RapidStill II
MODEL 65200
INSTRUCTION MANUAL
Product designs are subject to change without notice
© 2002 Labconco Corporation
65441 REV. B / ECO A631
Printed in U.S.A.
TABLE OF CONTENTS
Preface
Introduction
Components Shipped 1
General Description 2
Performance 3
Component Identification 4
Installation 4
Location 10
Electrical Connection 10
Water Connection 10
Drain Connection 11
NaOH Pump Connection 11
Optional Water Inlet Kit 12
Rear View of Standard RapidStill II 13
Rear View of RapidStill II w/Optional Water Inlet Kit Installed 14
Safety Precautions 15
Normal Operation
Standard Operating Procedure 16
Routine Maintenance 17
Expendables 18
Cleaning 19
Servicing the RapidStill II
Fuse Replacement 20
Removing the Boiler 20
Heating Element Replacement 21
Condenser Extension Replacement 21
Timer Replacement 22
NaOH System Service 22
Replacement Parts 24
Dimensions 26
TABLE OF CONTENTS
Specifications 27
Wiring Diagram 28
Troubleshooting 29
References 31
Warranty 32
Shipping Claims 33
Accessories 34
Contacting Labconco 35
INTRODUCTION
Components Shipped
Carefully check the contents of the carton for damage that might have occurred in transit. Do not
discard the carton or packaging material until all components have been checked against the
following component list and the equipment has been installed and tested.
As shipped, the carton should contain the following:
Part Number Description
65200 RapidStill II
65441 Instruction Manual
Installation Kit (Contains hoses and fittings)
1
INTRODUCTION
General Description
The Labconco RapidStill II is designed specifically for the determination of macro concentrations
of nitrogen. The RapidStill II performs rapid steam distillation from sulfuric acid digest prepared
from nitrogen-bearing materials such as food products, feeds, grains, soils, plant tissue, wastewater
effluent, organic wastes, etc. Sample digestions are accomplished using Labconco’s Rapid
Digestor systems, described in the Accessories section of this manual.
Figure 1
2
INTRODUCTION
Performance
The RapidStill II produces steam by heating a 1 liter flask (boiler) with a 1200 watt heating
element. Activation of the heater, the addition of water to the boiler, and the addition of NaOH to
the sample are all controlled by switches on the front control panel of the unit. An electric timer
on the control panel allows the distillation time to be set from 0 to 15 minutes. Typical distillation
times range from 5 to 10 minutes.
3
INTRODUCTION
Component Identification (Figure 2)
(1) Boiler Water Switch. This momentary contact switch fills the boiler with water. It is
interlocked to prevent its operation during the heating of the boiler. Water should
never be added to the boiler when it is hot and low on water (less than ¼ full) or dry.
Allow the boiler to cool before adding water.
(2) Boiler Heater Switch. The boiler heater switch activates the boiler heating element.
The Boiler Heater should never be turned on when the boiler is dry or low on water.
(3) NaOH Addition Switch. This momentary contact switch activates the NaOH pump to
pump caustic from a user-supplied vessel into the digestion tube. The switch is
interlocked to operate only when the boiler heater is on. At the end of every day, the
NaOH pump lines must be rinsed with purified water.
(4) Digestion Tube Clamping Device. The clamping device quickly and securely locates
the digestion tube against the connection stopper.
(5) Safety Door. The safety door surrounds the digestion tube and is designed to protect
the operator. The door should always be in the closed position during operation of the
RapidStill II.
(6) NaOH Delivery Tube. This tube is used to dispense the user-supplied caustic directly
into the digestion tube.
(7) Connection Stopper. The Viton* stopper located on the bottom of the distribution
head seals the digestion tube to the head. The connection stopper should be inspected
and cleaned after every operating session of the unit.
(8) Distribution Head. This distribution head acts as a junction for the steam and NaOH
delivery tubes. The central part of the distribution head acts as a trap by preventing the
NaOH from entering the receiving flask.
(9) Steam Inlet Tube. The steam inlet tube is PTFE (Teflon*) and dispenses steam
directly into the digestion tube.
*Viton is a registered trademark of E.I. Du Pont de Nemours & Co.
*Teflon is a registered trademark of E.I. Du Pont de Nemours & Co.
4
Component Identification
INTRODUCTION
Figure 2
5
INTRODUCTION
Component Identification (Figure 3)
(10) Condenser Extension. The condenser extension is a replaceable glassware fitting that
connects the condenser and distribution head.
(11) Condenser. The RapidStill II is equipped with a combined Allihn and spiral condenser
for efficient recovery of the distillate.
(12) Ventilation Valve. The ventilation valve prevents the distillate from being aspirated
back into the condenser after the distillation is completed. If the valve sticks closed,
remove it and wash out any material accumulated inside the valve.
(13) Safety Screen. The plastic safety screen is designed to protect the operator. The screen
should always be in the closed position during operation of the RapidStill II.
(14) Boiler Viewing Slot. Looking through this slot the operator can easily inspect the water
level in the boiler. Low and high water level marks are on the boiler flask to ease the
inspection and addition operations.
(15) Distillate Outlet Tube. This tube carries distillate from the condenser to the solution in
the receiving flask. The bulb of the tube must be totally immersed in the receiving
solution.
(16) Distillation Timer Switch. The infinitely adjustable 0-15 minute timer controls the
dispensing of steam into the digestion tube. It is interlocked to function only when the
boiler heater is on. As an additional safety measure, NaOH cannot be dispensed into
the digestion tube when the timer is in operation.
(17) Spillage Tray. The spillage tray is designed to collect spilled reagents and overflow.
The tray is removable and may be cleaned with ordinary soap and water.
6
Component Identification
INTRODUCTION
Figure 3
7
INTRODUCTION
Component Identification (Figure 4)
(18) Heater Cup Assembly. The heater cup assembly consists of the heater cup to support
the boiler, and the heating element itself.
(19) Boiler. The 1 liter boiler contains the boiling water that is the source of steam for the
distillation.
(20) Water Fill Valve. The valve dispenses water into the boiler when it is energized. The
inlet of the valve is equipped with a filter screen, to prevent fouling with particulate
matter.
(21) Plastic Check Valves. These valves function as vacuum breaks, preventing negative
pressurization of the system after it is shut off.
(22) Steam Control Valve. The steam control valve directs steam from the boiler to the
drain pipe during standby, or the steam delivery tube during distillation. The valve is
controlled by the timer switch.
(23) Drain Pipe. The drain pipe acts as a condenser for the steam not used in the distillation
and as a drain for the condenser cooling water. DO NOT restrict the discharge from the
drain pipe or its hose. The RapidStill II may be damaged by high water pressure.
(24) Flow Restrictor. The flow restrictor prevents the cooling water flow rate from
exceeding 1.0 gallon per minute. This minimizes water usage and prevents damage to
the unit.
(25) NaOH Pump. The peristaltic pump dispenses a user-supplied caustic solution from its
container directly into the digestion tube. The pump inlet and outlet are equipped with
quick connects to reduce the possibility of spillage during maintenance. The pump
must be rinsed with purified water at the end of every work day to prevent damage to
the pump or its fittings.
(26) Water Inlet Fitting. The water inlet fitting is a push-on style fitting designed to
connect tot the feed water line supplied in the installation kit.
(27) Electrical Connector. The electrical connector mates with the power cord supplied in
the installation kit.
(28) Fuse. The 15 amp fuse protects the RapidStill II from an electrical overload. Replace
this fuse with the appropriate replacement part. NEVER attempt to install a fuse with a
higher amperage rating.
8
Component Identification
INTRODUCTION
Figure 4
9
INSTALLATION
Location
The RapidStill II should be located on a level work surface, adjacent to appropriate electrical,
water and drain connections.
Electrical Connection
The electrical outlet should be rated for 115 VAC, 60 Hz, 15 Amps, and dedicated to the
RapidStill II.
Water Connection
The feed water should be municipal drinking water grade and of sufficient quality to prevent or
minimize scaling of the boiler. The feed water should have a minimum supply volume of 1 gallon
(3.8 liters) per minute, at 10 PSI.
Using the supplied braided water line, connect the tube to the water inlet fitting on the rear of the
RapidStill II as shown in Figure 4. To connect or disconnect the fittings, follow the instructions in
Figure 5, below. If your feed water promotes excessive scaling of the boiler, or has high NH3
levels, you may wish to install the Optional Water Inlet Kit, part #65442, described on page 12.
Figure 5
10
INSTALLATION
Drain Connection
Using the supplied molded drain hose, connect and clamp the hose to the drain outlet located at the
bottom of the drain pipe. The drain hose should be routed to an appropriate drain system, rated for
a minimum capacity of 2 gallons (7.6 liters) per minute. The RapidStill II’s drain pipe is designed
for gravity drainage. The drain hose and all connections must be below the level of the drain pipe
outlet. The drain hose connection to the drain system must meet all applicable local standards for
drain connections. DO NOT restrict the drain hose or its connections. Restrictions of the
drain line may produce a pressure buildup in the RapidStill II, resulting in damage to the
unit and water leakage.
NaOH Pump Connections
Using either the silicone tubing supplied in the installation kit, or another acceptable type of
tubing, connect the NaOH pump inlet quick connector to the tubing. Connect the connector to the
pump inlet by pressing it straight in until the connector ‘clicks’ and locks in place. The connector
can be removed by depressing the metal button on the body of the connector and pulling the
connector straight out. Place the other end of the tubing into the user-supplied caustic container.
Provisions should be made for the easy removal of the tube from the caustic container, and its
placement into a container of purified water for rinsing of the system at the end of each work
session.
11
INSTALLATION
Optional Water Inlet Kit
With the purchase and installation of the Optional Water Inlet Kit, part #65442, two separate water
supplies may be used to feed the RapidStill II; ordinary tap water may be used to supply the
condenser while purified water is fed to the boiler.
To function properly, the purified water source must be capable of delivering 1 gallon (3.8 liters)
per minute at a minimum of 5 PSI. The purified water supply pressure should not exceed 20 PSI.
The kit is installed as follows:
(1) Unplug the RapidStill II and disconnect the feed water and drain lines, so the unit can
be turned around.
(2) Turn the unit around and locate the water inlet fitting as shown in Figure 6.
(3) Locate the optional water inlet hole just above the water inlet fitting, as shown in
Figure 6.
(4) Install the supplied bulkhead union in a manner similar to the water inlet fitting below
it. DO NOT overtighten the nut on the bulkhead union; it may damage the fitting.
(5) Remove the flow restrictor assembly from the T-shaped fitting. Discard the short
length of rigid plastic tubing that runs from the outlet of the flow restrictor to the Tshaped fitting.
(6) Disconnect the condenser inlet fitting from the T-shaped fitting, as shown in Figure 6.
(7) Plug the flow restrictor outlet into the condenser inlet fitting, as shown in Figure 7.
(8) Install the braided tube assembly supplied with the kit from the bulkhead union
installed in Step #4 to the T-shaped fitting.
(9) Install the supplied plug into the open port of the T-shaped fitting.
(10) When completed, the installation should appear as shown in Figure 7. The upper
bulkhead fitting (that was just installed) supplies the boiler with water and may be
connected to a purified water source. The lower bulkhead fitting (the original fitting)
will now supply only the condenser with cooling water and should remain connected to
an appropriate supply of feed water (tap water).
12
Rear View of Standard RapidStill II
INSTALLATION
Figure 6
13
INSTALLATION
Rear View of RapidStill II with Optional Water Inlet Kit Installed
Figure 7
14
SAFETY PRECAUTIONS
The disposal of substances used in connection with this equipment may be governed by various
federal, state or local regulations. All users of this equipment are urged to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon
water, land or air and to comply with such regulations.
The RapidStill II should not be operated in damp conditions or those suspect of an explosion and
should be situated to allow adequate room and ventilation during its normal usage.
The RapidStill II employs the following: electrical devices, heating element, hot water, steam,
pressurized water and steam lines. Care should be taken when installing, operating, or servicing
the unit.
Ensure that the RapidStill II is connected to electrical service in accordance to local and national
electrical codes. Failure to do so may create a fire or electrical hazard.
The RapidStill II is designed to be connected to a cold, potable water supply purified by municipal
water treatment facilities. The installation of the optional water inlet kit allows for the use of
purified water to supply the boiler. Never connect the RapidStill II to non-potable, unprocessed
surface or well water systems. The use of inadequate water supplies may damage the unit.
Always wear appropriate eye protection, protective gloves and clothing when using the RapidStill
II.
Never operate the RapidStill II without the Safety Screen and Safety Door in their proper position.
Never turn on the boiler heater when the boiler flask is dry or low on water. Do not let the boiler
run dry. Do not attempt to refill the boiler when it is dry or low on water and hot. Failure to
ensure proper water level in the boiler, or attempting to fill it when hot may result in the breakage
of the boiler flask and/or damage to the heating element.
At then end of the day, rinse the caustic delivery system with purified water. Remove any
accumulated spillage or deposits from the surfaces of the unit to prevent corrosion or damage.
15
NORMAL OPERATION
Standard Procedure
(1) Turn on the cooling water, allowing it to flow through the condenser. The flow rate
will be regulated to 1 gallon per minute (3.8 liters per minute).
(2) Depress the ‘Boiler Water’ switch. Looking through the Boiler viewing slot, fill the
boiler approximately 2/3 full, or to the top line of the flask. If the boiler fills too
slowly, slightly increase the flow rate of the cooling water supply. If the Optional
Water Inlet Kit is installed and the boiler fills too slowly, increase the pressure or flow
rate of the purified water supply. When the proper water level is obtained, release the
switch.
(3) Turn the ‘Boiler Heater’ switch to the ‘ON’ position. After approximately 10 minutes,
or when the water in the boiler is at a steady boil, the unit is ready for operation.
(4) Place the digestion tube with a digested sample in the RapidStill II, giving the tube a
slight twist to assure a complete seal.
(5) Place a receiver flask under the Distillate Outlet Tube. Make sure that the outlet tube is
fully submerged.
(6) Add NaOH solution to the digestions tube by depressing the ‘NaOH Addition’ switch.
For each 5 ml of concentrated sulfuric acid used in the digestion process, add
approximately 15 ml of 50% NaOH solution to make the distillation solution strongly
alkaline. Use the graduated decal on the front panel of the RapidStill II as an
approximate gauge of the volume in the digestion tube.
(7) Turn the distillation Time switch to the desired time setting. Be sure to allow enough
time for the distillation solution to reach boiling.
(8) When the distillation is completed, the unit will return to a standby position, with the
boiler heater still in operation.
(9) Remove the digestion tube, using appropriate heat and chemically resistant gloves.
(10) If there are to be additional distillations and the boiler water level is low, turn the
‘Boiler Heater’ switch off and depress the ‘Boiler Water’ switch on. Allow the boiler
to refill with water, release the ‘Boiler Water’ switch and turn the ‘Boiler Heater’
switch on. When the water in the boiler resumes boiling, the RapidStill II is ready for
another distillation.
(11) Titrate the distillate in the receiving flask. If the temperature of the solution exceeds
120°F (50°C), check the flow rate of the condenser cooling water.
16
ROUTINE MAINTENANCE
Under normal operation, your RapidStill II will require little routine maintenance. The following
maintenance schedule is recommended:
After Every Day
(1) Rinse the caustic pump, its delivery system and the distribution head as follows:
(a) Install a clean empty digestion tube in place. Remove the caustic supply tubing
from the caustic vessel and place it in a vessel of purified water.
(b) Turn on the cooling water and fill the boiler as described on page 16.
(c) Turn on the boiler heater.
(d) Depress ‘NaOH Addition’ switch and hold it on until all of the caustic has been
purged out of the system and into the distillation tube.
(e) Remove the digestion tube and dispose of the liquid appropriately.
(f) Replace the digestion tube and fill it approximately half full by depressing the
‘NaOH Addition’ switch.
(g) When the water in the boiler is at a rolling boil, turn the distillation timer to
approximately 10 minutes.
(h) At the end of the distillation cycle, turn the boiler heater and the cooling water off.
Remove the digestion tube wearing appropriate heat and chemically resistant
gloves. Dispose of the liquid appropriately.
(2) Clean the exterior surfaces of the RapidStill II using a soft cloth and a solution of mild
soap and water to remove any spilled chemicals or deposits.
Weekly
(1) Examine the boiler for any build up of deposits. Accumulate deposits in the boiler may
be removed by dilute solution of hydrochloric acid, or by using commercially available
descaling solutions that are compatible with glass.
USE APPROPRIATE PROTECTIVE SAFETY EQUIPMENT WHEN HANDLING
CLEANING SOLUTIONS. ALWAYS FOLLOW THE CLEANING SOLUTION
INSTRUCTIONS REGARDING THEIR USE, SAFETY PRECAUTIONS TO BE
FOLLOWED, AND DISPOSAL.
For instructions on how to remove the boiler, refer to ‘Removing the Boiler’ in the
Service section of this manual on page 20.
(2) Examine all plumbing and steam lines, ensuring that the tubing is intact. Examine all
tubing connections. Examine the connection stopper for deterioration or cracking.
17
EXPENDABLES
The following is a brief list of replacement parts:
PART NO. DESCRIPTION
13444 Fuse, 15 Amp
65230 Boiler Flask
65394 Heating Element
65436 Condenser Extension
13594 Plastic Check Valve
13022 Switch, Rocker DPDT
13033 Switch, Rocker Momentary Contact
16240 Tubing, Silicone, 1/2 x 5/16 inch (ordered by the foot)
16241 Tubing, Silicone, 9/32 x 5/32 inch (ordered by the foot)
65448 Peristaltic Pump Tube
65206 Cap # GL 18 with gasket
65212 Cap # GL 32 with gasket
18
CLEANING
Every day the caustic pump, delivery system and distribution head should be cleaned as described
in the ‘ROUTINE MAINTENANCE’ section of this manual.
Accumulated deposits or scale in the boiler may be removed by removing the boiler and washing it
with a dilute solution of hydrochloric acid or a commercially available scale remover that is
compatible with glass.
USE APPROPRIATE PROTECTIVE SAFETY EQUIPMENT WHEN
HANDLING CLEANING SOLUTIONS. ALWAYS FOLLOW THE
CLEANING SOLUTION INSTRUCTIONS REGARDING THEIR USE,
SAFETY PRECAUTIONS TO BE FOLLOWED AND DISPOSAL.
For instruction on how to remove the boiler, refer to the ‘Removing the Boiler’ in the ‘SERVICE’
section of this manual.
The exterior of the unit should also be cleaned after each work session using a soft cloth and a
solution of mild soap and water to prevent the accumulation of deposits.
19
SERVICING THE RAPIDSTILL II
Fuse Replacement
(1) Unplug the unit from electrical service.
(2) Using a small screwdriver or coin, turn the slotted fuse holder ¼ turn counterclockwise.
(3) Pull the fuse and holder straight out. Remove the fuse from its holder by pulling the
fuse straight out.
Replace the fuse with a proper replacement part only. DO NOT attempt to replace the
fuse with one of a higher amperage rating.
(4) To reinstall the fuse, reverse the above steps.
Removing the Boiler
(1) Unplug the RapidStill II from electrical service.
(2) Turn the unit around to gain access to the boiler flask.
(3) Remove the head of the boiler by pulling it straight up. If the head is stuck onto the
boiler, apply water to the joint to loosen it.
(4) Pull the ring that secures the boiler straight up until it clears the neck of the boiler flask.
The boiler can now be removed.
(5) To reinstall the boiler, reverse the above steps.
20
SERVICING THE RAPIDSTILL II
Heating Element Replacement
(1) Unplug the RapidStill II.
(2) Remove the boiler as described on page 20.
(3) Remove the perforated screen surrounding the heating element by removing the three
screws that secure it.
(4) Disconnect the two heating element wires from the wiring harness by pulling the
electrical connectors straight apart. Remove the ground wire from the bottom of the
heater cup by pulling the wire straight down.
(5) Remove the four nuts and lockwashers that secure the heating element cup and its
platform to the frame of the RapidStill II.
(6) Pull the heating element cup and its platform straight away from the frame.
(7) Remove the heating element cup from its platform by removing the three screws on the
underside of the cup.
(8) Remove the heating element from the cup by removing the two heating element
bulkhead nuts located on the bottom of the cup. Pull the element and its wires straight
out of the cup.
(9) Install the new element by reversing the above steps.
Condenser Extension Replacement
(1) Rotate the safety screen assembly up until it is fully open.
(2) Loosen the knurled nut that secures the condenser extension to the distribution head.
Remove the plastic clamp that connects the extension to the condenser.
(3) While supporting the condenser, use a Phillips screwdriver to remove the screws that
secure the condenser bracket straps to the condenser bracket.
(4) Rotating the condenser out of the way, pull the extension straight out of the distribution
head.
(5) Remove the knurled nut and its sealing ring from the old extension tube, and install it
on the new tube, noting the correct orientation of the nut and washer.
(6) Install the new extension tube, orienting the drip point of the tube to the bottom.
Reverse steps 1-4 to complete the installation.
21
SERVICING THE RAPIDSTILL II
Timer Replacement
(1) Unplug the RapidStill II from electrical service.
(2) Remove the four screws that secure the front panel on the base of the unit and pull the
panel straight out.
(3) Using an allen wrench, loosen the two set screws that secure the timer knob on its shaft.
Pull the knob straight off.
(4) Disconnect the electrical connections on the timer, noting the terminals’ orientation.
(5) Using the proper wrench, loosen the hex nut that secures the timer to the front panel
and pull the timer out of the panel.
(6) Install the new timer by reversing the above steps.
NaOH System Service
The tubing in the NaOH delivery system should not require replacement if properly rinsed after
each work session. To replace the peristaltic pump tube, proceed as follows:
(1) If possible, purge the NaOH delivery system and peristaltic pump with purified water,
as described in the Routine Maintenance section on page 17.
(2) Unplug the RapidStill II from electrical service.
(3) Turn the unit around to gain access to the peristaltic pump.
(4) Remove the four small Phillips screws as shown in Figure 8.
(5) Remove the pump cover, exposing the pump tube.
(6) Pull the pump tube straight out of the pump housing.
(7) Thoroughly rinse the tube and remove the pump fittings and clamps. Retain the fittings
and clamps for use on the new tube.
(8) Install the new tube by reversing the above steps.
22
SERVICING THE RAPIDSTILL II
Figure 8
23
REPLACEMENT PARTS
ITEM QTY. PART NO. DESCRIPTION
1 1 65394 Heating Element
2 1 65230 Boiling Flask
3 1 65416 Boiler Head
4 1 65435 Balance Tee
5 2 13594 Plastic Check Valve
6 1 13635 Steam Control Valve
7 1 44115 Water Fill Valve
8 1 16240 Tubing, Silicone, 1/2 x 5/16 inch
9 1 16241 Tubing, Silicone, 9/32 x 5/32 inch
10 1 65388 Flow Restrictor Assembly
11 1 65448 Peristaltic Pump Tube
12 1 13444 Fuse, 15 Amp
Figure 9
24
REPLACEMENT PARTS
ITEM QTY. PART NO. DESCRIPTION
13 2 13033 Switch, Momentary Contact
14 1 13022 Switch DPDT
15 1 65229 Connection Stopper
16 2 65206 Cap # GL 18 with gasket
17 1 65207 Dispensing Tube – NaOH
18 1 65203 Distribution Head
19 1 65212 Cap # GL 32 with gasket
20 1 65436 Condenser Extension
21 1 65410 Condenser
22 1 65213 Ventilation Valve
23 1 2128801 Distillation Outlet Tube
24 1 65434 Timer Assembly
Figure 10
25
DIMENSIONS
Figure 11
26
SPECIFICATIONS
Electrical Requirements:
Heating Element:
Boiler Capacity:
Condenser Flow Rate:
Timer:
115 VAC, 15 Amps,
60 Hz, single phase
1200 Watt, 115 VAC
1 liter total volume,
750 ml operating volume
1 gallon per minute (3.8 liters per minute)
0-15 minutes, infinitely adjustable
27
WIRING DIAGRAM
Figure 12
28
TROUBLESHOOTING
PROBLEM CAUSES CORRECTIVE ACTION
Unit will not operate
at all
Boiler doesn’t fill
Heating element
doesn’t work
NaOH pump doesn’t
run
NaOH pump runs,
but doesn’t pump
Tripped circuit breaker Check facility’s circuit breaker
Blown fuse Replace fuse
Power cord not plugged
in
‘Boiler Heater’ switch is
on
Cooling water off or flow
rate insufficient
Water fill valve plugged
or defective
‘Boiler Water’ switch
defective
Heating element is
defective
‘Boiler Heater’ switch is
defective
‘Boiler Heater’ switch is
off
Distillation Timer is set in
the timing mode
NaOH pump is defective Replace the NaOH pump
NaOH tube is kinked or
restricted
Peristaltic pump tube
damaged
Peristaltic pump is
damaged
Plug in cord
Turn off boiler heater before
filling
Check flow rate of condenser
cooling water
Clean inlet screen of filter;
replace valve
Replace switch
Replace heating element
Replace switch
The boiler heater must be on for
the NaOH pump to operate
The Distillation timer must be
set to ‘0’ for the NaOH pump to
work
Check all lines for kinks or
blockage
Replace peristaltic pump tube
Replace peristaltic pump
29
TROUBLESHOOTING
PROBLEM CAUSES CORRECTIVE ACTION
Water is noisy when
flowing through the
unit
Steam drains
erratically; steam
valve is noisy during
standby
Boiling flask breaks
Recoveries are low
Recoveries are too
high
Excessive water flow rate Reduce the water flow rate
slightly
Drain hose is kinked or
elevated above the drain
pipe
Flask has gone dry Do not let flask go dry
Water added when boiler
is dry or low on water and
hot
Viton seal is leaking Clean/replace the Viton seal
Receiving tube is not
completely submerged
Not collecting enough
distillate
Excessive NH3 in feed
water
Drain hose must flow
unrestricted to a drain below the
drain pipe
Do not add water to the boiler
when it is hot and dry, or low on
water
The receiving tube must be
completely submerged in the
receiving vessel
Increase distillation time
Connect to a different water
source; install Optional Water
Inlet Kit #65442 and feed
purified water to the boiler
30
REFERENCES
Rapid Kjeldahl Methodology for the Determination of Nitrogen in Paper Products. 1993.
Labconco Corporation, Kansas City, MO.
Rapid Kjeldahl Methodology for the Determination of Total Kjeldahl Nitrogen in Water. 1993.
Labconco Corporation, Kansas City, MO.
Methodology for the Determination of Alcohol in a Mixture by Direct Distillation. 1993. Labconco
Corporation, Kansas City, MO.
Methodology for the Determination of Ammonia in Water by Direct Distillation. 1993. Labconco
Corporation, Kansas City, MO.
Rapid Kjeldahl Methodology for the Determination of Nitrogen in Meat Products. 1993. Labconco
Corporation, Kansas City, MO.
Rapid Kjeldahl Methodology for the Determination of Nitrogen in Feeds, Foods, Grains, Cereals,
and Grasses. 1993. Labconco Corporation, Kansas City, MO.
Rapid Kjeldahl Methodology for the Determination of Protein Content in Milk. 1993. Labconco
Corporation, Kansas City, MO.
31
WARRANTY
We are committed to providing our customers with quality equipment and service after the sale.
Part of this objective involves keeping you informed of changes and new product additions. We,
therefore, request that you take a moment to fill out the product registration card so we many know
your location as well as some of the reasons that prompted you to purchase our product.
Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas
of defective material and workmanship, provided such defect results from normal and proper use
of the equipment.
The warranty for all Labconco products will expire one year from date of installation or two years
from date of shipment from Labconco, whichever is sooner, except the following:
• Purifier® Delta® Series Biological Safety Cabinets carry a three-year warranty from date
of installation or four years from date of shipment from Labconco, whichever is sooner.
• Carts carry a lifetime warranty.
• Glassware is not warranted from breakage when dropped or mishandled.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the
event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product.
If the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will
repair or replace all defective parts to restore the unit to operation. Under no circumstances shall
Labconco Corporation be liable for indirect, consequential, or special damages of any kind. This
statement may be altered by a specific published amendment. No individual has authorization to
alter the provisions of this warranty policy or its amendments. Lamps and filters are not covered
by this warranty. Damage due to corrosion or accidental breakage is also not covered.
WARNING: The disposal and/or emission of substances used in connection with this equipment
may be governed by various federal, state or local regulations. All users of this equipment are
urged to become familiar with any regulations that apply in the user’s area concerning the
dumping of waste materials in or upon water, land or air and to comply with such regulations.
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SHIPPING CLAIMS
If shipment is received in visibly damaged condition, be certain to make a notation on the
delivering carrier’s receipt and have his agent confirm the damage on your receipt. Otherwise, the
damage claim may be refused.
If concealed damage or pilferage is discovered, notify the carrier immediately and retain the entire
shipment intact for inspection. Interstate Commerce Commission rules require that the claim be
filed with the carrier within 15 days after delivery.
NOTE: Do not return goods. Goods returned without prior authorization will not be accepted.
Labconco Corporation and its dealers are not responsible for shipping damage. Claims must be
filed directly with the freight carrier by the recipient. If authorization has been received to return
this product, by accepting this approval, the user assumes all responsibility and liability for
biological and chemical decontamination and cleansing. Labconco reserves the right to refuse
delivery of any products which do not appear to have been properly cleaned and/or
decontaminated prior to return.
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ACCESSORIES
Accessory Part # Description
23080
23012
23540
2350025
2304005
2304025
2303005
2303025
65442
Rapid Digestor - 4
Temperature control unit with indicator light,
adjustable from ambient to 450°C and 4-place digestion
unit designed for 250 ml digestion tubes (not included).
Rapid Digestor - 25
Temperature control unit with light, adjustable from
ambient to 450° and 25-place digestion unit designed
for 250 ml digestion tubes (not included).
4-Place Fume Removal System
Borosilicate glass manifold with 4 eductors designed to
rest atop the digestion tubes. A water aspirator (not
included) is required.
25-Place Fume Removal System
Borosilicate glass manifold with 25 eductors designed
to rest atop the digestion tubes. A water aspirator for
40 PSI water pressure is included.
Straight Digestion Tube – Package of 5
Made of borosilicate glass with heavy retention lip and
round bottom.
Straight Digestion Tube – Package of 25
Made of borosilicate glass with heavy retention lip and
round bottom.
Volumetric Digestion Tube – Package of 5
Has an easy-to-read calibration mark at 250 ml and
built-in construction for maximum refluxing and
digestion speed. Made of borosilicate glass with heavy
retention lip and round bottom.
Volumetric Digestion Tube – Package of 25
Has an easy-to-read calibration mark at 250 ml and
built-in constriction for maximum refluxing and
digestion speed. Made of borosilicate glass with heavy
retention lip and round bottom.
Optional Water Inlet Kit
Allows the user to connect the condenser and the boiler
to separate water supplies.
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CONTACTING LABCONCO
If you have any questions that are not addressed in this manual or if you need technical assistance,
please contact Labconco’s Customer Service Department at 1-800-821-5525, Labconco’s Product
Service Department at 1-800-522-7658 or either department at 1-816-333-8811, between the hours
of 7:00 a.m. and 6:00 p.m. Central Standard Time.
Labconco’s mailing address is:
Labconco Corporation
8811 Prospect Avenue
Kansas City, Missouri 64132-2696
Visit Labconco through the Internet at:
http://www.labconco.com
or
e-mail: labconco@labconco.com
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