Ocean Optics Dragon User Manual

Installation
Dragon and Quantum Software Installation and Operation Manual Document Number 203-00000-DRA-02-0210
Offices: Ocean Optics, Inc. World Headquarters
830 Douglas Ave., Dunedin, FL, USA 34698
Phone 727.733.2447 Fax 727.733.3962
8 a.m.– 8 p.m. (Mon-Thu), 8 a.m.– 6 p.m. (Fri) EST
203-00000-DRA-02-
E-mail: Info@OceanOptics.com (General sales inquiries)
Orders@OceanOptics.com (Questions about orders) TechSupport@OceanOptics.com (Technical support)
Additional Offices:
Regional Headquarters Maybachstrasse 11 73760 Ostfildern
Phone 49-711 34 16 96-0 Fax 49-711 34 16 96-85 E-Mail Sales@Mikropack.de
Ocean Optics Asia
666 Gubei Road, Kirin Tower, Suite 601B, Changning District, Shanghai, PRC. 200336
Phone 86.21.5206.8686
Fax 86.21.5206.8686 E-Mail Sun.Ling@OceanOptics.com
Ocean Optics EMEA
Sales and Support Center Geograaf 24, 6921 EW DUIVEN, The Netherlands
Phone 31-26-3190500
Fax 31-26-3190505 E-Mail
Info@OceanOptics.eu
Copyright © 2010 Ocean Optics, Inc.
All rights reserved. No part of this publication may be reproduced, stored in a retrieval system, or transmitted, by any means, electronic, mechanical, photocopying, recording, or otherwise, without written permission from Ocean Optics, Inc. This manual is sold as part of an order and subject to the condition that it shall not, by way of trade or otherwise, be lent, resold, hired out or otherwise circulated without the prior consent of Ocean Optics, Inc. in any form of binding or cover other than that in which it is published.
Trademarks
All products and services herein are the trademarks, service marks, registered trademarks or registered service marks of their respective owners.
Limit of Liability
Ocean Optics has made every effort to ensure that this manual as complete and as accurate as possible, but no warranty or fitness is implied. The information provided is on an “as is” basis. Ocean Optics, Inc. shall have neither liability nor responsibility to any person or entity with respect to any loss or damages arising from the information contained in this manual.
Table of Contents
About This Manual......................................................................................................... iii
Document Purpose and Intended Audience..............................................................................iii
Document Summary..................................................................................................................iii
Product-Related Documentation ............................................................................................... iii
Warranty........................................................................................................................ iii
Chapter 1: Introduction .....................................................................1
Product Overview .......................................................................................................... 1
Features ........................................................................................................................ 2
System Requirements ................................................................................................... 2
Shipment Components .................................................................................................. 2
Other Accessories Available.......................................................................................... 3
Chapter 2: Installing Dragon.............................................................5
Overview ....................................................................................................................... 5
Quantum Software Installation....................................................................................... 5
Dragon Installation......................................................................................................... 5
Connect Spectroscopic Accessories.............................................................................. 6
Chapter 3: Quantum Software Icons ................................................7
Overview ....................................................................................................................... 7
Integration time
Intensity mode
Dark spectrum
Reference spectrum
Color fill
Transmission mode ....................................................................................................... 11
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Table of Contents
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Absorbance mode ................................................................................................ 11
Smoothing
Average scans ...........................................................................................................................12
Pixel smoothing ......................................................................................................................... 12
............................................................................................................ 12
Snapshot ............................................................................................................ 13
Zoom
New graph
..................................................................................................................... 14
............................................................................................................ 14
Cursor ........................................................................................................................... 15
Reference emission lines............................................................................................... 15
Chapter 4: Experiments.....................................................................19
Concentration wizard ............................................................................................ 19
Kinetics wizard
Tips for successful kinetics experiments ................................................................................... 23
..................................................................................................... 23
Appendix: Maintenance.....................................................................29
Fiber care ...................................................................................................................... 29
Spectrometer care......................................................................................................... 29
Troubleshooting............................................................................................................. 30
Index ...................................................................................................31
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About This Manual
Document Purpose and Intended Audience
This document provides you with installation and operation instructions for your Dragon spectrometer.
Document Summary
Chapter Description
Chapter 1: Introduction
Chapter 2: Quantum Software Icons
Chapter 3: Experiments
Appendix: Maintenance
Provides an overview of spectroscopy and spectrometers.
Contains a list of the icons and their functions in Quantum software.
Provides a variety of experiments to perform using Dragon and Quantum software.
Provides suggested maintenance and a table of possible problems and suggested solutions.
Product-Related Documentation
You can access documentation for Ocean Optics products by visiting our website at
http://www.oceanoptics.com
document from the available drop-down lists. Or, use the of the web page.
You can also access operating instructions for Ocean Optics products on the
Resources
Engineering-level documentation is located on our website at
CD included with the system.
. Select Technical → Operating Instructions, then choose the appropriate
Search by Model Number field at the bottom
Software and Technical
Technical → Engineering Docs.
Warranty
Ocean Optics offers a 90-day warranty on Dragon spectrometers. You must first contact Customer Support and obtain a Return Merchandise Authorization (RMA) number. Please contact Ocean Optics for specific instructions when returning a product.
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About This Manual
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iv 203-00000-DRA-02-
Chapter 1
Introduction
Product Overview
The Ocean Optics Dragon is a high-value miniature spectrometer that delivers 350 – 900 nm spectral coverage with a minimum 2.0 (FWHM) optical resolution with a 50 micron fiber. Dragon includes Quantum operating software for performing basic spectroscopy functions such as absorbance, transmission and emission. The spectrometer has an SMA 905 connector for attaching patch cords and other accessories.
Dragon is low-cost and has a small footprint, making it ideal as a general purpose instrument for budget­conscious teaching and research labs. It uses a detector with 300 active pixels.
Data programmed into a memory chip on each Dragon includes wavelength calibration coefficients, linearity coefficients, and the serial number unique to each spectrometer. Our Quantum spectrometer operating software simply reads these values from the spectrometer — a feature that enables hot swapping of spectrometers among computers.
Dragon connects to a computer via the USB port and draws power from the host computer, eliminating the need for an external power supply.
Ocean Optics Dragon Spectrometer
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Chapter 1: Introduction
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Features
A 2048-element linear silicon CCD array detector Responsive from 350 to 900 nm An optical resolution of ~2.0 nm (FWHM) with a 50 micron fiber Integration times from 3 ms to 65 seconds Embedded microcontroller allows programmatic control of all operating parameters EEPROM storage for
Wavelength Calibration Coefficients
Linearity Correction Coefficients
Other configuration parameters
Low power consumption 12 bit, 1MHz A/D Converter USB connector for interfacing to a computer
System Requirements
You can use Dragon’s USB connectivity with a PC running the Microsoft Windows operating system.
Shipment Components
The following information and documentation ships with the Red Tide Spectrometer:
Packing List
The packing list is inside a plastic bag attached to the outside of the shipment box (the invoice arrives separately). It lists all items in the order, including customized components in the spectrometer (such as the grating, detector collection lens, and slit). The packing list also includes the shipping and billing addresses, as well as any items on back order.
USB Cable (USB-CBL-1)
Use this cable to connect your spectrometer to a computer running on a Windows, Mac or Linux operating system.
Dragon CD
Each order ships with a CD that contains Quantum software and these operating instructions. You need Adobe Acrobat Reader version 6.0 or higher to view these files.
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Chapter 1: Introduction
Other Accessories Available
Visit us at www.OceanOptics.com for a complete list of products available for all of your spectroscopy needs.
Fibers Light Sources Integrated Sampling Systems Cuvettes Filter Holders
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Chapter 1: Introduction
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.
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Chapter 2
Installing Dragon
Overview
You must install the Quantum software application prior to connecting Dragon to your computer. The Quantum software installation installs the drivers required for Dragon installation. If you do not install Quantum first, the system will not properly recognize Dragon.
Quantum Software Installation
The Quantum software used to operate your Dragon spectrometer is on the Dragon CD. Double-click on the Quantum Software setup.exe file and follow the prompts in the Installation Wizard.
Dragon Installation
Procedure
Follow the steps below to connect Dragon to a computer via the USB port:
1. Install Quantum software (setup.exe) from the Dragon CD on the destination computer.
2. Locate the USB cable (USB-CBL-1) provided with Dragon.
3. Insert the square end of the cable into the side of Dragon containing the USB port.
4. Insert the rectangular end of the cable into the USB port of the computer.
5. If you have an optical fiber, connect it to the SMA connector on the other end of the spectrometer.
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Chapter 3: Quantum Software Icons
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Once you install the software and hardware and establish your sampling system, you are ready to take measurements.
Connect Spectroscopic Accessories
To find operating instructions for Dragon-compatible products (such as light sources, sampling chambers, and probes), consult the
http://www.oceanoptics.com/technical/operatinginstructions.asp.
Software and Technical Resources CD or the Ocean Optics website at
The following are typical configurations for absorbance, transmission irradiance and reflection experiments.
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