Loctite 243 Technical Data Sheet

Technical Data Sheet
LOCTITE® 243™
(TDS for new formulation of Loctite®243™) August-2016
LOCTITE® 243™ provides the following product characteristics:
Technology Acrylic Chemical Type Dimethacrylate ester Appearance (uncured) Blue liquid Fluorescence Positive under UV light
LMS
LMS
Components One component -
requires no mixing
Viscosity Medium, thixotropic Cure Anaerobic Secondary Cure Activator Application Threadlocking Strength Medium
This Technical Data Sheet is valid for LOCTITE® 243™ manufactured from the dates outlined in the "Manufacturing Date Reference" section
LOCTITE® 243™ is designed for the locking and sealing of threaded fasteners which require normal disassembly with standard hand toolsThe product cures when confined in the absence of air between close fitting metal surfaces and prevents loosening and leakage from shock and vibrationThe thixotropic nature of LOCTITE® 243™ reduces the migration of liquid product after application to the substrateLOCTITE 243™ provides robust curing performance. It not only works on active metals (e.g. brass, copper) but also on passive substrates such as stainless steel and plated surfacesThe product offers high temperature performance and oil tolerance. It tolerates minor surface contaminations from various oils, such as cutting, lubrication, anti-corrosion and protection fluids
NSF International Registered to NSF Category P1 for use as a sealant where
there is no possibilty of food contact in and around food processing areas. Note: This is a regional approval. Please contact your local Technical Service Center for more information and clarification.
NSF International Certified to ANSI/NSF Standard 61 for use in commercial and
residential potable water systems not exceeding 82° C. Note: This is a regional approval. Please contact your local Technical Service Center for more information and clarification.
TYPICAL PROPERTIES OF UNCURED MATERIAL
Specific Gravity @ 25 °C 1.08 Flash Point - See SDS
Viscosity, Brookfield - RVT, 25 °C, mPa·s (cP):
Spindle 3, speed 20 rpm 1,300 to 3,000
Viscosity, Cone & Plate, 25 °C, mPa·s (cP):
Cone 35/2°Ti @ shear rate 129 s
-1
350
TYPICAL CURING PERFORMANCE
Cure Speed vs. Substrate
The rate of cure will depend on the substrate used.The graph below shows the breakaway strength developed with time on M10 steel nuts and bolts compared to different materials and tested according to ISO 10964.
100
Steel
75
Cr free, Zinc organic
50
25
% of Full Strength on Steel
0 1min 5min10min 30min 1h 3h 6h 24h 72h
®
Brass
Stainless steel
Zinc dichromate
Cure Time
Cure Speed vs. Bond Gap
The rate of cure will depend on the bondline gap.Gaps in threaded fasteners depends on thread type, quality and size The following graph shows shear strength developed with time on steel pins and collars at different controlled gaps and tested according to ISO 10123
100
75
50
0.05 mm
0.15 mm
25
% of Full Strength on Steel
0 1min 5min10min 30min 1h 3h 6h 24h 72h
0.25 mm
Cure Time
LMS
TDS LOCTITE® 243™, August-2016
Cure Speed vs. Temperature
The rate of cure will depend on the temperatureThe graph below shows the breakaway strength developed with time at different temperatures on M10 steel nuts and bolts and tested according to ISO 10964
120
100
80
60
40
20
% of Full Strength on Steel
0 1min 5min10min 30min 1h 3h 6h 24h 72h
40 °C
22 °C
5 °C
Cure Time
Cure Speed vs. Activator
Where cure speed is unacceptably long, or large gaps are present, applying activator to the surface will improve cure speedThe graph below shows the breakaway strength developed with time on M10 zinc dichromate steel nuts and bolts using Activator 7471™, 7649™, 7088™ and 7091™ and tested according to ISO 10964
100
80
Prevail Torque @ 180°, ISO 10964, Unseated:
M10 black oxide bolts and mild steel nuts
M6 black oxide bolts and steel nuts N·m 1
M16 black oxide steel bolts and mild steel nuts
3/8 x 16 steel nuts and bolts N·m 3
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 black oxide bolts and mild steel nuts
3/8 x 16 steel nuts and bolts N·m 15
Prevail Torque @ 180°, ISO 10964, Pre-torqued to 5 N·m:
M10 black oxide bolts and mild steel nuts
3/8 x 16 steel nuts and bolts N·m 3.5
Compressive Shear Strength, ISO 10123:
Steel pins and collars N/mm² ≥7.6
Cured for 1 week @ 22 °C
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 zinc phosphate nuts and bolts N·m 26
M10 stainless steel nuts and bolts N·m 17
N·m 5 (lb.in.) (40)
(lb.in.) (8) N·m 13
(lb.in.) (115)
(lb.in.) (26)
N·m 24 (lb.in.) (210)
(lb.in.) (130)
N·m 4 (lb.in.) (35)
(lb.in.) (30)
(psi) (≥1,100)
(lb.in.) (230)
(lb.in.) (150)
LMS
60
40
20
% of Full Strength on Steel
0 1min 5min10min 30min 1h 3h 6h 24h 72h
7088™
7091™
7471™
No Activator
Cure Time
TYPICAL PERFORMANCE OF CURED MATERIAL
Adhesive Properties
Cured for 24 hours @ 22 °C
Breakaway Torque, ISO 10964, Unseated:
M10 black oxide bolts and mild steel nuts
M6 black oxide bolts and steel nuts
M16 black oxide steel bolts and mild steel nuts
3/8 x 16 steel nuts and bolts N·m 12
N·m 26 (lb.in.) (230)
N·m 3 (lb.in.) (26)
N·m 44 (lb.in.) (390)
(lb.in.) (106)
7649™
TYPICAL ENVIRONMENTAL RESISTANCE
Cured for 1 week @ 22 °C
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 zinc phosphate steel nuts and bolts
Hot Strength
Tested at temperature
120
100
80
60
40
20
% Strength @ 22 °C
0
0 50 100 150 200
Temperature, °C
Henkel Americas +860.571.5100
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
TDS LOCTITE® 243™, August-2016
Cold Strength
This product has been tested to -75°C (-100 F). This product may work below this temperature, but has not been tested.
Heat Aging
Aged at temperature indicated and tested @ 22 °C
150
125
100
% Initial Strength @ 22 °C
120 °C
100 °C
150 °C
75
200 °C
50
25
0
0 1000 2000 3000 4000 5000
180 °C
Exposure Time, hours
Heat Aging/Hot Strength
Aged under conditions indicated and tested at temperature
120
100
80
60
180 °C
40
20
% Initial Strength @ 22 °C
0
0 1000 2000 3000 4000 5000
100 °C
120 °C
150 °C
200 °C
Exposure Time, hours
Chemical/Solvent Resistance
Aged under conditions indicated and tested @ 22 °C.
% of initial strength
Environment °C 500 h 1000 h 5000 h
Motor oil 125 110 115 115
Unleaded gasoline 22 100 95 100
Brake fluid 22 105 110 125
Water/glycol 50/50 87 120 125 130
Acetone 22 85 85 80
Ethanol 22 95 90 90
E85 Ethanol fuel 22 95 100 95
B100 Bio-Diesel 22 110 110 125
DEF (AdBlue®)
22 61 59 70
Breakloose Torque, ISO 10964, Pre-torqued to 5 N·m:
M10 Stainless steel nuts and bolts
% of initial strength
Environment °C 500 h 1000 h 5000 h
Sodium Hydroxide, 20% 22 105 105 95
Phosphoric Acid, 10% 22 110 105 110
GENERAL INFORMATION This product is not recommended for use in pure oxygen and/or
oxygen rich systems and should not be selected as a sealant for chlorine or other strong oxidizing materials.
For safe handling information on this product, consult the Safety Data Sheet (SDS).
Where aqueous washing systems are used to clean the surfaces before bonding, it is important to check for compatibility of the washing solution with the adhesive. In some cases these aqueous washes can affect the cure and performance of the adhesive.
This product is not normally recommended for use on plastics (particularly thermoplastic materials where stress cracking of the plastic could result). Users are recommended to confirm compatibility of the product with such substrates.
Directions for use:
For Assembly
1.
For best results, clean all surfaces (external and internal) with a LOCTITE®cleaning solvent and allow to dry
2. If the cure speed is too slow, use appropriate activator. Please see the Cure Speed vs. Activator graph for reference. Allow the activator to dry when needed
3. Shake the product thoroughly before use
4. To prevent the product from clogging in the nozzle, do not allow the tip to touch metal surfaces during application
5. For Thru Holes, apply several drops of the product onto the bolt at the nut engagement area
6. For Blind Holes, apply several drops of the product to the lower third of the internal threads in the blind hole, or the bottom of the blind hole
7. For Sealing Applications, apply a 360° bead of product to the leading threads of the male fitting, leaving the first thread free. Force the material into the threads to thouroughly fill the voids. For bigger threads and voids, adjust product amount accordingly and apply a 360° bead of product on the female threads also
8. Assemble and tighten as required
For Disassembly
1. Remove with standard hand tools
2. In rare instances where hand tools do not work because of excessive engagement length, apply localized heat to nut or bolt to approximately 250 °C. Disassemble while hot
3. Apply localized heat to the assembly to approximately 250 °C. Disassemble while hot
Henkel Americas +860.571.5100
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
TDS LOCTITE® 243™, August-2016
For Cleanup
1.
Cured product can be removed with a combination of soaking in a LOCTITE® solvent and mechanical abrasion such as a wire brush
Loctite Material Specification
LMS dated June-29, 2009. Test reports for each batch are available for the indicated properties. LMS test reports include selected QC test parameters considered appropriate to specifications for customer use. Additionally, comprehensive controls are in place to assure product quality and consistency. Special customer specification requirements may be coordinated through Henkel Quality.
Storage
Store product in the unopened container in a dry location. Storage information may be indicated on the product container labeling.
Optimal Storage: 8 °C to 21 °C. Storage below 8 °C or greater than 28 °C can adversely affect product propertiesMaterial
removed from containers may be contaminated during use. Do not return product to the original container. Henkel Corporation cannot assume responsibility for product which has been contaminated or stored under conditions other than those previously indicated. If additional information is required, please contact your local Technical Service Center or Customer Service Representative.
Conversions
(°C x 1.8) + 32 = °F kV/mm x 25.4 = V/mil mm / 25.4 = inches µm / 25.4 = mil N x 0.225 = lb N/mm x 5.71 = lb/in N/mm² x 145 = psi MPa x 145 = psi N·m x 8.851 = lb·in N·m x 0.738 = lb·ft N·mm x 0.142 = oz·in mPa·s = cP
Manufacturing Date Reference
This Technical Data Sheet is valid for LOCTITE® 243™ manufactured from the dates below:
Made in: First manufacturing date:
EU July 2013 Brazil July 2010 China August 2009 India August 2009 U.S.A. December 2009
The manufacturing date can be determined from the batch code on the pack. For assistance please contact your local Technical Service Center or Customer Service Representative.
LMS
Note:
The information provided in this Technical Data Sheet (TDS) including the recommendations for use and application of the product are based on our knowledge and experience of the product as at the date of this TDS. The product can have a variety of different applications as well as differing application and working conditions in your environment that are beyond our control. Henkel is, therefore, not liable for the suitability of our product for the production processes and conditions in respect of which you use them, as well as the intended applications and results. We strongly recommend that you carry out your own prior trials to confirm such suitability of our product. Any liability in respect of the information in the Technical Data Sheet or any other written or oral recommendation(s) regarding the concerned product is excluded, except if otherwise explicitly agreed and except in relation to death or personal injury caused by our negligence and any liability under any applicable mandatory product liability law.
In case products are delivered by Henkel Belgium NV, Henkel Electronic Materials NV, Henkel Nederland BV, Henkel Technologies France SAS and Henkel France SA please additionally note the following:
In case Henkel would be nevertheless held liable, on whatever legal ground, Henkel’s liability will in no event exceed the amount of the concerned delivery.
In case products are delivered by Henkel Colombiana, S.A.S. the following disclaimer is applicable:
The information provided in this Technical Data Sheet (TDS) including the recommendations for use and application of the product are based on our knowledge and experience of the product as at the date of this TDS. Henkel is, therefore, not liable for the suitability of our product for the production processes and conditions in respect of which you use them, as well as the intended applications and results. We strongly recommend that you carry out your own prior trials to confirm such suitability of our product. Any liability in respect of the information in the Technical Data Sheet or any other written or oral recommendation(s) regarding the concerned product is excluded, except if otherwise explicitly agreed and except in relation to death or personal injury caused by our negligence and any liability under any applicable mandatory product liability law.
In case products are delivered by Henkel Corporation, Resin Technology Group, Inc., or Henkel Canada Corporation, the following disclaimer is applicable:
The data contained herein are furnished for information only and are believed to be reliable. We cannot assume responsibility for the results obtained by others over whose methods we have no control. It is the user's responsibility to determine suitability for the user's purpose of any production methods mentioned herein and to adopt such precautions as may be advisable for the protection of property and of persons against any hazards that may be involved in the handling and use thereof. In light of the foregoing, Henkel Corporation specifically
disclaims all warranties expressed or implied, including warranties of merchantability or fitness for a particular purpose, arising from sale or use of Henkel Corporation’s products. Henkel Corporation specifically disclaims any liability for consequential or incidental damages of any kind, including lost profits. The discussion herein of various processes or
compositions is not to be interpreted as representation that they are free from domination of patents owned by others or as a license under any Henkel Corporation patents that may cover such processes or compositions. We recommend that each prospective user test his proposed application before repetitive use, using this data as a guide. This product may be covered by one or more United States or foreign patents or patent applications.
Trademark usage
Except as otherwise noted, all trademarks in this document are trademarks of Henkel Corporation in the U.S. and elsewhere. ® denotes a trademark registered in the U.S. Patent and Trademark Office.
Reference 0.4
Henkel Americas +860.571.5100
For the most direct access to local sales and technical support visit: www.henkel.com/industrial
Henkel Europe
+49.89.320800.1800
Henkel Asia Pacific
+86.21.2891.8859
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