the desired menu option is highlighted.
MB45 19
4.2 Menu operation (cont)
How to enter alpha numeric data and make selections
Certain menu options can have names or numerical entries made. When
prompted to enter information, use the arrow buttons as follows:
Press the
and to highlight an item in a menu.
Press the
or it can be used to highlight an item in a menu.
Press the
display or it can be used to highlight an item in a menu.
Press the Enter button to accept entry.
How to access various displays
There are six displays available when the Moisture Analyzer is running a
test and at the end of the test. The Display button on the front panel when
pressed repeately accesses each of the six displays during the run mode
of the analyzer and cycles though each display in the order shown below.
The displays indicate the Test ID, Temperature/Time, Initial Weight, actual
temperature, elasped time duration of the test, either moisture, solids,
percent regain, grams, a graph representing the actual test progress and
statistics.
and arrow buttons to scroll through numbers or alphabet
arrow button to advance to the next character in the display
arrow button to go back to the previous character in the
Press×Display
Press
Display
Ö
Press
Display
Õ
TEST ID:
TEMP/TIME:
INITIAL WT:
100 C
08:11
-DEFAULT-
100°C / 10:00
0.930 GRAMS
0.00
* %SOLIDS
Press
Display
Ö
PressØDisplay
Press
Display
Õ
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