The Leica EM TXP is a unique target preparation device especially
developed for cutting and polishing samples prior to examina tion by SEM, TEM and LM techniques. It excels with challenging
speci mens where pinpointing and preparing barely visible targets
becomes easy. Before the Leica EM TXP, sawing, milling grinding
and polishing exactly to the target was often a very time-consuming and difficult procedure as points of interest were easily
missed and specimens often difficult to handle due to their small
size. With the Leica EM TXP such samples can easily be prepared.
Leica Design by W. Hölbl
90° rotation view
Processing observation
Front face observation
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System
Integrated Viewing System
Stereo microscopic target observation
during the working process
With the specimen pivot arm the sample can be observed during
preparation at an angle between 0° and 60°, directly onto the front
face, or 90° to the front face for distance determination with an
eyepiece graticule. The Leica EM TXP features brilliant ring LED
top light and optimized backlight illumination for excellent viewing.
■ Accurate location and preparation of microtargets
Front side decapsuled integrated circuit
■ Observation with a stereo microscope
■ Multifunctional machine processing
■ Automatic process control
■ to produce a mirror-like surface quality
SM LED gold wire bond
PCB cross section with soldered pin
PCB cross section
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Process Possibilities
Once the sample is clamped into the specimen holder and inserted in the pivot arm, the specimen can be:
– milled
– sawed
– ground
– and polished
without removing the sample from the Leica EM TXP and simply
changing the tools while observing the process directly through
the steromicroscope. The tool and sample are enclosed within a
protective chamber with a transparent cover for safety. This prevents access to moving parts and avoids particulate matter
escaping. During milling a low-noise extraction and filtration unit
with a Hepa filter (optional) provides a safe, dust-free environment.
Diamond and tungsten carbide millers
Diamond disc cutter
Lapping inserts 15, 9, 6, 3, 1, 0.5 μm
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Integrated Automatic Process Control
Let the Leica EM TXP do the job
The Leica EM TXP automatic process control mechanism saves
you from time-consuming routine sample preparation:
– with the automatic E-W guiding mechanism
– with the force-regulated feed control
– with the countdown function
and level sensor for the integrated lubricant cooling system
– Pivot arm lever
– Hand wheel for manual feed in steps of
0.5, 1, 10 and 100 μm
– Control panel for manual operation and setting
of all parameters for automatic preparation
Peristaltic
cooling system
Peristaltic cooling system
E-W guiding mechanism
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Application Examples
Target preparation on surfaced sample for incident light LM and SEM
All processing steps are carried out consecutively on the Leica EM TXP without removing the sample for pinpointing the area of
interest via another microscope or for making any adjustments. Preparing specimens observed during operation with the inte-
grated stereo microscope avoids the time consuming interruption of locating the target with a stand alone microscope and then
re-aligning the sample in the polishing instrument.
➔
Sawing
Observation via stereo microscope of the Leica EM TXP
Sample Thinning for transmitted light LM or prior to ion thinning for TEM
Specimen thinning with the Leica EM TXP offers the advantage of observing the complete process during treatment and distance
monitoring at each process step without the need to remove the sample for checking in another instrument.
➔
1st side preparation as described
above.
Mill a supporting stub with
the disc cutter so it is parallel to
the prepared face in step 1.
Set the advance counter to zero.
Fix the prepared 1st side with
wax onto the prepared stub without removing it from the holder.
Or directly in the Leica EM TXP
with glue.
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➔
Grinding/polishing
The saw is set to the desired
value (e.g. 100 μm) and the second
side preparation begins (here
sawing).
The second side is then polished.
The thickness of the sample can
be observed on the advance
counter display.
The area of interest via the stereo microscope of the Leica EM TXP
➔
Front face observation with the
Leica EM TXP. Here the sample
thickness is 25 μm.
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IC: Silicon soldered on copper paddle
Result: Target-prepared integrated circuit. Gold wire bonding on Si (LM image)
Incident lightIncident and transmitted lightTransmitted light
Result: Target prepared integrated circuit. Gold wire bonding on Si .... 25 μm section (LM image)
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View the Details
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Leica Microsystems –
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