LaMotte S-XL-1128 User Manual

QUAT TEST KIT
L
Mott
MODEL QAC2-DC • CODE 7057
QUANTITY CONTENTS CODE
15 mL *Phenolphthalein Indicator, 0.5% *2258-E 15 mL *Sulfuric Acid, 0.5 N *6090-E 60 mL Quat Titrating Solution 3996-H 30 mL Toluidine Blue O Indicator 3995-G 60 mL EDTA Solution 7117-H 1 Test Tube, 5-10-15-20-25 mL, plastic, w/cap 0715 1 Quat/Polyquat Endpoint Color Chart 3613-CC
*WARNING: Reagents marked with an * are considered to be potential health hazards. To view or print a Material Safety Data Sheet (MSDS) for these reagents go to www.lamotte.com. To obtain a printed copy, contact LaMotte by e-mail, phone or fax.
To order individual reagents or test kit components, use the specified code number.
PRO CE DURE
1. Rinse test tube (0715) with sample water. Fill with desired sample size selected from the table.
Sample Size Equivalence (ppm Per Drop)
25 mL 1 drop = 2 ppm 10 mL 1 drop = 5 ppm 5 mL 1 drop = 10 ppm
2. Add 5 drops EDTA Solution (7117). Swirl to mix. NOTE: If the hardness of the sample is greater than 500 ppm, add 5
more drops of EDTA Solution.
3. NOTE: If pH of the sample is below 8.3, proceed to Step 4. Add 2 drops of *Phenolphthalein Indicator, 0.5% (2258). Swirl to
mix. If colorless, proceed to Step 4. If pink, add *Sulfuric Acid, 0.5N (6090) dropwise, until the pink color disappears.
4. Add Toluidine Blue O Indicator (3995) as follows:
Stop
25 mL sample, add 8 drops; 10 mL sample, add 3 drops; 5 mL sample, add 2 drops.
Swirl to mix. Sample should turn light blue.
5. While swirling test tube, add Quat Titrating Solution (3996) one drop at a time, until color changes from blue to purple. Hold bottle vertically. For best results, when the color change is first detected, use the Endpoint Color Chart (3613-CC) as shown to match the color of the solution exactly to the endpoint. Continue adding Quat Titrating solution one drop at a time, until color matches endpoint. Count the number of drops added.
6. Calculate result in ppm.
25 mL sample: subtract three (3) from number of drops used in Step 5. Multiply by 2.
10 mL sample: subtract one (1) from number of drops used in Step 5. Multiply by 5.
5 mL sample: subtract one (1) from number of drops used in step
5. Multiply by 10. Record as ppm Quat. NOTE: The quat equivalence is based on n-alkyldimethylbenzyl
ammonium chloride, molecular weight 360. If a quat of different molecular weight is tested, multiply the equivalence by:
equivalence
molecular weight
´
360
LaMOTTE COM PANY
Helping Peo ple Solve An a lyt i cal Challenges
PO Box 329 • Chestertown • Mary land • 21620 • USA
800-344-3100 • 410-778-3100 (Out side USA) • Fax 410-778-6394
Visit us on the web at www.lamotte.com
SM
03/10
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