LaMotte TDS 5 User Manual

TC-3000e • Code 1964-EPA
TC-3000i • Code 1964-ISO
Version 1.5 • Code 1964-MN • 11-27-07
WARNING! This set contains chemicals
WARNING! This set contains chemicals
that may be harmful if misused. Read
that may be harmful if misused. Read
cautions on individual containers
cautions on individual containers
carefully. Not to be used by children
carefully. Not to be used by children
except under adult supervision.
except under adult supervision.
Introduction
Turbidity
WhatisTurbidity?.............................5
HowisTurbidityMeasured?........................5
TakingTurbidityWaterSamples.......................7
Chlorine
WhatisChlorine?.............................7
HowisChlorineMeasured?........................7
TakingChlorineWaterSamples ......................8
Color
WhatisColor?..............................8
HowisColorMeasured? .........................8
SampleDilutionTechniques...........................9
Options and Set Up
FactoryDefaultSettings ............................10
ResettoFactoryDefaultSettings.........................10
Turbidity
SelectingTurbidityUnits..........................10
SelectingaTurbidityCalibrationCurve...................11
Chlorine
SelectingChlorineUnits .........................13
SelectingaChlorineReagentSystem ...................14
Averaging.................................15-16
SettingDate&Time............................16-17
SelectingaLanguage.............................18
SettingAutoShutdown.............................19
Data Logging .............................20-21
Tube Positioning Ring...........................22
Analysis and Calibration
Turbidity
Analysis...............................23-25
DilutionProcedures ...........................26
PreparationofTurbidity-FreeWater...................26-27
TurbidityStandards............................28
CalibrationProcedure.........................28-32
TestingTips .............................32-33
Chlorine
Analysis.................................33
TabletDPDReagents.........................33-38
LiquidDPDReagents.........................39-44
CONTENTS 3
Dilutionprocedures ...........................45
StandardSolutions..........................45-48
CalibrationProcedure-Tablets ....................48-51
CalibrationProcedure-Liquid.....................48-51
TestingTips...............................52
Color
Analysis...............................52-54
DilutionProcedures ...........................54
StandardSolutions............................54
CalibrationProcedure.........................55-58
TestingTips...............................58
Troubleshooting Guide..........................59
General Operating Information
Overview.................................60-61
TheKeypad..................................62
TheDisplay&Menus............................63-65
Tube ....................................65
PC Link ..................................66
Output....................................66
ComputerConnection.............................66
Battery Operation
ReplacingtheBattery..............................66
Maintenance
Cleaning...................................66
MeterDisposal................................67
Repairs....................................67
General Information
PackagingandDelivery ............................68
GeneralPrecautions..............................68
SafetyPrecautions...............................68
Limits of Liability ................................68
Specifications...............................69-70
StatisticalandTechnicalDefinitionsRelatedtoProductSpecifications........71
ContentsandAccessories ...........................72
EPACompliance ...............................73
ISOCompliance ...............................73
CECompliance................................73
Warranty...................................73
4 CONTENTS
INTRODUCTION
TURBIDITY
What is Turbidity?
Turbidity is an aggregate property of the solution, water in most cases. Turbidity is not specific to the types of particles in the water. They could be suspended or colloidal matter and they can be inorganic, organic or biological. At high concentrations turbidity is perceived as cloudiness or haze or an absence of clarity in the water. Turbidity is an optical property that results when light passing through a liquid sample is scattered. The scattering of light results in a change in the direction of the light passing through the liquid. This is most often caused when the light strikes particles in solution and is scattered backward, sideways and forward. If the turbidity is low much of the light will continue in the original direction. Light scattered by the particles allows the particle to be ”seen” or detected in solution. Just as sunlight passing through a window is scattered by dust particles in the air, allowing them to be seen.
In the past 10 years, turbidity has become more than just a measure of water clarity. Because of the emergence of pathogens such as Cryptosporidium and Giardia, turbidity now holds the key to assuring proper water filtration. In 1998, the EPA published the IESWTR (interim enhanced surface water treatment rule) mandating turbidities in combined filter effluent to read at or below 0.3 NTU. By doing so, the EPA hoped to achieve a 2 log (99%) removal of Cryptosporidium. There is presently consideration to lower this to 0.1 NTU. The trend has been to check the calibration of on-line turbidimeters with hand-held field units. The optical design and low detection limit of the TC-3000 allow very accurate readings for such calibrations.
The meter also allows the user to choose the units of measure for expressing turbidity. While nephelometric turbidity unit (NTU) has been the standard for years, FNU (formazin nephelometric unit) and FAU (formazin attenuation unit) are now being used in ISO 7027 units. American Society of Brewing Chemists (ASBC) units and European Brewery Convention (EBC) units allow the brewing industry to check process waters.
How is Turbidity Measured?
Scattered Turbidity 90°
and Color Detector
Chlorine Detector
Turbidity Light
Direct Turbidity Detector
Source
IR LED 860nm: 3000i Tungsten Lamp: 3000e and stabilization detector
Chlorine LED 525nm
and stabilization detector
Color UV LED 375nm
and stabilization detector
INTRODUCTION 5
Turbidity is measured by detecting and quantifying the scattering of light in water (solution). Turbidity can be measured in many ways. There are visual methods and instrumental methods. Visual methods are more suitable for samples with high turbidity. Instrumental methods can be used on samples with both high and low levels of turbidity.
Two visual methods are the Secchi Disk method and the Jackson Candle method. The Secchi Disk method is often used in natural waters. A black and white Secchi Disk is lowered into the water until it can no longer be seen. It is then raised until it can be seen again. The average of these two distances is known as the “Secchi Depth”. The Jackson Candle method uses a long glass tube over a standard candle. Water is added or removed from the tube until the candle flame becomes indistinct. The depth of the water measured with a calibrated scale is reported as Jackson Turbidity Units (JTU). The lowest turbidity that can be determined with this method is about 25 NTU.
There are two common methods for instruments to measure turbidity. Instruments can measure the attenuation of a light beam passing through a sample and they can measure the scattered light from a light beam passing through a sample. In the attenuation method, the intensity of a light beam passing through turbid sample is compared with the intensity passing through a turbidity-free sample at 180° from the light source. This method is good for highly turbid samples. The most common instrument for measuring scatter light in a water sample is a nephelometer. A nephelometer measures light scattered at 90° to the light beam. Light scattered at other angles may also be measured, but the 90° angle defines a nephelometric measurement. The light source for nephelometric measurements can be one of two types to meet EPA or ISO specifications. The EPA specifies a tungsten lamp with a color temperature of 2,200–3,000 K. The units of measurement for the EPA method are nephelometric turbidity units (NTU). The ISO specifies a light emitting diode (LED) with a wavelength of 860 nm and a spectral bandwidth less than or equal to 60 nm. The units of measurement for the ISO method are formazin nephelometric units (FNU). The TC-3000e meets the EPA specification and the TC-3000i meets the ISO specification. The nephelometric method is most useful for low turbidity.
The TC-3000 is a nephelometer that is capable of measuring turbidity by both the attenuation method and the nephelometric method. It uses a detector placed at 180° to the light source for the attenuation method. It uses a detector placed at 90° to the light source for the Nephelometric method. The TC-3000 also has a third detector that monitors the intensity of the light source. It uses this detector to improve instrumental stability and minimize calibration drift. The TC-3000 also has a signal averaging option to improve the stability of readings on low turbidity samples.
The TC-3000 has two different turbidity calibrations, formazin and Japan Standard. The formazin calibration is the EPA and ISO approved method of calibrating nephelometers. This calibration can be used with user prepared formazin standards or commercially purchased formazin standards. LaMotte Company approved AMCO
TM
standards labeled for use with the TC-3000 can also be used with the formazin calibration. Stablcal
â
standards below 50 NTU should not be used to calibrate the
TC-3000. The Japan Standard calibration is a calibration for a Japanese Water Works standard.
It is based on Japanese formulated polystyrene turbidity standards. This calibration should only be use to meet Japanese Water Works requirements. The Japanese polystyrene standards can only be purchased in Japan. Formazin, AMCO and Stablcal
6 TURBIDITY
â
standards cannot be used with this calibration.
T AKING TURBIDITY WATER SAMPLES
Clean plastic or glass containers may be used for turbidity samples. Ideally, samples should be tested soon after collection and at the same temperature as when collected.
CHLORINE
What is Chlorine?
Chlorine is added to water systems to sanitize the water. There are various forms of chlorine that are added to water. These can be gas, liquid (commonly called bleach or sodium hypochlorite), calcium hypochlorite mixtures, stabilized chlorine products and as chlorine generated using salt. When these forms of chlorine are added, they react with water to form free chlorine, hypochlorous acid. If free chlorine reacts with ammonia, it will form various types of combined chlorine (chloramines). Depending on the chlorine to ammonia ratio, these can be mono, di or tri chloramines.
Because free chlorine can react with precursors in the water to form carcinogenic trihalomethanes (THMs), many water systems have switched to chloramines. In these systems, free chlorine and ammonia are added together and controlled to form monochloramine. Although not as active a sanitizer as free chlorine, chloramine is less likely to form THMs. Since it is a slower sanitizer, the concentration of chloramine in water is higher than the concentration of free chlorine in water distribution systems.
The present EPA limit of chlorine in water systems is 4.0 ppm. The amount of chlorine used to process waste may be higher than this.
Many states also establish limits on the amount of chlorine that can be discharged into a body of water after waste processing. These usually are less than 0.1 ppm. The low detection limit of the TC-3000 makes it ideal for such measurements. Because of its wide range, the TC-3000 can be used to measure the water used in the wastewater process, in a distribution system and for many low level discharge requirements.
How is Chlorine Measured?
The most common methods for measuring chlorine are colorimetric methods. In colorimetric methods, chlorine reacts with reagents added to a water sample. The reaction of the chlorine with the reagents produces a color. The intensity of the color produced is proportional to the concentration of chlorine in the sample. The intensity of the color can be measured by visual comparison with a calibrated color chart or othere types of visual color comparators. Visual methods suffer due to the subjective observations of the person judging the colors.
The TC-3000 uses EPA approved DPD reagents to react with chlorine. In the absence of iodide, free available chlorine reacts instantly with DPD to produce a pink color. Subsequent addition of potassium iodide (DPD 3) causes a reaction with combined form of chlorine. The TC-3000 electronically measures the color produced in these reactions in comparison to a colorless water sample. First it measures the intensity of a light beam passing through a clear colorless sample, the blank. Then it measures the intensity of light passing through the pink reacted sample. The TC-3000 uses the ratio of these two measurements to calculate the concentration of chlorine and displays the result. The TC-3000 uses the EPA approved wavelength of 525 nm, to make these measurements.
CHLORINE 7
Taking Chlorine Water Samples
Chlorine solutions are not stable and should be analyzed immediately. Samples may be collected in glass. Amber or opaque bottles are recommended since exposure to sunlight or agitation will decrease chlorine concentrations. It is best to fill bottles completely to assure there is no air in the container. If sampling from a tap, allow the water to run for a minute to assure a proper sample.
COLOR
What is Color?
Many different dissolved or suspended materials contribute to the color of water. These can include industrial wastes, plant materials, metals and plankton. There are two terms used to define color. If one examines a water sample straight from a water source, the color of the water is its apparent color. To ascertain the color of the water without the contribution of suspended substances and is called true color. True color can increase after precipitation, and decrease in drier weather.
Some bodies of water can change color quickly, depending on the runoff conditions and plant life around them. Wind can also stir up substances more in shallower bodies of water causing quick color change. Major contributors are tannins, hemic acids, and inorganic minerals. Color can be critical, since as the color increases, the amount of light that penetrates the water decreases, and thus submerged plant life, that depend on this light for photosynthesis, will decrease.
How is Color Measured?
Since most natural waters have color that is similar to a solution of chloroplatinate and cobalt, the APHA specifies the use of dilute chloroplatinate/cobalt color standards to define color values. In the APHA method, the color of a water sample is compared visually to 6 to 9 chloroplatinate/cobalt standards. However, visual methods suffer due to the subjective observations of the person judging the colors. To eliminate this source of error, color can be measured electonically with a spectrophotometer, or colorimeter liekt the TC-3000.
The TC-3000 is calibrated with APHA color standards at 375 nm. This wavelength was found to give the greatest sensitivity with chloroplatinate/cobalt color standards, thus most natural waters. The meter electronically measures color in comparison to a colorles water sample. First it measures the intensity if a light beam passing through a clear colorless sample, the blank. Then it measures the intensity of light passing through the colored sample. The TC-3000 uses the ration of these two measurements to calculate the color and displays the result. The results are expressed in APHA color units (cu). The TC-3000 can use signal averaging to improve accuracy when measuring very low levels of color. Not valid, unless a correlation chart has been constructed.
There is no standard wavelength for measuring color and it is common for meters to use different wavelengths. Since chloroplatinate/cobalt standards will have different absorbance values at various wavelengths, comparing results from the TC-3000 to meters using wavelengths other than 375 nm is not valid.
Meters using different wavelengths will only give the same reading when measuring chloroplatinate/cobalt standards since they are both calibrated to those standards. When measuring natural water, meters using different wavelengths should not be
8 COLOR
expected to give the same result because the absorbance spectrum of natural water is usually not identical to the absorbance spectrum of chloroplatinate/cobalt standards. The reading that the meter displays is a correlation between the color of the sample water and the color standards at a fixed wavelength. The correlation, and reading, will change as the wavelength changes The TC-3000 takes advantage of this fact by selecting a wavelength that gives much greater sensitivity when measuring the color of most natural waters, than single wavelength meters that use much higher wavelengths.
Taking Color Water Samples
Samples should ideally be collected in glass containers. Perform the analysis soon after sampling since the color may change with time. For true color determinations, remove turbidity by filtration or centrifugation.
SAMPLE DILUTION TECHNIQUES
If a test result is out of the range of the meter, it must be diluted. The test should then be repeated on the diluted sample. The following table gives quick reference guidelines for dilutions of various proportions.
Amount of Sample Deionized Water to Bring
Multiplication Factor
Final Volume to 10 mL 10 mL 0 mL 1 5mL 5mL 2
2.5 mL 7.5 mL 4 1mL 9mL 10
0.5 mL 9.5 mL 20
All dilutions are based on a final volume of 10 mL so several dilutions will require small volumes of the water sample. Graduated pipets should be used for all dilutions. If volumetric glassware is not available, dilutions can be made with the colorimeter tube. Fill the tube to the 10 mL line with the sample and then transfer it to another container. Add 10 mL volumes of deionized water to the container and mix. Transfer 10 mL of the diluted sample to the colorimeter tube and follow the test procedure. Repeat the dilution and testing procedures until the result falls within the range of the calibration. Multiply the test result by the dilution factor. For example, if 10 mL of the sample water is diluted with three 10 mL volumes of deionized water, the dilution factor is four. The test result of the diluted sample should be multiplied by four.
SAMPLE DILUTION TECHNIQUES 9
OPTIONS & SET UP
FACTORY DEFAULT SETTINGS
Settings that have user options have been set at the factory to default settings.
The factory default settings are:
Turbidity Units NTU Turbidity Calibration formazin Chlorine Units ppm Chlorine Calibration Tablet Averaging Disabled Date Format MM/DD/YY Language English Auto Shutdown Disabled
RESET TO FA CTORY DEFAULT SETTINGS
To return the meter to the factory settings, turn the meter off. Hold down *IOK button. Press ON. Release both buttons. Press *IOK button to select the default settings. Meter will turn off and the factory settings will be restored. Restoring the factory settings will remove the user-level calibration but not the zeroing. To change the default settings follow the instructions in the following sections.
TURBIDITY
The default units are NTU and the default calibration curve is formazin. To change the settings:
Selecting Turbidity Units
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK
to select Options.
10 OPTIONS & SETUP • TURBIDITY
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
3. Scroll down and then press *IOK
to select Turbidity .
Options
Averaging
* Turbidity
Chlorine Date/Time
16:02:19 01/04/05
4. Press the *IOK to select Units. Turbidity
*Units
Calibration
16:02:19 01/04/05
5. Scroll down and then press *IOK
to select units. Available units are: NTU
(Nephelometric Turbidity Units); FNU (Formazin Nephelometric Units); ASBC (American Society of Brewing Chemists); EBC (European
Units *NTU
FNU ASBC EBC
16:02:19 01/04/05
Brewery Convention)
Note:
If Attenuation is chosen as a calibration curve. The result will be reported in
FAU (Formazin Attenuation Units).
6. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
Selecting A Turbidity Calibration Curve
1. Press ON to turn the meter on.
1.3
OPTIONS & SETUP • TURBIDITY 11
2. Scroll down and then press *IOK to
select Options.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
3. Scroll down and then press *IOK
to select Turbidity .
4. Scroll down and then press *IOK
to select Calibration.
5. Scroll down and then press *IOK
to select a Calibration curve. Select a calibration option based on the composition of the standards that will be used to calibrate the meter. Available options are: Formazin, Pol ystyrene, Attenuation.
For the most accurate results, the Attenuation option should be chosen when samples are over 500 NTU. The range for the attenuation option is 40–4000 NTU.
Options
Averaging
* Turbidity
Chlorine Date/Time
16:02:19 01/04/05
Turbidity
Units
* Calibration
16:02:19 01/04/05
Turbidity
Units
* Calibration
16:02:19 01/04/05
Calibration * Formazin
Japan Standard Attenuation
16:02:19 01/04/05
Note: StablCalâstandards below 50 NTU should not be used to calibrate the TC-3000. The diluent has a different refractive index than traditional formazin standards and will affect the results. The Japan Standard calibration mode should be used only with Japanese Polystyrene Standards (0–100 NTU).
12 OPTIONS & SETUP • TURBIDITY
6. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
CHLORINE
The default units are ppm and the default calibration curve is for DPD Tablet reagents. To change the settings:
Selecting Chlorine Units
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK to select Options.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
3. Scroll down and then press *IOK to select Chlorine.
Options
Averaging Turbidity
* Chlorine
Date/Time
16:02:19 01/04/05
4. Press the *IOK to select Units. Chlorine
*Units
Calibration
16:02:19 01/04/05
OPTIONS & SETUP • CHLORINE 13
5. Scroll up and then press *IOK to
select a unit for the chlorine results. Available options are: mg/L
Units *mg/L
ppm
(milligrams per liter) or ppm (parts per million)
16:02:19 01/04/05
6. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
Selecting A Chlorine Calibration/Reagent System
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK to select Options.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
3. Scroll down and then press *IOK to select Chlorine.
Options
Averaging Turbidity
* Chlorine
Date/Time
16:02:19 01/04/05
4. Scroll down and then press *IOK to select Calibration.
Chlorine
Units
* Calibration
16:02:19 01/04/05
14 OPTIONS & SETUP • CHLORINE
5. Scroll down and then press *IOK to select a chlorine reagent system.
The options are: Tabl et or Liquid.
Calibration *Tablet
Liquid
16:02:19 01/04/05
6. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
AVERAGING
The averaging option is available for color and turbidity testing. It allows the user to average multiple readings. This option will improve the accuracy of samples with readings that may tend to drift with time. When the two, five or ten reading options have been selected, the meter will show a running average of the readings that have been taken until the final average is displayed. The default setting is disabled. To change the setting:
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK to select Options.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
3. Press *IOK to select Averaging. Options
* Averaging
Turbidity Chlorine Date/Time
16:02:19 01/04/05
OPTIONS & SETUP • AVERAGING 15
4. Scroll down and then press *IOK to select an averaging option.
Available options are:
Disabled, 2 Measurements, 5 Measurements, 10 Measurements.
Note: The current setting.
5. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
Note: When the Averaging option is selected, it will take longer to get the final result and more power will be used.
is displayed next to the
*
SETTING THE DATE AND TIME
1. Press ON to turn the meter on.
Averaging Disabled * 2 Measurements
5 Measurements 10 Measurements
16:02:19 01/04/05
1.3
2. Scroll down and then press *IOK to select Options.
3. Scroll down and then press *IOK to select Date/Time.
16 OPTIONS & SETUP • SETTING THE DA TE & TIME
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
Options
Turbidity Chlorine
* Date/Time
Language
16:02:19 01/04/05
4. Press *IOK to select Set Date or scroll down and then press *IOK to select Set Time or Date Format.
Date/Time *Set Date
Set Time Date Format
16:02:19 01/04/05
5. When setting the time or the date, use the or to change the highlighted number on the display. Press *IOK to accept the value and move to the next value.
When choosing a date format, use the or to select a date format. Press *IOK to accept the format.
Set Date
01/04/05
q , * , p
16:02:19 01/04/05
Set Date
01/04/05
16:02:19 01/04/05
Set Date
01
01/04/05
16:02:19 01/04/05
Date/Time *Set Date
Set Time Date Format
04
q , * , p
q , * , p
05
16:02:19 01/04/05
6. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
OPTIONS & SETUP • SETTING THE DA TE & TIME 17
SELECTING A LANGUAGE
The default setting is English. To change the setting:
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK
to select Options.
3. Scroll down and then press *IOK
to select Language.
4. Scroll down and then press *IOK
to select a language. Available languages are: English,
French, Spanish, Japanese (Kana), Portuguese, Italian.
5. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
Options
Chlorine Date/Time
* Language
Auto Shutdown
16:02:19 01/04/05
Language * English
Frances Español Japanese
16:02:19 01/04/05
18 OPTIONS & SETUP • SELECTING A LANGUAGE
SETTING AUTO SHUTDOWN
The power saving Auto Shutdown feature will turn the meter off when a button has not been pressed for a set amount of time. The default setting is disabled. To change the setting:
1. Press ON to turn the meter on.
1.3
2. Scroll down and then press *IOK
to select Options.
3. Scroll down and then press *IOK
to select Auto Shutdown.
4. Scroll up and then press *IOK to
select a shutdown time. Available options are: 5minutes,
10 minutes, 30 minutes, Disabled.
5. Press to exit to a previous menu or make another menu selection or press OFF to turn the meter off.
Main Menu
Measure Data Logging
* Options
16:02:19 01/04/05
Options
Chlorine Date/Time
Language * Auto Shutdown 16:02:19 01/04/05
Auto Shutdown * 5 Minutes
10 Minutes
30 Minutes
Disabled 16:02:19 01/04/05
OPTIONS & SETUP • SETTING AUTO SHUTDOWN 19
DAT A LOGGING
The default setting for the data logger is start (on). The meter will log the last 4004 data points.
1. Press ON to turn the meter on.
1.3
2. Scroll down and press *IOK to
select Data Logging.
3. Press *IOK to view the last data
point that was logged.
4. Press or to scroll through the saved data points.
Main Menu
Measure
* Data Logging
Options
16:02:19 01/04/05
Data Logging *View
Stop Erase
16:02:19 01/04/05
304 / 304
25.6 cu
Color 12:48:35 09/11/04 16:02:19 01/04/05
304 / 304
1.58 NTU
Turbidity (F) 16:26:58 09/11/04 16:02:19 01/04/05
Note:
If the data logger is empty because it has never been used or has just been
erased, the view function will not work.
20 DATA LOGGING
Or scroll down and press *IOK to select Stop or Start to stop or start the data logging feature.
Data Logging
View
*Stop
Erase
16:02:19 01/04/05
Data Logging
View
*Start
Erase
16:02:19 01/04/05
Or scroll down and press *IOK to select Erase to empty all logged data points from the memory.
5. Press OFF to turn the meter off or press to exit to a previous menu or make another menu selection.
Data Logging
View Stop
* Erase
16:02:19 01/04/05
DATA LOGGING 21
TUBE POSITIONING RING
N
The Tube Positioning Ring
To put a ring on a tube, remove the cap from the tube. The tube positioning ring has two tapered notches and one
squared-off notch. Place the ring on the tube with the squared-off notch closest to the top of the tube and tapered notches closer to the bottom of the tube. Align the single, squared-off notch with the vertical, white indexing line that is printed on the tube. Place the tube flat on a hard surface and firmly press the ring onto the tube with equal pressure distributed along the top of the ring.
To remove a ring, invert the uncapped tube on a soft surface, such as a paper towel. Press down on the ring with equal pressure distributed around the ring.
SQUARED-OFF
NOTCH
INDEXING
E
LI
ANAL YSIS & CALIBRATION
TURBIDITY
The default units are NTU and the default calibration curve is formazin. When (F)is displayed in the upper right corner of the display, this indicates that the meter is in the formazin mode. For the most accurate results, a user calibration should be performed. The Attenuation calibration option should be used when samples are over 500 NTU. The Japan Standard calibration mode should be used only with Japan Standards (0–100 NTU). To change the settings see the Set Up instructions (see page 10).
22 TUBE POSITIONING RING • ANAL YSIS & CALIBRATION • TURBIDITY
Analysis
1. Press ON to turn the meter on.
2. Press *IOK to select Measure. Main Menu
* Measure
Data Logging Options
16:02:19 01/04/05
3. Press *IOK to select Turbidity. Measure
* Turbidity
Color Chlorine
16:02:19 01/04/05
4. Rinse a clean tube (0290) three times with the blank.
For the most accurate results, use thesametubefortheblankandthe sample.
1.3
5. Fill the tube to the fill line with the blank. Pour the blank down the inside of the tube to avoid creating bubbles.
ANALYSIS & CALIBRATION • TURBIDITY 23
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