Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas of
defective material and workmanship, provided such defect results from normal and proper use of the
equipment. Glassware is not warranted from breakage when dropped or mishandled.
The warranty for Protector® Work Stations will expire one year from date of installation or two years
from date of shipment from Labconco, whichever is sooner.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the
event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product. If
the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will repair or
replace all defective parts to restore the unit to operation. Under no circumstances shall Labconco
Corporation be liable for indirect, consequential, or special damages of any kind. This statement may
be altered by a specific published amendment. No individual has authorization to alter the provisions
of this warranty policy or its amendments. Lamps and filters are not covered by this warranty.
Damage due to corrosion or accidental breakage is not covered.
The information contained in this manual and the accompanying products are copyrighted and all rights
reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design
changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be
accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier.
Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery
carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by
various federal, state, or local regulations. All users of this equipment are required to become familiar with
any regulations that apply in the user’s area concerning the dumping of waste materials in or upon water,
land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to
user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact
Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821-5525
or 1-816-333-8811, between the hours of 7:00 a.m. and 6:00 p.m., Central Standard Time.
Part #3939000, Rev. F
ECO J105
ORIGINAL INSTRUCTIONS
TABLE OF CONTENTS
CHAPTER 1: INTRODUCTION 1
Typographical Conventions 3
CHAPTER 2: PREREQUISITES 4
Support, Vibration & Movement Requirements 5
Location and Air Current Requirements 5
Exhaust and Blower Requirements 5
Electrical Requirements 6
Space Requirements 6
CHAPTER 3: GETTING STARTED 7
Unpacking Your Enclosure 8
Installing the Enclosure on a Supporting Structure & Work Surface 8
Connecting to the Exhaust System 9
Installation of Carbon Filters for Room Exhaust 14
Connecting the Electrical Supply Source to the Enclosure 15
Set the Face Velocity with Speed Control Adjustment 18
Validating the Protector Workstation Enclosure 18
Sealing the Enclosure to the Work Surface 19
CHAPTER 4: HIGH PERFORMANCE FEATURES AND
SAFETY PRECAUTIONS 20
Components 21
Safety Precautions 25
CHAPTER 5: APPROPRIATE APPLICATIONS FOR YOUR
ENCLOSURE 28
Routine Daily Work Procedures 28
Suitable Applications 29
Carbon Filter Applications 30
Definition of Terms 30
Appropriate Chemicals for Carbon Filters 31
Hazardous Misapplications for Carbon Filters with
Volatile Chemicals 32
Chemical Carcinogen Use with Carbon Filters 32
Prohibited Acid Use 33
CHAPTER 6: MAINTAINING YOUR ENCLOSURE 34
Routine Maintenance Schedule 34
Setting the Inflow Face Velocity with the Speed Control Adjustment 35
Guardian 500 Airflow Monitor Kit No. 3944700 or 3944701 36
Guardian 500 Component Identification 37
Guardian Digital 1000 Operation 43
Guardian Digital 1000 Installation Procedure 43
Digital 1000 Calibration 46
Digital 1000 Alternate Calibration Procedure – Constant
Volume Conditions 47
Determination of When to Replace Carbon Filters and
How to Replace 51
Calculating Carbon Filter Life 54
Fluorescent Light Replacement 55
Motorized Impeller Replacement 55
Speed Control Replacement 57
CHAPTER 7: ACCESSORIZING & MODIFYING YOUR
ENCLOSURE 58
CHAPTER 8: TROUBLESHOOTING 65
APPENDIX A: ENCLOSURE COMPONENTS AND
REPLACEMENT PARTS 68
APPENDIX B: DIMENSIONS AND EXHAUST OPTIONS 73
APPENDIX C: PROTECTOR WORK STATION
SPECIFICATIONS 75
APPENDIX D: QUICK CHART FOR THE PROTECTOR
WORK STATION 76
APPENDIX E: REFERENCES ON VENTILAITON, SAFETY,
OCCUPATIONAL HAZARDS, BIOSAFETY
AND DECONTAMINATION 77
DECLARATION OF CONFORMITY 80
1
!
Chapter 1:
Introduction
Congratulations on your purchase of a Labconco Protector® Work Station. Your
enclosure provides personnel protection through superior containment while
conserving energy at OSHA approved velocities as low as 60 feet per minute. It is
the result of Labconco’s more than 50 years of experience in manufacturing fume
hoods and more than 30 years of experience in manufacturing filtered enclosures.
These enclosures will effectively contain toxic or noxious fumes and chemicals
when properly installed and operated. Each enclosure uses either a carbon filter
for exhausting low concentrations to the room or an accessory remote blower or
accessory FilterMate Portable Exhauster for exhausting high concentrations to the
outside. The carbon filters are available with three different carbons for adsorbing
organic vapors, formaldehyde or ammonia and amines. The accessory FilterMate
Portable Exhauster can also filter particulates. The Protector Work Stations offer
many unique features to enhance safety, performance, and energy savings. To take
full advantage of them, please acquaint yourself with this manual and keep it
handy for future reference. If you are unfamiliar with how high performance
Protector Work Stations operate, please review Chapter 4: High Performance Features and Safety Precautions before you begin working in the enclosure. Even
if you are an experienced user, please review Chapter 5: Using Your Protector Work Station, which describes the features so that you can use the enclosure
efficiently. See chart that follows for application review and contact Labconco for
additional ordering information.
If the unit is not operated as specified in this manual it may
impair the protection provided by the unit.
Si l'unité n'est pas utilisée comme spécifié dans ce manuel il
peut diminuer la protection fournie par l'unité.
Product Service 1-800-522-7658
Chapter 1: Introduction
2
No.
Use Protector Work
Station Model No’s.
Filter
Blower
Application
Exhaust
1.
3930000 (115V)
3930020 (230V)
Carbon Filter*
Organic Vapor,
Formaldehyde or
Ammonia
Built-In
Integral
Motorized
Impeller
If ducting to the outside is not
feasible, the filters keep low
level concentrations below
OSHA recommended time
weighted averages, restoring
clean air to the laboratory.
To the room
2.
3930001 (115V)
3930021 (230V)
None
Remote
Blower or
House Exhaust
Best choice for high level
concentrations or when chemical
concentrations are unknown or
unpredictable
To the outside
3.
3930001 (115V)
3930021 (230V)
FilterMate
Carbon Filter*
and/or HEPA
Filter for
particulates
FilterMate
Portable
Exhauster
Best choice when particulate
removal is required in addition
to carbon filtration and ducting
to the outside is not feasible
To the room
Protector Work Station 3930001 is
shown on Work Surface with Sink
6942003 and Telescoping Base
Stand 3746702. Blower, ductwork,
work surface and supporting base
must be ordered separately.
* It is recommended that a Labconco product specialist review the chemical
application to determine if it is suitable. Consult Chapter 5 and Chapter 6.
Product Service 1-800-522-7658
Chapter 1: Introduction
3
!
!
Typographical Conventions
Recognizing the following typographical conventions will help you understand and
use this manual:
Steps required to perform a task are presented in a numbered format.
Comments located in the margins provide suggestions, reminders, and
references.
Critical information is presented in boldface type in paragraphs that are
preceded by the exclamation icon. Failure to comply with the information
following an exclamation icon may result in injury to the user or permanent
damage to the enclosure.
Critical information is presented in boldface type in paragraphs that are
preceded by the wrench icon. A trained certifier or contractor should only
perform these operations. Failure to comply with the information following a
wrench icon may result in injury to the user or permanent damage to your
hood.
Important information is presented in capitalized type in paragraphs that are
preceded by the pointer icon. It is imperative that the information contained in
these paragraphs be thoroughly read and understood by the user.
CAUTION – See Manual. When this symbol is on the unit it indicates a
caution that is detailed in this manual.
ATTENTION - Voir manuel. Lorsque ce symbole est sur l'unité, il indique une
mise en garde qui est indiqué dans ce manuel.
Product Service 1-800-522-7658
4
Chapter 2:
Prerequisites
Before you install the enclosure, you need to prepare your site for installation.
You must be certain that the area is level and of solid construction. In addition, a
dedicated source of electrical power should be located near the installation site to
power the enclosure, and other apparatus. Additionally, the enclosure should be
strategically placed in the lab to provide efficient workflow.
Carefully read this chapter to learn the requirements for your installation site:
The support, vibration and movement requirements.
The location and air current requirements.
The exhaust and blower requirements.
The electrical power requirements.
The space requirements.
Refer to Appendix B: Dimensions for complete enclosure dimensions.
Refer to Appendix C: Specifications for complete enclosure electrical and
environmental conditions, specifications and requirements.
Product Service 1-800-522-7658
Chapter 2: Prerequisites
5
Enclosure
Width
Model Description
Face
Velocity
(fpm)
Exhaust
Volume
(CFM)
Initial Static
Pressure Loss
for Enclosure
with Remote
Blower
Integral
Blower
Noise
Pressure
(dbA)
4'
4' Protector Work Station
60
80
100
150
200
250
.06"
.10"
.16"
57-59
62-64
69-71
!
Support, Vibration and Movement
Requirements
At a minimum, the supporting structure usually consists of a base cabinet or base
stand and chemical-resistant work surface. See Chapter 3 for setting up installation.
Location and Air Current Requirements
The Protector Work Stations have been designed to contain hazards by negating
typical cross drafts and turbulence within the opening. Normal air movement does
not affect installation of the Protector Work Station. However, as a precautionary
safety measure and a higher level of quality management, it is recommended that
the Protector Work Station be placed in an area to avoid:
High traffic areas where walking might cause an air disturbance or be a
nuisance.
Overhead or wall HVAC diffusers, fans, radiators or other lab equipment
producing air currents.
Next to doorways or windows that may be opened.
Do not position the unit so that it is difficult to operate the main
disconnect device.
Ne placez pas l'appareil de sorte qu'il est difficile de faire
fonctionner le dispositif principal de déconnexion.
Exhaust and Blower Requirements
The Protector Work Station draws room air past the operator and through the
enclosure. This contaminated air is either pulled through a carbon filter and
exhausted to the room or exhausted outside by a remote blower.
Data for the exhaust volume and enclosure static pressure loss are listed for the
Protector Work Station at face velocities of 60, 80 and 100 fpm.
Proper blower selection can be determined from these exhaust requirements and
the total system static pressure loss for outside exhaust. The enclosure must be
connected to either a dedicated blower or a house exhaust system.
Product Service 1-800-522-7658
Chapter 2: Prerequisites
6
!
Labconco offers accessory remote blowers and transition adapters listed in Chapter 7.
Labconco also offers accessory FilterMate Portable Exhausters listed in Chapter 7.
Contact Labconco for blower sizing assistance.
If the enclosure is connected directly to a house exhaust system,
an adjustable damper (or valve) must be installed to control the
airflow properly. This is equally important when a house exhaust
system is controlling multiple enclosures. See Chapter 7 for
accessory Adjustable Damper ordering information.
Electrical Requirements
Standard duplex electrical receptacles should be nearby for connecting the
enclosure or other equipment. The enclosures for remote blower exhaust include
iris pass-throughs to allow electrical cords through the back of the enclosure
without leaving a large hole for contaminants to escape.
The remote blower for the Protector Work Station may be connected to the blower
switch on the enclosure. There is an outlet on the back of the upper light housing
for this specific purpose. We recommend a maximum amperage of 6 amps for this
circuit to the remote blower. Please refer to the wiring diagrams in Appendix C.
Connect the blower wires to the remote blower per local electrical codes.
Space Requirements
The dimensions for the different models are shown in Appendix B: Dimensions.
Product Service 1-800-522-7658
7
!
Chapter 3:
Getting Started
Now that the site for your Protector Work Station is properly prepared, you are
ready to unpack, inspect, install, and validate your system. Read this chapter to
learn how to:
Unpack and move the enclosure.
Set up the enclosure with the proper supporting structure and work surface.
Connect to an exhaust system (only applicable for remote blower).
Installation of carbon filters (only applicable for integral blower exhausted
to the room).
Connect the electrical supply.
Set the face velocity with the speed control adjustment, only applicable for
integral blower.
Arrange validation for the enclosure.
Seal the enclosure to the work surface.
Depending upon which model you are installing, you may need common
mechanical and electrical installation tools in addition to wrenches, ratchets,
sockets, a nut driver set, a flat-blade screwdriver, a Phillips screwdriver, and a
carpenter level to complete the instructions in this chapter.
Each enclosure weighs either 85 or 105 lbs. each (37 or 46 kg).
The shipping container allows for lifting with a mechanical lift
truck or floor jack. If you must lift the enclosure manually,
follow safe-lifting guidelines. Do not lift by the front air
foil.
Product Service 1-800-522-7658
Chapter 3: Getting Started
8
The United
States
Interstate
Commerce
Commission
rules require
that claims be
filed with the
delivery
carrier within
fifteen (15)
days of
delivery.
!
Unpacking the Enclosure
Carefully remove the shrink-wrap or carton on the enclosure and inspect it for
damage that may have occurred in transit. If damaged, notify the delivery carrier
immediately and retain the entire shipment intact for inspection by the carrier.
DO NOT RETURN GOODS WITHOUT THE PRIOR
AUTHORIZATION OF LABCONCO. UNAUTHORIZED
RETURNS WILL NOT BE ACCEPTED.
IF ENCLOSURE WAS DAMAGED IN TRANSIT, YOU MUST
FILE A CLAIM DIRECTLY WITH THE FREIGHT CARRIER.
LABCONCO CORPORATION AND ITS DEALERS ARE NOT
RESPONSIBLE FOR SHIPPING DAMAGE.
Do not discard the packing material until you have checked all of the components
and tested the enclosure. We recommend that you do not remove the enclosure
from its shipping container until it is ready to be placed in its final location. Move
the unit by placing a flat, low dolly under the shipping skid, or by using a floor
jack.
Do not move the enclosure by tilting it onto a hand truck.
Installing the Enclosure on a Supporting
Structure and Work Surface
Use caution when lifting or moving the enclosure.
When installing the enclosure onto a chemical-resistant work surface or benchtop,
ensure that the structure can safely support the combined weight of the enclosure
and any related equipment. The work surface should be at least as wide as the
enclosure to properly support it. The front of the enclosure should be aligned
within 0.3" of the front of the work surface. Mounting holes are provided in the
Labconco accessory work surfaces to secure the enclosure.
Product Service 1-800-522-7658
Chapter 3: Getting Started
9
Work Surface Specifications
The work surface should be smooth, rigid, and durable, such as a chemicalresistant epoxy resin. The surface should be non-porous and resistant to the
powders, solvents and chemicals used in conjunction with the enclosure. The
work surface should also contain a dished recessed area for containing primary
spills.
Work Surface and Enclosure Installation
1. Level the base cabinet or stand and the work surface. Work surface should
be placed flush with the front of the base stand or cabinet as shown in
Figure 3-1.
2. Position the work surface in its intended location and with the front of the
work surface towards you. (Rear mounting holes are located close to the
rear edge.)
3. Secure the work surface to the base stand or cabinet with a structural
adhesive or silicone sealant.
4. Insert the supplied mounting screws in the four holes. Allow a minimum
of 1/8" clearance under the head of the screw for positioning the enclosure.
(On 6942003 work surface with sink, the fasteners are omitted and the
enclosure is secured to the work surface with silicone sealant.
5. Place the enclosure on the work surface and slide the rear flange and front
air foil flanges under the mounting screw heads.
6. Tighten the four screws to complete the installation.
If the accessory histology/pathology work surface with sink is to be installed
(Labconco #6942003) then use general plumbing to connect the hot and cold water
supply lines and sink drain line. The valves are supplied with 1/2" OD slip joint
by 1/4" NPT female connector. The drain line requires 1-1/2" NPT female pipe
connector and an optional polypropylene P-trap (Labconco P/N 1432600)
See Chapter 7 for Dimensions on work surfaces.
Product Service 1-800-522-7658
Chapter 3: Getting Started
10
3912401 (6") Exhaust Transition shown
for Connection to Remote Blower
3944700 Guardian 500
Airflow Monitor (115V)
3930001 Protector
Work Station, 115V
Remote Blower
Control
Panel
3908402 Dished Work Surface
3746702 Telescoping Base
Stand
3930000 Protector Work Station,
115V w/ Integral Blower
Exhausts through Carbon Filters
to the Room
Typical Exhaust Holes
Integral Blower Power Inlet
connected via Power Cord
from Back of Control Panel
Digital Airflow Sensor
3908800 Guardian
Digital 1000 Airflow
Monitor (115V)
Control Panel
6942003 Dished Work
Surface w/ Built-In Sink,
HW & CW Valves,
Gooseneck, and Sprayer
Sink Location
3746702 Telescoping Base Stand
Figure 3-1
Product Service 1-800-522-7658
Chapter 3: Getting Started
11
!
!
Connecting to the Exhaust System
(Required on Protector Work Station for
Remote Exhaust)
ATTENTION: The weight of the exhaust ductwork system
must be supported independently of the enclosure
superstructure or damage may occur.
The exhaust system should be installed by a qualified HVAC
contractor.
The exhaust connection on the remote Protector Work Station Enclosure has been
designed to accept a 2" x 10" (5.1cm x 25.4cm) nominal transition adapter. See
Chapter 7 for ordering accessory Transition Adapters. Labconco manufactures
transition adapters for either top or bottom exhaust and for both 5" dia. hose or 6"
dia. duct. Review Chapter 2 for remote blower and FilterMate Portable Exhauster
exhaust prerequisites and review Chapter 7 for ordering blower exhaust equipment.
For your convenience several exhaust options are shown in Figures 3-2 and 3-3.
Consult Labconco Customer Service should you require help sizing your blower
for the exhaust volume and system static pressure loss.
To ensure compatibility, the selected exhaust duct material
should match the enclosure, procedures and chemical
applications.
Product Service 1-800-522-7658
Chapter 3: Getting Started
12
Figure 3-2
5" Top Exhaust for Remote Protector Work Station
Connected to a FilterMate Portable Exhauster
5" ID Hose included
with FilterMate
3912400 5" ID Top
Exhaust Adapter
included with FilterMate
3930001 Protector Work
Station for Remote
Exhaust (115V)
Optional 3944700
Guardian 500
Airflow Monitor
(115V)
Accessory
3908402 Dished
Work Surface
Accessory 4' Base
Cabinet
Optional FilterMate
Portable Exhauster
Product Service 1-800-522-7658
13
Figure 3-3
Back View of Protector Work Station with Lower 6"
Remote Exhaust
3930001 Protector Work
Station for Remote
Exhaust (115V)
Optional Accessory
3913100 Exhaust
moved to Top
3912403 6" Lower Exhaust
(Accessory)
Airflow Monitor
Chapter 3: Getting Started
Cover Plate
Transition Adaptor
Product Service 1-800-522-7658
Chapter 3: Getting Started
14
Filter Type
Appropriate Use
Organic Vapor
Activated Carbon
3924200
10.5 lbs.
Adsorbs organic compounds designated by NIOSH
guidelines as acceptable for use with chemical
cartridge-type respirators. Concentrations in the
enclosure’s work area must not exceed the IDLH for
the chemical and the exhaust from the enclosure must
be perfectly monitored not to exceed the TWA.
Formaldehyde
(Formalin)
3924201
13.3 lbs.
Formaldehyde requires the use of an impregnated
carbon. Concentrations in the enclosure’s work area
must not exceed the IDLH for the chemical and the
exhaust from the enclosure must not exceed the TWA.
Ammonia and
Amines
3924202
15.2 lbs.
Treats ammonia, low molecular weight amines and
other bases designated by NIOSH as acceptable for use
with ammonia cartridge type respirators. Requires the
use of an impregnated carbon. Concentrations in the
enclosure’s work area must not exceed the IDLH for
the chemical and the exhaust from the enclosure must
not exceed the TWA.
!
Installation of Carbon Filters for Room
Exhaust
For carbon filter installation, first unthread the knobs on the perforated baffle
located inside the enclosure in the upper corners. Use caution when slowly
lowering the perforated baffle. See Figure 6-4 in Chapter 6 for location of the
perforated baffle and knobs. See the following list of available carbon filters
below and in Chapter 7. All carbon filters are simply installed with the gasket side
on the downstream exhaust side. Install the correct carbon filter for the application
and call Labconco for assistance. Two carbon filters must be installed behind the
perforated baffle. These two filters provide additional capacity and mixing of the
air stream for proper performance. If using both a formaldehyde filter and organic
vapor filter at the same time you must place the formaldehyde filter downstream of
the organic vapor filter. (With the perforated baffle tilted down, the formaldehyde
filter is on top of the organic vapor filter.)
Important: Carbon filters do not provide any particulate
protection, but provide odor control for low level
concentrations below OSHA recommended time weighted
averages.
Product Service 1-800-522-7658
Chapter 3: Getting Started
15
Connecting the Electrical Supply Source
to the Enclosure
115V Models
Simply connect the 115V power cord supplied to the IEC electrical supply plug on
the back of the enclosure, then connect the integral blower power cord from the
motorized impeller outlet on the exhaust to the back of the upper light control
panel. If operating at 50 Hz operations, integral blower performance maximum
airflow will be reduced by 17%. See Figure 3-4 on the following page.
For the remote blower used for Protector Work Stations, follow the wiring diagram
in Appendix C and wire the remote blower wires to the switched outlet on the back
of the upper light control panel. These wires are switched by the blower switch.
Refer to Figure 3-5.
The maximum circuit load for the blower is 6 amps. The lights and airflow
monitor are powered from a standard duplex electrical receptacle located nearby
for connecting the power cord. All wiring for the Protector Work Station should
be performed by a licensed electrician and conform to local codes. In most cases,
the remote blower Protector Work Station for use with a remote blower will
require the use of an additional power cord routed from the switched power outlet
on the back. See Figure 3-5 and power cord, item 24 in Figure A-2. Modify the
power cord, item 24, in Figure A-2 for connection to the remote blower via a
customer supplied junction box located nearby. The grounding connection shall
not be made to the terminal box cover of the remote blower. The building
electrical supply system for the remote blower should include overload protection
such as a switch or circuit breaker in close proximity and within easy reach of the
operator. The switch or circuit breaker shall be marked as the disconnecting
device. Consult NEC-2002 for proper installation.
Product Service 1-800-522-7658
Chapter 3: Getting Started
16
Speed Control
Main Inlet Power
Switched Power Outlet to Blower
Motor (Regulated by Speed Control)
Circuit Breaker
Auxiliary Switched Power Outlet for Airflow
Monitor
Blower Motor Power
Cord Connection
Integral Blower
Motorized
Impeller Power
Inlet
Exhausts to
the Room
Back of Airflow
Monitor
Protector Work Station with Integral Blower Power Cord
Figure 3-4
and Speed Control
Product Service 1-800-522-7658
17
Figure 3-5
Protector Work Station for Remote Exhaust
Main Inlet Power
Switched Power Outlet to Remote Blower
Motor using Modified Power Cord
For 6" Connection to
Remote Blower
Circuit
Breaker
Not Shown – Auxiliary Switched Outlet
Chapter 3: Getting Started
for Airflow Monitor
Product Service 1-800-522-7658
Chapter 3: Getting Started
18
!
230V Models
The same procedure applies for the 230V except it is shipped without a plug.
Install the appropriate plug for your electrical specifications per local codes.
Do not use any detachable power cord that is not adequately rated
for the unit.
Ne pas utliser un fil électrique amovible qui n’est pas du tension
nominale de l’appareil.
Set the Face Velocity with the Speed
Control Adjustment
For Protector Work Stations with integral blower, adjustment of the speed control
gives the correct face velocity and is located behind the upper light control panel.
The face velocity should be adjusted from 60 to 100 fpm. (Consult your Safety
Officer for airflow recommendations for your application). Containment is
maximized at a setting within this range. Working at the lowest face velocity
appropriate for the application will give the quietest operation. Face velocity
measurements are made using an anemometer. An electric anemometer can be
obtained from your laboratory supply dealer. Face velocity measurements should
be taken in accordance with the Industrial Ventilation Manual. (See Appendix E)
Using a small Phillips screwdriver, adjust the speed control to give the required
face velocity. See Figure 3-4 to locate the speed control. The face velocity is
increased by turning the speed control counter clockwise and clockwise to
decrease face velocity.
Validating the Protector Work Station
Enclosure
To determine the actual face velocity at the sash opening, airflow velocity readings
are taken. This should be done across the sash opening of the enclosure in
accordance with the Industrial Ventilation Manual. (See Appendix E) The
“average face velocity” is achieved by taking readings in two rows across the
enclosure with the readings 6" from the ends and evenly spaced every 12"; the first
row is 3" down from the upper sash foil and the second row is 3" up from the work
surface. A total of eight readings are taken for the 4' enclosure and then averaged.
Refer to Chapter 2 for proper airflow volumes for your particular model.
The Protector Work Station enclosures have been tested at Labconco’s airflow test
facility per ASHRAE 110-1995. (See Appendix E) All enclosures achieve an “as
manufactured rating” of less than 0.05 part per million (ppm) at 4 liters per minute
(lpm); AM <0.05 (Consult Labconco for individual ratings). For “field use”
ASHRAE testing contact Labconco for a certified on-site contractor. While no
enclosure can compensate for improper technique, these tests confirm that the
Protector Work Station enclosures provide a safe working environment.
Product Service 1-800-522-7658
Chapter 3: Getting Started
19
!
NOTE: Face velocity profiles and smoke testing should be
performed frequently per your organization’s quality system to
ensure safe performance.
Sealing the Enclosure to the Work
Surface
When the enclosure has been set in place it may be sealed at the work surface to
prevent spilled materials from collecting under the walls. A bead of silicone
sealant is recommended to seal the enclosure to the work surface.
Product Service 1-800-522-7658
20
1
Chapter 4:
High Performance Features and
Safety Precautions
High Performance Features
The patented1 Protector Work Stations are designed to meet the needs of the
laboratory scientist, and provide superior containment while conserving energy at
OSHA approved “low flow” velocities as low as 60 feet per minute. The
enclosures have been tested to effectively contain toxic and noxious materials
when properly installed and operated. What makes the enclosures so unique is the
revolutionary way they direct air into and through the contaminated air chamber.
Labconco engineered the enclosures to minimize the effects of turbulence. The
containment-enhancing and aerodynamic designs of the upper sash foil, side air
foils, lower air foil, upper dilution air supply, and rear perforated baffle all work in
concert to produce horizontal airflow patterns that significantly reduce powder,
chemical and particulate concentrations through the work area.
These concentrations of materials are predominantly removed on the “first pass” of
airflow through the chamber resulting in high performance containment.
The Protector Work Station with integral blower is designed only for low-level
concentrations for use with carbon filters and exhausting to the room. The
Protector Work Station for use with a remote blower is designed for high-level
concentrations for exhausting to the outside.
U.S. Patent No. 6,461,233
Product Service 1-800-522-7658
Chapter 4: High Performance Features & Safety Precautions
21
Figure 4-1
Protector Work Station for use with Remote Blower
10
4
15
19
7 9 8
17
1
2
5
6
14
3
20 Not Shown
16 Not Shown
13
Product Service 1-800-522-7658
Chapter 4: High Performance Features & Safety Precautions
22
Figure 4-2
Protector Work Station with Integral Blower
11
10
12
13
15
18 4 7
8
17 w/ Sink
1
2 5 6
14
3
20 Not Shown
16 Not Shown
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Figure 4-3
Figure 4-4
1. Aerodynamic Clean-Sweep™ Air Foil has a unique shape that allows air
to sweep the work surface for maximum containment. The Clean-Sweep™
openings create a constant protective barrier from contaminants. Should
the operator inadvertently block the airflow entering the air foil, air
continues to pass under the air foil and through the Clean-Sweep openings.
See Figures 4-1, 4-2 and 4-3.
2. Containment-Enhancing Upper Sash Foil includes an open air passage
directly atop the sash foil to bleed air into the hood chamber and direct
chemical concentrations away from the sash opening. The radiused sash
foil sweeps airflow into the enclosure with minimal turbulence. See
Figures 4-1, 4-2 and 4-4.
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3. Upper Dilution Air Supply provides bypass air from above the work area.
This feature constantly bathes the inside of the sash with clean air and
reduces chemical concentrations along the sash plane, near the critical
breathing zone. Five to seven percent of the required air volume is
introduced through the upper dilution air supply. The upper dilution air
supply also reduces stagnant pockets of air in the upper interior. See
Figures 4-1 and 4-2.
air streams to the three-zoned sections of the perforated baffle. The threezoned sections have increasingly more open area at the bottom that help
form laminar airflow. This minimizes the potential for air to roll forward
preventing contaminants from moving toward the sash opening. The
majority of contaminants are highly diluted, captured and removed on the
first pass through the enclosure. See Figures 4-1 and 4-2.
5. Side-Entry Air Foils allow turbulence-free air to enter the enclosure from
the sides and allow clean air to sweep the interior walls of the enclosure.
See Figures 4-1 and 4-2.
6. Ergonomic Slope of 20 degrees provides maximum visibility and comfort,
reduces glare thereby minimizing operator fatigue. See Figures 4-1 and 4-2.
7. Internal Work Space provides necessary depth to perform work inside the
Protector Work Station without it extending outside the enclosure or resting
on the lower air foil. Remote blower model provides 23" working depth
and integral blower model provides 17.19" working depth. See Figures 4-1
and 4-2.
8. Safety Glass Sash with Spring-Loaded Latch has a wiping seal for
maximum containment and features a spring-loaded latch to secure sash
open for loading and cleaning. The sash must be down for normal
operation. See Figures 4-1 and 4-2.
9. Utility Ports with Iris (Work Station for Remote Exhaust Only) allows
electrical cords and data cords to pass through the back of enclosure without
leaving a large hole for contaminants to escape. The enclosure ships with
both solid plugs and iris plugs. See Figure 4-1.
Digital Airflow Monitor continuously monitors airflow. An audio/visual
alarm alerts the user to low airflow conditions on both the Guardian 500 and
Guardian 1000 Digital airflow monitors. The Guardian™ 1000 Digital
Airflow Monitor also displays a face velocity value, provides an RS232
output, a night setback mode and several auxiliary relay ports. Both airflow
monitors are available options on all Protector Work Station models. See
Figure 4-1 and 4-2. See Chapter 6 for complete details, installation and
calibration.
the need for a remote blower when using low level concentrations of
chemicals. The impeller wheel is dynamically balanced. See Figure 4-2.
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Chapter 4: High Performance Features & Safety Precautions
25
12. Speed Control (Integral Blower Models Only) regulates the speed of the
motorized impeller and is used by the certifier to validate and adjust the
inflow velocity. It is located behind the upper light assembly. See Figures
4-2 and Figure 3-4.
13. Space-Saving Design increases effective laboratory workspace, because
the impeller and carbon filter are self-contained on integral blower models.
On remote blower models, the interior space is increased to 23" interior
depth vs. 17.19" for integral blower models. See Figure 4-1.
14. Sash. The sash is constructed of 1/4 inch tempered safety glass. It pivots
up for loading and cleaning. See Figures 4-1 and 4-2.
15. Control Panel. The control panel, which is located above the sash,
contains the control switches and the electronics. See Figures 4-1 and 4-2.
16. Lamp Ballast (Not Shown) for the fluorescent lamp is located behind the
control panel.
17. Accessory Work Surface is dished and contoured to fit the dimensions of
the enclosure to contain spills. For histology/pathology applications, a wet
chemistry work surface is available with a sink and valves. See Chapter 7.
18. Carbon Filters (for Integral Blower Models Only) are necessary on
integral blower models. Carbon filters are designed to remove small
amounts of noxious fumes and chemicals. The carbon filters are supported
behind the perforated baffle. Two carbon filters are required. Carbon
filters are listed in Chapter 7. See Figure 4-2 and Figure 6-4.
are available to duct to the outside. The exhaust connection allows the
operator additional protection from hazardous fumes or vapors and should
always be used if carbon filters capacity are not appropriate for your
application. See figures in Chapter 3 and Chapter 7 to order.
20. Utility Shelves (not shown) allow the user to hold utensils and printers on
shelves inside the enclosure. See Chapter 7.
Safety Precautions
1. Although the enclosure has been engineered to maintain optimum operator
safety, caution should always be used while working. Prior to using the
enclosure, check to make sure that the exhaust blower is operating and that
air is entering the enclosure at its specified face velocity. The use of an
airflow monitor is recommended to alert the user to a problem with airflow.
2. Use good housekeeping in the enclosure at all times. Clean up spills
3. Do not overload the work surface with apparatus or work material. The safe
operation of the enclosure is based upon having proper airflow through the
structure. Do not place large objects directly on the work surface. Instead,
elevate the object 3/4" on blocks to allow a flow of air under the object and
into the rear baffle exhaust slots. Ensure blocks are level and secured in place.
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Chapter 4: High Performance Features & Safety Precautions
26
4. Blocking large portions of the rear baffle will change the airflow pattern in
the enclosure causing turbulence. (Do not store containers or supplies
against the rear baffle, as this will affect airflow).
5. Always work with your hands as far back into the enclosure as possible.
Keep all chemicals, materials and apparatus inside the lower air foil of the
enclosure.
6. Do not work in this enclosure without the exhaust system running.
7. General acid use, as well as Perchloric acid use in this enclosure is prohibited.
8. High-level radioisotope materials are prohibited in this enclosure. Consult
your Safety Officer.
9. Avoid cross drafts and limit traffic in front of the enclosure. Air
disturbances created may draw contaminants out of the enclosure.
10. A qualified certification technician should test the enclosure before it is
initially used.
11. The use of safety goggles, protective clothing, gloves and any other
personal protective equipment recommended by your safety officer should
be used.
12. The sash must remain in the down position while using the enclosure to
ensure containment.
13. Proper performance of the enclosure depends largely upon its location and
the operator’s work habits. Consult the references in Appendix D.
14. The enclosure should be recertified whenever it is serviced or relocated and
at least annually thereafter.
15. Avoid the use of flammable gases or solvents in the enclosure if possible.
Care must be taken to ensure against the concentration of flammable or
explosive gases or vapors. Use of an open flame should be avoided in the
enclosure. Gases under high pressure should not be used in the enclosure
as they may disrupt the airflow patterns.
16. Manipulations that generate gases or vapors from toxic chemicals or
radionuclides must be evaluated carefully from the standpoint of buildup to
dangerous levels above the TWA of the chemical.
17. Ensure that the work station is connected to electrical service in accordance
with local and national electrical codes. Failure to do so may create a fire
or electrical hazard. Do not remove or service any electrical components
without first disconnecting the work station from electrical service.
18. Carbon filters are disposed as hazardous waste. The user is responsible for
recording the chemicals adsorbed or treated by the filters and disposing
properly.
19. Ensure only trained operators use the enclosure. New users should review
the User’s Manual and become familiar with the operation of the enclosure.
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Chapter 4: High Performance Features & Safety Precautions
27
20. If the work station is to be used in a confined space, make sure the space is
well ventilated and the concentration of toxic contaminants cannot
accumulate greater than the TWA.
21. Proper operation of the enclosure depends largely upon the enclosure
location and the operator’s work habits. The enclosure should be located
away from traffic patterns, doors, fans, ventilation registers, fume hoods,
and any other air-handling device that could disrupt its airflow patterns.
Consult Chapter 2: Prerequisites and Chapter 3: Getting Started sections
of this manual for further details.
22. Only chemicals that can be safely adsorbed and treated with specific carbon
based filters are appropriate for use in this enclosure. Two carbon filters
must always be used. Contact Labconco for chemical assessment.
23. The warning properties (i.e., odor, taste) of the volatile organic compounds
or other material being used in the enclosure must be adequate to provide
an early indication that the carbon filters may be saturated or inadequate.
Contact Labconco for help with chemical assessment.
24. Use the smallest possible quantity of chemical(s) within the enclosure and
never exceed the amount that can be effectively adsorbed by the carbon
filters before breakthrough.
25. For all procedures, adjust face velocity between 60 and 100 FPM for
effective operation.
26. Leave the blower on for at least one minute after work in the enclosure has
been completed.
27. If a chemical is spilled on the work surface, DO NOT switch off the
blower until all traces have been removed.
28. Tag the enclosure with appropriate warning if filters have been removed for
service.
29. If the blower fails during use, processes should cease and the area should
be vacated and ventilated.
30. Always refer to the NIOSH Pocket Guide to Chemical Hazards before
proceeding (See Appendix E). For additional help with filter and chemical
selection contact Labconco at 1-800-821-5525 or 1-816-333-8811.
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28
Chapter 5:
Appropriate Applications for
Your Enclosure
Now that the installation of your enclosure is completed, you are ready to use your
Protector Work Station. Read this chapter to learn about:
1. Routine Daily Work Procedures.
2. Suitable Applications.
3. Carbon Filter Applications.
4. Definition of Terms.
5. Appropriate Chemicals for Carbon Filters.
6. Hazardous Misapplications for Carbon Filters.
7. Chemical Carcinogen use with Carbon Filters.
8. Prohibited Acid Use. (On Integral Blower Models)
Routine Daily Work Procedures
Planning
Thoroughly understand procedures and equipment required before
beginning work.
Arrange for minimal disruptions, such as room traffic or entry into the
room while the enclosure is in use.
Start-up
Turn on exhaust system and accessory light.
Only raise the sash for loading and cleaning.
Check the baffle air slots for obstructions.
Allow the enclosure to operate unobstructed for 1 minute.
Wear a long sleeved lab coat and rubber gloves. Use protective eyewear.
Wear a protective mask if appropriate. Consult your Safety Officer for
additional personal protective equipment recommendations.
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Chapter 5: Appropriate Applications for Your Enclosure
29
Loading Materials and Equipment
Load only the materials required for the procedure. Do not overload the
enclosure.
Do not obstruct the air foil, or rear baffle slots.
Large objects should not be placed close together and should be elevated
above the work surface to permit airflow to sweep under the equipment.
After loading, wait one minute to purge airborne contaminants from the
work area.
Work Techniques
Keep all materials inside the lower air foil, and perform all contaminated
operations as far to the rear of the work area as possible.
Segregate all clean and contaminated materials in the work area.
Avoid using techniques or procedures that disrupt the airflow patterns of
the enclosure.
Final Purging
Upon completion of work, the enclosure should be allowed to operate for
two to three minutes undisturbed, to purge airborne contaminants from the
work area before shutting off the blower.
Unloading Materials and Equipment
Objects in contact with contaminated material should be surface
decontaminated before removal from the enclosure.
All open trays or containers should be covered before being removed from
the enclosure.
Shutdown
Turn off the exhaust system and light.
Suitable Applications
NIOSH (National Institute for Occupational Safety and Health, USA) has
established guidelines for chemical cartridge and HEPA filtered respirators.
Suitable applications for the carbon filtered enclosures are based on these
guidelines. As with respirators, chemical contaminants are adsorbed or treated by
carbon.
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Chapter 5: Appropriate Applications for Your Enclosure
30
Carbon Filter Applications (sold as an
accessory for Integral Blower Models)
Release of low concentrations of vapors effectively adsorbed or treated in
carbon based filters.
Treatment of low-level carcinogens or suspected carcinogens. (See Chemical
Carcinogens in Chapter 5)
Procedures that may have traditionally been done on the open bench (low
levels only).
Odoriferous chemicals that are an unpleasant nuisance.
Other applications, not fitting the above guidelines, would be better suited with the
exhaust ducted to the outside by using a Protector Work Station with remote
blower.
REFERENCES TO NIOSH OR OSHA GUIDELINES AND
REGULATIONS APPLY TO ANY WORK PLACE UNDER THE
JURISDICTION OF THE U.S. DEPARTMENT OF LABOR.
OTHER COUNTRIES OUTSIDE THE U.S. HAVE
ESTABLISHED STANDARDS, WHICH MAY DIFFER
SLIGHTLY FROM THOSE USED AS GUIDELINES FOR THIS
PRODUCT. IT IS THE USER’S RESPONSIBILITY TO
BECOME AWARE OF LOCAL REGULATIONS GOVERNING
THE SAFE USE AND DISPOSAL OF CHEMICALS AND
CARBON FILTERS. KNOWLEDGE OF ESTABLISHED SAFE
EXPOSURE LEVELS IS IMPERATIVE TO THE PROPER USE
OF CARBON FILTERED ENCLOSURES.
Definition of Terms
NIOSH – National Institute for Occupational Safety and Health/Mine Safety and
Health Administration. (U.S.A.)
TWA – Recommended Exposure Limits expressed as a Time Weighted Average.
The exposure limit for that chemical for up to a 10-hour workday, 40 hours a
week. Expressed in units of parts per million or milligrams per cubic meter.
Odor Threshold – The value in parts per million or milligrams per cubic meter for
which one might expect to smell a chemical’s presence in the air. This value is
very subjective and detection will vary with the sensitivity of one’s nose. The
period of time until the odor threshold is reached in the exhaust stream can be
estimated from Labconco’s exclusive chemical assessment program. Contact
Labconco on carbon filter life for specific applications. See Chapter 6.
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31
!
Saturation Level or Time – There is a limit to the amount of chemical that can be
adsorbed by activated carbon or neutralized by chemically-treated carbon. Once
the capacity of the carbon is reached, it is considered to be saturated and will
adsorb (or neutralize) no further material; the outlet concentration of the chemical
will equal the inlet concentration from that point until the filter is replaced. (Note
that the capacity of activated carbon is not a constant, but varies with the inlet
concentration). Labconco Product Specialists can determine the estimated
saturation time for a particular chemical.
IDLH (Immediately Dangerous to Life and Health). An atmosphere that poses
an immediate hazard to life or produces immediate irreversible health effects.
IDLH concentrations should not be approached in the enclosure.
Appropriate Chemicals for Carbon Filters
Below is a general set of rules to determine appropriateness of chemical usage.
Selected organic chemicals considered to be occupational
carcinogens by NIOSH can be used in the filtered enclosure
with carbon filters under rigid restrictions. See separate
discussion on next page on carcinogens for special instructions.
Organics must have time weighted exposure limits (TWA) of 1 PPM or greater.
Chemicals must have a detectable odor at concentrations below the TWA for the
chemical.
Chemicals must be designated by NIOSH guidelines as acceptable for use with
chemical cartridge-type respirators (the exception is formaldehyde and
ammonia/amines, which used impregnated carbon). Chemicals not listed by
NIOSH in the Pocket Guide must be approved by Labconco Product Specialist (or
Engineering).
Inlet concentration must never exceed the IDLH (Immediately Dangerous to Life
and Health) concentrations.
Chemicals having a recommendation by NIOSH of at least “Escape GMFOV”
(Gas Mask Full-Face Respirator).
When evaporating a mixture of chemicals, the chemical having the lowest TWA
will be used to determine if the mixture meets the guidelines.
Call a Labconco Product Specialist at 1-800-821-5525 for assistance in
determining chemical appropriateness.
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Chapter 5: Appropriate Applications for Your Enclosure
32
!
Hazardous Misapplications for Carbon
Filters with Volatile Chemicals
There is one scenario where the accessory carbon filter misapplication would be a
part of a hazardous condition. If the user continues to operate the enclosure with
any of the following conditions present a potentially hazardous condition will exist:
1. The inlet concentration of vapors is greater than the TWA.
2. The carbon filter becomes saturated.
3. The ventilation of the room is insufficient to dilute the exhaust of the
enclosure to below the TWA for the chemical.
When the inlet concentration is greater than the TWA, extra measures must be
taken to monitor the filter and number of room air exchanges.
Chemical Carcinogen Use with Carbon
Filters
Selected carcinogens may be used safely with carbon filters under the following
restrictions.
The use of a vented fume hood or ventilated enclosure with
ducting to the outside is always the preferred method when
working with carcinogens. The carbon filters should only be
used as a last resort when venting to the outside is not an
option.
The potential carcinogens are listed in the NIOSH Pocket Guide to Chemical
Hazards as “Ca.” Each potential carcinogen must have a TWA of 1 or greater;
have minimum respirator recommendation of Escape GMFOV, and an odor
threshold significantly lower than the TWA for the chemical.
The inlet concentration or the evaporation rate of the chemical must never exceed
the TWA for the chemical.
Consult a Labconco Technical Specialist for estimated saturation life. See Chapter
6 for an example of estimating saturation life. Another source is the Labconco
chemical guide for carbon filtered enclosures.
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Chapter 5: Appropriate Applications for Your Enclosure
33
Prohibited Acid Use
The Protector Work Station with Integral Blower motorized impeller cannot be
exposed to acids. Where applications require the use of acids a vented fume hood,
or vented enclosure should be used with a remote blower and ducted to the outside.
Consult Labconco for other small enclosures suitable for acid work. No
exceptions are permitted, as the Protector Work Station with Integral Blower
impeller life span will be limited with acid use. Additionally, the Protector Work
Station for use with a remote blower cannot be used with acids because the acids
will corrode the stainless steel baffle. Consult Labconco for Protector XVS
Enclosures suitable for acid work.
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Chapter 6
Maintaining Your Enclosure
Monitoring airflow and changing the carbon filters (if equipped) is the primary
maintenance required.
Review this chapter on maintenance for the following:
1. Routine Maintenance.
2. Speed control adjustment and setting the inflow face velocity.
3. Operating and calibrating the airflow monitors.
4. Determination of when to replace carbon filters and how to replace.
5. Calculating carbon filter life.
6. Fluorescent light replacement.
7. Motorized impeller replacement.
8. Speed control replacement.
Routine Maintenance Schedule
Weekly
Wipe down the interior surfaces of the enclosure with a disinfectant or
cleaner, depending upon the usage of the unit and allow to dry.
Using a damp cloth, clean the exterior surfaces of the enclosure,
particularly the front and top to remove any accumulated dust.
Operate the exhaust system, noting the airflow velocity through the
enclosure using a source of visible smoke. Airflow monitors are
recommended for constant monitoring.
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Chapter 6: Maintaining Your Enclosure
35
CARBON
Monthly (or more often as required)
Determine the actual face velocity through the sash opening of the
enclosure where the average reading should be at the specified velocity.
(Use calibrated thermal anemometer or other approved apparatus). Airflow
alarms are recommended for constant monitoring.
The enclosure rear baffle should be checked for any blockage to ensure that
the enclosure is maintaining proper airflow.
All weekly activities.
While the enclosure is filled with the contaminant, test filter condition on
carbon filters using the appropriate gas detector tube at intervals of 20% of
the total estimated time. The exception to the 20% recommendation is
formaldehyde or any carcinogen or suspected carcinogen. These hazardous
chemicals must be checked at least every 10% of the total estimated time.
Gas detector tubes for the specific chemicals that are being used in the
enclosure can be obtained from your laboratory supply dealer.
Replace carbon filters when chemical breakthrough is indicated by odor,
time, detector tube, or for some chemicals, analytical instrumentation. See
“Replacing Carbon Filters” section of this manual in Chapter 6.
Annually
Replace the fluorescent lamps.
Have the enclosure speed and carbon filters (if equipped) validated by a
qualified certification technician.
All monthly activities.
Setting the Inflow Face Velocity with the
Speed Control Adjustment
1. The speed control is located behind the switched control panel. See Figure
6-1.
2. Adjust the speed control with a small Phillips screwdriver by turning the
screw counterclockwise to increase blower speed or clockwise to decrease
the blower speed. The speed control is very sensitive, so proceed with
caution.
3. Measure the inflow velocity per the averaging technique outlined in
Chapter 3 and adjust the speed control slowly for the desired speed. Allow
the speed to stabilize and re-measure the inflow velocity to confirm.
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Chapter 6: Maintaining Your Enclosure
36
Speed Control Adjusted Slowly
with Small Phillips Screwdriver
(CCW to Increase or CW to
Decrease
Exhausts to the Room
Figure 6-1
Speed Control Used on Integral Blower Protector Work Station
Guardian™ 500 Airflow Monitor Kit No.
3944700 or 3944701
The Guardian 500 Airflow Monitor is designed to continuously monitor airflow
through enclosures and fume hoods. This permanently installed device provides
both visual and audible alarms to alert the user of abnormal airflow conditions. A
green light on the front of the monitor indicates normal flow conditions. When flow
conditions lower than the set point are encountered, a flashing red light is activated
along with an audible alarm. To temporarily mute the audible alarm, press and
release the test/reset button. The Guardian 500 Airflow Monitor has a built-in
sensor, 3 relay inputs and 1 relay output. The relay inputs can be configured for
night setback, external alarm, and sash high alarm. The night setback features
disables the alarm. The relay output is configured for Low Air Alarm.
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37
1.
Air Inlet
A portion of the air coming into the enclosure passes
through the air inlet and across the flow sensors.
2.
Normal Flow Indicator
This green light indicates normal flow conditions.
3.
Alarm Indicator
This red light is activated approximately 10-30 seconds
after the low flow set point is reached. Low flow set
points are 10-20 fpm below normal flow.
4.
Mute Button
If no alarm is present, this button will cause the red
lamp to light and the audible alarm to sound. If an
alarm is present, the button will silence the audible
alarm.
5.
Adjustment for Alarm
Set Point
This potentiometer is used to set the low flow indicators
for the alarm. It is adjusted with a small screwdriver.
2
3 1 4
5
Figure 6-2
Component Identification
Guardian 500 Component Identification
See Figure 6-2 below.
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Chapter 6: Maintaining Your Enclosure
38
Guardian 500 Installation Procedure
1. The enclosure comes prepared to except the Guardian™ 500 Airflow
Monitor.
2. First remove the large 1.19" dia. gray hole plug. See Figure 6-3. See Figure
6-4 only to reference internal assembly of the airflow monitor. Locate the
elbow, locknut, and washer and install it in the 1.19" dia. hole per Figure 6-3
and Figure 6-4. The enclosure baffle pivots down to install the elbow, washer
and locknut.
3. Cut the 1" hose supplied with the kit to 15.5" approximate length and install
it between the airflow sensor and the elbow.
4. Secure the Guardian 500 Airflow Monitor to the enclosure with double stick
tape as shown in Figure 6-5. The airway passage between the alarm module
and the enclosure is now complete.
5. Locate the metal hose cover and install with double stick tape per Figure 6-5.
6. Locate the power supply transformer. One end should already be connected
to the two-pin connector labeled 15 VDC on the back of the alarm module
and through the strain relief bushing. If disconnected, then reconnect to
power the airflow monitor. Plug the 115V power supply into a standard
115V duplex receptacle, the back of the accessory FilterMate portable
exhauster or the back of the accessory light. For 230V, plug into a standard
receptacle with your specific outlet plug. (It is recommended that the
airflow monitor be connected directly to the FilterMate switched
auxiliary outlet so the airflow monitor is powered at the same time.)
7. Installation is now complete.
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39
Figure 6-3
Hole Plug and Mounting Screws Location
Remove Large 1.19"
Dia. Hole Plug
Install Elbow,
Locknut and
Washer
Chapter 6: Maintaining Your Enclosure
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Chapter 6: Maintaining Your Enclosure
40
Figure 6-4
Guardian 500 Details
Display
Guardian 500
Monitor
Guardian 500 Calibration Procedure
Each alarm module and enclosure/fume hood is unique and needs to be individually
calibrated in the field. The procedure for the adjustment is as follows:
1. Double check the installation to make sure that monitor and power supply are
properly installed.
2. Allow 10 minutes for the monitor to warm up once power has been connected.
3. Determine the low flow set point for your monitor. This is the value where the
monitor will first indicate a low flow condition. The red light will be on for this
value. Refer to your industrial hygiene officer for the proper low flow set point or
consult the table below.
4. Adjust your enclosure/fume hood airflow to the low flow set point as previously
determined. The exhaust flow can be lowered by adjusting the speed control on the
FilterMate or by using an adjustable damper on the exhaust blower. Typical alarm
conditions are set at face velocities of 10 to 20 feet per minute below the normal
operating conditions due to supply air and exhaust air fluctuations, as well as room
air cross drafts. See note 8 if the low airflow volume or sash opening cannot be
adjusted.
5. Using a properly calibrated thermoanemometer, determine the velocity through the
face of the enclosure by taking a detailed velocity traverse. Divide the face area
into equal increments. One reading per square foot of face area is normally
recommended for an accurate traverse. Compute the average velocity for this area.
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Chapter 6: Maintaining Your Enclosure
41
Enclosure Operating In Flow Speed
Alarm Condition Set Point Speed
100 fpm
80 - 90 fpm
80 fpm
60 - 70 fpm
60 fpm
40 - 50 fpm
6. If the red light alarm is on, slowly turn the adjustment screw counterclockwise until
the green light is activated. If the green light is on, slowly turn the adjustment
screw clockwise until the red light comes on. Slowly turn the adjustment screw
back until the red light is activated. It is important that these adjustments be done
in small increments, at intervals about 30 seconds apart to allow for delayed
reaction of the alarm itself. The alarm low flow set point should now be set and the
red light activated.
7. Readjust the enclosure airflow to its normal operating levels. The green light
should now be activated. Calibration is now complete.
8. Note: If the low airflow volume or sash opening cannot be adjusted, then a 1/4 to 1/3
of a turn counterclockwise can be adjusted to set the airflow alarm condition at 1025% below normal operating levels.
Guardian 500 Alarm Activation
The audio and visual alarm will activate approximately 10-30 seconds after an alarm condition is
detected. To temporarily mute the audible alarm, press and release the test/reset button.
NOTE: After an alarm condition has been detected, the red light will stay on. The
audible alarm will remain muted until airflow returns to normal levels.
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Chapter 6: Maintaining Your Enclosure
42
Figure 6-5
Guardian 500 Installation
Monitor
Enclosure
Accessory Light
Hose Cover
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Chapter 6: Maintaining Your Enclosure
43
Guardian™ Digital Kit No 3908800 or
3908801
Guardian Digital 1000 Operation
The Guardian Digital Airflow Monitor consists of the airflow sensor, the Alarm Unit
and the 15 VDC power supply. For 115V operation the alarm unit is powered by
plugging the power supply into the factory-prepared digital airflow monitor socket.
For 230V operation, the Alarm Unit is powered by plugging the power supply into a
building outlet. The alarm has “Enter”, “+”, and “-” buttons to program the monitor.
There is also a green LED “SAFE”, yellow LED “CAUTION”, and red LED
“LOW” with audible alarm for airflow conditions. The audible alarm can be
permanently muted if desired. The Guardian Digital 1000 Airflow Monitor displays
a face velocity value, provides an RS232 communications port to a PC or building
computer system, can be configured for external input connections such as night
setback or external alarm and provides up to three output relays that can be
configured. For complete detailed information, please refer to the separate Labconco
1000 Alarm User’s Manual provided with the enclosure.
Guardian Digital 1000 Installation Procedure
1. The enclosure comes prepared to accept the Guardian Digital airflow
monitor system.
2. First remove the large 1.19" dia. gray hole plug. See Figure 6-6. See
Figure 6-7 only to reference internal assembly of the airflow monitor.
Locate the elbow, locknut, and washer and install it in the 1.19" dia. hole
per Figure 6-6 and Figure 6-7. The enclosure baffle pivots down to install
the elbow, washer and locknut.
3. Cut the 1" hose supplied with the kit to 10.5" approximate length and
install it between the airflow sensor and the elbow.
4. Secure the Guardian Digital alarm to the enclosure with double stick tape
as shown in Figure 6-9. The airway passage between the alarm module and
the enclosure is now complete.
5. Locate the metal hose cover and install with double stick tape per Figure 6-8.
6. Locate the power supply transformer. One end should already be
connected to the two-pin connector labeled 15 VDC on the back of the
alarm module and through the strain relief bushing. If disconnected, then
reconnect to power the airflow monitor. Plug the 115V power supply into
a standard 115V duplex receptacle, the back of the accessory FilterMate
portable exhauster or the back of the accessory light. For 230V, plug into a
standard receptacle with your specific outlet plug. (It is recommended
that the airflow monitor be connected directly to the FilterMate
switched auxiliary outlet so the airflow monitor is powered at the same
time.)
7. Installation is now complete.
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Chapter 6: Maintaining Your Enclosure
44
Figure 6-6
Hole Plug and Mounting Screws Location
Remove Large 1.19"
Dia. Hole Plug
Install Elbow,
Figure 6-7
Digital 1000 Airflow Monitor Details
Display Digital
1000 Monitor
Airflow
Sensor
Locknut and
Washer
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Chapter 6: Maintaining Your Enclosure
45
Enclosure
Accessory Light
Monitor
Hose Cover
Figure 6-8
Digital 1000 Airflow Monitor Installation
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Chapter 6: Maintaining Your Enclosure
46
Low Air
Alarm
Set Point
Enclosure
Operating In
flow Speed
Low
Calibration
Set Point
High
Calibration
Set Point
40 - 50 fpm
60 fpm
40 - 60 fpm
100 – 120 fpm
60 - 70 fpm
80 fpm
50 - 90 fpm
100 – 150 fpm
80 – 90 fpm
100 fpm
50 – 110 fpm
100 – 170 fpm
Digital 1000 Calibration
1. Calibrate the airflow monitor according to the instruction manual that
comes with the kit. To successfully calibrate, it will be necessary to change
the face velocity by adjusting the airflow exhaust volume. The exhaust
volume can be adjusted with the speed control on the FilterMate or by
using an adjustable damper on the exhaust blower. Typical calibration
conditions are set at face velocity air sample differences of at least 20 feet
per minute. The airflow monitor is factory set to be calibrated with a
difference of at least 50 fpm and can be changed by changing the
“lower/higher air sample difference”. The following suggested in flow face
velocity speeds are recommended to successfully calibrate. Typical low air
alarms are set 10-20 fpm below operational speeds. Follow Step 2 below
and review the Labconco 1000 Alarm User’s Manual that comes with the
airflow monitor.
2. Go to setup and then CAL CONFIG MENU and change the “lower/higher
air sample difference” to 20 fpm. This will allow you to successfully
calibrate with values of a minimum of 20 fpm difference.
3. While in CAL CONFIG MENU, change the “sensor difference” from 10%
to 3%.
4. While in CAL CONFIG MENU, adjust the red low air alarm to the desired
setting such as 55 fpm. Then adjust the yellow “CAUTION or
WARNING” to 59 fpm. Then adjust the “CAUTION or WARNING” air
reset to 3 fpm. This sets the alarm condition.
5. To complete the CAL CONFIGURATION, be sure to enter “DONE”.
6. To start the calibration mode, use the Labconco 1000 Manual and enter
“CALIBRATION” mode on the display from the SETUP menu.
7. Follow the instructions on the display and alter the low exhaust volume
with the speed control on the FilterMate or exhaust damper. Measure the
average face velocity and enter the low value on the display. Be careful not
to block the opening. The low exhaust volume calibration will take about 5
seconds.
8. Now alter the high exhaust volume with the speed control on the FilterMate
or exhaust damper. Measure the average face velocity and enter the high
value on the display. The high value must be at least 20 fpm greater than
the low value. The high exhaust volume calibration will take about 5
seconds.
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Chapter 6: Maintaining Your Enclosure
47
CAUTION WARNING
“YELLOW LED” Setting
LOW ALARM
“RED LED”
Setting
Low Calibration
Set Point
Sash Open
(fpm)
High Calibration
Set Point
or Enclosure
Operating
Inflow Speed
Sash Closed
Range
user defined
(fpm)
Suggested
Set Point
(fpm)
Range
user defined
(fpm)
* Suggested
Set Point
(fpm)
8" Sash
Height
10" Sash
Height
43 – 53
51
40 – 50
48
27
23
60 fpm
63 – 73
67
60 – 70
64
37
30
80 fpm
83 - 93
83
80 - 90
80
47
37
100 fpm
9. Be sure to enter “DONE” after successfully completing the low and high
calibration set points.
10. Once calibration is completed, go to “RUN” and hit “ENTER”. The value
should read close to the high calibration set point.
11. To lower the face velocity to the operating point, simply alter the exhaust
volume with the speed control on the FilterMate or exhaust damper. Then
recheck the face velocity with an anemometer to confirm the display on the
digital airflow monitor.
Digital 1000 Alternate Calibration Procedure Constant Volume Conditions
1. To successfully calibrate, it will be necessary to change the face velocity by
opening and closing the enclosure’s sash. The airflow monitor is factory set
to be calibrated with a difference of at least 50 fpm and can be changed by
adjusting the “lower/higher air sample difference”. The in flow face
velocity speeds provided in the chart below are suggested to successfully
calibrate the Digital 1000.
2. Before proceeding with calibration, it will first be necessary to configure
the airflow monitor. Go to the setup and then CAL CONFIG MENU and
adjust the “lower/higher air sample difference” to 10 fpm. This will allow
you to successfully calibrate with minimum difference values of 10 fpm.
3. While in CAL CONFIG MENU, change the “sensor difference” from 10%
to 3%.
4. While in CAL CONFIG MENU, adjust the red low alarm to the desired
setting (See the chart below for range and suggested settings). Then adjust
the yellow “CAUTION or WARNING” to the desired setting (See the chart
below for range and suggested settings). Then adjust the “CAUTION or
WARNING” air reset to 3 fpm. This sets the alarm condition.
* Because of airflow fluctuations in a typical laboratory environment Labconco suggests
setting the “RED LED” low alarm set point to 20% below the enclosure’s operating speed.
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Chapter 6: Maintaining Your Enclosure
48
5. To complete the CAL CONFIGURATION, be sure to enter “DONE”. If
needed, refer to the Configuration procedure provided on the following page for additional details.
6. To start the calibration mode, enter “CALIBRATION” mode on the display
from the SETUP menu.
7. Follow the instructions on the display and simulate the low exhaust volume
by fully opening the sash. You may measure the average face velocity for
the low calibration set point or utilize the calculated value provided in the
chart above. The average face velocity for the low set point is accurately
measured by dividing the opening of the enclosure into equal area grids
consisting of at least 9 data collection points and measuring the velocity at
the center of each grid with a calibrated thermo anemometer. Enter the low
value on the display. Be careful not to block the opening. The low exhaust
volume calibration will take about 5 seconds.
8. Now simulate the high exhaust volume by fully closing the sash to its
normal operating position. Measure the average face velocity for the high
calibration set point to confirm that the source of constant air volume is
providing the desired face velocity for the enclosure. The average face
velocity for the high set point is accurately measured by dividing the
opening of the enclosure into equal area grids consisting of at least 3 data
collection points and measuring the velocity at the center of each grid with
a calibrated thermo anemometer. Enter the high value set point on the
display. The high value must be at least 10 fpm greater than the low value.
The high exhaust volume calibration will take about 5 seconds.
9. Be sure to enter “DONE” after successfully completing the low and high
calibration set points.
10. Once calibration is completed, go to “RUN” and hit “ENTER”. The value
should read close to the high calibration set point.
11. With the sash fully open, the Digital 1000 monitor should go into “RED
Note: Enter Button stores information and +/- Buttons allow for scrolling.
1. Push the “ENTER” Button on the face of the alarm until the “SET UP”
Menu is displayed.
2. Scroll to “SET UP” and hit “ENTER”.
3. The PASSWORD MENU displays (The Password is 0000). Press the
ENTER button repeatedly until the CAL CONFIG MENU is displayed.
4. In the CAL CONFIG MENU set the following:
* (Suggested Air Alarm Settings) Refer to the chart on the previous page for a
range of air velocity settings that may be used.
5. To complete the CAL CONFIG, be sure to enter “DONE”. You are
returned to the Main Menu.
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Chapter 6: Maintaining Your Enclosure
50
Guardian 1000 Digital Alarm
(Digital Display, LED’s, Keypads)
Airflow Sensor
Airflow Sensor
(2 Required)
Back of Guardian 1000
Digital Alarm Module
Route Sensor
Airflow Sensor
Airflow Sensor
Switched Auxiliary Power
Power Supply
Spacer
Figure 6-9
Guardian 1000 Digital Airflow Monitor
Outlet for Airflow Monitor
Cable here from
alarm Module to
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Chapter 6: Maintaining Your Enclosure
51
Determination of When to Replace
Carbon Filters and How to Replace
Both carbon filters MUST be replaced when any one of the following two
conditions are met:
1. The filtered enclosure outlet (exhaust) concentration approaches the inlet
concentration, indicating filter saturation.
2. The odor in the work area becomes intolerable or the concentration of the
chemical in the work area is greater than the TWA.
There are four means of determining when its time to change the carbon filters (not
shown in the order of preference).
Odor - A person’s sensitivity to odor, tolerance of odor and their comfort level
under odoriferous conditions vary with the individual. While odor is an indicator
that chemicals are passing through the carbon filter, several points need to be
understood:
Odor within the room is not necessarily an indication of saturation or
hazardous exposure concentrations.
Odor can be used as a prompt to sample the chemical concentration on the exit
side of the carbon filter.
Organic chemicals approved for use in the filtered enclosure have odors that
are detectable before reaching the time weighted exposure limits.
Detection Tubes - Color change indicators can be used to measure the
concentration of the chemical at the exit side of the carbon filter or in the outlet
exhaust. A kit including syringe pump and flexible tubing can be purchased as an
accessory from Labconco (Catalog # 6924900). Labconco Customer Service
Representatives are supplied with detector tube catalog numbers, as well as
telephone numbers to direct you to where to purchase these items.
For Organic, Formaldehyde and Ammonia, chemical specific detector tubes should
be purchased when installing fresh filters. Each kit contains instructions on how
many strokes of the syringe are required to obtain the stated sensitivity. The
sampling syringe is connected to the filtered enclosure exhaust. Connect the
syringe to the detector tube while the system is running and pull the air through the
tube with the syringe. Each stroke of the syringe represents a 100-ml sample and
corresponds to the number of strokes necessary to give the indicated color changes.
Due to the wide variety of organics and varying TWA’s, it is recommended that
specific detector tubes be purchased directly from Sensidyne, Draeger or your
laboratory supply dealer. Alternate detector pumps can also be purchased from
your laboratory supply dealers. The vast majority of detector tubes available start
measuring at the TWA. When a user observes a color change in the tube, they
should replace the filter immediately. If no detector tube for your specific
chemical is available, other means of detection must be used.
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Chapter 6: Maintaining Your Enclosure
52
Time - For applications that have very consistent inlet concentrations and
operating time, “Time” can be used to anticipate saturation or TWA levels based
on prior experience. However, this does not replace the need for sampling.
Consult Labconco technical specialist for an estimate of carbon filter life based on
chemical usage. Detector tubes, or analytical instrumentation should always be
used to determine concentrations in the carbon filter. It is recommended that the
carbon filters be checked with detector tubes or other means at intervals of 20% of
the total estimated filter life. The exception to the 20% recommendation is
formaldehyde and any carcinogen or suspected carcinogen. These more hazardous
chemicals must be checked at least every 10% of the total estimated time.
Analytical Instrumentation - This is the most accurate means of measuring
concentrations of any chemical. It is the method of choice when no detector tubes
are available or the tubes are not sensitive enough to measure at the TWA
concentration for the chemical. This method is also to be used to determine
saturation when the chemical concentration is below the measurement range of
detector tubes.
Carbon Filter Replacement Procedure – See Figure 6-10 for Carbon Filter
Replacement.
1. The carbon filters are replaced by first removing the two knobs, which hold
the rear perforated baffle in place. Then carefully lower the perforated
baffle, which is heavy because of the carbon filters.
2. Carefully remove both carbon filters.
3. If using formaldehyde, the formaldehyde filter is always placed
downstream of the organic vapor filter. (The formaldehyde filter is on top
of the organic vapor filter in the loading position. The same applies with
ammonia and formaldehyde. No specific placement is required with
organic vapor and ammonia.
4. Re-install the new carbon filters with the gasket up or on the downstream
side.
5. Pivot the perforated baffle up and replace and tighten the knobs.
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Chapter 6: Maintaining Your Enclosure
53
Knob for Releasing
Carbon Filters
First Carbon Filter
First Carbon Filter
Gasket
Handle to Lower
Perforated Baffle
Second Carbon Filter
Perforated Baffle Pivot
Motorized Impeller located
here after both carbon filters
Figure 6-10
Carbon Filter Replacement
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Chapter 6: Maintaining Your Enclosure
54
Number
of
Filters
Filter Size
Pounds of
Formasorb
Carbon
Adsorbed weight of
Formaldehyde
Adsorption
Volume of
Formalin
1
36 x 18 x 1
13.3
1.33 lbs./604g
1512 ml
= 7.8 weeks before filter saturation
=. 17 ml/min
Calculating Carbon Filter Life
Labconco developed a modeling program to estimate the filter life for typical
carbon filters. Since filter life is dependent on the chemical used, the airflow, filter
size, and the dwell time, refer to the Chemical Guide for the Paramount® Filtered
Enclosure. The estimated life for carbon filters for the Protector Work Stations
with integral blower is conservatively calculated at 50% or half of the published
values for the Paramount in the Chemical Guide. For example, if you use
isopropyl alcohol to disinfect and use approximately 100 ml per week during 2
hours of use per day then follow these steps to calculate the concentration in parts
per million (ppm). Important: Two filters are always required for operation. If
mixing filter types, then use 25%.
Steps for Calculating PPM and Filter Life
1. Determine the amount of the proposed chemical lost to evaporation over a
given amount of time. For example, if you use isopropyl alcohol and lose
approximately 100 ml per week during 2 hours of use per day.
2. Convert the amount lost into ml/min. For this example:
100 ml X 1 week X 10 hours = 100 ml lost
week 10 hours use 600 minutes 600 minutes
3. Convert ml/min to PPM by multiplying ml/min by the conversion factor
found in the second to the last column on the right. For isopropyl alcohol
.17 x 41 = 7.0 PPM.
4. Find the PPM value on the chart that comes closest to the value you just
calculated in step #3. In this example, round up to 10 PPM, which is close
to the calculated 7.0. We may approximate the filter life to be around 155
hours of actual use, but use 50% of this for the filters or 78 hours.
5. Insert the estimated filter life into the estimated usage to determine how
long filters will last.
78 hours filter life
10 hours per week use
6. These values are for two organic vapor filters. If mixing the filters with
formaldehyde or ammonia, then use 25% instead of 50%.
Formaldehyde only
For formaldehyde, use 10% of the impregnated carbon weight. Formalin is 37%
formaldehyde by weight. The density of formalin is 1.08 g/ml. These values are
for one filter. If using two filters, then double the adsorption volume.
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Chapter 6: Maintaining Your Enclosure
55
Number
of
Filters
Filter Size
Pounds of
Ammonasorb
II Carbon
Adsorbed weight of
Ammonia
Adsorbed
Volume of 50%
Ammonia
Solution
1
36 x 18 x 1
15.2
1.52 lbs./ 690 g
1382ml
!
Ammonia only
For ammonia, use 10% of the impregnated carbon weight. Assume use of a 50%
solution of ammonia for these calculations. These values are for one filter. If
using two filters, then double the adsorption volume.
Fluorescent Light Replacement
1. Disconnect the power.
2. Locate the two Phillips machine screws on top of the light and remove.
Lift up the light assembly.
3. Rotate and remove the old fluorescent lamp.
4. Reinstall the new fluorescent lamp and screws in reverse order.
5. Power the unit up and try the new fluorescent lamp.
Motorized Impeller Replacement
The motorized impeller must be replaced as a complete unit. When the motorized
impeller is replaced, the capacitor may also be replaced. See Appendix A for
Replacement Parts Diagram. See Figure 6-11 for an isometric view of the
motorized impeller.
Do NOT contact blower wheel while still in motion.
NE PAS être en contact avec la roué du ventilateur tant qu’il est
en marche.
1. Wear appropriate personal protective equipment to decontaminate the filtered
enclosure and then unplug from the electrical outlet.
2. Lower carbon filters per removal procedure outlined in this chapter.
3. Consult the wiring diagram in Appendix C of the manual and disconnect all the
wires of the motorized impeller. Be sure to connect wires on the new motor in
the same way the old motor was wired.
4. Remove the machine screws that support the plenum pan with the air intake
hole for the motorized impeller.
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Chapter 6: Maintaining Your Enclosure
56
Figure 6-11
Motorized Impeller Replacement
Motorized Impeller and Motor Bracket
located behind Plenum Pan
Motorized Impeller
Inlet
Machine Screws to
support Plenum Pan
Plenum Pan
!
5. Remove four nuts in the motor bracket and the four screws and lockwashers to
the bracket.
ATTENTION: High-speed blower. Never operate impeller
with housing off.
6. Replace the capacitor with a new one of equal voltage and capacity.
7. Reassemble the new motorized impeller by reversing the assembly steps.
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Chapter 6: Maintaining Your Enclosure
57
Speed Control Replacement
1. Follow the procedure to replace the fluorescent light to access the speed
control.
2. Remove the light reflector after following the light removal procedure. This
allows access to the speed control.
3. Remove the two nuts holding the speed control. Refer to Appendix A for
Replacement Parts Diagram.
4. Disconnect all wires leading to the speed control. Connect wires on new speed
control in the same position as the old speed control.
5. Reassemble to the system in the same position and with the same screws that
were removed earlier.
Product Service 1-800-522-7658
58
Catalog #
Description
Dimensions (W x D x H)
6942003
Black w/sink, 4-foot wide
48" x 26.75" x 1.25" includes
valves HOT/CW gooseneck
and sprayer
3908402
Black, 4-foot wide
48" x 26.66" x 1.00"
Chapter 7:
Accessorizing and Modifying
Your Enclosure
There are several ways to accessorize the enclosure for your individual
requirements. These include the addition of accessory work surfaces, airflow
monitors, exhaust transition adapters, remote blowers, exhaust dampers,
FilterMate Portable Exhausters, carbon filters, storage cabinets, stands and
utility shelf kit.
1. Work Surfaces
An optional dished work surface is available to attach to the enclosure.
Dished work surfaces are contoured to fit the dimensions of the Protector
Work Stations to contain spills. Epoxy is chemical resistant. Work
surfaces are available either with or without a sink. See Chapter 3 for
illustrations and below for dimensions of work surfaces. See Appendix B
for Protector Work Station dimensions.
NOTE: 6942003 Work Surface with sink may be mounted on Base Stands
3746702 or 3746712.
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Chapter 7: Accessorizing & Modifying Your Enclosure
59
Spray hose
with nozzle
1.25"
11"
4.38"
6.5"
work surface
gooseneck
faucet
15"
9.75"
48"
9.35"
2.7"
9.75"
3"
26.75"
17.25"
3.5"
faucet
controls
3.5"
TOPVIEW
RIGHT SIDE
FRONT
TOP
6942003 Work Surface with Sink
Fabricated from durable epoxy resins, this unique work surface is designed to
accept standard dissecting boards and is dished to contain spills. It resists
corrosion and will not stain or absorb liquids. Easy to clean, the work surface
comes with a 10" x 14" x 6" deep molded epoxy sink. Fixtures include a
chrome-plated gooseneck faucet with vacuum breaker, two chrome-plated
faucet controls, and a spray nozzle with hose. Sink requires a 1.5" drain
connection. 48" w x 26.75"d x 1.25" thick. Shipping weight 115 lbs (52 kg).
This work surface may be mounted on Telescoping Base Stand 3746702 or
3746712.
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Chapter 7: Accessorizing & Modifying Your Enclosure
60
Catalog #
Description
3944700
Guardian 500 Airflow Monitor, 115V, 60 Hz
3944701
Guardian 500 Airflow Monitor, 230V, 50 Hz
3908800
Guardian 1000 Digital Airflow Monitor 115V, 60 Hz
3908801
Guardian 1000 Digital Airflow Monitor 230V, 50 Hz
Catalog #
Description
Material
3912400
Upper connection, 5" Hose
Coated Steel, Epoxy Coated
3912401
Upper connection, 6" Duct
Coated Steel, Epoxy Coated
3912402
Lower connection, 5" Hose
Coated Steel, Epoxy Coated
3912403
Lower connection, 6" Duct
Coated Steel, Epoxy Coated
CFM @ Static Pressure-Inches of H2O
S.P.
0.0"
0.125"
0.25"
0.50"
0.75"
0.87"
CFM
595
560
515
420
300
167
Catalog #
Description
Shipping Wt.
(lbs./kg.)
4863500
Remote Blower, 115 V, 60 Hz. 4.4 amps
35/16
4863501
Remote Blower, 115/230 V, 50 Hz, 5.6/2.8 amps
35/16
7053501
Explosion-Proof Remote Blower, 115 V, 60 Hz,
4.4 amps
40/18
2. Guardian™ 1000 Digital Airflow Monitor or Guardian™ 500 Airflow
Monitor
The Guardian 1000 Digital Airflow Monitor or Guardian 500 Airflow
Monitor allows you to continuously monitor airflow through the enclosure.
The rear exhaust plenum and upper light is factory prepared to mount either
monitor.
Adapter connects to the enclosure (on remote Protector Work Stations)
from either the top or the bottom of the rear plenum so the duct can be
routed either up or down, respectively. The transition is available for either
5.00" ID hose or 6" OD duct. The 5.00" ID hose upper connection is
standard and included with the FilterMate.
4. Remote Blowers (For Remote Protector Work Station Only)
Has a 1/4 hp direct drive motor and corrosion-resistant epoxy-coated steel
housing and wheel with blower inlet of 6.00" ID. Outlet dimensions are
4.25" x 7.38" OD.
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Chapter 7: Accessorizing & Modifying Your Enclosure
61
Catalog #
Description
3924000
6" Epoxy Coated Steel In-Line adjustable damper
4724200
6" PVC In-line adjustable damper
Catalog #
Voltage
Filter
Exhaust
Connection
Exhaust
Airflow
(cfm)
3970000
115 Volt/60 Hz
HEPA
None
280
3970001
115 Volt/60 Hz
Carbon
None
280
3970002
115 Volt/60 Hz
HEPA
Thimble to outside
280
3970003
115 Volt/60 Hz
HEPA/Carbon
None
220
3970004
115Volt/60 Hz
Carbon/Carbon
None
220
3970020
230 Volt/50 Hz
HEPA
None
280
3970021
230 Volt/50 Hz
Carbon
None
280
3970022
230 Volt/50 Hz
HEPA
Thimble to outside
280
3970023
230 Volt/50 Hz
HEPA/Carbon
None
220
3970024
230Volt/50 Hz
Carbon/Carbon
None
220
Figure 7-1
5. Exhaust Dampers (For Remote Protector Work Station Only)
Exhaust dampers allow an adjustment required to maintain proper airflow
for roof-mounted blowers or house exhaust systems.
6. FilterMate Portable Exhausters and Filters (For use with Remote
Protector Work Station Only)
For filtered exhaust, Labconco offers FilterMate Portable Exhausters
capable of exhausting up to 280 cfm of HEPA or carbon filtered air or up to
220 cfm of combination HEPA/Carbon or Dual Carbon filtered air when
connected to the enclosure.
HEPA Filter (For FilterMate Only)
Part #3707900 is 99.99% efficient on particles 0.3 micron.
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Chapter 7: Accessorizing & Modifying Your Enclosure
62
Filter Classification
Part #
x Pounds
Organic
3923400
12.0 lbs. activated carbon
Formaldehyde
3923401
14.0 lbs. impregnated carbon
Ammonia
3923402
16.0 lbs. impregnated carbon
Catalog
Number
Filter Size
Pounds of
Carbon
Carbon Type
For Use With
Adsorbtion
Weight
Adsorbtion
Volume
3924200
18 x 36 x 1
11.0
RL10 Organic
Vapor
Organic Vapors
Varies, see
Chemical
Guide
Varies, See
Chemical Guide
and Chapter 6
3924201
18 x 36 x 1
13.3
Impregnated
Formasorb
Formaldehyde
10%, 1.33 lbs.
1512 ml of 37%
Formalin
3924202
18 x 36 x 1
15.2
Impregnated
Ammonasorb II
Ammonia
and
Amines
10%, 1.52 lbs.
1382 ml of 50%
Ammonia
Solution
HEPA Filter Bag-In/Bag-Out Bag (For FilterMate Only)
Part #3776002 helps contain hazardous particulate matter during filter
changing operations.
Carbon Filter (for FilterMate Only)
Provides granular activated carbon or impregnated carbon.
7. Carbon Filters (Only for Protector Work Station with Integral Blower)
IMPORTANT NOTE: Two filters are always required or a
combination of filters. If using formaldehyde and organic vapor, the
formaldehyde filter is placed downstream of the exhaust of the organic
vapor filter.
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Chapter 7: Accessorizing & Modifying Your Enclosure
63
SOLVENT
ACID
Size/Description
Dual Doors
Right Hinge
Left Hinge
Dual Doors
Right Hinge
Left Hinge
48"
9902000
-
-
9901000
-
-
36"
9902100
-
-
9901100
-
-
30"
9902200
-
-
9901200
-
-
24" - 9902300
9902400
-
9901300
9901500
18" - - - -
9901400
9901600
12" - - - - - -
48" w/Self-Closing Doors
9903000
- - - - -
36" w/Self-Closing Doors
9903100
- - - - -
30" w/Self-Closing Doors
9903200
- - - - -
24" w/Self-Closing Doors
-
9903300
9903400
- - -
24" ADA
-
9906000
9906100
-
9905000
9905200
24" ADA w/Self-Closing
Doors
-
9906200
9906300
- - -
18" ADA - - - -
9905100
9905300
12" ADA - - - - - -
STANDARD BASE
VACUUM PUMP
Size/Description
Dual Doors
Right Hinge
Left Hinge
Dual Doors
Right Hinge
Left Hinge
48"
9900000
- - - - -
36"
9900100
- - - - -
30"
9900200
- - - - -
24" - 9900300
9900600
- - -
18" - 9900400
9900700
-
9907000
9907100
12" - 9900500
9900800
- - -
48" w/Self-Closing Doors
- - - - -
-
36" w/Self-Closing Doors
- - - - -
-
30" w/Self-Closing Doors
- - - - -
-
24" w/Self-Closing Doors
- - - - -
-
24" ADA
-
9904000
9904300
- - -
24" ADA w/Self-Closing
Doors
- - - - -
-
18" ADA
-
9904100
9904400
- - -
12" ADA
-
9904200
9904500
- - -
Stands
3746702
Telescoping Stand with Fixed Feet, 48" x 29" x 27.5" to 33.5"
3746712
Telescoping Stand with Locking Casters, 48" x 29" x 27.5" to 33.5"
8. Storage Cabinets and Stands
9. Utility Shelves 3925000
Three shelves hold items inside the enclosure. One shelf may be used for
the printer, one shelf for spatulas and weigh brushes, and one
miscellaneous shelf. The shelves hang from slots in the rear baffle.
Product Service 1-800-522-7658
Chapter 7: Accessorizing & Modifying Your Enclosure
64
Catalog #
Description
4868600
8 Feet of 5" ID gray flexible polypropylene hose (included with
FilterMate). General purpose chemical resistant hose suitable in
pharmaceutical applications.
1921000
5" T-Bolt Hose Clamp (two included with FilterMate)
3927500
8 Feet of 5" ID Clear smooth bore static dissipation hose with two hose
clamps. Suitable in clean rooms or pharmaceutical applications.
3927600
8 Feet of 6" ID Black thermoplastic hose with two 6.09" ID cuffs.
Includes two 6" hose clamps. Suitable for connection to house exhaust
and pharmaceutical applications.
1921500
6" T-Bolt Hose Clamp
10. Hoses, Hose Clamps, and Hose Kits
Provides alternatives for ducting.
Product Service 1-800-522-7658
65
PROBLEM
CAUSE
CORRECTIVE ACTION
Contaminants outside
of enclosure.
Improper user
techniques for the
enclosure.
See “Certifying the Enclosure” Chapter
3 and “Safety Precautions” Chapter 4
sections in the manual. (Ref. Appendix
D).
Restriction of the
baffle air slots or
blockage of the
exhaust outlet.
Remove obstruction to ensure that all
air slots and the exhaust outlet are
unobstructed.
External factors are
disrupting the
enclosure airflow
patterns or acting as a
source of
contamination.
See “Location Requirements” Chapter
2, “Certifying the Enclosure” Chapter
3, and “Safety Precautions” Chapter 4
sections of this manual. (Ref. Appendix
D).
Enclosure has
improper face
velocity.
Have enclosure certified and check
exhaust system. Check carbon filters
for loading. Check accessory
FilterMate HEPA filters for loading.
Adjust enclosure speed control.
Enclosure should have an average face
velocity of 60-100 fpm.
Chapter 8:
Troubleshooting
Refer to the following table if your Protector Work Station fails to operate
properly. If the suggested corrective actions do not solve your problem, contact
Labconco for additional assistance.
Product Service 1-800-522-7658
Chapter 8: Troubleshooting
66
PROBLEM
CAUSE
CORRECTIVE ACTION
Blower won’t
operate.
Unit not plugged
into outlet.
Plug the enclosure into appropriate
electrical service.
Circuit breaker(s)
or Ground Fault
Interrupter.
Reset circuit breaker.
Blower wiring is
disconnected.
Inspect blower wiring.
Blower switch is
defective.
Replace switch.
Motorized impeller
or blower is
defective.
Replace motorized impeller or blower. See
Chapter 6.
Low face velocity
or poor
containment of
contaminants.
Enclosure sash not
closed.
Close sash to the lowest position.
HEPA filter
clogged on
FilterMate.
Replace HEPA filter or increase speed.
Carbon filter loaded
with chemicals.
Replace carbon filter.
Blower and lights
won’t operate.
Unit not plugged
into outlet.
Plug enclosure into appropriate electrical
service.
Circuit breaker(s)
tripped.
Reset or replace circuit breaker.
Lights do not work.
Lamp not installed
properly.
Inspect lamp installation.
Lamp wiring
disconnected.
Inspect lamp wiring.
Defective lamp.
Replace lamp.
Light switch is
defective.
Replace light switch.
Defective electronic
ballast.
Replace ballast.
Airflow monitor
malfunction.
No power.
No lights.
No display.
Power cable to circuit board is
disconnected and needs to be connected.
Sensor cable needs to be connected. Power
supply is not plugged into proper voltage;
plug in power supply. Verify that all
airflow monitor interface cables are
connected. Check circuit breaker on
enclosure.
No audible alarm.
Alarm has been temporarily silenced using
“SILENCE ALARM” or “enter” buttons.
Product Service 1-800-522-7658
Chapter 8: Troubleshooting
67
PROBLEM
CAUSE
CORRECTIVE ACTION
Airflow Monitor
Malfunction
(Continued)
Wrong alarm set
point.
Airflow monitor was not properly
adjusted. Repeat calibration steps
outlined in this manual in Chapter 6
or in the supplied Guardian 1000
Digital Monitor Manual.
Constant audible
alarm.
Check airflow and calibration of
airflow monitor. See Chapter 6.
Continuous alarm.
Check the face velocity of the
enclosure as the airflow of the
system may have changed. If
incorrect, adjust the speed control to
increase face velocity. The HEPA
filter on the accessory FilterMate
may have become loaded. If face
velocity is correct, calibrate the
airflow monitor outlined in this
manual in Chapter 6.
Monitor alarms; air
way to airflow
monitor sensor is
blocked by insects,
dust or debris.
Lightly clean the airway with clean
air. Be careful not to touch sensitive
electrical components.
Audible disable
will not stay
operational.
An alarm condition must be
continuously present before the
audible alarm can be silenced. If
flow conditions fluctuate near the
alarm set point, the airflow monitor
will automatically reset it. Action
should be taken to bring the
enclosure airflow into proper
operating parameters or adjust the
alarm set point lower.
Product Service 1-800-522-7658
68
Appendix A:
Enclosure Components and
Replacement Parts
The components that are available for your Protector Work Station are listed. The
parts shown are the most commonly requested. If other parts are required, please
contact Product Service.
Product Service 1-800-522-7658
Appendix A: Enclosure Components & Replacement Parts
69
Item
Qty.
Part Number
Description
1 1 3906500
Glass, Side
2 1 3906102
Glass, Sash 4'
3 1 3905202
Sash Assembly, 4'
4 1 3905602
Lower Air Foil, 4'
5A 1 3929800
Bracket, Air Foil R.H.
5B 1 3929801
Bracket, Air Foil L.H.
6A 1 3907500
Stop, Sash R.H.
6B 1 3907501
Stop, Sash L.H.
7A 1 6916500
Latch, Sash
7B 1 3906700
Bracket, Latch
7C 1 1927403
Spring, Compression Latch
7D 2 1893206
Screw, 8-32 x .38" Lg. Phillips Pan S.S. Type F
8A 2 1889316
Screw, 10-24 x 1.00 PH Phil SS
8B 2 1912108
Washer, Plastic .194 ID x .380 OD
8C 2 7868402
Bushing, Spacer .31 x .63
9
2.3 Ft.
6913700
Wiper Seal, Sash
10A 2 1936800
Bushing Heyco Closed 1.50 Dia.
10B 2 1934601
Bushing, Heyco with Flex Shutter 1.50 Dia.
11A 2 3915400
Side Air Foil
11B 4 1889912
Screw #6-32 x .75" Oval HD Type F S.S.
12A 1 3932100
Reflector, Light 4'
12B 8 1894808
Screw, Deflector #8 x ½ PH
13 1 9721901
Lamp, Fluorescent 4' (F25T8)
14A 1 3932200
Wiring Harness, Main 115V
14B 1 3932201
Wiring Harness, Main 230V
15 1 3929300
Label, Front Protector Work Station
16 2 1307000
Rocker Switch, 2 Position
17A 1 3921700
Motorized Impeller, 115V
17B 1 3921701
Motorized Impeller, 230V
18A 1 1306600
Capacitor, 115V 15 MFD
18B 1 1306800
Capacitor, 230V 4 MFD
19 1 1294000
Ballast, Fluorescent 115V or 230V
20A 1 3922100
Speed Control, 115V
20B 1 3922101
Speed Control, 230V
21A 2 3924200
Carbon Filter, Organic Vapor 18x36x1
21B 2 3924201
Carbon Filter, Formaldehyde 18x36x1
21C 2 3924202
Carbon Filter, Ammonia 18x36x1
22A 1 1334500
Power Cord, Main 115V
22B 1 1334100
Power Cord, Main 230V
23A 1 1327201
Circuit Breaker, 10A
23B 2 1327204
Circuit Breaker, 5A
Product Service 1-800-522-7658
Appendix A: Enclosure Components & Replacement Parts
70
Item
Qty.
Part Number
Description
24 1 1306000
Integral Blower Power Cord, IEC
25 1 1595619
Hole Plug, 0.50 Dia.
26 1 1595621
Hole Plug, 1.187 Dia.
27 2 1879400
Knob, Perforated Baffle Integral Blower
28A 1 3931500
Perforated Baffle Assy, Integral Blower
28B 2 3931600
Baffle Support
29 1 3938400
Perforated Baffle, Remote Blower
30 1 3929200
Wiring Harness, Integral Blower
31 2 3932700
Standoff, Light Support, ½ Hex x 10-24
32A 1 3913100
Cover Plate, Remote Exhaust
32B 2 1893008
Screw, #8-32 x .50 Self-Tapping
Product Service 1-800-522-7658
Appendix A: Enclosure Components & Replacement Parts
71
31, Internal
28
30, Internal
Guardian 1000 Digital Monitor
16
13, Not Shown
27, Not Shown
12
21
9
1
15 7 3 2 6
11
4
5
Guardian 1000 Digital
Monitor
20
24
19, Internal
23
22
14, Internal
Guardian Digital
Sensor
26
17, 18, Internal
25
30, Internal
Product Service 1-800-522-7658
Figure A-1
Protector Work Station with Integral Blower
Appendix A: Enclosure Components & Replacement Parts
72
Figure A-2
Protector Work Station for use with Remote Blower
6" Exhaust Collar Shown
Guardian 500 Monitor
16
29
13, Not Shown
12
8
9
1
31, Internal
15 7 3 2 6
11
4
15 Guardian 500 Monitor
20
22
14, Internal
19, Internal
6" Exhaust Collar Shown
26
25
5
10
32
23
24
Product Service 1-800-522-7658
73
Appendix B:
Dimensions and
Exhaust Options
Product Service 1-800-522-7658
Appendix B: Dimensions & Exhaust Options
74
B-1
Product Service 1-800-522-7658
75
Appendix C:
Protector Work Station
Specifications
This Appendix contains technical information about all the Protector Work Station
enclosures including electrical specifications and environmental operating conditions.
Indoor use only.
Maximum altitude: 6562 feet (2000 meters).
Ambient temperature range: 41° to 104°F (5° to 40°C).
Maximum relative humidity: 80% for temperatures up to 88°F (31°C),
decreasing linearly to 50% relative humidity at 104°F (40°C).
Main supply voltage fluctuations not to exceed ±10% of the nominal
voltage.
Transient over-voltages according to Installation Categories II (Over-
voltage Categories per IEC 1010). Temporary voltage spikes on the AC
input line that may be as high as 1500V for 115V models and 2500V for
230V models are allowed.
Used in an environment of Pollution degrees 2 (i.e., where normally only
non-conductive atmospheres are present). Occasionally, however, a
temporary conductivity caused by condensation must be expected, in
accordance with IEC 664.
Product Service 1-800-522-7658
76
Model Size
4'
Sash Height from Work Surface (inches)
8.00
Total Open Area with Bypass (sq. ft.)
2.50
Exhaust Airflow Volume at 80fpm (CFM)
200
Alarm Airflow Volume at 60 fpm (CFM)
150
*Motor Horsepower (HP)
0.30
*Capacitor (MFD, Volts)
15MFD, 115V
4MFD, 230V
Fluorescent Lights
F25T8
Appendix D:
Quick Chart for the Protector
Work Stations
*excludes remote Protector Work Station, since it has no integral blower.
To determine the actual face velocity at the sash opening, airflow velocity readings
will need to be taken. This should be done across the sash opening of the
enclosure in accordance with the Industrial Ventilation Manual. (See Appendix E)
The “average face velocity” is achieved by taking readings in two rows across the
enclosure with the readings 6" from the ends and evenly spaced every 12"; the first
row is 3" down from the upper sash foil and the second row is 3" up from the work
surface. A total of eight readings are taken for the 4' Protector Work Station and
then averaged.
Product Service 1-800-522-7658
77
Appendix E:
References on Ventilation,
Safety, Occupational Hazards,
Biosafety & Decontamination
Many excellent reference texts and booklets are currently available. The following
is a brief listing:
Laboratory Ventilation Standards
Federal Register 29 CFR Part 1910
Non-mandatory recommendations from “Prudent Practices.”
Fume hoods should have a continuous monitoring device
Face velocities should be between 60-100 linear feet per minute (lfpm)
Average 2.5 linear feet of hood space per person
Occupational Health and Safety
U.S. Department of Labor
200 Constitution Avenue N.W.
Washington, DC 20210
(202) 523-1452
www.osha.gov
Industrial Ventilation-ACGIH
Fume hood face velocities between 60-100 lfpm
Maximum of 125 lfpm for radioisotope hoods
Duct velocities of 1000-2000 fpm for vapors, gasses and smoke
Stack discharge height 1.3-2.0 x building height
Well designed fume hood containment loss, <0.10 ppm
Industrial Ventilation, A Manual of Recommended Practice.
24th Edition, 2001
American Conference of Governmental Industrial Hygienists
1330 Kemper Meadow drive
Cincinnati, OH 45240-1634
(513) 742-2020
www.acgih.org
Product Service 1-800-522-7658
Appendix E: References
78
ASHRAE 110-1995 Method of Testing Performance of Fume Hoods
Evaluates fume hood’s containment characteristics
Three part test: Smoke generation, Face velocity profile, Tracer gas release @ 4 liters
per minute
Rated As Manufactured (AM), As Installed (AI) and As Used (AU)
American Society of Heating, Refrigerating, and Air Conditioning Engineers
1791 Tullie Circle N.E.
Atlanta, GA 30329
(404) 636-8400
www.ashrae.org
ANSI Z9.5-1993 Laboratory Standard
Covers entire laboratory ventilation system.
Vertical stack discharge @ 2000-3000 fpm
New and remodeled hoods shall have a monitoring device
Ductless hoods should only be used with non-hazardous materials
Fume hood face velocities between 80 – 120 fpm
American Industrial Hygiene Association
2700 Prosperity Avenue, Suite 250
Fairfax, VA 22031
(703) 849-8888
www.aiha.org
SEFA 1-2002
Fume hood face velocities based on toxicity levels of chemicals
Class A – 125 to 150 fpm
Class B – 80 to100 fpm
Class C – 75-to 80 fpm
Test method – face velocity profile and smoke generation
Scientific Equipment & Furniture Association
1028 Duchess Drive
McLean, VA 22102
(703) 538-6007
www.sefalabs.com
NFPA 45 – 2002 Fire Protection for Laboratories Using Chemicals
Laboratory hoods should not be relied on for explosion protection
Exhaust air from fume hoods should not be recirculated
Services should be external to the hood
Canopy hoods only for non-hazardous applications
Materials of construction should have flame spread of 25 or less
80 to 120 fpm to prevent escape
NFPA 30 – 2000 Flammable and Combustible Liquids Code
Approved cabinets may be metal or wood
Vent location on cabinets are required
Venting of cabinets not a requirement
National Fire Protection Association
1 Batterymarch Park
P.O. Box 9101
Quincy, MA 02269-9101
(800) 344-3555
www.nfpa.org
Product Service 1-800-522-7658
Appendix E: References
79
General References
American Conference of Governmental Industrial Hygienists. Industrial Ventilation, A
Manual of Recommended Practice, Cincinnati, OH
ASHRAE Standard Committee. ASHRAE Standard Atlanta: ASHRAE Publications Sales
Department, 1995
British Standards Institution, Laboratory Fume Cupboards. Parts 1, 2 and 3, London: 1990
Department of Labor, Occupational Safety and Health Administration, 29 CFR Part 1910, Occupational Exposures to Hazardous Chemicals in Laboratories, Final Rule. Vol. 55,
No. 21. Washington D.C.:1990
DiBerardinis. L. et al. Guides for Laboratory Design, Health and Safety Considerations.
Wiley & Sons, 1987
McDermott, Henry, Handbook of Ventilation for Contaminant Control, 2nd Edition.
Butterworth Publishers, 1985.
NIH Guidelines for the Laboratory Use of Chemical Carcinogens. NIH Publication No.
81-2385.
Sax, N. Irving and Lewis, JR., Richard J. Rapid Guide to Hazardous Chemicals in the Workplace. Van Nostrand Reinhold, 1987.
Schilt, Alfred A. Perchloric Acid and Perchlorates. The G. Frederick Smith Chemical
Company, Columbus, OH: 1979.