CODE:M003857-3200839729-GZ0000590175
Responsive glass
membrane
Liquid junction
Protective cap
Body
Cap
Lead
Connector cover
Electrode connector
Temperature connector
Guard tube
Gel-filled pH Electrode (35660-54 / 35660-56)
Instruction Manual
December, 2019
This manual describes the operation of the gel-filled pH
electrode,
35660-54/35660-56. Be sure to read this manual
carefully, before using the electrode.
Conformable standards
This equipment conforms to the following standards:
RoHS: EN50581
9. Monitoring and control instruments
Authorised representative in EU
Cole-Parmer UK
9 Orion Court, Ambuscade Road
Colmworth Business Park
St Neots
Cambridgeshire
PE19 8YX, United Kingdom
Phone: +44-(0)1480-272279
Fax: +44-(0)1480-212111
Caution on use
Safety precautions
Chemical solution
If the internal material comes in contact with the hands or skin,
wash immediately with water.
Glass fragments
Glass fragments can cause injury.
The tip of the electrode are made of glass.
Be careful not to break them.
Points of concern
Do not give an excessive shock to the electrode.
Cracked or chapped electrode can not be used.Replace
such electrode with a new one.
Do not wet the connector with water or sample and do
not touch the connector with wet fingers. If it is wet
measured value might be erroneous.
If the dirt on the responsive glass membrane or liquid
junction can not be removed by pure water, clean them
with the other way referring to the Maintenance.
“ Maintenance ” (page 2).)
Avoid continuous measurement soaking in the strong
acidic or alkaline solution concentrated more than 0.01
mol/L. These solution may reduce the performance and
the lifetime of the electrode.
Do not to use the electrode in a solution in which
hydrofluoric acid (HF) is contained. Glassware will
corrode in the HF solution.
Avoid sudden temperature change over 50 °C on the
electrode. The body of the electrode might be deformed
or the glassware might be cracked.
Solid particles of silver chloride might be observed
floating in the inner solution of the responsive glass
membrane. This is not a problem and this will not affect
performances of the electrode.
Do not use the electrode in any place where operation
temperature is out of the specified range.
Do not swing the electrode like a pendulum, and do not
pull up the electrode by the lead wire. Also, avoid
(Refer to
hanging the electrode or the pH meter by the lead wire.
It may be a cause of breaking wires.
When disposing of the product, follow the related laws
and/or regulations of your country for disposal of the
product.
Packaged contents
Name Q’ty
Electrode 1 pc
Instruction manual (this book) 1 booklet
Specifications and parts description
Part name
Specifications
Electrode model 35660-54, 35660-56
Measurement range pH 0 to 14
Operation temperature range 0°C to 80°C
Storage temperature range 0°C to 50°C
Internal electrode Silver/silver chloride
Reference electrode system Double junction
Reference electrode internal
electrolyte
Liquid junction material Porous sintered polyethylene
Wetted material
Electrode length 150 mm
Ext. diam. of wetted part 16 mm
Liquid junction height
Cable length
Connector BNC/Mini plug
Temperature probe NTC
Maximum dipping depth 1 m
Zero point pH7.0
Body material is plastic. Do not use organic solvents (such as
acetone or toluene).
Polymer-gel, 3.3 mol/L KCl
Glass, butyl rubber, polycarbonate,
polyethylene
Approximately 15 mm
(from the tip of electrode)
10D: 1 m 20D: 2 m
Oakton Instruments
625 E. Bunker Ct. Vernon Hills, IL. 60061, USA
E-mail: info@4oakton.com
Phone number: (1)888-462-5866
For any questions regarding this product, please contact your local agency,
or inquire from the following website.
http://www.4oakton.com/
Preparations
Connecting to pH meter
1. Insert the electrode connector into the connector port
sleeve on the meter, after aligning with the pin. Do not
insert the connector unless it is aligned properly with the
connector port.
2. Press the electrode connector into the connector port on
the meter, while turning the connector to the right.
3. Slide the connector cover over the connector. Then,
push the cover in straight until it comes in light contact
with the meter case.
Do not turn the cover.
4. Insert the temperature connector into the jack on the
meter. Insert the connector firmly, until the O-ring on the
connector can no longer be seen.
5. Shake the electrode in the sample solution lightly to
remove bubbles
. If bubbles remain on the electrode
surface, accurate measurement cannot be performed.
The time for submerged measurement within 1 m of the
depth is limited in 30 minutes.
For the calibration and the measurement of the pH meter,
refer to the instruction manual of the pH meter.
Maintenance
Do not use organic solvents (such as acetone or
tetrahydrofuran) as cleaning solutions. Using such chemicals
may damage the body of the electrode or cause a decline in
performance.
Be sure to install the temperature connector. If not, accurate
measurement cannot be performed.
Measurement (calibration)
White crystal powder of KCl may appear around on the end of
the protective cap after long time storage. The powder may not
be a cause of trouble for measuring pH, and wash them with
pure water.
1. Remove the protective cap.
2. Clean the electrode with pure water (or deionized water)
and wipe it with filter paper or tissue paper, prior to every
immersion into
the standard or sample solution.
Dirt on the responsive glass membrane or the liquid junction
by the test solution may cause a decline in electrode
response and sensitivity or measurement error. If the
electrode is very dirty and cannot be washed clean using
pure water (or deionized water), perform cleaning as follows.
Cleaning of electrode
1. The responsive glass membrane can be cleaned by
wiping it with cotton gauze containing cleansing agent.
The liquid junction can be cleaned by applying it with
cotton gauze containing cleansing agent. (- 30 minutes)
Type of dirt Cleansing agent
General Diluted neutral cleansing agent
Oil Alcohol, or diluted neutral cleansing agent
Inorganic substance Hydrochloric acid approximately 1 mol/L
2. Rinse the electrode with pure water (or deionized water)
completely
.
3. When there are air bubbles inside the responsive glass
membrane, s
hake the electrode lightly to remove
bubbles.
4. Immerse the responsive glass membrane and the liquid
junction in the sample
solution completely.
2
3. Immerse the liquid junction completely into 3.33 mol/L
KCl solution for approximately 30 minutes before use.
Do not apply excessive force to the glass membrane on
wiping.
Be sure to perform calibration prior to measurement after
cleaning the electrode.