Labconco XPert 38876 User Manual

Labconco Corporation 8811 Prospect Avenue Kansas City, MO 64132-2696 800-821-5525, 816-333-8811 FAX 816-363-0130 E-MAIL labconco@labconco.com HOME PAGE www.labconco.com
User’s Manual
XPert® Nano Enclosures
Models
38872 Series 38885 Series 38873 Series 38886 Series 38874 Series 38875 Series 38876 Series
Please read the User’s Manual before operating the equipment.
Warranty
Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas of defective material and workmanship, provided such defect results from normal and proper use of the equipment. Glassware is not warranted from breakage when dropped or mishandled.
The warranty for XPert® Nano Enclosures will expire one year from date of installation or two years from date of shipment from Labconco, whichever is sooner. Warranty is non-transferable and only applies to the owner (organization) of record.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product. If the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation. Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages of any kind. This statement may be altered by a specific published amendment. No individual has authorization to alter the provisions of this warranty policy or its amendments. Lamps and filters are not covered by this warranty. Damage due to corrosion or accidental breakage is not covered.
Copyright © 2008, 2009, 2012, 2014, 2015 Labconco Corporation. All rights reserved.
The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier. Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525 or 1-816-333-8811, between the hours of 7:00 a.m. and 6:00 p.m., Central Standard Time.
Part #3881800, Rev. E
ECO J457
ORIGINAL INSTRUCTIONS
TABLE OF CONTENTS
CHAPTER 1: INTRODUCTION 1 Typographical Conventions 1
CHAPTER 2: PREREQUISITES 3
Support, Vibration & Movement Requirements 3 Temperature Variation Requirements 4 Humidity and Static Electricity Requirements 4 Location and Air Current Requirements 5 Exhaust and Blower Requirements 6 Electrical Requirements 7 Space Requirements 7
CHAPTER 3: GETTING STARTED 8
Unpacking the Enclosure 9 Stand and Cabinet Installation 10 Connecting to the Exhaust System (Optional) 11 Connecting the Electrical Supply Source 14 Set the Face Velocity with the Speed Control Adjustment 14
CHAPTER 4: HIGH PERFORMANCE FEATURES AND
SAFETY PRECAUTIONS 16
High Performance Features 16 Safety Precautions 20
CHAPTER 5: USING THE NANO ENCLOSURE 23
Routine Daily Work Procedures 23 ULPA Filter Applications, Suitability & Guidelines 24 Optional Ionizer 25 Prohibited Acid Use 26
CHAPTER 6: MAINTAINING THE NANO ENCLOSURE 27
Routine Maintenance Schedule 27 Decontamination 28 Determination of When to Replace ULPA Filters 28 How to Install New ULPA Filter with the Bag-In/Bag-Out 29 Filter Leak Test 30 Setting Inflow Face Velocity with the Speed Control Adjustment 32 Calibrate and Operate the Airflow Monitors 32
Guardian Digital 1000 Airflow Monitor 35 Programming the Guardian 1000 Digital Alarm 35 Initial Certification 39 Re-Certification 39 Fluorescent Light Replacement 39 Motorized Impeller Replacement 40 Speed Control Replacement 41 Maintenance on the Optional Ionizer 42 Trace Odor Carbon Filter Installation 43
CHAPTER 7: ACCESSORIZING THE NANO ENCLOSURE 44
Guardian Airflow Monitors 44 Canopy Exhaust Connection 45 Remote Blowers 45 Exhaust Dampers 47 Accessory Filters 47
CHAPTER 8: TROUBLESHOOTING 48
APPENDIX A: REPLACEMENT PARTS 51
APPENDIX B: DIMENSIONS 55
APPENDIX C: SPECIFICATIONS 61
APPENDIX D: QUICK CHART 62
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Chapter 1:
Introduction
Congratulations on your purchase of a Labconco XPert® Nano Enclosure. Your enclosure provides personnel protection through superior containment while conserving energy at OSHA approved velocities as low as 60 feet per minute. It is the result of Labconco’s more than 50 years of experience in manufacturing fume hoods and more than 30 years of experience in manufacturing filtered enclosures.
These enclosures will effectively contain toxic or noxious particulates when properly installed and operated. Each Nano Enclosure uses an ULPA filter, which is rated at least 99.999% efficient for 0.12-micron particles. The XPert Nano Enclosures offer many unique features to enhance safety, performance, and energy savings. To take full advantage of them, please acquaint yourself with this manual and keep it handy for future reference. The XPert Nano Enclosures include a true bag-in/bag-out ULPA filter to properly protect personnel during filter changing operations.
If the unit is not operated as specified in this manual it may impair the protection provided by the unit.
Si l'unité n'est pas utilisée comme spécifié dans ce manuel il peut diminuer la protection fournie par l'unité.
Typographical Conventions
Recognizing the following typographical conventions will help you understand and use this manual:
Steps required to perform a task are presented in a numbered format. Comments located in the margins provide suggestions, reminders, and
references.
Critical information is presented in boldface type in paragraphs that are
preceded by the exclamation icon. Failure to comply with the information following an exclamation icon may result in injury to the user or permanent damage to the enclosure.
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Chapter 1: Introduction
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Critical information is presented in boldface type in paragraphs that are
preceded by the wrench icon. Only a trained certifier or contractor should only perform these operations. Failure to comply with the information following a wrench icon may result in injury to the user or permanent damage to your Clean Bench.
Important information is presented in capitalized type in paragraphs that are
preceded by the pointer icon. It is imperative that the information contained in these paragraphs be thoroughly read and understood by the user.
CAUTION – See Manual. When this symbol is on the unit it indicates a
caution that is detailed in this manual.
ATTENTION - Voir manuel. Lorsque ce symbole est sur l'unité, il indique une
mise en garde qui est indiqué dans ce manuel.
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Chapter 2:
Prerequisites
Before you install the filtered enclosure, you must be certain that the area is level and of solid construction. In addition, a dedicated source of electrical power should be located near the installation site to power the filtered enclosure. Additionally, the enclosure should be strategically placed in the lab to provide efficient workflow.
Carefully read this chapter to learn the requirements for your installation site:
The support, vibration and movement requirements. The temperature variation requirements. The humidity and static electricity requirements. The location and air current requirements. The exhaust and blower requirements. The electrical power requirements. The space requirements.
Refer to Appendix B: Dimensions for complete enclosure dimensions. Refer to Appendix C: Specifications for complete filtered enclosure electrical and
environmental conditions, specifications and requirements.
Support, Vibration and Movement Requirements
At a minimum, the supporting structure usually consists of a base cabinet or stand. For weighing applications the ability for analytical balances to accommodate
vibration varies with type and brand. More advanced balances have improved tolerance, however in the preparation of a balance enclosure site, please consider the following:
Avoid tubular stands or mobile benches that have the potential of moving
when touched.
A bench that is rigidly mounted to the floor or fixed to the wall, but not both,
may be appropriate.
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The corners of a building typically have less vibration than the center. The bench with the balance enclosure should not contain any vibration-
producing equipment, such as shakers or pumps.
Marble slabs with dampening pads placed within the enclosure are also an
effective low cost means of controlling vibration.
The balance should be calibrated and verified at least annually; for best
results, the balance should be calibrated inside the enclosure while running at the desired face velocity.
Temperature Variation Requirements
The extent the balance readings are influenced by temperature variations is a function of the balance design. Most manufacturers would suggest that a temperature drift of 1-2°C is generally tolerable. Only validation through your Operational Qualification protocol can define what is acceptable. To minimize the potential for temperature variations:
Never install balances near heating sources such as radiators and hot plates. Do not place the balance and enclosure on a bench that would receive direct
sunlight.
Humidity and Static Electricity Requirements
Electrostatics can be troublesome in a balance enclosure. It is important to understand and, to the extent possible, control static charges. An electrostatic charged vessel, sample or enclosure can apply forces and lead to errors in weighing. The repulsion or attraction can be detected with micro, semi micro and analytical balances. Static charges can also lead to particulates being attracted to surfaces within the balance enclosure. Containment of harmful powders, prevention of cross-contamination and clean-up is enhanced when static attraction of powders is minimized. The construction of the XPert Nano Enclosure avoids the use of plastics, which are highly insulative.
To correct or ensure against electrostatic issues, the following additional measures may be prescribed to improve weighing operations.
Maintain a humidity level between 45 and 60%. The ability to sustain this
humidity range can be challenging depending upon the regional climate and HVAC system.
The XPert Nano Enclosure is offered with a factory installed ionizer which
will neutralize surface charges.
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Chapter 2: Prerequisites
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Material
Surface Resistivity
Example
Conductive
0 105 per square
Skin, Metals
Static dissipative
105 109 per square
Glass
Antistatic
109 1012 per square
Polyethylene bag
Insulative
1012 per square
Acrylic, Packing foam, Styrofoam
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Background on Electrostatics or Static Electricity
Electrostatic charges on a surface such as the wall of a balance enclosure are not created by moving air. Impurities within the air impinging upon surfaces dictate the polarity and magnitude of the charge. The process, triboelectrification, occurs when the dust particles contact the surface, creating friction and electrons move across the interface.
The ability of a material to become polarized is a property known as permittivity. On highly insulative materials like acrylic, ions or charged molecules are strongly bound to the surface by polarization forces. The higher the force, the higher is the permittivity value of the material. It is suggested by balance manufacturers that the use of high permittivity materials, such as plastic be avoided.
Since static electricity is a surface phenomenon, materials can also be classified by their surface resistivity measured in ohms per square. The table below lists the surface resistivity of various classes of material.
Surface Resistivity Table
Location and Air Current Requirements
The XPert line of Filtered Enclosures have been designed to contain hazards by negating typical cross drafts and turbulence within the opening. Air movement does not affect most modern balances with draft shields. However, as a precautionary safety measure and a higher level of control, it is recommended that the enclosure be placed in an area to avoid:
High traffic areas where walking might cause an air disturbance or be a
nuisance to balance readings.
Overhead or wall HVAC diffusers, fans, radiators or other lab equipment
producing air currents.
Next to doorways or windows that may be opened.
Do not position the unit so that it is difficult to operate the main disconnect device.
Ne placez pas l'appareil de sorte qu'il est difficile de faire fonctionner le dispositif principal de déconnexion.
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Enclosure
Width and
Sash
Opening
Face Velocity
(fpm)
Exhaust
Volume
(CFM)
XPert Station
Initial Static
Pressure Loss
with HEPA
filter (in w.g.)
XPert
System
Noise
Pressure db
(A)
Xpert System
Max.
Equivalent
Resistance (Ft)
Xpert System
Max. External
Static Pressure
2'
9.4" Sash
60 80
100
85 115 145
.35"- .41" .48" - .57" .62" - .72"
48-53
50-56
53-58
400 200
80
.20" .18" .13"
3'
9.4" Sash
60 80
100
130 175 220
.37" - .43" .53" - .62" .68" - .79"
48-53
53-57
58-61
130
50 25
.15" .11" .08"
4'
9.4" Sash
60 80
100
175 235 295
.40" - .46" .57" - .66"
.76" - .87".
49-54
58-61
62-66
100
50 25
.20" .18" .13"
5'
12" Sash
60 80
100
290 385 480
.38" - .46" .55" - .67" .72" - .85"
52-56
58-63
63-67
450 230 120
.22" .20" .15"
6'
12" Sash
60 80
100
350 465 580
.46" - .56" .67" - .81"
.87" – 1.03"
55-57
61-63
67-69
300 150
70
.20" .18" .13"
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Exhaust and Blower Requirements
The XPert Nano Enclosure uses an integral motorized impeller to draw room air past the operator and through the enclosure. This contaminated air is then pushed through the ULPA filter. The ULPA-filtered exhaust air is then forced out the top of the enclosure.
The ULPA-filtered exhaust air can be recirculated into the laboratory or exhausted outside with the addition of the Canopy Exhaust Connection and remote blower listed in Chapter 7. Electrical connections are covered in Chapter 2 for this configuration. Consult your local regulations or guidelines for ventilation of the filtered exhaust in nanoparticle applications.
If external exhaust is required, data for the exhaust volume, noise pressure and enclosure static pressure loss is listed for each filtered enclosure model at face velocities of 60, 80, and 100 fpm. Weighing and handling nano materials is best done with lower flow rates (60-70 fpm or 0.31-0.36 m/s).
Proper blower selection can be determined from these exhaust requirements and the total system static pressure loss. For outside exhaust, the enclosure must be connected to either a dedicated blower or a house exhaust system. Labconco offers accessory remote blowers listed in Chapter 7. Contact Labconco for blower sizing assistance.
If the enclosure is connected directly to a house exhaust system, an adjustable damper (or valve) must be installed to control the airflow properly. This is equally important when a house exhaust system is controlling multiple filtered enclosures. See Chapter 7 for accessory adjustable damper ordering information.
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Chapter 2: Prerequisites
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Electrical Requirements
Standard duplex electrical receptacles should be nearby for connecting the filtered enclosure, or other equipment, such as a balance for weighing operations. The enclosures include iris pass-thru to allow electrical cords through the back of the enclosure without leaving a large hole for contaminants to escape.
Space Requirements
The dimensions for the different models are shown in Appendix B: Dimensions.
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Chapter 3:
Getting Started
Now that the site for your XPert Nano Enclosure is properly prepared, you are ready to unpack, inspect, install, and validate your system. Read this chapter to learn how to:
Unpack and move the enclosure. Set up the enclosure with the proper supporting structure and work surface. Connect to an exhaust system if applicable. Connect the electrical supply. Set the face velocity with the speed control adjustment. Arrange validation for the enclosure.
Depending upon which model you are installing, you may need common mechanical and electrical installation tools in addition to wrenches, ratchets, sockets, a nut driver set, a large flat-blade screwdriver, a power drill or screwdriver, and a carpenter level to complete the instructions in the chapter.
Each enclosure model weighs between 173 to 443 lbs. each (78.47 to 200.94 kg). The shipping container allows for lifting with a mechanical lift truck or floor jack. If you must lift the
enclosure manually, follow safe-lifting guidelines. Do not lift
by the front air foil.
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Chapter 3: Getting Started
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The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Unpacking the Enclosure
Carefully remove the shrink-wrap or carton on the enclosure and inspect it for damage that may have occurred in transit. If damaged, notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier.
DO NOT RETURN GOODS WITHOUT THE PRIOR AUTHORIZATION OF LABCONCO. UNAUTHORIZED RETURNS WILL NOT BE ACCEPTED.
IF ENCLOSURE WAS DAMAGED IN TRANSIT, YOU MUST FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER. LABCONCO CORPORATION AND ITS DEALERS ARE NOT RESPONSIBLE FOR SHIPPING DAMAGES.
Do not discard the packing material until you have checked all of the components and tested the enclosure. We recommend that you do not remove the enclosure from its shipping container until it is ready to be placed into its final location. Move the unit by placing a flat, low dolly under the shipping skid, or by using a floor jack.
Do not move the enclosure by tilting it onto a hand truck.
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Chapter 3: Getting Started
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To change the height of the base stand, remove these four nuts, washers and bolts
Install four bolts and flat washers into base of cabinet
Stand and Cabinet Installation
1. The top surface of a base stand can be adjusted
from 27.5 to 34.50 inches (698mm to 876mm), in 1 inch (25mm) increments. Choose your optimum working height from the floor to the work surface.
2. Slide (4) leg extensions into base stand corner
posts and attach with larger diameter 5/16"-18 x 2-1/4 inch (57mm) long bolt, flatwasher, lockwasher and acorn nut. Ensure that the same height hole is selected for each leg. Tighten the leg bolts securely.
3. Move the base stand into its final location. For
stands with leveling feet, use a carpenter level to adjust in both planes as shown in figure below.
4. XPert Nano Enclosures have an integral
stainless steel work surface with mounting holes on the underside. Hardware is provided with the stand. Set the enclosure and work surface onto the stand with the front edge of the work surface flush (even) with the front edge of the stand. Loosely attach each of the four mounting locations of the work surface with the smaller diameter 1/4"-20 x 2.5 inch (63mm) long hex head bolts, nuts and washers. Tighten when all four bolts have been started.
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Chapter 3: Getting Started
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Connecting to the Exhaust System (Optional)
ATTENTION: The weight of the exhaust ductwork system must be supported independently of the enclosure superstructure or damage may occur.
The exhaust system should be installed by a qualified HVAC contractor.
The exhaust connection on the 2', 3' and 4' XPert Nano Enclosure have been designed to accept 6" diameter ductwork as shown in Figure 3-2. The 5' and 6' models have been designed for 10" diameter ductwork as shown in Figure 3-3. For the 2', 3' and 4' sizes, the exhaust connection ships uninstalled on the top and needs to be fastened with the screws provided. See Chapter 7 for ordering Canopy Exhaust Connection. Canopy Exhaust Connection aids in the removal of chemicals or applications where a higher degree of powder and particulate removal is required. Review Chapter 2 for exhaust prerequisites and review Chapter 7 for ordering blower exhaust equipment.
Consult Labconco Customer Service should you require help sizing your blower for the exhaust volume and system static pressure loss.
To ensure compatibility, the selected exhaust duct material should match the enclosure, procedures and chemical applications.
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Chapter 3: Getting Started
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Figure 3-2
FOR 6" NOMINAL EXHAUST DUCT CONNECTION 6.06" ID ON THE 2', 3' AND 4'
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Figure 3-3
10" NOMINAL ON THE 5' AND 6'
10.06" ID
Chapter 3: Getting Started
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Chapter 3: Getting Started
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Connecting the Electrical Supply Source to the Nano Enclosure
Simply connect the 115V power cord supplied to the IEC electrical supply plug on the back of the enclosure. If using at 50 Hz operations, blower performance maximum airflow will be reduced by 17%.
The same procedure applies for the 230V except it is shipped without a plug. Install the appropriate plug for your electrical specifications per local codes. All models use less than 5 amps.
All wiring for the XPert Nano Enclosure should be performed by a licensed electrician and conform to local codes.
Do not use any detachable power cord that is not adequately rated
for the unit.
Ne pas utliser un fil électrique amovible qui n’est pas du tension
nominale de l’appareil.
Set the Face Velocity with the Speed Control Adjustment
Adjustment of the speed control gives the correct face velocity and is located behind the front panel. The face velocity should be adjusted from 60 to 100 fpm. (Consult your Safety Officer for airflow recommendations for your application). Containment is maximized at a setting within this range. Working at the lowest face velocity permissible for the application will give the least turbulent, quietest operation. Face velocity measurements are made using an anemometer. An electric anemometer can be obtained from your laboratory supply dealer.
To determine the actual face velocity at the sash opening, airflow velocity readings are taken. This should be done across the sash opening of the enclosure in accordance with the Industrial Ventilation Manual. (See Appendix E) The
“average face velocity” is achieved by taking readings in two rows across the
enclosure with the readings 6" from the ends and evenly spaced every 12"; the first row is 3" down from the upper sash foil and the second row is 3" up from the work surface. Refer to Chapter 2 for proper airflow volumes for your particular model.
The XPert enclosures have been tested at Labconco’s airflow test facility per
ASHRAE 110-1995. All enclosures achieve an “as manufactured rating” of less than
0.05 part per million (ppm) at 4 liters per minute (lpm); AM <0.05 (Consult
Labconco for individual ratings). For “field use” ASHRAE testing contact Labconco
for a certified on-site contractor. For particulate powder validation, Labconco performed containment testing to validate the enclosures for sodium naproxen powders. The XPert enclosures demonstrated excellent containment when used by an operator using excellent technique and good containment when used by an operator using marginal technique. While no enclosure can compensate for improper technique, these tests confirm that the XPert Nano Enclosures provide a safe working environment.
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Chapter 3: Getting Started
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NOTE: Face velocity profiles and smoke testing should be performed
frequently per your organization’s quality system to ensure safe
performance.
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1
Chapter 4:
High Performance Features and
Safety Precautions
High Performance Features
The patented1 XPert Nano Enclosure is designed to meet the needs of the laboratory scientist, and provide superior containment while conserving energy at OSHA approved “low flow” velocities as low as 60 feet per minute. The filtered enclosures have been tested to effectively contain toxic and noxious materials when properly installed and operated. What makes the Labconco line of enclosures so unique is the revolutionary way they direct air into and through the contaminated air chamber. Labconco engineered them to minimize the effects of turbulence. The containment-enhancing and aerodynamic designs of the upper sash foil, side air foils, lower air foil, upper dilution air supply, and rear perforated baffle all work in concert to produce horizontal airflow patterns that significantly reduce powder, chemical and particulate concentrations through the work area.
These concentrations of materials are predominantly removed on the first pass of airflow through the chamber resulting in high performance containment. The plenum and the ULPA filter are jacketed by negative pressure. Should a leak occur in the filter gasket or the plenum, the contaminated air is recaptured and refiltered.
The XPert Nano Enclosure includes a true bag-in/bag-out ULPA filter disposal system to protect the worker from contact with hazardous powders and particulates. Users are encouraged to routinely check airflow with the use of the airflow monitor.
U.S. Patent No. 6,461,233 and U.S. Patent No. D538,941
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