Oakton 35660-54, 35660-56 Instruction Manual

CODE:M003857-3200839729-GZ0000590175
CAUTION
Note
Responsive glass membrane
Liquid junction
Protective cap
Body
Cap
Lead
Connector cover
Electrode connector
Temperature connector
Guard tube
Gel-filled pH Electrode (35660-54 / 35660-56)
Instruction Manual
December, 2019
This manual describes the operation of the gel-filled pH electrode,
35660-54/35660-56. Be sure to read this manual
carefully, before using the electrode.
Conformable standards
This equipment conforms to the following standards:
RoHS: EN50581
9. Monitoring and control instruments
Authorised representative in EU
Cole-Parmer UK 9 Orion Court, Ambuscade Road Colmworth Business Park St Neots Cambridgeshire PE19 8YX, United Kingdom Phone: +44-(0)1480-272279 Fax: +44-(0)1480-212111
Caution on use
Safety precautions
Chemical solution
If the internal material comes in contact with the hands or skin, wash immediately with water.
Glass fragments
Glass fragments can cause injury. The tip of the electrode are made of glass. Be careful not to break them.
Points of concern
Do not give an excessive shock to the electrode. Cracked or chapped electrode can not be used.Replace
such electrode with a new one.
Do not wet the connector with water or sample and do
not touch the connector with wet fingers. If it is wet measured value might be erroneous.
If the dirt on the responsive glass membrane or liquid
junction can not be removed by pure water, clean them with the other way referring to the Maintenance. “ Maintenance ” (page 2).)
Avoid continuous measurement soaking in the strong
acidic or alkaline solution concentrated more than 0.01 mol/L. These solution may reduce the performance and the lifetime of the electrode.
Do not to use the electrode in a solution in which
hydrofluoric acid (HF) is contained. Glassware will corrode in the HF solution.
Avoid sudden temperature change over 50 °C on the
electrode. The body of the electrode might be deformed or the glassware might be cracked.
Solid particles of silver chloride might be observed
floating in the inner solution of the responsive glass membrane. This is not a problem and this will not affect performances of the electrode.
Do not use the electrode in any place where operation
temperature is out of the specified range.
Do not swing the electrode like a pendulum, and do not
pull up the electrode by the lead wire. Also, avoid
(Refer to
hanging the electrode or the pH meter by the lead wire. It may be a cause of breaking wires.
When disposing of the product, follow the related laws
and/or regulations of your country for disposal of the product.
Packaged contents
Name Q’ty
Electrode 1 pc
Instruction manual (this book) 1 booklet
Specifications and parts description
Part name
Specifications
Electrode model 35660-54, 35660-56
Measurement range pH 0 to 14
Operation temperature range 0°C to 80°C
Storage temperature range 0°C to 50°C
Internal electrode Silver/silver chloride
Reference electrode system Double junction
Reference electrode internal electrolyte
Liquid junction material Porous sintered polyethylene
Wetted material
Electrode length 150 mm
Ext. diam. of wetted part 16 mm
Liquid junction height
Cable length
Connector BNC/Mini plug
Temperature probe NTC
Maximum dipping depth 1 m
Zero point pH7.0
Body material is plastic. Do not use organic solvents (such as acetone or toluene).
Polymer-gel, 3.3 mol/L KCl
Glass, butyl rubber, polycarbonate, polyethylene
Approximately 15 mm (from the tip of electrode)
10D: 1 m 20D: 2 m
Oakton Instruments
625 E. Bunker Ct. Vernon Hills, IL. 60061, USA E-mail: info@4oakton.com Phone number: (1)888-462-5866
For any questions regarding this product, please contact your local agency, or inquire from the following website. http://www.4oakton.com/
Preparations
Note
Note
C1
T1
T2
C2
Protective cap
Note
Note
Note
Connecting to pH meter
1. Insert the electrode connector into the connector port sleeve on the meter, after aligning with the pin. Do not insert the connector unless it is aligned properly with the connector port.
2. Press the electrode connector into the connector port on the meter, while turning the connector to the right.
3. Slide the connector cover over the connector. Then, push the cover in straight until it comes in light contact with the meter case. Do not turn the cover.
4. Insert the temperature connector into the jack on the meter. Insert the connector firmly, until the O-ring on the connector can no longer be seen.
5. Shake the electrode in the sample solution lightly to remove bubbles
. If bubbles remain on the electrode
surface, accurate measurement cannot be performed.
The time for submerged measurement within 1 m of the
depth is limited in 30 minutes.
For the calibration and the measurement of the pH meter,
refer to the instruction manual of the pH meter.
Maintenance
Do not use organic solvents (such as acetone or tetrahydrofuran) as cleaning solutions. Using such chemicals may damage the body of the electrode or cause a decline in performance.
Be sure to install the temperature connector. If not, accurate measurement cannot be performed.
Measurement (calibration)
White crystal powder of KCl may appear around on the end of the protective cap after long time storage. The powder may not be a cause of trouble for measuring pH, and wash them with pure water.
1. Remove the protective cap.
2. Clean the electrode with pure water (or deionized water) and wipe it with filter paper or tissue paper, prior to every immersion into
the standard or sample solution.
Dirt on the responsive glass membrane or the liquid junction by the test solution may cause a decline in electrode response and sensitivity or measurement error. If the electrode is very dirty and cannot be washed clean using pure water (or deionized water), perform cleaning as follows.
Cleaning of electrode
1. The responsive glass membrane can be cleaned by wiping it with cotton gauze containing cleansing agent. The liquid junction can be cleaned by applying it with cotton gauze containing cleansing agent. (- 30 minutes)
Type of dirt Cleansing agent
General Diluted neutral cleansing agent
Oil Alcohol, or diluted neutral cleansing agent
Inorganic substance Hydrochloric acid approximately 1 mol/L
2. Rinse the electrode with pure water (or deionized water) completely
.
3. When there are air bubbles inside the responsive glass membrane, s
hake the electrode lightly to remove
bubbles.
4. Immerse the responsive glass membrane and the liquid junction in the sample
solution completely.
2
3. Immerse the liquid junction completely into 3.33 mol/L KCl solution for approximately 30 minutes before use.
Do not apply excessive force to the glass membrane on
wiping.
Be sure to perform calibration prior to measurement after
cleaning the electrode.
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