Labconco Paramoun Ductless Enclosures User Manual

Labconco Corporation 8811 Prospect Avenue Kansas City, MO 64132-2696 800-821-5525, 816-333-8811 FAX 816-363-0130 E-MAIL labconco@labconco.com HOME PAGE www.labconco.com
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User’s Manual
Paramount® Ductless Enclosures
Models
69632 Series, 2' Widths 69633 Series, 3' Widths 69634 Series, 4' Widths 69635 Series, 5' Widths
69636 Series, 6' Widths
Please read the User’s Manual before operating the equipment.
Copyright © 2008, 2009, 2010, 2015 Labconco Corporation. All rights reserved.
Warranty
Labconco provides a warranty on all parts and factory workmanship. The warranty includes areas of defective material and workmanship, provided such defect results from normal and proper use of the equipment. Glassware is not warranted from breakage when dropped or mishandled.
The warranty for Paramount® Ductless Enclosures will expire one year from date of installation or two years from date of shipment from Labconco, whichever is sooner. Warranty is non-transferable and only applies to the owner (organization) of record.
This limited warranty covers parts and labor, but not transportation and insurance charges. In the event of a warranty claim, contact Labconco Corporation or the dealer who sold you the product. If the cause is determined to be a manufacturing fault, the dealer or Labconco Corporation will repair or replace all defective parts to restore the unit to operation. Under no circumstances shall Labconco Corporation be liable for indirect, consequential, or special damages of any kind. This statement may be altered by a specific published amendment. No individual has authorization to alter the provisions of this warranty policy or its amendments. Lamps and filters are not covered by this warranty. Damage due to corrosion or accidental breakage is not covered.
The information contained in this manual and the accompanying products are copyrighted and all rights reserved by Labconco Corporation. Labconco Corporation reserves the right to make periodic design changes without obligation to notify any person or entity of such change.
Returned or Damaged Goods
Do not return goods without the prior authorization from Labconco. Unauthorized returns will not be accepted. If your shipment was damaged in transit, you must file a claim directly with the freight carrier. Labconco Corporation and its dealers are not responsible for shipping damages.
The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Limitation of Liability
The disposal and/or emission of substances used in connection with this equipment may be governed by various federal, state, or local regulations. All users of this equipment are required to become familiar
with any regulations that apply in the user’s area concerning the dumping of waste materials in or upon
water, land, or air and to comply with such regulations. Labconco Corporation is held harmless with respect to user’s compliance with such regulations.
Contacting Labconco Corporation
If you have questions that are not addressed in this manual, or if you need technical assistance, contact Labconco’s Customer Service Department or Labconco’s Product Service Department at 1-800-821­5525 or 1-816-333-8811, between the hours of 7:00 a.m. and 6:00 p.m., Central Standard Time.
Part #6968600, Rev. E
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CHAPTER 1: INTRODUCTION 1
CHAPTER 2: PREREQUISITES 3
Support and Stability Requirements 3 Location and Air Current Requirements 4 Exhaust and Blower Requirements 4 Electrical Requirements 6 Space Requirements 6
CHAPTER 3: GETTING STARTED 7 Unpacking the Enclosure 8
Set Up the Ductless Enclosure on a Supporting Structure and Work Surface 8 Install Carbon Filters and/or HEPA Filters 11 Connect the Electrical Supply 12 Set Filter Life and Filter Check Timers 12 Initial Safety-First™ Vapor Sensor Warm Up Period 13 Reset or Change the Airflow Face Velocity (If Necessary) 13 Validate the Enclosure 14 Seal the Enclosure to the Work Surface 14 Connecting to the Exhaust System (If Applicable) 14
CHAPTER 4: PERFORMANCE FEATURES AND SAFETY
High Performance Containment 17 Safety-First™ Vapor Sensor 18 Smart-Flow Airflow Monitor 19 Quiet, Energy-Efficient ECM Impeller 19 Audible/Visual Alarms 19
Large Control Panel LCD Display 19
Ergonomic Sloped Front 20 Convenient Filter Replacement 20 Durable Construction 20 Fluorescent Light with Electronic Ballast 20 Utility Iris Ports 20
PRECAUTIONS 15
Maximum Visibility 21 Simple Electrical Connection 21 Safety Precautions 21 Misapplications that Could Result in a Hazardous Situation 24
CHAPTER 5: USING THE DUCTLESS ENCLOSURE 25
Information Center 25 Status Area 26 Operating the Pivoting Sash 26 Starting the Ductless Enclosure 26 The Paramount Touchpad 27 All Program Screens 28 Calibration Program Screens 31 Diagnostic Program Screens 32
User Selectable Features 33 Clock Timer Operation 33 Interval Timer Operation 33 Elapsed Timer Operation 33 Light Lamp Timer and Blower Timer 34 Blower Operation 34 Enclosure Set Up 34 Units of Measure 34 Security Lock 34 Filter Setup Display Options 35 Restoring Software Default Settings 35 Calibration 35 Diagnostic Test Operation 35 If a Check Airflow Activates 36 Resetting the Airflow Alert System 36 Working in the Paramount Ductless Enclosure 36
CHAPTER 6: MAINTAINING THE DUCTLESS ENCLOSURE 38 Routine Maintenance Schedule 38 Determination of When to Replace Carbon Filters 39 Determination of When to Replace HEPA Filters 41 Install Carbon Filters and/or HEPA Filters 42 Set Filter Life and Filter Check Timers 42 HEPA Filter Leak Test 42 Change the Airflow Face Velocity (If Necessary) 44 Initial Certification 44 Re-Certification 44 Fluorescent Light Replacement 45 Motorized Impeller Replacement 47 Main Control Board Replacement 48 Organic Sensor Board Replacement 49
CHAPTER 7: ACCESSORIZING THE DUCTLESS
ENCLOSURE 50
Filters 50 Work Surfaces 51 Work Surface with Deck Mounted Valves, Gooseneck,
and Cupsink 52 Base Stands, Accessory Shelves, Seismic Supports and Hydraulic Lift Base Stands 53 Storage Cabinets 54 Exhaust Transitions 55 Remote Blowers 56 Exhaust Dampers 57 Utility Shelf Kits and Holders 57 Syringe Pump Kit and Detector Tubes 57 Sash Closures 58
CHAPTER 8: TROUBLESHOOTING 59
APPENDIX A: REPLACEMENT PARTS 62
APPENDIX B: PARAMOUNT DIMENSIONS 65
APPENDIX C: SPECIFICATIONS 66
APPENDIX D: QUICK CHART 67
APPENDIX E: ESTIMATED FILTER LIFE CALCULATION 68
APPENDIX F: FILTRATION EFFICIENCY TEST RESULTS 70
Acetone 71 Ethyl Alcohol 72 Isopropyl Alcohol 73 Toluene 74 Hydrochloric Acid 75
1
CChhaapptteerr 11:: IInnttrroodduuccttiioonn
Congratulations on the purchase of a Labconco Paramount® Ductless Enclosure, commonly called a ductless fume hood. Unlike traditional fume hoods, the Paramount Ductless Enclosure is considered green as it conserves energy because it requires no ducting. The Paramount Ductless Enclosure is a self-contained work station that protects the operator from specified vapors and/or particulates released in the work area, through the use of carbon filters and/or HEPA filters. Typical organic solvents, formaldehyde, acid gases, ammonia, amines, particulates, and powders are contained inside the enclosure to protect the operator and then filtered. Purified air is drawn from the filters and returned to the room. Vapors are adsorbed on activated carbon filters or impregnated carbon filters and particulates/powders are filtered by the HEPA filter.
Each Paramount Ductless Enclosure includes the Safety-First™ Vapor Sensor that detects filter saturation and alerts the operator to replace the filters. The early warning provided by the Safety-First Vapor Sensor provides the user ample time (5-10% remaining filter life) to complete work in process before changing the filters. The Safety-First Vapor Sensor includes a primary and secondary sensor for redundant monitoring and the sensor detects typical organic solvents, smoke particulates, ammonia gases, formaldehyde gases, and hydrogen sulfide gases. The Paramount Ductless Enclosure is the result of Labconco’s years of experience in the design and manufacture of fume hoods and ductless hoods.
The Paramount Ductless Enclosure offers many unique features to enhance safety, performance, and ergonomics. Safety is illustrated with the Safety­First Vapor Sensor. Performance and Safety are illustrated with validated containment and patented aerodynamic features (U.S. Patent No. 6,461,233). Ergonomics is illustrated with the patented inclined design (U.S. Patent No. D538,941). To take full advantage of all features, please acquaint yourself with this manual and keep it handy for future reference. If you are unfamiliar with how ductless enclosures operate, please review Chapter 4: Performance Features and Safety Precautions, before you begin working.
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Chapter 1: Introduction
2
Even if you are an experienced ductless enclosure user, please review Chapter 5: Using the Ductless Enclosure; it describes the Paramount Ductless Enclosure features so that you can use it efficiently and effortlessly.
The Paramount Ductless Enclosure ships without any filters. Chapter 3: Getting Started and Chapter 6: Maintaining the Ductless Enclosure, must
be followed to properly select and install filters.
This manual and other technical information is available in PDF format at our website: www.labconco.com.
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3
CChhaapptteerr 22:: PPrreerreeqquuiissiitteess
Before you install the Paramount Ductless Enclosure, you need to prepare your site for installation. A dedicated source of electrical power should be located near the installation site to power the ductless enclosure and other apparatus. Additionally, the enclosure should be strategically placed in the lab to provide efficient workflow.
Carefully read this chapter to learn the requirements for your installation site:
The support and stability requirements.
The location and air current requirements.
The exhaust and blower requirements.
The electrical power requirements.
Space requirements.
Refer to Appendix B: Dimensions for complete enclosure dimensions. Refer to Appendix C: Specifications for complete enclosure electrical and
environmental conditions, specifications and requirements.
Support and Stability Requirements
At a minimum, the supporting structure usually consists of a base cabinet or stand and a chemically resistant work surface. Please consider the following:
Work surfaces should be of a thick rigid material that remains stable.
A bench that is rigidly mounted to the floor or fixed to the wall may
be appropriate.
Tubular stands or mobile benches with locking casters may be
appropriate.
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Chapter 2: Prerequisites
4
Location and Air Current Requirements
The Paramount Ductless Enclosures have been designed to contain hazards by negating typical cross drafts and turbulence within the opening. However, it is recommended that the enclosure be placed in an area to avoid:
High traffic areas where walking might cause an air disturbance or be a
nuisance.
Overhead or wall HVAC diffusers, fans, radiators or other lab equipment
producing air currents.
Near doorways or windows that may be opened.
Exhaust and Blower Requirements
The Paramount Ductless Enclosure uses a green, 95% energy efficient, electronically-commutated motorized (ECM) impeller to draw room air past the operator and through the enclosure (see Appendix D for power usage by model). This contaminated air is passed through filters and exhausted out the top of the enclosure. The filtered exhaust air is normally recirculated into the laboratory or may be exhausted outside with the addition of the Canopy Exhaust Connection and remote blower listed in Chapter 7. Contact Labconco for blower sizing assistance for exhausting to the outside. Electrical connections are covered in Chapter 2 for this configuration.
Data for the enclosure’s exhaust volume, noise pressure and face velocity are listed on the next page in chart form for each Paramount Ductless Enclosure model at face velocities of 60, 80, and 100 fpm. All models are shipped to operate at 75-80 fpm, but can be reset by the Safety Officer or certification technician through a password protected menu.
Important Note: If the enclosure is connected directly to a house exhaust system, an adjustable damper (or valve) must be installed to control the airflow properly. This is equally important when a house exhaust system is controlling multiple ductless enclosures. See Chapter 7 for information on accessories.
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Chapter 2: Prerequisites
5
Model No.
Voltage
Enclosure
Width
Internal
Working
Height
Sash
Opening
Exterior
Depth
Exterior
Height
Face
Velocity
(fpm)
Airflow
Exhaust
Volume
(CFM)
Noise
Pressure
(dbA)
6963200
100-115V
2'
22.7"
9.4"
29"
43.7"
60 80
100
85 115 145
50
54
59
6963220
208-230V
2'
22.7"
9.4"
29"
43.7”
60
80 100
85 115 145
50
54
59
6963300
100-115V
3'
22.7"
9.4"
29"
43.7"
60
80 100
130 175 220
46
52
56
6963301
100-115V
3'
32"
12"
29"
53"
60
80 100
170 230 285
52
57
62
6963302
100-115V
3'
32" x 360°
12"
29"
53"
60
80 100
170 230 285
52
57
62
6963320
208-230V
3'
22.7"
9.4"
29"
43.7"
60
80 100
130 175 220
46
52
56
6963321
208-230V
3'
32"
12"
29"
53"
60
80 100
170 230 285
52
57
62
6963322
208-230V
3'
32" x 360°
12"
29"
53"
60
80 100
170 230 285
52
57
62
6963400
100-115V
4'
22.7"
9.4"
29"
43.7"
60
80 100
175 235 295
53
57
62
6963401
100-115V
4'
32"
12"
29"
53"
60
80 100
230 305 380
57
62
67
6963402
100-115V
4'
32" x 360°
12"
29"
53"
60
80 100
230 305 380
57
62
67
6963403
100-115V
4'
35"
12"
35.5"
56"
60
80 100
230 305 380
59
62
67
6963420
208-230V
4'
22.7"
9.4"
29"
43.7"
60
80 100
175 235 295
53
57
62
6963421
208-230V
4'
32"
12"
29"
53"
60
80 100
230 305 380
57
62
67
6963422
208-230V
4'
32" x 360°
12"
29"
53"
60
80 100
230 305 380
57
62
67
6963423
208-230V
4'
35"
12"
35.5"
56"
60
80 100
230 305 380
59
62
67
6963501
100-115V
5'
32"
9.4"
29"
53"
60
80 100
220 295 370
57
62
67
6963503
100-115V
5'
35"
9.4"
35.5"
56"
60
80 100
220 295 370
57
62
67
6963521
208-230V
5'
32"
9.4"
29"
53"
60
80 100
220 295 370
57
62
67
6963523
208-230V
5'
35"
9.4"
35.5"
56"
60
80 100
220 295 370
57
62
67
6963601
100-115V
6'
32"
12"
29"
53"
60
80 100
350 465 580
57
61
66
6963603
100-115V
6'
35"
12"
35.5"
56"
60
80 100
350 465 580
57
61
66
6963621
208-230V
6'
32"
12"
29"
53"
60
80 100
350 465 580
57
61
66
6963623
208-230V
6'
35"
12"
35.5"
56"
60
80 100
350 465 580
57
61
66
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Chapter 2: Prerequisites
6
Electrical Requirements
Standard duplex electrical receptacles should be nearby for connecting the Paramount Ductless Enclosure and other equipment. The enclosures include iris pass-through ports to allow electrical cords through the back of the enclosure without leaving a large hole for contaminants to escape. (See Appendix C for amperage.)
There is no provision for controlling a remote blower for exhausting air from the Paramount Ductless Enclosure. If remote blower control is required, a qualified electrician may connect a wall-mounted power outlet switch receptacle nearby so that the switch controls both the remote blower and the outlet. The power cord for the Paramount is then plugged into this outlet.
Space Requirements
The dimensions for the different models are shown in the chart in Chapter 2 and detailed in Appendix B: Dimensions. To convert inches to millimeters, multiply by 25.4.
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7
CChhaapptteerr 33:: GGeettttiinngg SSttaarrtteedd
Now that the site for your Paramount Ductless Enclosure is properly prepared, you are ready to unpack, inspect, install, and validate your system. Read this chapter to learn how to:
Unpack and move the enclosure. Set up the enclosure with the proper supporting structure and work
surface.
Install carbon filters and/or HEPA filters. Connect the electrical supply. Set Filter Life and Filter Check Timers. Reset or change the face velocity, if necessary. Validate the enclosure. Seal the enclosure to the work surface. If applicable, connect to an exhaust system.
Depending upon which model you are installing, you may need common mechanical and electrical installation tools in addition to 5/16", 3/8", 7/16", and 1/2" wrenches, ratchets, sockets, a nut driver set, a flat-blade screwdriver, a Phillips screwdriver, and a carpenter level to complete the instructions in the chapter.
Note: Each enclosure model weighs between 125 to 350 lbs. (55 to 152 kg). The shipping container allows for lifting with a mechanical lift truck or floor jack. If you must lift the enclosure manually, follow safe-lifting
guidelines. Do not lift by the front air foil.
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Chapter 3: Getting Started
8
Unpacking the Enclosure
We recommend that you do not remove the enclosure from its shipping container until it is ready to be placed into its final location. Move the unit by placing a flat, low dolly under the shipping skid, or by using a floor jack.
Carefully remove the shrink-wrap or carton on the enclosure and inspect it for damage that may have occurred in transit. If damaged, notify the delivery carrier immediately and retain the entire shipment intact for inspection by the carrier.
Note: The United States Interstate Commerce Commission rules require that claims be filed with the delivery carrier within fifteen (15) days of delivery.
Note: Do not return goods without the prior authorization of Labconco. Unauthorized returns will not be accepted.
Note: If the enclosure was damaged in transit, you must file a claim directly with the freight carrier. Labconco Corporation and its dealers are not responsible for shipping damages.
Do not discard the packing material until you have checked all of the components and tested the enclosure.
Do not move the enclosure by tilting it onto a hand truck.
Set Up the Ductless Enclosure on a Supporting Structure and Work Surface
When installing the enclosure onto a chemical-resistant work surface or benchtop, ensure that the structure can safely support the combined weight of the enclosure and any related equipment. See Chapter 7: Accessorizing the
Paramount Ductless Enclosure for appropriate work surfaces, stands, and cabinets. The work surface should be at least as wide as the enclosure
to properly support it. The front of the enclosure should be aligned within
0.3" of the front of the work surface as shown in Figure 3-1. Mounting holes are provided in the Labconco accessory work surfaces to secure the enclosure. RTV Silicone sealant can be applied to seal the work surface to the enclosure.
Work Surface Specifications
The work surface should be smooth, rigid, and durable. The surface should be non-porous and resistant to the powders, solvents and chemicals used in conjunction with the Paramount Ductless Enclosure.
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Chapter 3: Getting Started
9
Work Surface and Enclosure Installation
1. Level the base cabinets and the work surface. Work surface should be placed flush with the front of the stand or base cabinet as shown in Figure 3-1.
2. Identify and position the work surface ensuring the mounting holes will align with the four screw locations on the base of the enclosure. (Rear mounting holes are located close to the rear edge.)
3. Secure the work surface to the base cabinet with a structural adhesive or silicone sealant.
4. Before moving the enclosure, insert the supplied mounting screws in the four holes. Allow a minimum of 1/8" clearance under the head of the screw for positioning the enclosure. For the stainless work surfaces, use a #10-24 x 3/8" hex washer head screw (Labconco part number 1885806).
5. Place the enclosure on the work surface and slide the rear flange and front air foil flanges under the mounting screw heads.
6. Tighten the four screws to complete the installation.
7. If desired, apply RTV silicone to seal the work surface and enclosure.
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Chapter 3: Getting Started
10
Figure 3-1
Paramount Ductless Enclosure Installation
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Chapter 3: Getting Started
11
6938100
HEPA Filter, 15" x 18" x 1.5", 99.99% efficient particulate on 0.3 micron
6938200
Activated Carbon Filter, Organic Vapor 7.5 lbs.
6938201
Impregnated Carbon Filter Acid-Sulfur 10 lbs.
6938202
Impregnated Carbon Filter, Ammonia-Amine 11 lbs.
6938203
Impregnated Carbon Filter, Formaldehyde-Formalin 10 lbs.
6938204
Mixed Bed Carbon Filter, Org. Vap., Acid-Sul., Ammon, Form (25% Mix) 10 lbs.
6938205
Impregnated Carbon Filter, Radioisotope 10 lbs.
Paramount
Size
Filter
Compartments
Required
No. of Filters
Total Organic
Vapor Filter Weight
2' 1 2
15 lbs.
3' 2 4
30 lbs.
4' 3 6
45 lbs.
5' 3 6
45 lbs.
6' 4 8
60 lbs.
Install Carbon Filters and/or HEPA Filters
Refer to Figure 3-2 for a view of the filter loading compartment with the front panel removed. The Paramount Ductless Enclosure ships without
filters that must be ordered separately. It is highly recommended that an extra set of new filters be on hand on a continuous basis.
To remove the front panel, use a Phillips screwdriver to loosen the two screws holding the front panel in position; slide the front panel forward and then up to remove. The filter loading compartment is hinged and supported by gas spring cylinders. Lift the handle up and remove the cardboard packing. The cardboard packing will be replaced with filters that always stack two high.
The Paramount Ductless Enclosure has seven different filter types identified below:
All impregnated Carbon Filters, specific chemical treated, have an organic vapor capacity of 25%. Mixed Bed Carbon Filters have an organic vapor capacity of 50%. For example, the Impregnated Acid Filter has 25% of 10 pounds or 2.5 pounds of organic vapor capacity. Thus, a common application using solvents with acids would require one Activated Carbon Filter for organic vapors and one Impregnated Acid Filter for acid vapors.
Any combination of two filter types may be used. Filters are always loaded with the gasket side up. If placing the Paramount Ductless Enclosure in a clean room, always place the HEPA filter above the carbon filter to eliminate any trace carbon particles from entering the clean room. Load the stacked filters into the individual filter compartments. The Paramount model sizes, filter compartments, and number of filters are listed below for installation convenience.
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Chapter 3: Getting Started
12
To install the filters, push the stacked filters to the stop in the rear of each filter compartment. After loading the stacked filters into the compartments, close the gas spring cylinders by pulling the handle down and compressing the filter gaskets. Filter installation is complete.
Figure 3-2
Filter Installation
Connect the Electrical Supply
Simply connect the 115V power cord supplied to the IEC electrical supply plug on the back of the enclosure. For 230V, the same procedure applies except it is shipped without a plug. Install the appropriate plug for your electrical specifications per local codes. (See Appendix C for amperage.)
Set Filter Life and Filter Check Timers
Once the filters are installed and electrical power is connected, it is necessary to set the Filter Life Timers in the Filter Setup menus described in Chapter 5:
Using the Ductless Enclosure. Consult the separate Paramount Chemical Guide, Appendix E: Estimated Filter Life Calculation, and/or Labconco
Specialist to determine the filter capacity. Through the use of all three sources, set the Filter Life Timers.
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Chapter 3: Getting Started
13
Initial Safety-First™ Vapor Sensor Warm Up Period
The Safety-First™ Vapor Sensor includes a 5V, 0.28W integrated heater and any detectable gas that accumulates during shipment must be driven off the organic sensor over an initial 10-30 minute warm up period with the blower activated. Refer to the Diagnostic Program Screen for Organic Sensor on page 32 in Chapter 5 to view the display of the millivolt levels of the Vapor Sensor. With new filters installed, the Organic Sensor should read between 1300-1500 millivolts after the initial 10-30 minute warm up period with the blower running. All filters should be changed upon completion of work once the Organic Sensor sees an increase of 400-500 millivolts with the display indicating “Replace Filters.”
Reset or Change the Airflow Face Velocity (If Necessary)
The face velocity for the Paramount Ductless Enclosure has been preset at the factory between 75-80 fpm. Important Note: Transport, altitude, and temperature differences may require a reset of the “Calibration” of the
“Pressure Sensor” as outlined in Chapter 5: Using the Ductless Enclosure. When “Calibration” of the “Pressure Sensor” is reset, it is best to try the
previously calibrated values of motor speed and airflow face velocity and then confirm the average face velocity through the enclosure sash opening. Adjust the motor speed and airflow face velocity as necessary after confirmation. Average face velocity measurements are made using a calibrated thermal anemometer and taking an average across the sash opening at 5" directly below the sash handle.
Additionally, the same “Calibration” menu in Chapter 5 should be used to change the face velocity to another value. For most applications, 75-80 fpm is ideal. However, there are some requirements for 100 fpm. Furthermore, the face velocity alarm has been preset at the factory at 60 fpm. If needed, follow the “Calibration” menu for the “Airflow Alarm” in Chapter 5 and adjust the alarm value between 10-20 fpm below the actual face velocity.
The Paramount Ductless Enclosure has been set up to accept the Smart­Flow feedback system. The Smart-Flow feature adjusts the motor speed automatically for filter pressure drop, barometric pressure, and room temperature, and maintains constant airflow velocity at the calibrated value. Note: At altitudes above or below 900 feet, the Paramount must be recalibrated to account for significant pressure changes that will have an effect on face velocity. Face velocity measurements are always made using a calibrated thermal anemometer and taking an average across the sash
opening. Follow the “Calibration” menu for “Pressure Sensor” as outlined in
Chapter 5: Using the Ductless Enclosure for recalibration of face velocity.
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Chapter 3: Getting Started
14
Validate the Enclosure
To determine the actual face velocity at the sash opening, airflow velocity readings are taken. Each Paramount Ductless Enclosure has been preset at 75-80 fpm. The “average face velocity” is achieved by taking readings across the enclosure with the readings 6" from the ends and evenly spaced every 12". Readings are measured at 5" directly below the upper sash handle. Refer to Chapter 2 for proper airflow volumes for your particular model.
The Paramount Ductless Enclosures have been tested at Labconco’s airflow test facility per ASHRAE 110-1995. All enclosures achieve an “as manufactured
rating” of less than 0.05 part per million (ppm) at 4 liters per minute (lpm); AM
<0.05 (Consult Labconco for individual ratings). For particulate powder validation, Labconco had containment testing performed to validate the enclosures for naproxen sodium powders. The Paramount Ductless Enclosures demonstrated excellent containment when used by an operator using excellent technique and good containment when used by an operator using marginal technique. While no enclosure can compensate for improper technique, these tests confirm that the Paramount Ductless Enclosures provide a safe working environment. For copies of these validation reports, contact Labconco at 800­821-5525 or 816-333-8811.
Seal the Enclosure to the Work Surface
When the enclosure has been set in place, it can be sealed at the work surface to prevent spilled materials from collecting under the walls. A bead of silicone sealant is recommended to seal the enclosure to the work surface.
Connecting to the Exhaust System (If Applicable)
WARNING: The weight of the exhaust ductwork system must be supported independently of the enclosure superstructure or damage may occur.
The exhaust system should be installed by a qualified HVAC contractor.
Normal operations with the Paramount Ductless Enclosure are exhausted into the room and the accessory Canopy Exhaust Connection is not required. The Canopy Exhaust Connection aids in the further removal of chemicals beyond the filters or applications where a higher degree of powder and particulate removal is required. However, if desired, the Canopy Exhaust Connection (see Chapter 7) accessory has been designed to accept 6" diameter ductwork. Review Chapter 2 for exhaust prerequisites and review Chapter 7 for ordering blower exhaust equipment. Consult Labconco should you require help sizing your blower for the exhaust volume and system static pressure loss. To ensure compatibility, the selected exhaust duct material should match the enclosure, procedures and chemical applications.
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15
CChhaapptteerr 44:: PPeerrffoorrm
maannccee FFeeaattuurreess aanndd
SSaaffeettyy PPrreeccaauuttiioonnss
The Paramount Ductless Enclosure is a self-contained filtered enclosure that protects the operator from specified vapors and particulates through the revolutionary combination of features to enhance safety, performance, and ergonomics. Carbon filters and/or HEPA filters must be installed.
All Paramount Ductless Enclosures have the following performance features as illustrated in Figure 4-1:
1. High Performance Containment
2. Safety-First™ Vapor Sensor
3. Smart-Flow Airflow Monitor
4. Quiet, Energy-Efficient ECM Impeller
5. Audible/Visual Alarms
6. Large Control Panel LCD Display
7. Ergonomic Sloped Front
8. Convenient Filter Replacement
9. Durable Construction
10. Fluorescent Light with Electronic Ballast
11. Utility Iris Ports
12. Maximum Visibility
13. Simple Electrical Connection
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Chapter 4: Performance Features and Safety Precautions
16
Figure 4-1
Performance Features
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High Performance Containment
The Paramount Ductless Enclosures use patented technology to direct air into and through the contaminated air chamber (U.S. Patent 6,461,233). The containment enhancing and aerodynamic designs of the lower Clean-
Sweep™ Air Foil, upper sash foil, side air foils, upper dilution air supply,
and zoned rear perforated baffle all work in concert to produce horizontal airflow patterns that significantly reduce chemical concentrations through the work area (illustrated in Figure 4-2). The unique lower air foil shape and Clean-Sweep openings sweep the work surface and create a constant protective barrier from contaminants. The radiused upper sash foil includes an open air passage directly atop the sash foil into the enclosure chamber and directs chemical concentrations away from the sash opening. The side entry air foils allow turbulence-free air to enter the enclosure from the sides and allow clean air to sweep the interior walls. The upper dilution air supply provides by-pass air from above the work surface to constantly bathe the inside of the sash and upper chamber with clean air to reduce chemical concentrations. The zoned rear perforated baffle directs horizontal laminar air streams to the three zones to minimize the potential for air to roll forward preventing contaminants from moving toward the sash opening.
Figure 4-2
Airflow Diagram
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Chemical Family
Chemical
Sensitivity Alert
Concentration
Odor
Threshold
(ppm)
Exposure
Limit TWA
(ppm)
Filter
Capacity
(%W)
Filter Type
Aldehydes & Ketones
Cyclohexanone
0.2-0.5 ppm
0.068
50
22%
OV
Mixture of Aliphatic Hydrocarbons
Gasoline
0.3-1.0 ppm
0.3
300
11%
OV
Particulates
Cigarette smoke
0.4-1.0 ppm
N/A
N/A
N/A
OV & HEPA
Aldehydes & Ketones
Acetone
0.5-1.0 ppm
4.58
250
2%
OV
Aromatic Hydrocarbons
Toluene
0.5-1.0 ppm
0.16
100
20%
OV
Ethers
Methyl Tert-Butyl Ether
0.5-1.0 ppm
0.053
50
9%
OV
Sulfur Compounds
Hydrogen Sulfide
0.5-2.0 ppm
0.0005
10
10%
AG, Acid-Sulfur
Nitrogen Compounds
Diethylamine
1.5-2.0 ppm
0.186
10
7%
OV
Esters
Ethyl Acetate
1.5-4 ppm
0.61
400
9%
OV
Ethers
Diethyl Ether
2-4 ppm
2.29
400
4%
OV
Aldehydes
Formaldehyde
2-4 ppm, best to use
other detector methods
0.87
0.1 ceiling,
0.016
10%
FORM
Nitrogen Compounds
Ammonia Solution (Ammonium Hydroxide)
2-5 ppm
5.75
25
10%
AM, Ammonia-
Amine
Alcohols
Ethyl Alcohol*
2.5-4 ppm
0.136
1000
1.3%
OV
Acids
Acetic Acid
5-6 ppm
0.016
10
4%
OV
Halogens
Chlorobenzene
5-8 ppm
0.741
10
20%
OV
Alcohols
Isopropyl Alcohol
8-11 ppm
22
200
7%
OV
Aliphatic Hydrocarbons
Hexane
9-15 ppm
21.9
50
11%
OV
Alcohols
Methanol*
15-25 ppm
141
200
0.1%,
very low
not recommended
Mineral Acids
Hydrochloric Acid
Not Detected, use other
detector means
0.77 5 17%
AG, Acid-Sulfur
*
Safety-First™ Vapor Sensor
The Safety-First™ Vapor Sensor detects filter saturation in the exhaust to alert the operator to replace the filters. The early warning provided by the Safety-First Vapor Sensor provides the user ample time (5-10% remaining filter life) to complete work in process before replacing the filters. The early warning signals with an intermittent beep and the LCD display message alerts the user to replace filters. The final warning signals with a constant alarm and the LCD display message alerts the user to replace filters. The Safety­First Vapor Sensor includes a primary and secondary backup sensor for redundant monitoring. Both sensors detect typical organic vapor solvents, smoke particulates, ammonia gases, formaldehyde gases and hydrogen sulfide gases. The Safety-First Vapor Sensor has an optimal detection range of 1-10 ppm. Typical concentrations tested by Labconco for chemicals in separate chemical families are listed in order of sensor sensitivity as follows:
Important Note: Clean up procedures using alcohols or volatile chemicals with low filter capacity could saturate the filters quickly.
Important Note: The vapor sensor does not detect mineral acid gases such
as hydrochloric acid, nitric acid, or sulfuric acid and other detector means such as a mineral acid sensor or interval timed sampling with sampling tubes must be used.
Chemical Safety Note: The chart above is only a guideline! Frequent chemical testing or filter monitoring is recommended for other chemicals. If chemical suitability is ever in question, always work below the acceptable exposure limit/TWA to maximize both safety and filter performance.
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Smart-Flow™ Airflow Monitor
The Smart-Flow™ Airflow Monitor continuously monitors airflow and displays face velocity. An audible/visual alarm alerts the user to low airflow conditions. The Smart-Flow Airflow Monitor enables the motor speed to automatically adjust for conditions such as temperature, barometric pressure, and filter loading and maintain constant programmed airflow speed. The Smart-Flow feedback maintains constant airflow speed through the use of constant velocity pressure measurement accomplished with a pitot tube and pressure sensor mounted on the control board. Transport, altitude, and temperature differences require the airflow re-calibration steps as outlined in
Chapter 5 and 6. Use the “Calibration” menu in Chapter 5 to reset the “Pressure Sensor” values for motor speed and airflow face velocity.
Quiet, Energy-Efficient ECM Impeller
The electronically commutated motorized (ECM) impeller is 95% energy
efficient providing “green” energy savings (See Appendix D). Because of
the high efficiency, the impeller runs extremely quiet for the comparative amount of airflow volume. All Paramounts run at or below 62 dbA at 80 fpm and most Paramounts run at or below 59 dbA at 80 fpm. By design, the ECM impeller is located after the filters assuring an intrinsically safe design where all contaminated air is filtered effectively. See Chapter 2: Prerequisites for complete airflow exhaust volume, noise pressure, and face velocities of 60, 80 and 100 fpm. The ECM impeller has a programmable blower timer should you desire additional “green” energy savings.
Audible/Visual Alarms
The audible/visual alarms remind the operator to check the filters with sampling tubes or replace the filter. Filter replacement alarms occur in audible/visual modes for both filter saturation activated by the Safety-First Vapor Sensor or the final filter elapsed time. A low airflow alarm occurs when the face velocity drops below programmed levels.
Large Control Panel LCD Display
The large (3" x 1.5") LCD message center provides continuous status reports for each filter, displays airflow speed, and displays alarm messages for both filters and airflow. The touchpad can be programmed for filter types, filter check times, and filter replacement times. Audible/visual alert time messages appear after the specified number of hours has elapsed. The audible/visual alarm reminds the operator to check the filters with sampling tubes or replace the filters. Filter replacement audible/visual alarms occur for both the Safety­First Vapor Sensor and final filter elapsed time.
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Ergonomic Sloped Front
The ergonomic slope provides maximum visibility and comfort, reduces glare, thereby minimizing operator fatigue. The space saving design (U.S. Patent No. D538,941) increases effective laboratory work space, because the impeller and filters are all self-contained within the enclosure and a separate filtered blower unit is not required.
Convenient Filter Replacement
The Paramount filter compartment was designed to make filter replacement convenient and easy. The gas spring assisted clamping mechanism opens effortlessly and applies uniform pressure across the entire top surface of the filters for leak-proof, one-step filter replacement from the front of the enclosure.
Durable Construction
Unlike comparable plastic or acrylic ductless fume hoods and enclosures, the Paramount Ductless Enclosure is manufactured with durable tempered safety glass and dry powder epoxy-coated aluminum and steel. The sides and sash are made from tempered safety glass that will not easily discolor or craze like plastic. The frame is made from dry powder epoxy-coated aluminum and steel providing further strength and corrosion resistance to solvents and acids.
Fluorescent Light with Electronic Ballast
The fluorescent light is located above the work area, out of contact with contaminated air and easy to service. All Paramounts have a fluorescent light and energy saving light timer with electronic ballast. The light timer is a programmable feature should you desire additional green energy savings.
Utility Iris Ports
All Paramounts have two utility iris ports that allow electrical cords and data cords to pass through the back of the enclosure without leaving a large hole for contaminants to escape. The enclosure ships with both solid plugs and iris ports for your convenience.
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Maximum Visibility
Visibility is maximized on all units with at least 270 degree visibility from both sides and the front pivoting sash. Some 3' and 4' models have 360 degree visibility which is especially useful in classroom demonstrations. See Chapter 2: Prerequisites for model differences and model numbers.
Simple Electrical Connection
All 100-115V Paramounts are pre-wired with circuit breaker and IEC electrical power cord that is simply plugged into a nearby electrical receptacle. 230V units are shipped without a plug. Install the appropriate plug for your electrical specification per local codes. All the impeller, light, and airflow monitor wiring is internal and no electrical wiring connections are needed. Paramounts are available in two voltages, 100-115V, 50/60 Hz and 230V, 50/60 Hz. See Chapter 2: Prerequisites for model numbers.
Safety Precautions
1. Although the enclosure has been engineered to maintain optimum operator safety, caution should always be used while working. Prior to using the enclosure, check to make sure that the exhaust blower is operating and that air is entering the enclosure at its specified face velocity. The airflow monitor will alert the user to a problem with airflow.
2. Use good housekeeping in the enclosure at all times. Clean up spills immediately. Periodically clean enclosure interior.
3. Do not overload the work surface with apparatus or work material. The safe operation of the enclosure is based upon having proper airflow through the structure. Do not place large objects directly on the work surface. Instead, elevate the object 3/4" on blocks to allow a flow of air under the object and into the rear baffle exhaust slots. Ensure blocks are level and secured in place.
4. Blocking large portions of the rear baffle will change the airflow pattern in the enclosure causing turbulence. (Do not store containers or supplies against the rear baffle, as this will affect airflow).
5. Always work with your hands as far back into the enclosure as possible. Keep all powders, chemicals and apparatus inside the lower air foil of the enclosure.
6. Do not work in this enclosure without the blower running and a face velocity of 60-100 fpm.
7. Perchloric acid use in this enclosure is prohibited.
8. High-level radioisotope materials are prohibited in this enclosure. Consult your Safety Officer.
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9. Avoid cross drafts and limit traffic in front of the enclosure. Air disturbances created may draw contaminants out of the enclosure.
10. A qualified certification technician should test the enclosure before it is initially used. The enclosure should be validated whenever it is relocated.
11. The use of safety goggles, protective clothing, gloves and any other personal protective equipment recommended by your safety officer should be used.
12. The sash must remain in the down position while using the enclosure.
13. Proper performance of the enclosure depends largely upon its location and the operator’s work habits. Consult the references in Appendix D.
14. The enclosure should be recertified whenever it is serviced or at least annually thereafter.
15. Use of an open flame must be avoided in the Paramount. Open flames may disrupt the airflow patterns in the cabinet and cause a fire hazard with volatile chemicals and solvents.
16. Handle new and used filters with care during installation and removal. Refer to Installation Instructions in this manual for proper handling of filters.
17. Saturated carbon filters and HEPA filters are to be disposed of as hazardous waste. The user is responsible for recording the chemicals adsorbed or removed by the filters and disposing of them properly.
18. Use in areas where only trained users have access to the enclosure.
Any new users must be trained and should also read this User’s
Manual.
19. Do not use the Paramount in a poorly ventilated area. If the Paramount is to be used in a confined space, make sure the space is well ventilated and the concentration of toxic contaminants cannot accumulate greater than the exposure limit/TWA.
20. The warning properties (i.e., odor, taste) of the volatile organic compounds or other material being used in the enclosure must be adequate to provide an early indication that the carbon filter may be saturated. In other words, it is best when the odor threshold is less than the exposure limit/TWA.
21. Highly toxic vapors, unknown reaction, hazardous particulate, or processes generating high levels of contaminants are not intended for use in the Paramount.
22. Labconco Filter labels are color coded to match NIOSH respirator types. Only chemicals which can be safely adsorbed/treated with the specific carbon based filters installed or removed by HEPA filters are appropriate for use in this enclosure.
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23. Use the smallest possible quantity of chemical(s) within the enclosure and never exceed the amount which can be effectively adsorbed by the filters before breakthrough.
24. Leave the blower on for at least one minute after work in the enclosure has been completed.
25. If a chemical is spilled on the work surface DO NOT switch off the blower until all traces of the chemical has been removed.
26. Make sure filters are installed prior to each use. Remove the front panel to install the filters.
27. If the blower fails during use, chemical processes should cease and the area should be vacated and ventilated before servicing the blower.
28. Always refer to the Paramount Chemical Guide and/or the NIOSH Pocket Guide to Chemical Hazards before proceeding. For additional help with filter and chemical selection, contact Labconco at 800-821­5525 or 816-333-8811.
29. The surface of the HEPA filter is fragile and should not be touched. Care must be taken to avoid puncturing the HEPA filter during installation or normal operation. If you suspect that a HEPA filter has been damaged DO NOT use the enclosure; contact a local certification agency or Labconco. Reference Chapter 6 for the HEPA filter certification procedure.
30. The HEPA filter in the enclosure will gradually accumulate airborne particulate matter from the room and from work performed in the enclosure. The rate of accumulation will depend upon the cleanliness of the room air, the amount of time the enclosure is operating and the nature of work being done in the enclosure.
31. Ensure that the ductless enclosure is connected to an electrical service in accordance with local and national electrical codes. Failure to do so may create a fire or electrical hazard. Do not remove or service any electrical components without first disconnecting the enclosure from electrical service.
32. Tag the enclosure with appropriate warning, if any filters have been removed for service.
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Misapplications that Could Result in a Hazardous Situation
There is one scenario where the Paramount’s misapplication could be a part
of a hazardous condition. That situation is where;
1. the Inlet Concentration is greater than the exposure limit/TWA,
2. the filter becomes saturated,
3. the user continues to operate,
4. and the ventilation of the room is insufficient to dilute the exhaust of the Paramount to below the exposure limit/TWA for the chemical.
Important Note: When the inlet concentration is greater than the exposure limit/TWA, extra measures must be taken to monitor the number of air room exchanges. A well designed room with proper air exchanges will properly dilute the exhaust from the Paramount by a multiplier of 25%.
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CChhaapptteerr 55:: UUssiinngg tthhee DDuuccttlleessss EEnncclloossuurree
Information Center
The Information Center is an LCD display located on the control panel. The center’s display is divided into three screens that alternate in normal mode, as shown below to display filter status, estimated filter life, filter type, filter replacement alarms, inflow face velocity, and airflow alarms.
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Status Area
The LCD displays the Paramount Ductless Enclosure’s condition during operation such as the filter types, face velocity, and bar graph to display the remaining filter life in hours. This line can display any of the following messages:
Filters OK
Both filters are operating properly. (No audible alarm)
Check Filter-t
The filter check life timer has expired as programmed and the filters should be checked with colormetric detector tubes or other instrumentation. (Intermittent audible alarm)
Replace Filter-s or -t
The filter needs to be replaced immediately as either the Safety-First Vapor Sensor (-s) has detected filter breakthrough or the filter final life timer (-t) has expired. (Continuous audible alarm; can be muted for 5 minutes) Note: The early warning signal that occurs with 5-10% remaining filter life is an intermittent audible alarm along with “Replace Filter-s.”
Check Airflow
The airflow patterns in the ductless enclosure have changed, resulting in a sudden change in the motor speed. This is most likely due to a blockage of the exhaust filter outlet, complete blockage of the filters, filter saturation, or motorized impeller failure. (Continuous audible alarm; can be muted for 5 minutes)
Operating the Pivoting Sash
You can open or close the sash by pivoting the sash. A latch or gas spring will retain the sash in the open position for loading only. Always work with the sash in the closed position.
Starting the Ductless Enclosure
1. To start the ductless enclosure, press the “Blower button.
2. To turn the fluorescent light on, press the “Light button.
Note: The sash must be completely closed before performing work in the enclosure.
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The Paramount Touchpad
The touchpad of the Paramount Ductless Enclosure is shown below. Take a moment to get familiar with the buttons, their location and function. Also familiarize yourself with the display located on the front. The display will report system functions, such as filter types, filter life, timer displays, filter status, and low airflow alarm messages.
Menu Button This button toggles the display between menu modes. When in the menu mode, this button returns you to the previous menu.
Filter Button – Automatically goes to the filter setup menu, which allows you to display and change the programmable filter parameters such as filter type, filter location, filter check time, and filter final time.
Mute Button – Allows you to temporarily mute an alarm for 5 minutes.
Select Up/Down Yes/No Buttons – Allows you to change options and
values in the menu mode.
Enter Button Allows you to enter or select a value or select an option in menu mode.
Timer Button Allows you to select either a repeating interval timer or an elapsed timer.
Blower Button Starts or stops the enclosure blower. When the blower button is activated, the inflow face velocity will register a face velocity.
Light Button Turns the fluorescent light on or off.
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All Program Screens
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Main Setup Screens
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Filter Setup Program Screens
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Calibration Program Screens
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Pressure Sensor Diagnostic Notes: X20 CAL example represents a pressure of 134 with the impeller off and 212 with the motor speed at 157 producing 90 fpm for this calibration example. With Smart Flow enabled, the Paramount maintains constant pressure as indicated by the pitot tube and pressure sensor to maintain constant airflow face velocity.
Organic Sensor Diagnostic Notes: Organic Sensor example represents sensor S1 calibrated in clean air at 1400 millivolts. When sensor S1 sees an increase of 400 millivolts to 1800 millivolts, the Early Warning “Replace Filter-s” appears on the LCD display with an intermittent beep as only 5-10% filter life remains. Filters should be changed upon completion of work. When sensor S1 sees an increase of 500 millivolts to 1900 millivolts, the Final “Replace Filter-s” Alarm sounds a continuous beep that can only be muted for 5 minutes.
Diagnostic Program Screens
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User Selectable Features
The Paramount Ductless Enclosure offers the user unsurpassed flexibility and convenience.
To access the menu, press the “MENU” button. The LCD display panel will show the first level menu. To select from the various menu options press the ” and “” buttons until the selected option is displayed.
Press “ENTER” to accept that option, or press “MENU” to return to the
previous menu.
For further explanation of the menu and its options, please refer to the Paramount Touchpad at the beginning of Chapter 5.
Clock Timer Operation
NOTE: The Timer button displays the menu functions of an Interval (countdown) Timer or Elapsed (stopwatch) Timer. The timers cannot be operated simultaneously.
To access the main timer menu, press the “TIMER” button anytime during normal operation. The main timer menu is shown on the LCD display. Use
the “” and “” buttons to highlight the Interval or Elapsed Timer. Press the “Enter” button to select the highlighted timer function.
Interval Timer Operation
1. When selected, the Interval Timer menu is displayed on the LCD.
The timer defaults to 0:00:00 (hours:minutes:seconds).
2. Press and hold the “” or “” buttons to increase or decrease the
timer interval.
3. When the proper interval is entered on the display, press the
“ENTER” button to start the timer.
4. When the timer reaches 0:00:00, an audible alarm will sound, and the
timer will reset itself and repeat the countdown.
5. Press the “ENTER” button to pause the timer.
6. Press the “MENU” button to clear the interval timer and return to the
main timer menu.
Elapsed Timer Operation
1. When selected, the Elapsed Timer menu is displayed on the LCD.
The timer defaults to 0:00:00 (hours:minutes:seconds),
2. Press the “ENTER” button to start the timer.
3. Press the “ENTER” button again to zero the timer.
4. Press the “MENU” button to clear the elapsed timer and return to the
main timer menu.
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Light Lamp Timer and Blower Timer
Both timers allow you to decide whether the fluorescent lamp or blower will operate continuously or for a limited time period that you select. This may be desired for energy-savings as well as a safeguard for light-sensitive materials.
Interval
When the “interval” option is selected, the Light Lamp Timer or Blower Timer menu is displayed.
Interval Timer
This window lets you set the amount of time for the fluorescent lamp to stay lit once activated or the blower to stay running. Use the
” and “buttons to select the amount of time, then press the ENTER” button to set the interval.
Continuous
In the continuous mode, the fluorescent lights or blower will remain on until the “LIGHT” button is pressed, or the BLOWER” button is pressed.
Blower Operation
This blower switch allows you to run the ductless enclosure and the face velocity will be displayed. Note: Always work in the ductless enclosure with the blower running.
Enclosure Set Up
These selections allow for the customization of the display and the ductless enclosure operation.
Units of Measure
This option allows you to select the air velocity units of measure. When
“Metric” is selected, the air velocities are displayed in meters-per- second. When “US” is selected, the velocities are displayed in feet-per-
minute.
Security Lock
NOTE: The security lock automatically reactivates and locks out the keypad.
The security lock feature prevents parameters of the Paramount from being changed by unauthorized users. To engage the security lock,
access the Security Lock submenu. Select the “ON” option, and press the “ENTER” button. Once engaged, the operator must enter the proper
password to lock or unlock the enclosure.
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Blower:
Smart-Flow enabled
Units of Measure:
fpm
Security Lock:
OFF, Non-secure
Timers:
Blower and Light Timers disabled.
Filter Timers:
Enabled; Interval set at 100 hours, Final set at 500 hours.
Filter Setup Display Options
This menu selection determines which filters are loaded and displayed in the lower and upper positions. One of seven filter types must be selected for each filter position.
The filter check time and filter final life must be selected next for each filter position. Consult Chapter 3, Appendix E, the Labconco Specialist, and the Paramount Chemical Guide for proper program times.
Restoring Software Default Settings
To restore the default settings to their original configuration:
1. Access the Menu, and select “SETUP. Press “ENTER.
2. In the Setup submenu, select “Restore Defaults. Press “ENTER.
Table of Default Settings
Calibration
This password-protected selection is for qualified certifiers to adjust the blower speed, face velocity, and the low airflow alarm setpoint. Certifier access code is set at 123.
Diagnostic Test Operation
When the “Diagnostic Test” menu is selected, the LCD allows “Keypad Test” to help troubleshoot any malfunction. The “Pressure Sensor”
displays pressure values to help troubleshoot an airflow malfunction. The “Organic Sensor” displays chemical breakthrough (millivolt readings) and alarm setpoints to troubleshoot an organic sensor malfunction.
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If a Check Airflow Activates
The most common causes of a check airflow alarm are:
Blockage of the inlet perforated baffle or exhaust outlet. Loading or blockage of the filters resulting in low airflow. Motorized impeller failure or faulty electrical connector to the impeller.
Note: If the alarm sounds during use, immediately take appropriate action to prevent contamination to you and other personnel in the area.
Resetting the Airflow Alert System
The Check Airflow Alarm automatically resets to normal operation and displays the face velocity once the face velocity has increased and stabilized.
Working In the Paramount Ductless Enclosure
Planning
Thoroughly understand procedures and equipment required before
beginning work.
Arrange for minimal disruptions, such as room traffic or entry into the
room while the cabinet is in use.
Start-up
Turn on blower and observe face velocity. Turn on the fluorescent light. Allow the enclosure to operate unobstructed for 1 minute. Wear a long sleeved lab coat with knit cuffs and over-the-cuff rubber
gloves. Use protective eyewear. Wear a protective mask if appropriate.
Loading Materials and Equipment
Only load the materials required for the procedure. Do not overload
the enclosure.
Do not obstruct the enclosure’s perforated baffle. Large objects should not be placed close together. Always operate with the sash in the closed position.
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Work Techniques
Keep all materials a minimum of 4 inches (100 mm) from the inside
of the lower air foil, and perform all contaminated operations as far to the rear of the work area as possible.
Segregate all clean and contaminated materials in the work area.
Arrange materials to minimize the movement of contaminated
materials into clean areas.
Keep all discarded contaminated material to the rear of the work area.
Avoid moving materials or the operator's hands and arms through the
front access opening during use.
Avoid the use of an open flame.
Avoid using techniques or procedures that disrupt the airflow patterns
of the enclosure.
Final Purging
Upon completion of work, the enclosure should be allowed to operate
for two to three minutes undisturbed, to purge airborne contaminants from the work area.
Unloading Materials and Equipment
Objects in contact with contaminated material should be surface
decontaminated before removal from the enclosure.
All open trays or containers should be covered before being removed
from the enclosure.
Wipe-Down
Wipe down the interior surfaces of the enclosure with suitable
solvent, disinfectant, or cleaner. Important Note: Clean up
procedures using alcohols or volatile chemicals with low filter capacity could saturate the filters quickly.
Dispose of used rubber gloves appropriately, and have
soiled/contaminated lab coats laundered properly.
Wash hands and arms thoroughly with soap.
Shutdown
Turn off the fluorescent light and enclosure blower to preserve filter life.
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CChhaapptteerr 66:: MMaaiinnttaaiinniinngg tthhee DDuuccttlleessss EEnncclloossuurree
Replacing the carbon filters, HEPA filters, and fluorescent light is the primary routine maintenance required.
Review this chapter on maintenance for the following:
Routine Maintenance. Determination of when to replace carbon filters. Determination of when to replace HEPA filters. Install carbon filters and/or HEPA filters. Set Filter Life and Filter Check Timers. HEPA filter leak test. Reset or change the inflow face velocity, if necessary. Initial Certification. Re-Certification. Fluorescent light replacement. Motorized impeller replacement. Main control board replacement. Organic sensor board replacement.
Routine Maintenance Schedule
Weekly
Wipe down the interior surfaces of the enclosure with a suitable
solvent, disinfectant, or cleaner, depending upon the usage of the unit and allow to dry.
Using a damp cloth, clean the exterior surfaces of the enclosure,
particularly the front and top to remove any accumulated dust.
Operate the exhaust system, noting the airflow velocity on the display
and airflow through the enclosure using a source of visible smoke.
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Quarterly (or more often as required)
Note the airflow velocity on the display. Determine the actual airflow
face velocity through the sash opening of the enclosure where the average reading should be at the specified velocity. (Use calibrated thermal anemometer or other approved apparatus).
The enclosure’s perforated baffle should be checked for any blockage
to ensure that the enclosure is maintaining proper airflow.
Replace carbon filters when chemical breakthrough is indicated by
organic sensor, odor, time, detector tube, or for some chemicals,
analytical instrumentation. See “Install Carbon Filters” section of this
manual in Chapter 3.
While the enclosure is filled with a contaminant, test filter condition
on carbon filters using the appropriate gas detector tube at intervals of 20% of the total estimated time. The exception to the 20% recommendation is formaldehyde or any carcinogen or suspected carcinogen. These hazardous chemicals must be checked at a minimum of every 10% of the total estimated time. Gas detector tubes for the specific chemicals that are being used in the enclosure can be obtained from your laboratory supply dealer.
All weekly activities.
Annually
Replace fluorescent lamps, if necessary. Replace HEPA filters if the face velocity drops below the
recommended speed for your facility as the airflow alarm alerts you.
Have the enclosure validated by a qualified certification technician.
See Certification and Recertification in Chapter 6.
All quarterly activities.
Determination of When to Replace Carbon Filters
The carbon filters MUST be replaced when any one of the following four conditions are met:
1. The Safety-First Vapor Sensor indicates chemical breakthrough with an audible alarm and the display reads “Replace Filters.”
2. The Filter Life timer has expired as programmed for typical usage.
3. Chemical odor in the work area is detectable, or the concentration of the chemical in the work area is greater than the exposure limit/TWA.
4. Gas detector tubes change color when sampling the ductless enclosure outlet (exhaust), indicating breakthrough.
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Chapter 6: Maintaining the Ductless Enclosure
40
Safety Note: The use of the organic sensor is not recommended for the determination of filter saturation when the exposure limit/TWA for the chemical is under 5 ppm. Other detection methods must be implemented unless testing is performed by the end user and the known exhaust concentration is below the acceptable exposure limit/TWA.
There are five means of determining when its time to change the carbon filters (not shown in the order of preference).
Odor - A person’s sensitivity to odor, tolerance of odor and their comfort level under odoriferous conditions vary with the individual. Odor is an indicator that chemicals are passing through the carbon filter. Additionally, several points need to be understood:
Odor can be used as a prompt to sample the exhaust to confirm
breakthrough.
Organic chemicals approved for use in the ductless hood usually have
odors that are detectable before reaching the time weighted exposure limits.
Safety-First Vapor Sensor - The organic sensor detects filter saturation from exhaust gas concentration to alert the operator to replace filters. The electronic sensor will signal when the concentration is under 5 ppm for most chemicals with a range of 0.1-30 ppm. The early warning provided by the Safety-First Vapor Sensor provides the user ample time (5-10% remaining filter life) to complete work in process before replacing the filters. The vapor sensor includes a primary and backup sensor for redundant monitoring and both sensors detect typical organic solvents, smoke particulates, ammonia gases, formaldehyde gases, and hydrogen sulfide gases; the vapor sensor does not detect mineral acid gases such as hydrochloric acid, nitric acid, or sulfuric acid. Consult the table in Chapter 4 for a partial listing of tested chemicals in order of sensitivity as the sensitivity differs for each chemical; most tested chemicals have a sensitivity alert concentration below 5 ppm as provided in the table in Chapter 4.
Detection Tubes - Color change indicators can be used to measure the concentration of the chemical at the exit side of the carbon filter, between filters, or in the outlet exhaust. A kit including syringe pump and flexible tubing can be purchased as an accessory from Labconco (Catalog #
6924900). Labconco Customer Service Representatives are supplied with detector tube catalog numbers, as well as telephone numbers to direct you to where to purchase these items.
For organic, mineral acid, formaldehyde and ammonia, chemical specific detector tubes should be purchased when installing fresh filters. Each kit contains instructions on how many strokes of the syringe are required to obtain the stated sensitivity. The sampling syringe is connected to the ductless enclosure exhaust. The hose from the sampling syringe inlet can be
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Chapter 6: Maintaining the Ductless Enclosure
41
inserted between the stacked filters to sample the lower filter or inserted through the holes in the blower exhaust cover to sample both filters. Connect the syringe to the detector tube while the system is running and pull the air through the tube with the syringe. Each stroke of the syringe represents a 100-ml sample and corresponds to the number of strokes necessary to give the indicated color changes. Due to the wide variety of organics and varying exposure limit/TWA’s, it is recommended that specific detector tubes be purchased directly from Sensidyne, Dräger or your laboratory supply dealer. Alternate detector pumps can also be purchased from your laboratory supply dealers.
The vast majority of detector tubes available start measuring at the exposure limit/TWA and the concentration value measured is not important. When a user observes any color change in the tube, they should replace the filter immediately. If no detector tube for your specific chemical is available, other means of detection must be used.
Time - For applications that have very consistent inlet concentrations and operating time, “Time” can be used to anticipate saturation or exposure limit/TWA levels based on prior experience. However, this does not replace the need for sampling. Consult Labconco Specialist for an estimate of carbon filter life based on chemical usage. Refer to Chapter 3 on how to “Set the Filter Life and Filter Check Timers.” Detector tubes, or analytical instrumentation should always be used to determine concentrations in the carbon filter. It is recommended that the carbon filters be checked with detector tubes or other means at intervals of 20% of the total estimated filter life. The exception to the 20% recommendation is formaldehyde and any carcinogen or suspected carcinogen. These more hazardous chemicals must be checked at least every 10% of the total estimated time.
Analytical Instrumentation - This is the most accurate means of measuring concentrations of any chemical. It is the method of choice when no detector tubes are available or the tubes are not sensitive enough to measure at the exposure limit/TWA concentration for the chemical. This method is also to be used to determine saturation when the chemical concentration is below the measurement range of detector tubes. One relatively low cost method of analytical instrumentation includes the use of a PID (photoionization detector) that measures gas concentrations and is available from RAE Systems or PID Analyzers, LLC.
Determination of When to Replace HEPA Filters
The HEPA filters in ductless enclosures gradually accumulate airborne particulate matter and powders from the enclosure and room. The rate of accumulation will depend upon the cleanliness of the room air, the amount of time the enclosure is operating, and the nature of work being done in the enclosure. Replace HEPA filters if the face velocity drops below the recommended velocity. Replace HEPA filters if it fails the HEPA Filter Leak Test in Chapter 6.
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Install Carbon Filters and/or HEPA Filters
Refer to the instructions in Chapter 3 on filter installation during startup.
Set Filter Life and Filter Check Timers
Refer to the instructions in Chapter 3 on setting the Filter Life and Filter Check Life Timers. Refer to the Filter Setup menus in Chapter 5.
HEPA Filter Leak Test
Purpose
After installing the new HEPA filter, the HEPA filter can be leak checked. This test is performed to determine the integrity of the HEPA filter, the filter housing, and the filter mounting frames. Leak testing is to be done by a qualified technician with calibrated equipment. Leak check testing is performed as a downstream average above the perforated exhaust cover above the motorized impeller. The filter passes the leak test at .01% or better. Reference Leak Testing and Photometer scanning from the Institute of Environmental Services (IES-RP-CC001.3)
Apparatus
1. An aerosol photometer ATI model 2D, 2E, 2G or equivalent. Air
Techniques Hamilton Associates inc. 11403 Cron Ridge Dr. Owings Mills, MD 21117
2. One aerosol generator of the Laskin nozzle(s) type. An aerosol of
mineral oil or suitable liquid shall be created by flowing air through it. The compressed air supplied to the generator should be adjusted to a pressure of 10± 1 psig. during operation. Air Techniques Inc. Model TDA-4A or equal. One nozzle at 10 psig is (67.5 cfm x 100ug/l)/(Vol. of air), For the 2' at 80 fpm or 115 cfm, one nozzle @10 psig is 6,750/115 cfm = 59 ug/l. For the 3' at 80 fpm or 230 cfm, one nozzle @ 10 psig is 29 ug/l. For the 4' at 80 fpm or 305 cfm, one nozzle at 10 psig is 22 ug/l. For the 5' at 80 fpm or 295 cfm, one nozzle at 10 psig is 23 ug/l. For the 6' at 80 fpm or 230 cfm (two impellers draw 465 cfm), one nozzle at 10 psig is 29 ug/l.
3. Mineral oil (Catalog #1491400).
4. Sampling Nozzle, Rectangular 1/2" x 3-1/4", Air Techniques, Inc.
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Procedure
For the ATI 2G Photometer
1. Turn on the photometer and allow it to operate for a minimum of 5 minutes. Leave the valve in the “CLEAR” setting.
2. Press the “ENTER” keypad. Press the “REF” keypad.
3. The display will display “P1” for approximately 1 second, and then display a numerical value.
4. Using the “^” or “ν” keypads, respectively, increase or decrease the numerical value until it equals 59 (2'), 29 (3'), 22 (4'), 23 (5'), 29 (6') for the enclosure at 80 fpm inflow velocity.
5. Press the “ENTER” Keypad. The photometer will scan for 15 seconds, and then the “0” keypad will flash. Press the “Enter” keypad. The unit
will scan for 5 seconds, the display will read “0000,” and the unit will
sound a confirming tone.
6. Set the valve to “DOWNSTREAM.” Place the palm of your hand over the sampling port of the pistol. There should be a strong vacuum at this port. If the vacuum is weak, contact Air Techniques Hamilton Associates.
7. Turn the enclosure on and let it operate for a minimum of 5 minutes.
8. Maintain the following airflows at 80 fpm; 2' (115 cfm), 3' (230 cfm), 4' (305 cfm.), 5' (295 cfm), 6' (230 cfm, each impeller).
9. Position the aerosol generator discharge in the intake of the baffle inside the enclosure. For 6' sizes with two impellers, position the generator to the far left and the far right to test each filter.
10. Start the aerosol generator (Pressure to be +/- 1 psig). (10 psig). Ensure that one Laskin nozzle is in the “open” position.
11. Allow the generator to operate for a minimum of 15 seconds. For all integral motorized impeller models, scan the downstream exhaust side of the HEPA filter by passing the sampling nozzle of the gun above the perforated exhaust cover above the impeller. Scan the entire periphery of the perforated exhaust cover, within 1 inch of the surface.
Acceptance
Aerosol penetration as a downstream average shall not exceed 0.01 percent measured by the photometer.
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Change the Airflow Face Velocity (If Necessary)
The Paramount has been tested and shipped at a face velocity of 75-80 fpm. If necessary, refer to the instructions in Chapter 3 to change the face velocity.
Refer to the “Calibration” menus in Chapter 5 that refer to the “Pressure
Sensor” and “Airflow Alarm.” The “Calibration” menus require a password
to protect the ductless enclosure integrity and the password can only be obtained from Labconco Product Service for certifier use. The “Airflow Alarm” should be set at 10-20 fpm below the normal operating face velocity and it was tested and shipped at 60 fpm.
Initial Certification
The ductless enclosure has been certified at the factory for an inflow velocity of 75-80 fpm. The ductless enclosure should be certified for the proper inflow velocity required by your Safety Officer. Transport, altitude, or
temperature differences may require the “Calibration” of the “Pressure
Sensor” to be reset as outlined in Chapter 5: Using the Ductless Enclosure.
If a HEPA filter is used, it is a conservative recommendation to perform the HEPA Filter Leak Test should there be any damage to the media caused during transport.
Re-Certification
Under normal operating conditions, the enclosure should be recertified at least annually if serviced. The certifier should perform the following tests.
Airflow Velocity Test. If necessary, reset the Airflow Face Velocity and
Motor Speed per the “Calibration” of the “Pressure Sensor” menu listed
in Chapter 5.
HEPA Filter Leak Test, if installed.
In addition, the following test should also be performed at the user’s discretion:
Smoke Test to determine proper airflow patterns.
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Chapter 6: Maintaining the Ductless Enclosure
45
Figure 6-1
Light Replacement
Fluorescent Light Replacement
1. Disconnect the power.
2. Locate the small light reflector located under the control panel shown
in Figure 6-1.
3. Remove the light reflector by removing two Phillips screws on the
bottom of the light reflector.
4. Remove the old fluorescent lamp from the light sockets and metal
support clips as shown in Figure 6-2.
5. Reinstall the new fluorescent lamp and light reflector in reverse order.
6. Power the unit up and try the new fluorescent lamp.
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Chapter 6: Maintaining the Ductless Enclosure
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Figure 6-2
Light Replacement
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Chapter 6: Maintaining the Ductless Enclosure
47
Motorized Impeller Replacement
The motorized impeller (ECM) must be replaced as a complete unit; it has over 50,000 hours of useful life as tested. See Appendix A for Replacement Parts Diagram. See Figure 6-3 for a view of the motorized impeller plenum assembly.
1. Disconnect all power and consult the wiring diagram on the back of the front panel and disconnect all the wires of the motorized impeller from the quick disconnect connector. Be sure to connect wires on the new motor in the same way the old motor was wired and not get the wires or hoses tangled in the impeller.
2. Remove four screws in the motorized impeller bracket that hold it down. Remove the motorized impeller and bracket.
WARNING: High-speed blower. Never operate impeller with housing off.
3. Reassemble the new motorized impeller by reversing the assembly steps.
Figure 6-3
Motorized Impeller Replacement
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Main Control Board Replacement
If the main control board is replaced, the Paramount must be calibrated per the menu screens in Chapter 5. See Appendix A: Replacement Parts, and reference Figure 6-4.
1. Consult the wiring diagram on the back of the front panel and disconnect all power.
2. Remove the hardware to rotate the header control panel.
3. Locate the connectors to the main control board and remove the connectors per the wiring diagram.
4. Label the two pressure hoses and remove the two pressure hoses from the control board. The hoses must be installed properly with the front hose
corresponding with the front “total pressure” hose from the motorized
impeller assembly (front to front throughout).
5. Remove the control board from the plastic display bezel by removing the four Phillips screws.
6. Reassemble the new control board in reverse order and follow the “Calibration” menu screens from Chapter 5 as the Pressure Sensor, Airflow Alarm, and Organic Sensor all need calibration.
Figure 6-4
Main Control Board
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Chapter 6: Maintaining the Ductless Enclosure
49
Organic Sensor Board Replacement
If the organic sensor board is replaced, the Paramount must be calibrated for
the “Organic Sensor. Contact Labconco Product Service. See Appendix A: Replacement Parts and reference Figure 6-5. Please note that the 6'
Paramount utilizes two organic sensor boards, one for each motorized impeller.
1. Consult the wiring diagram on the back of the front panel and disconnect all power.
2. Remove the organic sensor connector as shown in Figure 6-5.
3. Remove the four Phillips screws that mount the organic sensor board.
4. Install the new organic sensor board in reverse order. Note: Be careful with the delicate electronic sensors on the organic sensor board and do not move them or rotate them.
5. Follow the “Calibration” menu screens from Chapter 5 as the Organic Sensor needs calibration. A separate code and procedure is required and Product Service must be contacted.
Figure 6-5
Organic Sensor Board
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50
CChhaapptteerr 77:: AAcccceessssoorriizziinngg tthhee DDuuccttlleessss EEnncclloossuurree
Catalog #
Description
6938100
HEPA Filter, 15" x 18" x 1.5", 99.99% efficient particulate
6938200
Activated Carbon Filter, Organic Vapor 7.5 lbs.
6938201
Impregnated Carbon Filter Acid-Sulfur 10 lbs.
6938202
Impregnated Carbon Filter, Ammonia-Amine 11 lbs.
6938203
Impregnated Carbon Filter, Formaldehyde-Formalin 10 lbs.
6938204
Mixed Bed Carbon Filter, Org. Vap., Acid-Sul., Ammon, Form (25% Mix) 10 lbs.
6938205
Impregnated Carbon Filter, Radioisotope 10 lbs.
Paramount
Size
Filter
Compartments
Required
No. of Filters
Total Organic
Vapor Filter Weight
2' 1 2
15 lbs.
3' 2 4
30 lbs.
4' 3 6
45 lbs.
5' 3 6
45 lbs.
6' 4 8
60 lbs.
There are several ways to accessorize and/or modify the ductless enclosure for your individual requirements. These include the addition of carbon filters, HEPA filters, work surfaces, impregnated carbon filters, base stands, base stand shelves, storage cabinets, seismic support, exhaust transition, remote blowers, exhaust dampers, utility shelf kits, syringe pump kits, deck mounted valves with work surface and sash closures.
1. Filters
The Paramount Ductless Enclosure operates with seven different filter types with at least one filter type required for successful operation:
The Paramount model sizes, filter compartments, and number of filters are listed below for installation convenience.
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Catalog #
Description
Dimensions (W x D x H)
3909900
Black, 2' W x 29", Epoxy
24" x 29" x 1"
3909901
Black, 3' W x 29", Epoxy
36" x 29" x 1"
3909902
Black, 4' W x 29", Epoxy
48" x 29" x 1"
3909906
Black, 4' W x 35.5" Epoxy
48" x 35.5" x 1"
3975504
4' (Deep) Stainless w/Trough
48" x 35.5" x 0.8"
3909907
Black, 5' W x 29" Epoxy
60" x 29" x 1"
3909908
Black, 5' W x 35.5" Epoxy
60" x 35.5" x 1"
3975502
5' Stainless w/ Trough
60 x 29" x 0.8"
3975503
5' (Deep) Stainless w/ Trough
60" x 35.5" x 0.8"
3909910
Black, 6' W x 29" Epoxy
72" x 29" x 1"
3909911
Black, 6' W x 35.5" Epoxy
72” x 35.5" x 1"
3975602
6' Stainless w/ Trough
72" x 29" x 0.8"
3975603
6' (Deep) Stainless w/ Trough
72" x 35.5" x 0.8"
2. Work Surfaces
An optional work surface is available to attach to the ductless enclosure. The black epoxy work surfaces are contoured to fit the dimensions of the ductless enclosures to contain spills. The stainless work surfaces include a front trough to contain spills. See Figure 3-1 for installation.
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Catalog #
Description
6963800
3' w x 29" d Black Epoxy Work Surface w/three deck mounted valves, cupsink, and gooseneck
6963801
4' w x 29" d Black Epoxy Work Surface w/three deck mounted valves, cupsink, and gooseneck
6963802
5' w x 29" d Black Epoxy Work Surface w/three deck mounted valves, cupsink, and gooseneck
6963803
6' w x 29" d Black Epoxy Work Surface w/three deck mounted valves, cupsink, and gooseneck
3. Work Surface with Deck Mounted Valves, Gooseneck, and Cupsink
The work surfaces supplied with deck mounted valves allow the convenience of water, air, and vacuum along with a cupsink and cold water gooseneck fixture.
NOTE: Work Surfaces with Deck Mounted Service Fixtures cannot be used with a Protector Solvent Cabinet. Solvent Cabinets have a top that cannot be penetrated.
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Catalog #
Description
Size (if applicable)
3746700
2' Base Stand w/Feet
2' x 29" x 27.5"-33.5"
3746701
3' Base Stand w/Feet
3' x 29" x 27.5"-33.5"
3746702
4' Base Stand w/Feet
4' x 29" x 27.5"-33.5"
3746703
5' Base Stand w/Feet
5' x 29" x 27.5"-33.5"
3746704
6' Base Stand w/Feet
6' x 29" x 27.5"-33.5"
3746710
2' Base Stand w/Casters
2' x 29" x 27.5"-33.5"
3746711
3' Base Stand w/Casters
3' x 29" x 27.5"-33.5"
3746712
4' Base Stand w/Casters
4' x 29" x 27.5"-33.5"
3746713
5' Base Stand w/Casters
5' x 29" x 27.5"-33.5"
3746714
6' Base Stand w/Casters
6' x 29" x 27.5"-33.5"
3811100
2' Shelf, Base Stand
25.4” x 20.4"
3811101
3' Shelf, Base Stand
25.4" x 32.4"
3811102
4' Shelf, Base Stand
25.4" x 44.4"
3811103
5' Shelf, Base Stand
25.4" x 56.4"
3811104
6' Shelf, Base Stand
25.4" x 68.4"
3857000
Seismic Support Bracket Kit
N/A
3780310
Portable 3' SoLo Hydraulic Lift Base Stand, 115V
53.5" x 34.3" x 17.2"-36.8"
3780314
Portable 3' SoLo Hydraulic Lift Base Stand, 230V
53.5" x 34.3" x 17.2"-36.8"
3780311
Portable 4' SoLo Hydraulic Lift Base Stand, 115V
65.5" x 34.3" x 17.2"-36.8"
3780315
Portable 4' SoLo Hydraulic Lift Base Stand, 230V
65.5" x 34.3" x 17.2"-36.8"
3780312
Portable 5' SoLo Hydraulic Lift Base Stand, 115V
77.5" x 34.3" x 17.2"-36.8"
3780316
Portable 5' SoLo Hydraulic Lift Base Stand, 230V
77.5" x 34.3" x 17.2"-36.8"
3780313
Portable 6' SoLo Hydraulic Lift Base Stand, 115V
89.5" x 34.3" x 17.2"-36.8"
3780317
Portable 6' SoLo Hydraulic Lift Base Stand, 230V
89.5" x 34.3" x 17.2"-36.8"
3780300
3' Electric Hydraulic Lift Base Stand, 115V, 60Hz
36.0" W x 29.0" Dp
3780303
3' Electric Hydraulic Lift Base Stand, 230V, 50Hz
36.0" W x 29.0" Dp
3780301
4' Electric Hydraulic Lift Base Stand, 115V, 60 Hz
48.0" W x 29.0" Dp
3780304
4' Electric Hydraulic Lift Base Stand, 230V, 50 Hz
48.0" W x 29.0" Dp
3780302
6' Electric Hydraulic Lift Base Stand, 115V, 60 Hz
72.0" W x 29.0" Dp
3780305
6' Electric Hydraulic Lift Base Stand, 230V, 50 Hz
72.0" W x 29.0" Dp
3780400
3' Manual Hydraulic Lift Base Stand
36.0" W x 29.0 Dp
3780401
4' Manual Hydraulic Lift Base Stand
48.0" W x 29.0" Dp
3780402
6' Manual Hydraulic Lift Base Stand
72.0" W x 29.0" Dp
3784000
Portable Caster Kit for Electric and Manual
Hydraulic Lift Base Stands
N/A
4. Base Stands, Accessory Shelves, Seismic Supports, and Hydraulic Lift Base Stands
The following base stands, hydraulic lift base stands, accessory shelves, and seismic supports may be used with the accessory work surfaces to support the Paramount Ductless Enclosures. Hydraulic Lift Base Stands allow easy movement up and down and through doorways as they are portable and can be supplied with toe-locking casters.
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SOLVENT
ACID
Size/Description
Dual Doors
Right Hinge
Left Hinge
Dual Doors
Right Hinge
Left Hinge
48"
9902000
-
-
9901000
-
-
36"
9902100
-
-
9901100
-
-
30"
9902200
-
-
9901200
-
-
24" - 9902300
9902400
-
9901300
9901500
18" - - - -
9901400
9901600
48" w/Self-Closing Doors
9903000
- - - - -
36" w/Self-Closing Doors
9903100
- - - - -
30" w/Self-Closing Doors
9903200
- - - - -
24" w/Self-Closing Doors
-
9903300
9903400 - -
-
24" ADA
-
9906000
9906100
-
9905000
9905200
24" ADA w/Self-Closing Doors
-
9906200
9906300 - -
-
18" ADA - - - -
9905100
9905300
STANDARD BASE
VACUUM PUMP
Size/Description
Dual Doors
Right Hinge
Left Hinge
Dual Doors
Right Hinge
Left Hinge
48"
9900000
- - - - -
36"
9900100
- - - - -
30"
9900200
- - - - -
24" - 9900300
9900600 - -
-
18" - 9900400
9900700
-
9907000
9907100
12" - 9900500
9900800 - -
-
5. Storage Cabinets
The following storage cabinets may be used with the accessory work surfaces to support the Paramount Ductless Enclosures.
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Catalog #
Description
6963700
Canopy Exhaust Transition (Paramount)
3927600
Flexible Hose, 6" ID Black with 6.09" ID cuffs, suitable for pharmaceutical and clean room applications. 8' length with two hose clamps.
6. Exhaust Transitions
Canopy Exhaust Transitions connect each motorized impeller for ducting to the outside. The Canopy Exhaust Transition is available for 6" nominal duct (6' Paramount requiring two). The Canopy Exhaust Transition should be sealed to the top of the enclosure with silicone sealant to prevent leaks.
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CFM @ Static Pressure-Inches of H2O
S.P.
0.0"
0.125"
0.25"
0.50"
0.75"
0.87"
CFM
595
560
515
420
300
167
Catalog #
Description
Shipping Wt.
(lbs./kg.)
4863500
Remote Blower, 115 V, 60 Hz. 4.4 amps
35/16
4863501
Remote Blower, 115/230 V, 50 Hz, 5.6/2.8 amps
35/16
7053501
Explosion-Proof Remote Blower, 115 V, 60 Hz, 4.4 amps
40/18
Catalog #
HP
Description
CFM@RPM Ranges at Static Pressure (inches of H20)
Std.
EP
.25"
.38"
.50"
.62"
.75"
.88"
1.00"
7068200
1/4
Remote Blower, 115V, 60 Hz, 4.4 A
540@800
410@800
350@870
390@970
7068300
1/4
Explosion Proof Blower 115V, 60 Hz, 4.5 A
720@950
760@1050
710@1060
620@1060
7068400
1/3
Remote Blower, 115V, 60 Hz, 6.1 A
760@1050
710@1060
620@1060
430@1060
460@1150
500@1220
7068500
1/3
Explosion Proof Blower, 115V, 60 Hz, 6.4 A
850@1130
825@1160
790@1190
770@1220
740@1260
640@1260
Dimensions
A
7.16" B 7.00" C 8.13" D 6.81"
E
9.25"
Inlet
10.87" ID
Outlet
5.5"D x 10.0"W
Wheel
9.0" Dia.
7. Remote Blowers – used to exhaust to the outside only.
6" nominal ID inlet blower has a 1/4 hp direct drive motor and corrosion-resistant epoxy-coated steel housing and wheel with blower inlet of 6.00" ID. Outlet dimensions are 4.25" x 7.38" OD.
10" nominal ID inlet blower has a 1/4 hp or 1/3 hp adjustable belt drive motor and corrosion resistant epoxy coated steel housing and wheel with blower inlet of 10.87" ID. Outlet dimensions are 5.5" x 10" OD.
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Catalog #
Description
3924000
6" Epoxy Coated Steel In-Line adjustable damper
4724200
6" PVC In-line adjustable damper
5983400
10" PVC In-line adjustable
3776800
10" Airtight Damper (10" tall)
Catalog #
Description
6924900
Syringe Pump Kit
6925700
Detector Tubes, Ammonia – Pkg. of 3
6925800
Detector Tubes, Acid – Pkg. of 3
6926000
Detector Tubes, Formaldehyde – Pkg. of 3
8. Exhaust Dampers
Exhaust dampers allow adjustments required to maintain proper airflow for roof-mounted blowers or house exhaust systems.
9. Utility Shelf Kits and Holders
Labconco offers a utility shelf kit part number 3925000 consisting of three shelves to hold items inside the enclosure. One shelf may be used for the printer, one shelf for spatulas and weigh brushes, and one miscellaneous shelf. The shelves hang from slots in the rear baffle.
Labconco also offers a 3927700 Bottle Holder with a 3" diameter opening and a 3927800 Tissue Holder to hold a 4.63" x 4.75" box of tissues. These holders also hang from slots in the rear baffle.
10. Syringe Pump Kit and Detector Tubes
The Syringe Pump Kit and chemical specific detector tubes may be used as a timed detection means to determine filter replacement. Chemical specific organic vapor detector tubes and pumps may be ordered from your laboratory supply dealer or directly from Dräger, Inc. or Sensidyne.
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Catalog #
Description
6963900
2' w x 9.4" h Sash Closure
6963901
3' w x 9.4" h Sash Closure
6963902
3' w x 12" h Sash Closure
6963903
4' w x 9.4" h Sash Closure
6963904
4' w x 12" h Sash Closure
6963905
5' w x 9.4" h Sash Closure
6963906
6' w x 12" h Sash Closure
11. Sash Closures
All Paramount Ductless Enclosures have a standard sash opening at the bottom consisting of 9.4" or 12". Sometimes it is necessary to close the lower sash opening during operating procedures. The Sash Closure consists of bi-fold doors to close the opening.
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CChhaapptteerr 88:: TTrroouubblleesshhoooottiinngg
PROBLEM
CAUSE
CORRECTIVE ACTION
Replace Filters continuous alarm occurs
Improper final time programmed and
display reads “Replace
Filters-t”, (t = time)
See Chapters 3 and 5 to properly set the Filter Final Life Timer.
Organic sensor alarms and display reads “Replace Filters-s”, (s = organic sensor)
Organic sensor has detected filter breakthrough. Replace filters immediately. A spare set of filters should always be on hand. Consult Chapters 3, 4, and 5, the Labconco Specialist, and the Chemical Guide for estimated filter life based on specific chemical use. All chemicals have a different estimated filter life based on specific chemical use. Always limit chemical use, cover up chemicals when not in use and turn off blower to preserve filter life.
“Mute” will not stay
operational
The “Mute” alarm can only be off for 5 minutes and must be pushed every 5 minutes until the filters have been replaced. See Chapters 3, 5 & 6.
Check Filters intermittent alarm occurs frequently
Improper check time programmed and
display reads “Check
Filters-t”, (t = time)
See Chapters 3 and 5 to properly set the Filter Check Life Timer.
Refer to the following table if your ductless enclosure fails to operate properly. If the suggested corrective actions do not solve your problem, contact Labconco for additional assistance.
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Chapter 8: Troubleshooting
60
PROBLEM
CAUSE
CORRECTIVE ACTION
Replace filters intermittent alarm occurs
Organic sensor alarms intermittently and display reads “Replace Filters-s”, s = organic sensor
Organic sensor has detected filter breakthrough and only 5-10% of filter life remains. Replace filters with a spare set of filters stored. Consult Chapters 3, 4, and 5, Filter Specialist, and Chemical Guide for filter life based on specific chemical use. All chemicals have different life. Always limit chemical use, cover up chemicals and turn off blower when not in used to preserve life.
Carbon filter loaded with chemicals.
Replace carbon filter.
Contaminants outside of enclosure
Improper user techniques for the enclosure.
See “Validate the Enclosure” Chapter 3 and
“Safety Precautions” Chapter 4 sections in
the manual.
Restriction of the baffle air slots or blockage of the exhaust outlet.
Remove obstruction to ensure that all air slots and the exhaust outlet are unobstructed.
External factors are disrupting the enclosure airflow patterns or acting as a source of contamination.
See “Location Requirements” Chapter 2,
Validate the Enclosure” Chapter 3, and
“Safety Precautions” Chapter 4 sections of
this manual.
Enclosure has improper face velocity.
Have enclosure certified per Chapter 6 and check exhaust system. Check carbon filters and replace if necessary. Enclosure should have an average face velocity of 60-100 fpm.
Blower will not operate
Unit not plugged into outlet.
Plug the enclosure into appropriate electrical service.
Circuit breaker(s) or Ground Fault Interrupter.
Reset circuit breaker.
Blower wiring is disconnected.
Inspect blower wiring.
Blower switch is defective.
Replace membrane switch on control panel.
Motorized impeller is defective.
Replace motorized impeller. See Chapter 6.
Low face velocity
Enclosure sash not closed.
Close sash to the lowest position.
HEPA filter clogged.
Replace HEPA filter.
Blower and lights will not operate
Unit not plugged into outlet.
Plug enclosure into appropriate electrical service.
Circuit breaker(s) tripped.
Reset or replace circuit breaker.
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Chapter 8: Troubleshooting
61
PROBLEM
CAUSE
CORRECTIVE ACTION
Lights do not work
Lamp not installed properly.
Inspect lamp installation.
Lamp wiring disconnected.
Inspect lamp wiring. Defective lamp.
Replace lamp.
Light switch is defective.
Replace membrane switch on control panel.
Defective electronic ballast.
Replace ballast.
Airflow monitor malfunction
No audible alarm.
Alarm has been temporarily silenced using “mute” button.
Wrong alarm set point.
Airflow monitor alarm is preset at 60 fpm. Repeat calibration steps outlined in this manual in Chapter 3, Chapter 5 and Chapter 6.
Constant audible alarm.
Check airflow and calibration of airflow monitor. See Chapter 5 & 6.
Continuous alarm.
Check the face velocity of the enclosure as the airflow of the system may have changed. If incorrect, follow the calibration steps in Chapters 3, 5 and 6. The carbon filter pre-filter or HEPA filter may have become loaded.
Low airflow.
Check airflow and reset airflow monitor. See Chapter 5 & 6. Look for filter blockage or paper debris.
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62
AAppppeennddiixx AA:: RReeppllaacceem
meenntt PPaarrttss
Item
Quantity
Part No.
Description
1A 1 6938100
HEPA Filter, 99.99% efficient on 0.3 micron, particulate
1B 1 6938200
Activated Carbon Filter, Organic Vapor, 7.5 lbs.
1C 1 6938201
Impregnated Acid-Sulfur Filter, 10 lbs.
1D 1 6938202
Impregnated Ammonia-Amine Filter, 11 lbs.
1E 1 6938203
Impregnated Formaldehyde-Formalin Filter, 10 lbs.
1F 1 6938204
25% Mixed Bed Carbon Filter, OV, Acid-Sul, Ammon, Form, 10 lbs.
1G 1 6938205
Impregnated Radioisotope Filter, 10 lbs.
2A 1 3991500
Sash Assy., 2' Short (22.7" IH)
2B 1 3991501
Sash Assy., 3' Short (22.7" IH)
2C 1 6970100
Sash Assy., 3' Tall (32" IH)
2D 1 3991502
Sash Assy., 4' Short (22.7" IH)
2E 1 6970101
Sash Assy., 4' Tall (32" IH)
2F 1
Sash Assy., 4' Extra Tall (35" IH)
2G 1 6976300
Sash Assy., 5' Tall (32" IH)
2H 1
Sash Assy., 5' Extra Tall (35" IH)
2I 1 3957301
Sash Assy., 6' Tall (32" IH)
2J 1
Sash Assy., 6' Extra Tall (35" IH)
3A 1 3907500
Sash Stop R.H.
3B 1 3907501
Sash Stop L.H.
4A 1 6916500
Latch, Sash
4B 1 3906700
Bracket, Latch
4C 1 1927403
Spring, Compression
4D 2 1893206
Screw, 8-32 x .38" lg. Phillips Pan S.S., Type F
4E 2 3973204
Sash Gas Spring Assy., 15# (3')
4F 2 3973203
Sash Gas Spring Assy., 20# (4')
4G 2 3973200
Sash Gas Spring Assy., 30# (5', 6')
5
1.9'
6913700
Wiper, Sash Seal
6A 2 1936800
Bushing, Closed 1.50" Dia.
6B 2 1934601
Bushing, w/Flex Shutter 1.50" Dia.
7 2 3915403
Side, Air Foil
8A 1 3907700
Light Reflector, 2' w
8B 1 3907701
Light Reflector, 3' w
8C 1 3907702
Light Reflector, 4' w
8D 1 3907703
Light Reflector, 5' w
8E 1 3907704
Light Reflector, 6' w
8F
2, 4 or 6
3908899
Reflector Tape
8G 2 1889308
Screw, #10-24 x 0.50 Phillips
The components that are available for your ductless enclosure are listed. The parts shown are the most commonly requested. If other parts are required, please contact Product Service.
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Appendix A: Replacement Parts
63
Item
Quantity
Part No.
Description
9A 1 6964700
Front Panel, 2'
9B 1 6964701
Front Panel, 3'
9C 1 6964702
Front Panel, 4'
9D 1 6964703
Front Panel, 5'
9E 1 6964704
Front Panel, 6'
9F 1 6964101
Label, Front Panel
10 1 6964100
Membrane Switch
11A 1 6964300
ECM Motorized Impeller, 115V
11B 1 6964301
ECM Motorized Impeller, 230V
12A 1 6972200
Ballast, 2' (uses 1295510 ballast with mtg. bracket)
12B 1 1295400
Ballast (3', 4', 5', or 6')
13A 1 3708300
Lamp, Fluorescent 2' (F15T8-SP35)
13B 1 9721902
Lamp, Fluorescent 3' (F17T8)
13C 1 9721901
Lamp, Fluorescent 4' (F25T8)
13D 1 9721900
Lamp, Fluorescent 5' (F32T8)
13E 1 9721903
Lamp, Fluorescent 6' (F40T8)
13F 2 3836800
Lamp Holder Socket, Push-On
13G 2 3836700
Clip, Lampholder
14 1 6964500
Main Control Board
15A
1 or 2
6965200
Organic Sensor Board
15B 1 6967800
Harness, Organic Sensor, 2' w
15C 1 6967900
Harness, Organic Sensor, 3'-5' w
15D 1 6968000
Harness, Organic Sensor, 6' w
16A 1 6967500
Main Harness, 2' w
16B 1 6967600
Main Harness, 3', 4', 5', 6' w
16C 1 6967700
Main Harness, 6' w Extra ECM Blower
17A
1 or 2
1327204
Circuit Breaker, 5A (115V) - 2', 3', 4', 5' or (230V) - 6'
17B 2 1327200
Circuit Breaker, 3A (230V) - 2', 3', 4', 5'
17C 1 1327201
Circuit Breaker, 10A, 6' (115V)
18A
30'
1554304
Tubing, Pressure Sensor – Airflow
18B
1 or 2
6969300
Bracket, Pitot Tube – Airflow
18C
4 or 8
1449400
Fitting, Pitot – Airflow
18D 1 6977400
Connection Tee, 6' Unit
19A 1 1305800
Power Cord, 115V, Right Angle
19B 1 1305900
Power Cord, 230V, Right Angle
20A
1 or 2
6913000
Gas Assist Spring, Filter Clamping
20B
2 or 4
1906225
Jam Nut 3/8-16
20C
2 or 4
1910018
Lockwasher 3/8 Split
20D
2 or 4
1881712
Screw, 3/8-16 Hex, .75 lg.
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Appendix A: Components
64
A-1
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65
AAppppeennddiixx BB:: PPaarraam
moouunntt DDii
m
meennssiioonnss
Models
Paramount Description
A B C D E
F
6963200, -20
2' Short
24.0
22.7
23.4
29.0
43.7
9.4
6963300, -20
3' Short
36.0
22.7
23.4
29.0
43.7
9.4
6963301, -21
3' Tall
36.0
32.0
23.4
29.0
53.0
12.0
6963302, -21
3' x 360 Visibility
36.0
32.0
23.4
29.0
53.0
12.0
6963400, -20
4' Short
48.0
22.7
23.4
29.0
43.7
9.4
6963401, -21
4' Tall
48.0
32.0
23.4
29.0
53.0
12.0
6963402, -22
4' x 360 Visibility
48.0
32.0
23.4
29.0
53.0
12.0
6963403, -23
4' Deep
48.0
35.0
30.0
35.5
56.0
12.0
6963501, -21
5' Tall
60.0
32.0
23.4
29.0
53.0
9.4
6963503, -23
5' Deep
60.0
35.0
30.0
35.5
56.0
9.4
6963601, -21
6' Tall
72.0
32.0
23.4
29.0
53.0
12.0
6963603, -23
6' Deep
72.0
35.0
30.0
35.5
56.0
12.0
(All dimensions in inches)
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66
AAppppeennddiixx CC:: SSppeecciiffiiccaattiioonnss
This Appendix contains technical information about all the Paramount Ductless Enclosures including electrical specifications and environmental operating conditions.
Electrical Specifications
All 2', 3', 4', 5' Paramounts – 100-115V, 5 Amps, 50/60 Hz or 230V,
3 Amps, 50/60 Hz.
6' Paramounts – 100-115V, 10 Amps, 50/60 Hz or 230V, 5 Amps,
50/60 Hz.
Environmental Conditions
Indoor use only.
Maximum altitude: 10,000 feet (3,058 meters). Airflow must be
recalibrated at altitudes above or below 900 feet (275 meters).
Ambient temperature range: 41° to 104°F (5° to 40°C).
Maximum relative humidity: 80% for temperatures up to 88°F
(31°C), decreasing linearly to 50% relative humidity at 104°F (40°C).
Main supply voltage fluctuations not to exceed ±10% of the nominal
voltage.
Transient overvoltages according to Installation Categories II
(Overvoltage Categories per IEC 1010). Temporary voltage spikes on the AC input line that may be as high as 1500V for 115V models and 2500V for 230V models are allowed.
Used in an environment of Pollution degrees 2 (i.e., where normally
only non-conductive atmospheres are present). Occasionally, however, a temporary conductivity caused by condensation must be expected, in accordance with IEC 664.
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67
AAppppeennddiixx DD:: QQuuiicckk CChhaarrtt
Model No.’s
6963200, -20
6963300, -20
6963301, -02,
-21, -22
6963400, -20
6963401, -02,
-03, -21, -22,
-23
6963501, -03,
-21, -23
6963601, -03,
-21, -23
Model Size
2'
3'
3'
4'
4'
5'
6'
Sash Height from Work Surface
(inches)
9.4
9.4
12.0
9.4
12.0
9.4
12.0
Total Open Area with Bypass (sq.
ft.)
1.45
2.20
2.85
2.95
3.80
3.70
5.80
Exhaust Airflow Volume at 80fpm
(CFM)
115
175
230
235
305
295
465
Alarm Airflow Volume at 60 fpm
(CFM)
85
130
170
175
230
220
350
*Motor Horsepower (HP)
0.06
0.06
0.09
0.09
0.16
0.16
0.26
Fluorescent Lights
F15T8-SP35
F17T8
F17T8
F25T8
F25T8
F32T8
F40T8
Number of Filters
2 4 4 6 6 6 8
Blower Power (watts)
49
45
73
71
122
118
197
Light Power (watts)
22
24
24
32
32
39
53
Total Power w/display(watts)
66
65
93
99
150
153
241
Electric Energy Cost ($)
(based on 2000 hours per year and
$0.078/kwh)
$11
$11
$16
$16
$25
$26
$40
Operating Filter Cost ($)
(based on one annual organic filter change)
$400
$800
$800
$1200
$1200
$1200
$1600
Ductwork Installation Cost ($)
$0
$0
$0
$0
$0
$0
$0
Adaptability/Mobility Cost ($)
$0
$0
$0
$0
$0
$0
$0
Total Annual Operating Cost ($)
$411
$811
$816
$1216
$1225
$1226
$1640
Conventional Fume Hood Comparison
based on $7 per CFM at 100 fpm
$1015
$1540
$1995
$2065
$2660
$2590
$4060
Paramount Ductless Enclosure Wattage, Energy Use, and Operating Costs.
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68
AAppppeennddiixx EE:: EEssttiim
maatteedd FFiilltteerr LLiiffee CCaallccuullaattiioonn
The following examples are useful for estimating filter life so the Filter Life Timers can be set properly.
Organic Vapor Carbon Filter Life Consult the separate Paramount Chemical Guide and/or Labconco Specialist to determine the filter capacity for your chemical. For example, assume you are working with 10 ppm acetone in a 3' Paramount loaded with the required four filters. Acetone has a specific gravity SPGR = 0.79 with a molecular weight MW = 58.1. A 3' Paramount at 80 fpm uses 175 CFM or 4956 LPM. The evaporation rate in ml/min can be solved by the following equation: PPM = (SPGR/MW) * (24400000/Airflow (LPM)) * Evap. Rate (ml/min).
For 10 ppm acetone or 90 ml lost per week during 2 hours use per day, the equations are solved below:
There are 30 pounds of activated carbon in a 3' Paramount which equals 13,500 g. Thus, the carbon Filter Life Time is calculated for acetone with a 2% filter capacity at (13,500 g/0.12 g/min) / (1 hour/60 min) * 2% capacity = 38 hours. The Final Life Timer should be set for 40 hours, rounded up from 38 hours. The Check Life Timer should be set for 20-25% intervals or every 10 hours and the carbon filters can be validated every 10 hours to verify safe filter use.
Other chemicals such as ethyl acetate at 9% filter capacity and toluene at 20% filter capacity have much longer filter lives. For example, ethyl acetate at 10 ppm used in the 3' Paramount will have a Filter Life of 120 hours. Furthermore, toluene at 10 ppm used in the 3' Paramount will have a Filter Life of 240 hours. These three chemicals are summarized in the table that follows to show the Filter Life ranges and you should consult the Labconco Specialist and/or Paramount Chemical Guide for further information on other chemicals.
10 = (0.79/58.1) * (24400000/4956) * Evap. Rate (ml/min)
Evap. Rate = 0.15 ml/min = 90 ml/week * 1 week /10 hours use *
10 hours/600 minutes
Evap. Rate in (g/min) = 0.15 ml/min * 0.79 g/ml = 0.12 g/min
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Appendix E: Accessories
69
2' (2 Filters)
3' (4 Filters)
4' & 5' (6 Filters)
6' (8 Filters)
Inlet
Concentration
Evap.
Rate
(ml/min)
Organic
Chemical
SPGR
MW
Organic
Vapor
Adsorbed
Filter
Capacity
Estimated
Filter Life
Estimated
Check Life
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
10 ppm
0.15
Acetone
0.79
58.1
2%
40 hours
10 hours
135 g
171 ml
270 g
342 ml
405 g
513 ml
540 g
684 ml
10 ppm
0.20
Ethyl
Acetate
0.90
88.1
9%
120 hours
30 hours
608 g
675 ml
1216 g
1350 ml
1824 g
2025 ml
2432 g
2700 ml
10 ppm
0.22
Toluene
0.87
92.1
20%
240 hours
60 hours
1350 g
1552 ml
2700 g
3104 ml
4050 g
4656 ml
5400 g
6208 ml
2' (2 Filters)
3' (4 Filters)
4' & 5' (6 Filters)
6' (8 Filters)
Chemical
Impregnated
Carbon
Adsorbed
Filter Capacity
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
Adsorbed
Weight
Adsorbed
Volume
37% Hydrochloric Acid
17%
1530 g
3600 ml
3060 g
7200 ml
4590 g
10800 ml
6120 g
14400 ml
67% Nitric Acid
12%
1080 g
1150 ml
2160 g
2300 ml
3240 g
3450 ml
4320 g
4600 ml
96% Sulfuric Acid
11%
990 g
560 ml
1980 g
1120 ml
2970 g
1680 ml
3960 g
2240 ml
37% Formaldehyde or Formalin
10%
900 g
2250 ml
1800 g
4500 ml
2700 g
6750 ml
3600 g
9000 ml
50% Ammonia Solution (Ammonium Hydroxide)
10%
990 g
1980 ml
1980 g
3960 ml
2970 g
5940 ml
3960 g
7920 ml
If the inlet concentration is decreased to 1 ppm, then the estimated filter life will be increased by an average factor of 5. Likewise, if the inlet concentration is increased to 25 ppm, then the estimated filter life will be decreased by an average factor of 2. Experience with routine use will establish a predictable filter life that is representative of your specific chemical work.
Impregnated Carbon Filter Life To estimate impregnated carbon filter life for acids, formaldehyde-formalin, and ammonia, use the following chart below. The values in the chart below are expressed in weight (grams) and volume (milliliters) which can be used to estimate Filter Life from a known usage.
For example, you estimate that 37% hydrochloric acid is being used at 500 ml per week and want to know how to program the Filter Life timer for a 3' Paramount. A 3' Paramount uses 40 pounds of impregnated carbon at 17% estimated life before saturation. 17% of 40 pounds is equivalent to 3060 grams of available carbon. There are 424 g/L of hydrochloric acid in a 37% solution. Thus, there are 3060 grams/424 g per L or 7.2 Liters (7200 ml) of hydrochloric acid before saturation. Assuming there are 10 hours of use per week at 500 ml per week, the expected Final Life is programmed at 140 hours and the Check Life is programmed at 40 hours and it comes from the following calculation:
(7200 ml/500 ml/week) * 10 hours/week = 144 hours, rounded to 140 hours
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70
AAppppeennddiixx FF:: FFiillttrraattiioonn EEffffiicciieennccyy TTeesstt RReessuullttss
Exposure Evaporation No. of 3' Paramount Chemical Mass Detected Saturation Filtration Capacity Filtration
Chemical Limit Rate Filters Carbon Filter Mass Adsorbed Breakthrough Concentration Tested Theoretical Efficiency
Acetone 250 ppm 22 ppm 4 13500 grams 153 grams 1-2 ppm 1.1% 2.8% 39%
Ethanol or 1000 ppm 14 ppm 4 13500 grams 32 grams 6-9 ppm 0.3% 1.6% 19%
Ethyl Alcohol 1000 ppm 206 ppm 4 13500 grams 148 grams 6-9 ppm 1.1% 6.3% 17%
Isopropyl Alcohol 400 ppm 462 ppm 4 13500 grams 824 grams 8-11 ppm 6.1% 17.7% 34%
Toluene 100 ppm 155 ppm 4 13500 grams 1317 grams 0.5-1 ppm 9.8% 29.7% 33%
37% Hydrochloric 5 ppm 100 ppm 4 18000 grams 2529 grams 0.5-1 ppm 14.1% 17.0% 83%
Acid of treated carbon
Ductless enclosures require filtration efficiency testing to validate performance. Independent testing, conducted by a consultant and the University of Kansas, concluded the tested filtration efficiency for acetone, ethanol, isopropyl alcohol, toluene and hydrochloric acid was excellent. Filtration capacity is defined as a percentage of the chemical mass adsorbed compared to the total carbon filter weight. Utilizing analytical instrumentation, the organic vapor filter and acid vapor filter were both independently tested for filtration efficiency. The solvents and acids listed below were evaporated at both low and high evaporation rates. Low evaporation rates are typical in ductless enclosures in order to maximize useful carbon filter life. Both ethanol and acetone were specifically tested at low evaporation rates of 14ppm and 22ppm, respectively, to simulate real laboratory conditions of chemicals with low filter capacities. High evaporation rates of 100-462ppm were used for most of the organic solvents and mineral acid to accelerate the testing process of chemicals with higher filtration capacity and determine filter saturation and chemical breakthrough. The testing was designed to assess the filtration efficiency of the filters. As suggested by carbon manufacturers, carbon filters usually have a 30 percent to 40 percent filtration capacity of theoretical values for organic chemicals with higher carbon affinity. The test results show a filtration efficiency of 33-39 percent for chemicals with higher affinity for organic vapor carbon and directly in line with the 30-40 percent as suggested by carbon manufacturers. Since ethanol has very low filter capacity, it is not alarming that the filtration efficiency is 17-19 percent; the test results prove the practical matter of using low quantities of ethanol or any other chemical with very lower filter capacity. The mineral acid filtration efficiency of hydrochloric acid approached 83 percent of theoretical value and is attributed to the chemisorption process of the treated acid filters. To conclude, the filtration efficiency test data and charts indicate the ductless enclosure filtration was in line with carbon manufacturer expectations and will provide a safe working environment for controlled environments.
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Appendix E: Accessories
71
3' Paramount Model #6963300
Acetone (Reagent Grade) Test 9/10/08
SEFA 9 Method
0
0.5
1
1.5
2
2.5
3
0 20 40 60 80 100 120 140 160 180
Mass Adsorbed (grams) Acetone
Acetone Exhaust Concentration (ppm)
Acetone
Exposure limit
250 ppm
Temp. 22° C
Hum. 41%
175 CFM
80 fpm face
Evaporation by
heated container
Average evaporation
rate 0.32 ml/min. 21.9
ppm inlet conc.
30# carbon 4x8
coconut shell
Test time 11.25 hrs.
400 ppm current TLV
PID detector
1-2 ppm
Breakthrough with
153 grams filtration
capacity
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Appendix D: Accessories
72
0
20
40
60
80
100
120
140
0 100 200 300 400 500 600 700
Mass Adsorbed (grams)
Ethyl Alcohol Exhaust Concentration (ppm)
Ethyl Alcohol
or Ethanol
3' Paramount Model # 6963300
Ethyl Alcohol (Reagent Grade) Test 10/01/08
SEFA 9 Method
Exposure limit 1000
ppm
Temp. 20° C
Hum. 41%
175 CFM
80 fpm face
Evaporation by heated
container
Average evaporation
rate 2.44 ml/min. 206
ppm inlet conc.
30# carbon 4x8 coconut
shell
Test time 5.25 hrs.
1000 ppm current TLV
PID detector
6-9 ppm Breakthrough
with 148 grams filtration
capacity
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Appendix E: Accessories
73
3' Paramount Model # 6963300
2-Propanol (Reagent Grade) Test 9/16/08
SEFA 9 Method
0
50
100
150
200
250
300
350
400
450
0 500 1000 1500 2000 2500 3000
Mass Adsorbed (grams) 2-Propanol
2-Propanol Exhaust Concentration (ppm)
2-Propanol or
Isopropyl Alcohol
Exposure limit 400 ppm
Temp. 20° C
Hum. 41%
175 CFM
79 fpm face
Evaporation by heated
container
Average evaporation rate
7.13 ml/min. 462 ppm inlet
conc.
30# carbon 4x8 coconut
shell
Test time 7.15 hrs.
400 ppm current TLV
PID detector
8-11 ppm Breakthrough with
824 grams filtration capacity
Product Service 1-800-522-7658
Appendix D: Accessories
74
3' Paramount Model # 6963300
Toluene (Reagent Grade) Test 9/23/08
SEFA 9 Method
0
10
20
30
40
50
60
70
80
90
100
0 500 1000 1500 2000 2500
Mass Adsorbed (grams) Toluene
Toluene Exhaust Concentration (ppm)
Toluene
Exposure limit 100
ppm
Temp.22 C
Hum. 40%
175 CFM
79 fpm face
Evaporation by
heated container
Average evaporation
rate 3.32 ml/min. 155
ppm inlet conc.
30# carbon 4x8
coconut shell
Test time 12.25 hrs.
100 ppm current TLV
PID detector
0.5-1 ppm
Breakthrough with
1317 grams filtration
capacity
Product Service 1-800-522-7658
Appendix E: Accessories
75
0
0.5
1
1.5
2
2.5
3
3.5
4
4.5
0 500 1000 1500 2000 2500 3000
Mass Adsorbed (grams) HCL - Mass Calculated as 100% HCL
HCL Exhaust Concentration (ppm)
HCL mass calculated as
100% HCL
3' Paramount Model # 6963300
HCL Acid Test 10/02/08
SEFA 9 Method
Exposure limit 5 ppm
Temp. 20° C
Hum. 41%
175 CFM
79 fpm face
Evaporation by heated
container
Average evaporation rate
1.72 ml/min 100 ppm inlet
conc.
40# carbon 4x8 coconut
shell impregnated
Test time 24.6 hrs.
5 ppm current TLV
Detection: Continous
monitoring of exhaust at
1.5 ml/min with acid gas
colorimetric tubes until
begin of color change, then
exhaust sample every 15-
30 minutes with HCL
colorimetric tubes 1-10
ppm.
0.5-1 ppm Breakthrough
with 2529 grams filtration
capacity
Product Service 1-800-522-7658
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