Knick Protos 3400, Protos 3400X, Protos PHU 3400-110, Protos PHU 3400X-110 User Manual

Download

Page 1

The Art of Measuring.

Analysenmesssystem Protos 3400(X)

Messmodul Protos CONDI 3400 (X)-051 zur Leitfähigkeitsmessung mit induktiven Sensoren

Deutsch

Protos 3400(X)

User Manual

English

Process Analysis System

Protos PHU 3400(X)-110 Communication Module For Actuating Probe Controllers (Unical / Uniclean)

-Automatic pH Measurement-

Latest Product Information: www.knick.de

Page 2

Return of products under warranty

Please contact our Service Team before returning a defective device. Ship the cleaned device to the address you have been given. If the device has been in contact with process fluids, it must be decontaminated/ disinfected before shipment. In that case, please attach a corresponding certificate, for the health and safety of our service personnel.

Disposal

Please observe the applicable local or national regulations concerning the disposal of “waste electrical and electronic equipment”.

Trademarks

The following trademarks are used in this manual without further marking:

CalCheck®, Calimatic®, Protos®, Sensocheck®, Sensoface®, Unical®, VariPower®, Ceramat®, SensoGate® are registered trademarks of Knick Elektronische Messgeräte GmbH & Co. KG, Germany

Memosens® is a registered trademark of Endress+Hauser Conducta GmbH & Co. KG, Germany Knick Elektronische Messgeräte GmbH & Co. KG, Germany

SMARTMEDIA® is a registered trademark of Toshiba Corp., Japan

Knick

Elektronische Messgeräte GmbH & Co. KG Beuckestr. 22 14163 Berlin, Germany

Phone: +49 30 801 91 - 0 Fax: +49 30 801 91 - 200 Web: www.knick.de Email: [email protected]

Page 3

Protos PHU 3400(X)-110 Module

Return of products under warranty .................................................................................... 2

Disposal ......................................................................................................................................... 2

Trademarks ................................................................................................................................... 2

Intended Use .................................................................................................... 9

Conformity with FDA 21 CFR Part 11 .................................................................................. 9

Safety Information ........................................................................................ 10

Application in Hazardous Locations: PHU 3400X-110 Module ...............................10

Software Version ......................................................................................................................11

Modular Concept .....................................................................................................................13

Short Description .......................................................................................... 14

Short Description: FRONT Module ....................................................................................14

Short Description: Menu Structure ....................................................................................15

Short Description: BASE Module ........................................................................................ 17

Overview of the System Components .............................................................................18

PHU 3400(X)-110 Module ......................................................................................................20

Terminal Plate PHU 3400(X)-110 Module .................................................... 21

Inserting the Module .................................................................................... 22

Wiring Example VP and SixPlug ..........................................................................................23

Connecting the Probe Controller ................................................................. 25

Menu Selection .............................................................................................. 26

Menu Structure .............................................................................................. 26

Passcode Entry ............................................................................................... 27

Changing a passcode .....................................................................................................27

Configuring the Measurement Display .......................................................28

Start-Up .......................................................................................................... 30

Parameter Setting: Operating Levels .......................................................... 31

Administrator level .........................................................................................................31

Operator level ...................................................................................................................31

Viewing level .....................................................................................................................31

Parameter Setting: Locking a Function ...........................................................................32

Page 4

Table of Contents

Protos PHU 3400(X)-110 Module

Parameter Setting for PHU 3400(X)-110 .....................................................33

Activating Parameter Setting ..............................................................................................33

Settings of Sensor Data..........................................................................................................34

Sensoface ....................................................................................................................................36

SW 3400-005: Tolerance Adjustment ................................................................................ 39

Activating the Cal Tolerance Band ............................................................................40

Documenting Parameter Setting .......................................................................................47

ProgaLog 3000 Software (Option) forConfiguration and Documentation .......49

Configuration using "ProgaLog 3000" .....................................................................52

Logbook, Factory Setting ......................................................................................................53

Configuring a Current Output .............................................................................................54

Current Outputs: Characteristics ........................................................................................55

Output Filter ...............................................................................................................................57

NAMUR Signals: Current Outputs ......................................................................................58

NAMUR Signals: Relay Contacts ..........................................................................................59

Relay Contacts: Protective Wiring ......................................................................................60

Relay Contacts, Usage ............................................................................................................61

Relay Contacts: Sensoface Messages ................................................................................62

Rinse Contact .............................................................................................................................63

Limit Value, Hysteresis, Contact Type................................................................................64

Icons in the Measurement Display ....................................................................................64

OK1, OK2 Inputs: Specify Level ...........................................................................................65

Selecting Parameter Set (A, B) via OK2 Input ................................................................66

Signaling Active Parameter Set via Relay Contact .......................................................66

Unical 9000(X) Parameter Setting ............................................................... 67

Cal Preset Values Unical 9000 .....................................................................................68

Time Control ......................................................................................................................68

Page 5

Table of Contents

Protos PHU 3400(X)-110 Module

Parameter Setting: Program Flows ....................................................................................70

Cleaning (Continuous), Media Monitoring Off .....................................................70

Cal 2point (Continuous), Media Monitoring Off ..................................................71

Cal 1point (Continuous), Media Monitoring Off ..................................................72

Parking .................................................................................................................................74

Measurement (Short-Time), Media Monitoring Off ............................................75

Cal 2point (Short-Time), Media Monitoring Off ...................................................76

Cal 1point (Short-Time), Media Monitoring Off ...................................................77

Service .................................................................................................................................78

Configuring the Program Flow ...................................................................................79

Entering a Program Name ............................................................................................79

Editing a Program Step .................................................................................................79

Configuring a Function .................................................................................................80

Activating Monitoring ...................................................................................................80

Parameter Setting: Installation ............................................................................................81

Selecting the Measurement Procedure ...................................................................82

External Control via DCS ...............................................................................................82

Control via Process Control Cystem (DCS) ......................................................................83

Control Programs and Meas. Procedures ........................................................................84

Sensor Detection .............................................................................................................85

Probe ....................................................................................................................................85

Configuring Media Monitoring ...........................................................................................86

Media Adapter ..................................................................................................................87

Additional Media (2) .......................................................................................................87

Start-Up ...............................................................................................................................87

System Forecast (Ceramat, SensoGate) ....................................................... 88

Reference / Probe Travel Profiles ...............................................................................89

Creation of a Probe Travel Profile and Presentation in Protos ........................89

Setting the System Forecast Parameters .........................................................................90

System Forecast: Reference Profile ...........................................................................91

System Forecast: Tolerance Specifications ............................................................. 93

System Forecast: Diagnostic Messages ...................................................................95

System Forecast: RecordingonSmartMediaCard ..............................................96

Page 6

Table of Contents

Protos PHU 3400(X)-110 Module

Uniclean 900(X) Parameter Setting ............................................................. 98

Measuring Module ..........................................................................................................99

Time Control ......................................................................................................................99

Parameter Setting: Program Flows ................................................................................. 101

Rinsing (Continuous) ...................................................................................................101

Cleaning (Continuous) ................................................................................................102

Parking .............................................................................................................................. 104

Measuring (Short-Time) .............................................................................................105

Service .............................................................................................................................. 106

Editing a Program Step ..............................................................................................107

Configuring a Function .............................................................................................. 107

Parameter Setting: Installation .........................................................................................108

Selecting a Measurement Procedure .................................................................... 109

External Control via DCS ............................................................................................ 109

Control via Process Control System (DCS) ...................................................................110

Control Programs and Meas. Procedures ..................................................................... 111

Sensor Detection .......................................................................................................... 112

Probe ................................................................................................................................. 112

Media Adapter ............................................................................................................... 113

Additional Media (2) .................................................................................................... 113

Start-Up ............................................................................................................................ 113

Calibration / Adjustment ............................................................................114

Calibration Methods ............................................................................................................ 116

One-Point Calibration ................................................................................................. 116

Two-Point Calibration ................................................................................................. 116

Three-Point Calibration .............................................................................................. 116

Sensor Replacement (First Calibration) ................................................................ 116

Temperature Compensation ............................................................................................. 117

Automatic Calibration .........................................................................................................118

Manual Electrode Calibration ........................................................................................... 120

HOLD Function During Calibration ................................................................................ 122

Page 7

Table of Contents

Protos PHU 3400(X)-110 Module

Selecting a Calibration Method ....................................................................................... 123

Calimatic Automatic Buffer Recognition .............................................................124

Calibration with Manual Entry of Buffer Values ................................................ 126

Product Calibration .....................................................................................................128

Calibration by Entering Data from Premeasured Electrodes ....................... 130

ORP Calbration/Adjustment .................................................................................... 132

ISFET Zero Adjustment ..............................................................................................134

Maintenance of PHU 3400(X)-110 ..............................................................136

Sensor Monitor ....................................................................................................................... 136

Temp Probe Adjustment.....................................................................................................136

Probe Maintenance via Protos 3400(X) .....................................................137

Diagnostics Functions ................................................................................. 141

Point of Meas Description ......................................................................................... 141

Logbook ........................................................................................................................... 141

Device Description ....................................................................................................... 142

Diagnostics of PHU 3400(X)-110 ..................................................................................... 143

Module Diagnostics.............................................................................................................. 143

Sensor Monitor .............................................................................................................. 143

Calibration Timer .......................................................................................................... 144

Tolerance Adjustment .................................................................................................144

Cal Record ....................................................................................................................... 145

Sensor Network Diagram .......................................................................................... 145

Statistics ........................................................................................................................... 145

Diagnostics of Unical 9000(X) ...........................................................................................146

Unical Status ................................................................................................................... 146

Unical Network Diagram ........................................................................................... 146

Diagnostics of Uniclean 900(X) ........................................................................................ 147

Uniclean Status .............................................................................................................. 147

Diagnostic Messages of System Forecast ..................................................................... 148

Setting Diagnostics Messages as Favorite ................................................149

Page 8

Table of Contents

Protos PHU 3400(X)-110 Module

Message List ........................................................................................................................... 151

Messages ...................................................................................................... 152

System Forecast Messages ................................................................................................ 161

Error Messages of Unical 9000(X) .................................................................................... 162

Error Messages of Uniclean 900(X) ................................................................................. 168

Specifications ...............................................................................................172

Appendix: ..................................................................................................... 176

Minimum Spans for Current Outputs ............................................................................ 176

Buffer Table "Mettler-Toledo" ............................................................................................ 177

Buffer Table "Knick CaliMat" .............................................................................................. 178

Buffer Table "DIN 19267" .................................................................................................... 179

Buffer Table "NIST Standard" (DIN 19266: 2000-01).................................................. 180

Buffer Table "Techn. Buffers to NIST" .............................................................................. 181

Buffer Table "Hamilton" ....................................................................................................... 182

Buffer Table "Kraft" ................................................................................................................ 183

Buffer Table "Hamilton A" ................................................................................................... 184

Buffer Table "Hamilton B" ................................................................................................... 185

Buffer Table "HACH" ............................................................................................................. 186

Buffer Table "Ciba"................................................................................................................. 187

Buffer Table "Reagecon"...................................................................................................... 188

SW 3400-002: Specifiable Buffer Sets ............................................................................ 189

Overview of Parameter Setting ..................................................................190

Index ............................................................................................................. 196

Menu Selection ............................................................................................ 210

Quick Access .................................................................................................211

Page 9

Intended Use

The module is used for simultaneous pH, ORP, and temperature measurement with glass electrodes. It allows connection of the Unical 9000(X) probe controller for fully automated pH measurement, cleaning, and calibration or the Uniclean 900(X) for fully automated pH measurement. The PHU 3400X-110 module is intended for operation in locations subject to explosion hazards which require equipment of Group II, device category 2(1), gas/dust.

Conformity with FDA 21 CFR Part 11

In their directive “Title 21 Code of Federal Regulations, 21 CFR Part 11, Electronic Records; Electronic Signatures“ the US American health agency FDA (Food and Drug Administration) regulates the production and processing of electronic documents for pharmaceutical development and production. This results in requirements for measuring devices used for corresponding applications. The following features ensure that the Protos 3400(X) modular process analysis system meets the demands of FDA 21 CFR Part 11:

Electronic Signature

Access to the device functions is regulated and limited by individually adjustable codes – “Passcodes“. This prevents unauthorized modification of device settings or manipulation of the measurement results. Appropriate use of these passcodes makes them suitable as electronic signature.

Audit Trail Log

Every change of device settings can be automatically recorded and documented in the Audit Trail Log on the SmartMedia card. The recording can be encrypted.

Page 10

Safety Information

Application in Hazardous Locations

Caution!

Never try to open the module! If a repair should be required, return the module to our factory.

If the specifications in the instruction manual are not sufficient for assessing the safety of operation, please contact the manufacturer to make sure that your intended application is possible and safe.

Be sure to observe during installation:

• Switch off power supply before replacing or inserting a module.

• Protect the signal inputs of the modules against electrostatic discharge.

• Before commissioning it must be proved that the device may be connected with other equipment.

• Observe correct shielding: To avoid interferences, the cable shielding must be completely covered by the ESD shielding cap.

Application in Hazardous Locations: PHU 3400X-110 Module

The module is approved for operation in hazardous locations. Observe all applicable local codes and standards for the installation of electrical equipment in hazardous locations. For orientation, please refer to IEC 60079-14, EU directives 2014/34/EU and 1999/92/EC (ATEX), NFPA 70 (NEC), ANSI/ISA-RP12.06.01.

• When installing the device in a hazardous location, observe the specifications of the EC-Type-Examination Certificate and, if applicable, of the Control Drawing (download: www.knick.de).

• Before commissioning you must prove that the device may be connected with other equipment, such as a supply unit including cables and wires.

• In hazardous locations the device shall only be cleaned with a damp cloth to prevent electrostatic charging.

• Devices and modules which have already been used shall be subjected to a professional routine test before they may be operated in another zone or another type of protection.

Page 11

Software Version

PHU 3400(X)-110 Module

Device Software Protos 3400(X)

The PHU 3400(X)-110 module is supported by software version 5.0 or higher.

Module Software PHU 3400(X)-110

Software version 3.x

Query actual device/module software

When the analyzer is in measuring mode: Press menu key, open Diagnostics menu: Device description

Menu Display Device description

Device description

Module FRONT 3400-011 Operating panel Protos Hardware: 1.1, Software: A.2 Serial number: 08150815

Module

FRONT

Return

Device description

Module PHU 3400-110 Input for pH, ORP and °C Hardware: 1, Software: 3.0 Serial number: 471101147

Module

FRONT

Return

BASE

7.00 pH

22.7 °C

Options

7.00 pH

22.7 °C

Options

Device hardware and software version

Provides information on all modules installed: Module type and function, serial number, hardware and software version and device options. Select the different modules (FRONT, BASE, slots 1 - 3) using the arrow keys.

Query module software

Module PHU 3400-110, hardware and software version, serial number – here installed in slot3.

Page 12

Page 13

Modular Concept

Basic unit, measuring modules, additional functions

The Protos 3400(X) is an expandable modular process analysis system. The basic unit (FRONT and BASE modules) provides three slots which can be equipped by the user with any combination of measuring or communication modules. The software capabilities can be expanded by additional functions (options). Additional functions must be ordered separately. They are supplied with a device-specific TAN for function release.

Protos 3400(X) Modular Process Analysis System

Additional functions

Activation via device-specific TAN

SmartMedia card

Data recording

ProgaLog 3000

Windows® software for parameter setting and data evaluation

3 module slots

for free combination of measuring and communication modules

Measuring modules

• pH / ORP / Temp

• O2 / Temp

• Noncontacting conductivity / Temp

• Contacting conductivity / Temp

• Memosens sensors

Communication modules

• OUT (additional switching and current outputs)

• PID (analog and digital controller)

• Profibus PA

• Foundation Fieldbus

• FIU (radio, Memosens, Unical) (software occupies 2 slots)

• Unical probe controller

Documentation The basic unit is accompanied by a CD-ROM containing the complete documentation. Latest product information as well as user manuals for earlier software releases are available at

www.knick.de.

Page 14

Short Description

Short Description: FRONT Module

4 captive screws

for opening the analyzer (Caution! Make sure that the gasket between FRONT and BASE is properly seated and clean!)

%Air

°C

24.0°C

25.8°C

Transflective LC graphic display

(240 x 160 pixels) white backlighting, high resolution and high contrast.

Measurement display

User interface

with plaintext menus as recommended by NAMUR. Menu texts can be switched to: German, English, French, Italian, Swedish/Portuguese or Spanish. Intuitively acquirable menu logic, based on Windows standards.

Secondary displays

2 softkeys

with context-sensitive functions.

Red LED

signals failure (On) or maintenance request/function check (flashing) according to NE 44.

Control panel

3 function keys (menu, meas, enter) and 4 arrow keys for menu selection and data entry

Green LED

Voltage supply okay

5 self-sealing cable glands

M20 x 1.5 for entry of voltage supply and signal lines

Page 15

Short Description: Menu Structure

Basic functions: Calibration, Maintenance, Parameter setting, Diagnostics

Menu groups

Parameter setting

Calibration

Maintenance

Measure

Passcode:

Selection of further menu items:

1147

Module 1 Module 2 Module 3

2958

BASE

Module 1 Module 2 Module 3

1246

Operator level

1989

Administrator level

SYSTEM FRONT BASE

Module 1 Module 2 Module 3

Legend:

1) Pressing the menu key accesses menu selection.

2) Pressing the meas key returns to measurement.

3) Menu groups are selected using the arrow keys

4) Press enter to confirm, enter passcode

5) Further menu items are displayed

6) Selected functions of the Diagnostics menu can be recalled via softkey even when in measuring mode

Diagnostics

Message list Point of meas description Logbook Device description

FRONT BASE Module 1 Module 2 Module 3

Page 16

Short Description: FRONT Module

View into the open device (FRONT module)

Slot for SmartMedia card

• Data recording The SmartMedia card expands the measurement recorder capacity to > 50000 records.

• Exchange of parameter sets 5 parameter sets can be stored on the SmartMedia card, 2 of them can be loaded simultaneously to the analyzer and be switched by remote control. Parameter sets can be transmitted from one analyzer to the other.

• Function expansions are possible with additional software modules, which are released using transaction numbers (TAN).

• Software updates

Terminal plates of “hidden” modules

Each module comes with an adhesive label containing the contact assignments. This label should be sticked to the inner side of the front (as shown). Then, the terminal assignments remain visible even if further modules are inserted.

Replacing the front module

Pull off power cord and ground wire. To separate the FRONT module from the BASE module, turn the retaining screws of the pivot hinge by 90°.

The circumferential sealing

guarantees IP 65 protection and allows spray cleaning / disinfection.

NOTICE! Keep clean!

Page 17

Short Description: BASE Module

View into the open device (BASE module, 3 function modules installed)

Module equipment

Module identification: Plug & Play. Up to 3 modules can be combined as desired. Several input and communication modules are available.

Note

Only one module can be connected in addition to a FIU 3400(X)-140/141 module.

BASE module

2 current outputs (free assignment of process variable) and 4 relay contacts, 2 digital inputs. VariPower broad-range power supply unit, 20 ... 265 V AC/DC, suitable for all public mains supplies in the world.

Power supply units, Ex version:

100 ... 230 V AC or 24 V AC/DC

WARNING! Do not touch the terminal compartment, there may be dangerous contact voltages!

Important notice concerning SmartMedia Card

The SmartMedia card may be inserted or replaced with the power supply switched on. Before a memory card is removed, it must be “closed” in the maintenance menu. When closing the device, make sure that the sealing is properly seated and clean.

Page 18

Overview of the System Components

Fully Automated Process Analysis System

The fully automated process analysis system consists of the following components

• Protos 3400(X) (modular process analysis system)

• Unical 9000(X) / Uniclean 900(X) (automatic control of retractable fittings)

• Ceramat WA 150(X) (retractable fitting with ceramic sealing to the process)

The system is operated from the Protos 3400(X). Four operating modes are provided: calibration, parameter setting, maintenance, diagnostics.

The PHU 3400(X)-110 module consists of 2 functional groups:

• PHU 3400(X)-110 (measuring circuit)

• Unical 9000(X) / Uniclean 900(X) (probe control)

Protos 3400(X)

25.6 °C09.03.07

Max. 10 m

To probe (pH/temp) max. 20 m

Media adapter

with metering pumps (calibration buffers, cleaning agent

Compressed air

Power supply

e.g. Unical 9000(X)

Service

Rinse water

Media connection

Max. 10 m

switch

Ceramat WA 150(X)

with pH sensor

Page 19

Overview of the System Components

Protos 3400(X) Basic Unit and Controller Module for Retractable Fittings PHU 3400(X)-110 and Unical 9000(X) / Uniclean 900(X) Probe Controller

Protos 3400(X) basic unit. The PHU 3400(X)-110 module is located in one of the 3 module slots available.

Module

slot

Module

slot

Module

slot

SMARTMEDIA

OK 1

VariPower

Protos 3400(X)

OK 2

Contacts

K1, K2, K3

I 1

I 2

Alarm

PHU 3400(X)-110 controller module for retractable fittings and Unical 9000(X) / Uniclean 900(X) probe controller:

Unical 9000 (X)

Uniclean 900(X)

Unical

pH, ORP MΩ, kΩ

PHU 3400(X)-110 module

0(4) ... 20 mA

Temp

Probe

RTD

Temp

Interface

Page 20

PHU 3400(X)-110 Module

Measuring Circuit and Probe Control Function Blocks

For a direct access to the function descriptions related to the Unical 9000(X)/ Uniclean 900(X) probe controller, please refer to the overview on the back page of this manual.

You can document your specific settings for the Unical 9000(X) / Uniclean 900(X) probe controller in the Excel spreadsheet from the CD-ROM (supplied with Protos 3400(X) or as download at www.knick.de)

Measuring Circuit and Probe Control Function Blocks

Probe Controller

The PHU 3400(X)-110 module allows connection of the Unical 9000(X) probe controller for fully automated pH measurement, cleaning, and calibration or the Uniclean 900(X) probe controller for fully automated pH measurement.

Measuring Circuit

Even without the Unical 9000(X) / Uniclean 900(X), the PHU 3400(X)-110 module is a fully fledged pH measuring module for simultaneous pH, ORP and temperature measurement with glass electrodes. This instruction manual describes the whole functionality of the PHU 3400(X)-110 module corresponding to the following menu groups:

• Calibration

• Maintenance

• Parameter setting

• Diagnostics

The Protos 3400(X) is an expandable modular process analysis system. For latest product information, please refer to:

www.knick.de

Page 21

Terminal Plate PHU 3400(X)-110 Module

Terminal Plate PHU 3400-110 Module:

Attaching the Terminal Plates

The terminal plates of the lower modules can be sticked to the inner side of the door. This facilitates maintenance and service.

Page 22

Inserting the Module

Note: Be sure to connect the shielding properly!

The terminals 2 and 8 are covered by an ESD shield. To connect the sensor cable, just pull it back.

Switch off power supply

Open the device (loosen the 4 screws at the front)

Place module in slot (D-SUB connector)

Tighten fastening screws of the module

Open ESD shielding cap (covering terminals 2 and 8)

Connect sensor cable.

To avoid interferences, the cable shielding must be completely covered by the ESD shielding cap. Close ESD shielding cap (covering terminals 2 and 8)

Connect RS 485 interface to probe controller

(terminals 16 ... 19) Close device, tighten screws at the front

Switch on power supply

10.

Set parameters

11.

Make sure that the cable glands are tightly closed to protect against humidity.

Page 23

Wiring Example 1

Wiring Example VP and SixPlug Multisense electrode (pH/ORP/temp) with solution ground (SG)

PHU 3400-110

Green

Core

Shield

Blue

Green

White

GN/YE

Yellow

Brown

White

UNICAL 9000(X)

Page 24

Wiring Example 2

Wiring Example VP and SixPlug Electrode (pH/temp) without solution ground (SG)

PHU 3400-110

Jumper

GN/YE

Green

Core

Shield

White

Green

Yellow

Brown

White

UNICAL 9000(X)

Page 25

Connecting the Probe Controller

Probe Controller for Fully Automated Measurement, Cleaning and Calibration

Unical 9000X Uniclean 900(X)

RS 485 A

RS 485 B

GND

Power

Unical 9000(X) / Uniclean 900(X) Controller

The Unical 9000(X) / Uniclean 900(X) probe controllers come with installation manuals, free download at www.knick.de.

Green

Yellow

Brown

White

Protos module PHU 3400(X)-110

RS 485 A

RS 485 B

GND

6.8 V (supply)

Page 26

Menu Selection

After switching on, the analyzer performs an internal test routine and automatically detects the number and type of modules installed. Then, the analyzer goes to measuring mode.

Menu selection

Select:

Return to meas

[enter]

24.0°C

°C

25.8°C

1 Pressing menu accesses menu selection. 2 Pressing meas returns to measurement.

3 Arrow keys for selecting a menu group 4 enter key for confirming a selection

8.06 pH

25.1 °C

Lingua

Menu Structure

Calibration Maintenance Parameter setting Diagnostics

Measuring

Passcode

1147

(as delivered)

Selection of further menu items:

Menu groups (Select using arrow keys)

2958

1246

Operator level

1989

Administrator level

Page 27

Passcode Entry

To enter a passcode

Select the position using the left/right keys, then edit the number using the up/down keys. When all numbers have been entered, press enter to confirm.

To change a passcode

• Open the menu selection (menu)

• Select parameter setting

• Administrator level, enter passcode

• Select System control: Passcode entry

Display

Passcode entry (Administrator)

cal

Calibration

maint

opl

Passcode entry (Administrator)

cal

maint

opl

If you lose the adm passcode, system access will be locked!

Calibration

Change passcode Maintenance

Operator level

Return Info

7.00 pH

25.6 °C

Off

7.00 pH

25.6 °C

On Off

1147

Off

System control: Passcode entry

Changing a passcode “Passcode entry” menu

When this menu is opened, the analyzer displays a warning (Fig.). Passcodes (factory settings): Calibration 1147 Maintenance 2958 Operator level 1246 Administrator level 1989

If you lose the passcode

for the Administrator level, system access will be locked! Please consult our technical support!

To change a passcode

Select “On” using arrow keys, confirm with enter. Select the position using the left/right keys, then edit the number using the up/down keys. When all numbers have been entered, confirm with enter.

Page 28

Configuring the Measurement Display

Select menu: Parameter setting/Module FRONT/Measurement display

Pressing meas (1) returns the analyzer to the measuring mode from any function. All process variables coming from the modules can be displayed. The table on the next page describes how to configure the measurement display.

Measurement display

Typical measurement display

24.0°C

°C

25.8°C

Secondary displays

Additional values, also date and time, can be displayed depending on the modules installed.

Softkeys

In measuring mode, the softkeys allow selection of values for the secondary displays or control of functions (user defined).

Page 29

Menu Display Configure measurement display

7.00 pH

Menu selection

Select:

Return to meas

Parameter setting (Administrator)

System control

Module FRONT 3400-011

Module BASE 3400-021

Module PHU 3400-110

Probe control

Module PH 3400-035

Return

Module FRONT 3400-011 (Administrator)

Languages

Measurement display

Measurement recorder

Return

Measurement display (Administrator)

Main display

1st primary value 2nd primary value Viewing angle

25.6 °C

[enter]

Lingua

7.00 pH

25.6 °C

7.00 pH

25.6 °C

English

7.00 pH

+65° C

1 primary value

2 primary values

Configure measurement display

Press menu key to select menu. Select parameter setting using arrow keys, confirm with enter. Select: “Administrator level”: Passcode 1989 (default setting).

Parameter setting: Select “Module FRONT”

Front module: Select “Measurement display”

Measurement display: Set the number of primary values (large display) to be displayed

%Air %O

°C

mg/l

mg/l ppm mbar pH

7.00 pH

25.6 °C

values

Abort

Measurement display (Administrator)

Main display

1st primary value

2nd primary value

Viewing angle

Abort

Select process variable(s) to be displayed and confirm by pressing enter.

To return to measurement: press meas

Page 30

Start-Up

Prerequisite

Mechanical and electrical installation of the components has been performed according to the separately enclosed operating and installation instructions (free download at www.knick.de):

• Protos 3400(X)

• Unical 9000(X) or Uniclean 900(X)

• Ceramat WA 150(X) (or other retractable fittings)

Warning!

Before working on the retractable fitting, it must be moved into SERVICE position. Be sure to read and observe the user manual of the retractable fitting!

Caution!

Be sure to execute the following steps in the specified order!

1) Insert the PHU 3400(X)-110 module (see Page 22)

2) Connect sensor cable and probe controller (see Pages 23...25)

3) Configure the PHU 3400(X)-110 module (Page 34)

Page 31

Parameter setting

Parameter Setting: Operating Levels

Viewing level, Operator level, Administrator level

Note: HOLD mode (Setting: BASE module)

Display

Menu selection

Select:

Return to meas

Parameter setting

Viewing level Operator level

Administrator level

Return

Module FRONT (Administrator)

Languages

Measurement display

Measurement recorder KI recorder

[enter]

(All Data) view (Operation Data) opl

(All Data) adm

English

11.03 pH

25.6 °C

Lingua

11.03 pH

25.6 °C

11.03 pH

25.6 °C

Viewing level, Operator level, Administrator level

Open parameter setting

From the measuring mode: Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm.

Administrator level

Access to all functions, also passcode setting. Releasing or blocking a function for access from the Operator level.

Functions which can be blocked for the Operator level are marked with the "lock" symbol. The functions are released or blocked using the softkey.

Return

Module FRONT

Languages

Measurement display

Measurement recorder

KI recorder

Return

Release

English

11.03 pH

25.6 °C

Operator level

Access to all functions which have been released at the Administrator level. Blocked functions are displayed in gray and cannot be edited (Fig.).

Viewing level

Display of all settings. No editing possible!

Page 32

Parameter Setting: Locking a Function

Administrator level: Enabling/locking functions for Operator level

Note: HOLD mode (Setting: BASE module)

Menu Display

Parameter setting (Administrator)

System control Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Module PH 3400-035

Return

Module PHU 3400-110 (Administrator)

Input filter Sensor data

Cal preset values

TC process medium

ORP/rH value Delta function

Return

Module PHU 3400-110 (Administrator)

Input filter Sensor data

Cal preset values

TC process medium

ORP/rH value Delta function

Return

Module PHU 3400-110 (Administrator)

Input filter

Sensor data

Cal preset values

TC process medium

ORP/rH value

Delta function

Return

11.03 pH

25.0°C

11.03 pH

25.0°C

Block

11.03 pH

25.0°C

Release

11.03 pH

25.0°C

Administrator level: Enabling / locking a function

Example: Blocking access to the

calibration adjustments from the Operator level

Open parameter setting

Select Administrator level. Enter passcode (1989). Select “Module PHU” (for example) using arrow keys, press enter to confirm.

Select “Cal preset values” using arrow keys, “Block” with softkey.

Now, the “Cal preset values” line is marked with the “lock” icon. This function cannot be accessed from the Operator level any more. The softkey function changes to “Release”.

Open parameter setting

Select Operator level, passcode (1246). Select “Module PHU” (for example). Now, the locked function is displayed in gray and marked with the “lock” icon.

Page 33

Parameter Setting for PHU 3400(X)-110

Activating parameter setting

Menu Display Parameter setting

11.03 pH

[enter]

25.0°C

Lingua

11.03 pH

25.0°C

11.03 pH

25.0°C

Block

Menu selection

Select:

Return to meas

Parameter setting (Administrator)

System control

Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Module PH 3400-035

Return

Module PHU 3400-110 (Administrator)

Input filter

Sensor data Cal preset values

TC process medium ORP/rH value Delta function

Return

Activating Parameter Setting

From the measuring mode: Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm. Passcode as delivered: 1989

Select "Module PHU 3400-110", press enter to confirm.

Select parameter using arrow keys, press enter to confirm.

During parameter setting the analyzer is in HOLD mode:

Current outputs and relay contacts behave as configured (BASE module).

Page 34

Settings of Sensor Data

With “Auto“, the tolerance limits for the monitoring criteria are determined by the analyzer. They are displayed in gray. These values cannot be edited. With ”Individual”, the tolerances can be adjusted.

Note: HOLD mode active.

Parameter Default Selection / Range / Notes

Input filter

• Pulse suppression

Sensor data

• Sensor type

• Temperature detection

- Temperature probe

- Measuring temp

- Cal temp

• Sensoface

• Sensor monitoring details

- Slope Nominal Min Max Message

- Zero point Nominal Min Max Message

- Sensocheck Ref el Nominal Min Max Message

- Sensocheck Glass el Nominal Min Max Message

- Response time Response time Max Message

- Calcheck

Meas distance Max Message

Off

Standard

Pt 1000 Manual Manual Default

Auto

59.2 mV/pH

53.3 mV/pH

61.0 mV/pH Maint. request Auto

07.00 pH

06.00 pH

08.00 pH Maint. request Auto

5.0 kΩ

3.1 kΩ

100.0 kΩ Off Auto

120.0 MΩ

28.6 MΩ

350.0 MΩ Off Auto 0000 sec Off

Auto

3.20 pH Off

Off, On (suppression of fast transients at the input)

Standard, ISFET (ISFET: Insert PH 3400-032 module)

Pt100, Pt1000, NTC 8.55 kΩ, NTC30kΩ (sensor) Auto, manual: Default +25.0 °C (entry) Auto, manual: Default +25.0 °C (entry) Default, Individual

Auto, Individual Can only be set with “Individual” selected

Off, failure, maintenance request Auto, Individual Can only be set with “Individual” selected

Off, failure, maintenance request Auto, Individual (not for sensor type ISFET) Can only be set with “Individual” selected

Off, failure, maintenance request Auto, Individual

Off, failure, maintenance request Calcheck: checks the difference between calibration buffers and measured values Auto, Individual

Off, failure, maintenance request

Page 35

Parameter Setting of PHU 3400(X)-110

Note: HOLD mode active

Display Display Parameter selection

7.00 pH

Module PHU 3400-110 (Administrator)

Input filter

Sensor data

Cal preset values

TC process medium

ORP/rH value

Delta function

Return

Sensor data (Administrator)

Sensor type

Temperature detection

Sensoface

Slope Zero

Sensocheck Ref el

Abort

Calcheck (Administrator)

Meas distance max +02.00 pH

Message

Abort

20.1 °C

BlockBlock

7.00 pH

20.1 °C

StandardStandard

(Pt100)

Off

7.00 pH

20.1 °C

Off

Failure

Maint. request

Sensor data

Sensor data are preset depending on the sensor type. Gray display lines cannot be edited. Sensoface provides information on the sensor condition (evaluating the sensor data). Great deviations are signaled. Sensocheck can be switched off. The following parameters are monitored: Slope, zero, reference impedance (for ISFET sensors), glass impedance (pH electrodes), response time, CalCheck. The tolerance limits are displayed in gray. Limit violations can be signaled by a message (either "failure" or "maintenance request").

Sensor monitoring details

Slope Zero

Sensocheck Ref el

Sensocheck Glass el Response time Calcheck

Abort

(Auto) (Auto) (Auto)

7.00 pH

20.1 °C

Sensor monitoring details

With “Auto” selected, the limits calculated by the analyzer are used (displayed in gray). With “Sensor monitoring Individual”, the tolerance limits for the parameters are displayed in black and can be set.

Page 36

Sensoface

Sensoface is a graphical indication of the sensor condition – Sensocheck must have been activated during parameter setting.

Sensocheck:

Automatic monitoring of glass and

24.3°C

The “smileys” provide information on wear and required maintenance of the sensor (“friendly” - “neutral” - “sad”).

Menu Display Activate Sensocheck

reference electrode

Menu selection

Select:

Return to meas

Parameter setting (Administrator)

System control Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Return

Sensocheck Ref el (Administrator)

Nominal Min Max

Message

Abort

[enter]

005.0 kOhm

003.1 kOhm

100.0 kOhm

Off Failure

Maint. request

7.00 pH

25.6°C

Lingua

7.00 pH

25.6°C

7.00 pH

25.6°C

Open menu selection

Select parameter setting Enter passcode (Administrator)

Select (“PHU”) module. Confirm with enter

Select “Sensor data”. Confirm with enter. Then select “Sensocheck Ref el”. (Fig.) Assign function and confirm with enter.

Page 37

Sensoface is “sad” ...

The “Diagnostics / Module PHU / Sensor network diagram” shows all current sensor parameters in a graphic diagram.

Sensor network diagram

1 - Slope

2 - Zero point

3 - Ref impedance

4 - Glass impedance

5 - Response time 6 - Cal timer

7 - Calcheck

Return

Sensoface Criteria

Parameter

Slope

Zero

Reference impedance

Glass impedance

7.00 pH

24.1°C

Info

Standard*

59.2

7.00

Rcal **

Sensor Network Diagram

“Diagnostics / Module PHU / Sensor network diagram”. Tolerance limit violations can be seen at a glance. Critical parameters (inner circle) are flashing. Parameters displayed in gray have been disabled during parameter setting or do not apply to the currently selected sensor.

Critical range

< 53.3 or > 61

< 6.00 or > 8.00

< 0.6 Rcal or > 100 kΩ + 0.5 Rcal

< 0.3 Rcal or > 3.5 Rcal

Response time Fine Standard Coarse

Calibration timer

Calcheck

120 sec 80 sec 60 sec

When 80 % expired

Difference meas. value / buffer > 3.2 pH

* Applies to standard electrodes with pH = 7.00 ** Rcal is determined during calibration

Page 38

Parameter Setting of PHU 3400(X)-110

Cal preset values

Note: HOLD mode active

Cal Preset Values

Parameter Choices (default in bold print)

• Calimatic buffer Knick: 2.00 4.01 7.00 9.21

Merck/Riedel: 2.00 4.00 7.00 9.00 12.00 DIN 19267: 1.09 4.65 6.79 9.23 12.75 NIST standard: 4.006 6.865 9.180 NIST technical: 1.68 4.00 7.00 10.01 12.46 Hamilton: 2.00 4.01 7.00 10.01 12.00 Kraft: 2.00 4.00 7.00 9.00 11.00 Hamilton A: 2.00 4.01 7.00 9.00 11.00 Hamilton B: 2.00 4.01 6.00 9.00 11.00 Hach: 4.01 7.00 10.00 Ciba: 2.06 4.00 7.00 10.00 Reagecon: 2.00 4.00 7.00 9.00 12.00

• Drift check Fine: 1.2 mV/min (Abort after 180 sec)

Standard: 2.4 mV/min (Abort after 120 sec)

Coarse: 3.75 mV/min (Abort after 90 sec)

• Calibration timer

Monitoring Auto, Off, Individual Calibration timer 0168h Entry with “Individual”; Off = 0000 Adaptive cal timer Off, On

• Cal tolerance band Tolerance band check: Off, On

Tolerance Zero +00.20 pH (entry) Tolerance Slope +002.0 mV/pH (entry)

• ORP check Test period: 010 s (entry) Test difference: 0010 mV (entry)

Tolerance Adjustment

(Additional function SW 3400-005) During calibration this function checks the zero and slope values and automatically performs an adjustment when the tolerance band is exceeded. The parameters are stored in the tolerance band recorder (Diagnostics menu).

Control via Probe Controller

(Parameter setting / Probe control / Cal preset values / Cal mode / Adjustment)

With “Cal tolerance band check” switched on, data are only taken over when they exceed the limits defined by the tolerance band.

Page 39

SW 3400-005: Tolerance Adjustment

Program Flow

Start tolerance band

Calibration /

Adjustment ?

Zero > Tolerance ?

Slope > Tolerance ?

Yes

First Calibration?

New entry

Zero + Slope

T-band check?

Yes

Erase tolerance band

Calibration

Old tolerance band

End of tolerance band

Adjustment

New tolerance band

Manual check

Page 40

Activating the Cal Tolerance Band

Select menu: Parameter setting/System control/Release of options Note: The TAN for releasing an additional function is only valid for the device with the corresponding serial number!

Display

Menu selection

Select:

Return to meas

Parameter setting

Viewing level Operating levels

Administrator level

Return

Parameter setting (Administrator)

System control

Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Return

Release of options (Administrator)

001 KI recorder

002 Buffer sets

003 Adaptive timer

005 Cal tolerance band

006 Current characteristic

Return

[enter]

(All Data) view (Operation Data) opl

(All Data) adm

7.00 pH

25.6 °C

Lingua

7.00 pH

25.6 °C

7.00 pH

25.6 °C

7.00 pH

25.6 °C

Activating an additional function

Menu selection

Open parameter setting. From the measuring mode: Press menu key to select menu. Select parameter setting using arrow keys, confirm with enter.

Parameter setting

Select Administrator level using arrow keys, confirm with enter. Enter passcode and confirm (Passcode as delivered: 1989).

Select system control using arrow keys, confirm with enter. Then select Release of options using arrow keys, confirm with enter.

Release of options

Select the additional function to be

Inactive Inactive Inactive Active Inactive

released (“Cal tolerance band”). Set option to “active”. Enter the TAN at the prompt. (Note: The TAN is only valid for the device with the corresponding serial number, see previous page.) The option is available after the TAN has been entered.

Page 41

Parameter Setting of PHU 3400(X)-110

Cal preset values: Calimatic buffer, Cal timer, Cal tolerance band

Note: HOLD mode active

Menu Display Cal preset values

7.00 pH

Module PHU 3400-110 (Administrator)

Input filter

Sensor data

Cal preset values

TC process medium ORP/rH value Delta function

Return

Cal preset values (Administrator)

Calimatic buffer

Knick 2.00 4.01

Drift check Calibration timer Cal tolerance band

Abort

Cal timer (Administrator)

Calibration timer

Adaptive cal timer

Return

20.1 °C

Block

7.00 pH

20.1 °C

Knick

Mettler-Toledo Merck/Riedel DIN 19267 NIST standard

NIST technical Hamilton

7.00 pH

20.1 °C

168 h

Off

Calimatic buffer

For automatic calibration, you must define the buffer set you want to use. For calibration, you must then use buffer solutions from this buffer set. The order does not matter. The selected buffer set with the nominal values of the individual buffer solutions is displayed in gray. The “Calimatic buffer” menu shows all buffer sets available. Select buffer set with enter.

Calibration timer

Entry of the time interval until the next due calibration.

Adaptive calibration timer

Automatically reduces the time until the next due calibration when the electrode is exposed to high stress (temperature, extreme pH values).

Cal tolerance band (Administrator)

Calibration data taken over when tolerance band exceeded

Tolerance band check

Tolerance Zero Tolerance Slope

Return

7.00 pH

20.1 °C

Off

+00.20 pH

002.0 mV/pH

Tolerance adjustment

If the measured value leaves the tolerance band specified here for zero and slope, an adjustment is automatically performed during calibration.

Page 42

Parameter Setting of PHU 3400(X)-110

TC process medium, ORP/rH value, delta function: Default settings and selection range

Parameter Choices (default in bold print)

• TC process medium Off, linear, ultrapure water, table

Linear: enter temperature factor +XX.XX %/K

• ORP/rH value

Reference electrode Ag/AgCl, KCl 1 mol/l

Ag/AgCl,KCI 3mol/l Hg, Tl/TlCl, KCl 3.3 mol/l Hg/Hg2SO4, K2SO4 sat

ORP conversion to SHE No, Yes Calculate rH with factor No, entry of factor

• Delta function Off, pH, mV+ORP or rH: entry of delta value

Temperature compensation of process medium

Linear temperature compensation, reference temp fixed at 25 °C

pH(25 °C) = pHM + TC/100 % (25 °C - TM)

(25 °C)

= pH value compensated to 25 °C pHM = Measured pH value (temp-corrected) TC = Temperature factor [%/K] T

= Measured temperature [° C]

Page 43

Parameter Setting of PHU 3400(X)-110

TC process medium

Note: HOLD mode active

Menu Display TC process medium

7.00 pH

Module PHU 3400-110 (Administrator)

Input filter Sensor data Cal preset values

TC process medium

ORP/rH value

Delta function

Return

TC process medium (Administrator)

Return

TC process medium (Administrator)

TC at 00°C:

TC at 05°C:

TC at 10°C:

TC at 15°C:

TC at 20°C:

Abort

Table

Off linear Ultrapure water

Table

+00.00%

+00.00% +00.00%

+00.00%

24.0 °C

Block

7.00 pH

24.0 °C

7.00 pH

24.0 °C

Info

TC process medium

You can choose from:

• Linear (entry of TC coefficient)

• Ultrapure water

• Table When measuring media with a known temperature behavior, the output pH value can be corrected using a table. TC can be entered in 5 °C steps for temperatures between 0 and +95°C. Then, the output pH value is corrected by the corresponding TC value depending on the measuring temperature. Intermediate values are linearly interpolated. In the case of lower or higher temperatures (< 0 °C or > +95 °C), the last table value is used for calculation. If the delta function has been activated (see Pg 42) simultaneously with temperature compensation, the temperature is compensated first and then the delta value is subtracted.

Outp I1 5.70 mA

°C

Favorites menu

When the TC correction for process medium is switched on, ”TC” appears in the display in measuring mode.

Page 44

Parameter Setting of PHU 3400(X)-110

ORP/rH value, delta function

Note: HOLD mode active

Menu Display ORP/rH value, delta function

ORP/rH value (Administrator)

Ref el

ORP conversion rH with factor

Abort

Delta function (Administrator)

Delta function

Delta value

Return

Ag/AgCl, KCl 1m

Ag/AgCl, KCl 3m Hg,Ti/TiCl,KCl 3.5m Hg/Hg2SO4,K2SO4 sat

Off

mV ORP rH

7.00 pH

20.1 °C

7.00 pH

20.1 °C

ORP/rH value

• Select type of reference electrode:

Ag/AgCl, KCl 1 mol/l (silver/silver chloride) Ag/AgCl, KCl 3 mol/l (silver/silver chloride) Hg, Tl/TlCl, KCl 3.3 mol/l (Thalamid) Hg/Hg2SO4, K2SO4 saturated (mercury sulfate)

• ORP conversion to SHE

• Calculate rH with factor

Delta function

When a delta value is entered, the system calculates the difference.

Output value = measured value – delta value

The output value controls all outputs and is shown on the display. When the delta function has been activated simultaneously with temperature compensation, the temperature is compensated first and then the delta value is subtracted.

Outp I1 5.70 mA

∆

°C

Favorites menu

When delta function is switched on, “∆” appears in the display in measuring mode.

Page 45

Parameter Setting of PHU 3400(X)-110

Messages: Default settings and selection range

Parameter Choices (default in bold print)

• pH value Off, device limits max., Variable limits:

- Failure Limit LO

- Warning Limit LO

- Warning Limit HI

- Failure Limit HI

• ORP value Off, device limits max., Variable limits:

- Failure Limit LO

- Warning Limit LO

- Warning Limit HI

- Failure Limit HI

• rH value Off, device limits max., Variable limits:

- Failure Limit LO

- Warning Limit LO

- Warning Limit HI

- Failure Limit HI

• Temperature Off, device limits max., Variable limits:

- Failure Limit LO

- Warning Limit LO

- Warning Limit HI

- Failure Limit HI

• mV value Off, device limits max., Variable limits:

- Failure Limit LO

- Warning Limit LO

- Warning Limit HI

- Failure Limit HI

Device limits max.

+ 16.00 pH

(maximum range of measuring module)

Variable limits (range limits specified)

- 02.00 pH

Page 46

Parameter Setting of PHU 3400(X)-110

Messages

Note: HOLD mode active

Menu Display

Messages (Administrator)

Messages pH value

Messages ORP value Messages rH value Messages Temperature Messages mV value

Return

Messages pH value (Administrator)

Monitoring

Abort

Messages (Administrator)

Monitoring

Failure Limit Lo

Warning Limit Lo Warning Limit Hi Failure Limit Hi

Return

7.00 pH

25.6°C

7.00 pH

25.6°C

Off Device limits max.

Variable limits

7.00 pH

25.6°C

Variable limits

–02.00 pH

–02.00 pH +16.00 pH +16.00 pH

Messages

All parameters determined by the measuring module can generate messages.

Device limits max.

Messages are generated when the process variable (e.g. pH) is outside the measurement range. The “Failure” icon is displayed, the NAMUR failure contact is activated (BASE module, factory setting: contact K4, N/C contact). The current outputs can signal a 22 mA message (user defined).

Variable limits

For the “failure” and “warning” messages you can define upper and lower limits for message generation.

Message icons

Failure (Failure limit HiHi/LoLo)

Maintenance (Warning limit Hi/Lo)

Limit indication (here: lower range)

Message list

D062

Warn

P018

Warn Temp alarm HI

P030

Warn Zero range

D013

Saturation %Air Alarm HI

P210

Fail Wrong ISM sensor Warn Tolerance band

P092

Return

Sensocheck

7.00 pH

25.6°C 8 messg.

Diagnostics menu

When the “Maintenance” or “Failure” icons are flashing in the display, you should call the Diagnostics menu. The messages are displayed in the “Message list”.

Page 47

Documenting

Documenting Parameter Setting

You must reproducibly document all parameter settings in the device to achieve a high level of system and device security according to GLP. For that purpose, an Excel file is provided (on the CD-ROM shipped with the basic device) to enter the parameter settings.

The Excel file provides one worksheet for each module with columns for the following parameters: Factory settings, parameter set A, parameter set B. Enter your settings as parameter set A or B. The gray cells in the parameter set B column cannot be modified since they contain sensor-specific values which cannot be changed by parameter set switchover. Here, the values listed under parameter set A apply.

Page 48

Documenting Parameter Setting

From the application window of the Excel file, select the worksheet for the module the parameter settings of which you want to document. Set the parameters of the respective module and enter the selected values in the corresponding cells of the module worksheet.

NOTICE!

Display

The "HOLD" mode is active during parameter setting.

HOLD. The NAMUR “HOLD” contact (function check) is active (factory setting: Module BASE,

Contact K2, N/O contact). Current output response is user-defined:

• Current meas.: The currently measured value appears at the current output

• Last usable value: The last measured value is held at the current output

• Fixed 22 mA: The output current is at 22 mA

Page 49

ProgaLog 3000 Software (Option) forConfiguration and Documentation

The ProgaLog 3000 software is available for convenient configuration of the Protos 3400(X) process analysis system. The user interface can be switched to the Protos display languages English, German, French, Spanish, Italian, Swedish or Portuguese. The software comes on CD-ROM. It runs under Windows® 8 / 7 / XP. A card reader for SmartMedia cards is required for transferring the configuration files between PC and Protos 3400.

Configuration with ProgaLog 3000

Insert a SmartMedia card formatted as "memory card" into the analyzer. First, the configuration data are written to the SmartMedia card. These data can then be read and edited by the ProgaLog 3000 software.

1. Save the configuration data at the Protos 3400(X)

Parameter setting/System control/Copy configuration. With “Save“ configuration, the complete device configuration (except the passcodes) is written on the memory card.

2. Close and remove the SmartMedia card

Select "Maintenance / Close memory card", then remove the card.

3. Read out SmartMedia card with "ProgaLog 3000"

Open the "File / SmartMediaCard" menu of the ProgaLog 3000 software to read out the configuration data stored on the SmartMedia card. Now, you can edit all parameters at your PC. Save the edited configuration file to the SmartMedia card. Then, insert the SmartMedia card into the Protos 3400(X) analyzer.

Fig.: ProgaLog 3000 menu: File

Page 50

ProgaLog 3000 Software for Configuration and Documentation

4. Edit configuration data using ProgaLog 3000

When the configuration data have been loaded, the software lists the connected modules with all available configuration parameters:

Fig.: ProgaLog 3000 configuration data

The parameters are listed according to the modular device structure. All configuration parameters (except the "Sensor data details", which are determined by digital sensors) can be edited at the PC. After having finished the configuration, save the data to the SmartMedia card.

Page 51

ProgaLog 3000 Software for Configuration and Documentation

Configuring the parameters, e.g. relay contact usage:

Input errors are indicated by red highlighting:

5. Save the configuration data to SmartMedia card

7.00 pH

Copy configuration (Adminstrator)

Identical module equipment required for transfer

Configuration

Return

25.6 °C

Load

Save

6. Load the configuration data to the

Protos 3400(X)

Parameter setting / System control / Copy configuration. Select “Load configuration” to write the complete device configuration (except the passcodes) to the Protos 3400(X).

Page 52

ProgaLog 3000 Software for Configuration and Documentation

Configuration using "ProgaLog 3000"

In the "Configurator" menu you can preconfigure a complete Protos 3400(X) process analysis system with up to 3 modules at your PC.

1. Select your configuration from the modular system components offered in the left-hand field.

2. Click the right arrow (-->) to add the components or remove components by clicking (<--).

3. Now configure the parameters for the selected system components.

4. Save the configuration.

You can save the configuration to a memory card that has been pre-

formatted in the Protos 3400(X) and transfer them to analyzers with identical module configurations.

Page 53

Logbook

Factory setting

Logbook, Factory Setting

Parameter setting/System control/Logbook

Note: HOLD mode

Display Logbook, Factory setting

Logbook (Administrator)

Log failure

Log warning Erase logbook

Yes

7.00 pH

25.6 °C

Logbook

Select which messages are to be logged in the logbook. The last 50 events are recorded with date and time. This permits quality management

Return

7.00 pH

Logbook

04/13/10 09:50 Measurement active 04/13/10 09:36 Parameter setting active 04/12/10 17:52 Measurement active 04/12/10 17:44 Parameter setting active 04/12/10 17:40 Wrong passcode 04/12/10 17:04 Measurement active 04/12/10 16:53 Diagnostics active

Return

Logbook

F223 04/13/10 09:50 Diagnostics active F222 04/13/10 09:36 Parameter setting active F224 04/12/10 17:52 Measurement active

25.6 °C

7.00 pH

25.6 °C

documentation to ISO 9000 et seq.

The logbook can be called from the diagnostics menu (Fig.). Pressing the right softkey displays the message identifier.

Additional function SW 3400-104: Extended logbook for recording data on SmartMedia card (TAN).

Return

Factory setting (Administrator)

The factory setting erases all your set parameters!

Measuring system

Return

7.00 pH

25.6 °C

Yes

Factory Setting

Allows resetting the parameters to their factory setting. When this menu is opened, the analyzer displays a warning (Fig.).

Page 54

BASE module

Current outputs

Current Outputs, Contacts, OK Inputs

Select menu: Parameter setting/Module BASE

Note: HOLD mode active

Display

Module BASE (Administrator)

Output current I2 Contact K4 (NAMUR Failure) Contact K3 (NAMUR maintenance) Contact K2 (NAMUR HOLD) Contact K1 (Limit)

Inputs OK1, OK2

Return

Output current I1 (Administrator)

Variable

Curve Output Start End Behavior during messages

Abort

Output current I1 (Administrator)

Variable

Curve

Output Start End Output filter

Abort

7.00 pH

19.2°C

Block

7.00 pH

19.0 °C

7.00 pH

19.0 °C

Off

°C rH S/cm °C g/kg

°C

Linear

Trilinear Function Table

Parameter setting BASE module

To configure current output

Configuring a Current Output

• Call up parameter setting

• Enter passcode

• Select “Module BASE”

• Select “Output current I1”

• Select “Output current ...”

• Select measured variable

• Select Curve, e.g. “linear”: The measured variable is represented by a linear output current curve. The desired range of the measured variable is specified by the values for “Start” and “End”.

Assignment of Measured Values: Start (4 mA) and End (20 mA)

Example 1: Range pH 0 - 14 Example 2: Range pH 5 - 7

Output current

[mA]

5 7

Advantage: Higher resolution in range of interest

[mA]

[pH]

Page 55

Current Outputs: Characteristics

Select menu: Parameter setting/Module BASE

• Linear characteristic

The process variable is represented by a linear output current curve.

Output current

[%]

100

Start

End

Process variable

• Trilinear characteristic

Two additional vertices must be entered:

Output current

[%]

100

2nd vertex Y

1st vertex Y

Start

1st vertex X

End

2nd vertex X

Process variable

• Note: Bilinear characteristic

For a bilinear characteristic, identical parameters are entered for the two

vertices (1st vertex, 2nd vertex).

Page 56

• Function characteristic

Nonlinear output current characteristic: allows measurements over several

decades, e.g. measuring very low values with a high resolution and high values with a low resolution. Required: Entering a value for 50 % output current.

Output current

[%]

100

Entry for “50 % point”: e.g.: 10 % of measured value

End

Equation

Process variable

Output current (4 to 20 mA) = 16 mA + 4 mA

E + S - 2 * X50%

K =

S: Start value at 4 mA X50%: 50% value at 12 mA (output current range 4 to 20 mA) E: End value at 20 mA M: Measured value

Logarithmic output curve over one decade:

S: 10 % of maximum value X50%: 31.6 % of maximum value E: Maximum value

Logarithmic output curve over two decades:

S: 1 % of maximum value X50%: 10 % of maximum value E: Maximum value

X50% - S

(1+K)x

1+Kx

x =

M - S

E - S

Page 57

Output Filter

Time interval

Time averaging filter

To smoothen the current output, a low-pass filter with adjustable time interval can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached. The time interval can be set from 0 to 120 sec. If the time interval is set to 0 sec, the current output follows the input.

Note:

The filter only acts on the current output and the current value of the secondary display, not on the measurement display, the limit values or the controller!

Process variable

0 (4) - 20 mA

Time interval 0 ... 120 sec

Page 58

Current outputs: Behavior during messages

NAMUR Signals: Current Outputs

Behavior during messages: HOLD, 22mA signal

Behavior during messages

Depending on the configuration (“Messages”) the current outputs switch to:

• Currently measured value

• Last measured value (HOLD function)

Behavior during messages

HOLD

22mA message

83.1 % Air

19.0°C

Current meas.

Last usable value

Fixed 22 mA

• Fixed value (22 mA) In the case of a fault a 22 mA signal can be

Abort

generated for the selected process variable (1st primary value).

Output current [mA]

"Current meas."

HOLD

“Last usable value”

HOLD

“fix (22 mA)”

HOLD

Message when the current range is exceeded

As delivered, the “Maintenance request” (Warn) message is generated when the current range is exceeded (< 3.8 mA or > 20.5 mA). This setting can be changed in the Parameter setting menu of the respective measuring module at “Messages”.

To generate a “Failure” message, the limit value monitoring must be set to “Variable limits”: Parameter setting - <measuring module> - Messages - Variable limits - Failure limit ...

Enter the same values for the failure limits as for the current output: Parameter setting - Module BASE - Output current - Variable Start / End.

Page 59

NAMUR Signals: Relay Contacts

Failure, maintenance request, HOLD (function check)

As delivered, the floating relay outputs of the BASE module are assigned to the NAMUR signals:

Failure Contact K4, normally closed

(signaling current failure)

Maintenance request Contact K3, normally open contact HOLD Contact K2, normally open contact

NAMUR signals: Factory setting of contacts

• Select parameter setting

• Administrator level

• Select “Module BASE” (Fig.) You can define a delay time for “Maintenance request”

and “Failure”, resp. If an alarm message is released, the contact will only be activated after expiry of this delay time.

Module BASE (Administrator)

Output current I1 Output current I2

Contact K4

Contact K3 Contact K2 Contact K1

(NAMUR failure)

(NAMUR maintenance) (NAMUR HOLD) (Limit)

Return

7.00 pH

19.0°C

Block

Failure is active when a value has exceeded (or fallen below, resp.) a preset ”Failure Limit Hi” or ”Failure Limit Lo”, when the measured value is out of range, or in the event of other failure messages. That means that the equipment no longer operates properly or that process parameters have reached a critical value. Failure is disabled during "HOLD" (Function check).

Maintenance request is active when a value has exceeded (or fallen below, resp.) a preset "Warning Limit Hi" or "Warning Limit Lo", or when other warning messages have been activated. That means that the equipment is still operating properly but should be serviced, or that process parameters have reached a value requiring intervention. Warning is disabled during "HOLD" (function check).

HOLD is active:

• during calibration

• during maintenance (current source, meas. point maintenance)

• during parameter setting at the Operator level and the Administrator level

• during an automatic rinsing cycle

Page 60

Relay Contacts: Protective Wiring

Protective wiring of relay contacts

Relay contacts are subject to electrical erosion. Especially with inductive and capacitive loads, the service life of the contacts will be reduced. For suppression of sparks and arcing, components such as RC combinations, nonlinear resistors, series resistors and diodes should be used.

Typical AC applications

with inductive load

1 Load 2 RC combination, e.g. RIFA PMR 209 Typical RC combinations

e.g. capacitor 0.1 µF resistor 100 ohms / 1 W

3 Contact

Caution!

Make sure that the maximum ratings of the relay contacts are not exceeded even during switching!

Information concerning relay contacts

As delivered, the relay contacts are suitable for low signal currents (down to approx. 1 mA). If currents above approx. 100 mA are switched, the gold plating is destroyed during the switching process. After that, the contacts will not reliably switch low currents.

Page 61

Relay contacts

Relay Contacts

Parameter setting/Module BASE/Relay contacts

Display Setting the relay contacts

Usage

Variable Limit value Hysteresis Effective direction

Contact type

Module BASE

Alarm (K4)

Contact K1 (Administrator)

NAMUR maintenance NAMUR HOLD

Limit value

Rinse contact Parameter set B active

Return

USP output

7.00pH

19.2°C

Relay Contacts, Usage

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select “Contact ...”

• “Usage” (Fig.)

The BASE module provides 4 relay contacts (max. AC/DC rating 30 V / 3 A each). Contact K4 is provided for failure message. The switching behavior (normally open or normally closed), as well as a switch-on or switch-off delay can be defined.

Default settings of the user-definable relay contacts of the BASE module:

K3: NAMUR maintenance request K2: NAMUR HOLD (function check) K1: Limit value

Contact assignment:

See terminal plate of BASE module

K1-K3 are user definable (“Usage”):

• NAMUR maintenance

• NAMUR HOLD

• Limit value

• Rinse contact

• Parameter set B active

• USP output (COND module only)

• KI rec. active

• Sensoface

• Alarm control

Page 62

Relay Contacts: Sensoface Messages

Parameter setting/Module BASE/Relay contacts/Usage/Sensoface

Display Parameter setting (Sensoface)

Module BASE (Administrator)

Output current I1 Output current I2

Contact K4

Contact K3

Contact K2 Contact K1

Contact K1 (Administrator)

Usage

Variable Limit value Hysteresis Effective direction Contact type

Return

(NAMUR Failure)

(NAMUR maintenance) ( Sensoface) ( Sensoface)

NAMUR maintenance NAMUR HOLD Limit value

Sensoface

Parameter set B active USP output

7.00 pH

19.0°C

Block

7.00 pH

19.2°C

Assign Sensoface messages to relay contacts

When more than one measuring module is used, the Sensoface messages of the modules can be assigned to different contacts.

Relay contacts, usage

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select contact e.g. K1)

• Assign Sensoface message of desired measuring module to selected relay contact

Set contact parameters

• (e.g. "N/O")

• Set ON / OFF delay.

Contact K1 (Administrator)

Usage

Contact type ON delay OFF delay

7.00pH

19.2°C

Sensoface

N/O 0010 s 0010 s

Return

Page 63

Rinse contact

Rinse Contact

Parameter setting/Module BASE/Relay contacts/Usage/Rinse contact

Display Configuring the rinse contact

Contact K1 (Administrator)

Usage

Variable Limit value Hysteresis Effective direction

Contact type

Return

Contact K1 (Administrator)

Usage

Rinse interval

Rinsing lead time

Rinse duration Measurement lead time

Contact type

Return

NAMUR maintenance NAMUR HOLD Limit value

Rinse contact

Parameter set B active USP output

7.00 pH

19.2°C

7.00pH

19.2°C

Rinse contact

000.0 h 0010 s 0016 s

0010 s

N/O

Relay contacts, usage

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select contact e.g. K1)

• “Rinse contact” (Fig.)

Set rinse contact parameters

• Set rinse interval

• Set rinse duration

• During the defined "lead time" the "HOLD" mode is active.

• Select contact type (e.g. "N/O")

Please note when configuring the "Rinse contact" function

• "HOLD" mode (e.g. during parameter setting) delays the execution of the "Rinse contact" function.

• Up to 3 rinse functions (contacts K1 ... K3) can be configured independently.

• The individual rinse functions are not synchronized with each other.

Time response

HOLD Contact Kx Lead time Rinse duration Shut-off delay

Page 64

Limit value

Limit Value, Hysteresis, Contact Type

Parameter setting/Module BASE/Relay contacts/Usage

Menu Usage as limit value

7.00 pH

Contact K1 (Administrator)

Usage

Variable Limit value Hysteresis Effective direction

Contact type

Return

NAMUR maintenance NAMUR HOLD

Limit value

Rinse contact

Parameter set B active USP output

19.2°C

Limit value

Effective direction min

Signal

Hysteresis +

Limit value

Contact

Icons in the Measurement Display

Measured value exceeds limit:

Relay output: Limit value

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select “Contact ...”

• “Usage: Limit” (Fig.)

Limit value

Effective direction max

Signal

Limit value

Hysteresis -

Contact

Measured value falls below limit:

Hysteresis

Tolerance band around the limit value, within which the contact is not actuated. Serves to obtain appropriate switching behavior at the output and suppress slight fluctuations of the measured variable (Fig.)

Contact type

Specifies whether the active contact is closed (N/O) or open (N/C).

Page 65

OK1, OK2 Inputs: Specify Level

Parameter setting/Module BASE/Inputs OK1, OK2

Note: HOLD mode (Setting: BASE module)

Menu Display Setting the OK inputs

Inputs OK1, OK2 (Administrator)

For OK2 usage see “Function control matrix”

OK1 usage

OK2 usage

Return

Inputs OK1, OK2 (Administrator)

For OK2 usage see “Function control matrix”

OK1 usage

Input OK1

Input OK2

Return

Off

HOLD

active 10 ... 30 V

active < 2 V

7.00 pH

19.2°C

7.00 pH

19.2°C

OK1 usage

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select “Inputs OK1/OK2”

• Select “OK1 usage”

OK1/OK2 switching level

• Open parameter setting

• Enter passcode

• Select “Module BASE”

• Select “Inputs OK1/OK2”

• Specify active switching level

The BASE module provides 2 digital inputs (OK1, OK2). The following functions (depending on the parameter setting) can be started via a control signal:

• OK1: “Off” or “HOLD”

• OK2: Select: System control / Function control matrix. (“Off”, “Parameter set A/B”, “Start KI recorder”)

Module BASE

OK1

OK2

You must specify the switching level for the control signal: (active 10...30 V or active < 2 V).

Page 66

Switching Parameter Sets via OK2

Parameter setting / System control / Function control matrix

Note: HOLD mode (Setting: BASE module)

Parameter Sets

2 complete parameter sets (A, B) can be stored in the analyzer. You can switch between the parameter sets using the OK2 input. The currently activated set can be signaled by a relay contact. An icon in the measurement display shows which parameter set is active: or

Menu Display

Function control matrix (Administrator)

Input OK2

Left softkey Right softkey

Profibus DO 2

Return

Contact K3 (Administrator)

Usage

Contact type ON delay OFF delay

Abort

83.1 % Air

24.8°C

ParSet KI rec. Fav Unical

NAMUR maintenance! NAMUR HOLD

Limit value Rinse contact

Parameter set B active

USP output

– –

Connect

83.1 % Air

24.8°C

Parameter sets

Selecting Parameter Set (A, B) via OK2 Input

• Open parameter setting

• System control

– –

• Function control matrix

––

• Select “OK2”

• Connect “Parameter set A/B”

Signaling Active Parameter Set via Relay Contact

• Open parameter setting

• BASE module

• Select contact

• Usage: “Parameter set ...”.

Note

The selection has no effect when working on SmartMedia card with SW 3400-102.

Page 67

Setting the Unical 9000(X) parameters

Unical 9000(X) Parameter Setting

Functional Capabilities

Setting Adjustable parameters Page

• Control Off, Unical 9000, Uniclean 900

• Cal preset values Buffer set as configured in the PHU 3400-110 Cal Buffer 1 Calimatic (automatic) or selection of a buffer Cal Buffer 2 Calimatic (automatic) or selection of a buffer Cal mode Adjustment, Calibration Cal timer program Off, Cleaning, Cal 2pt, Cal 1pt, Parking, User1, User2

• Time control Fixed interval, Week program:

Fixed interval: Select program, interval Week program: Configuration of program flows

• Program flow Individual adaptation of program steps for:

Cleaning, Cal 2point, Cal 1point, Service, Parking, User 2, User 1

• Installation External control (DCS) Off, On

DCS inputs (36...39) active 10...30 V or active < 2 V M/S input (42/43) active 10...30 V or active < 2 V A/M input (40/41) active 10...30 V or active < 2 V Output DCS 34 Measuring, Alarm DCS outputs (31…34) N/O, N/C

• Sensor detection On, Off

• Immersion lock Off, Sensocheck Glass el

• Access manual control Access code required. All valves can be actuated separately.

• Probe Probe type (Ceramat, SensoGate, InTrac, Others) Move time max. Adjustable; default setting 0015 s Sealing water On, Off Cavity rinsing Off, Interval, Continuous Check interval On, Off (On: Entry: Check after x travels) Maintenance interval On, Off (On: Entry: Maintenance after x travels)

• Rinse water Monitoring: Off, Process value, Temperature

• Media adapter (I ... III) (up to 3 metering pumps)

• Additional media (1...2) Monitoring of medium (Off, Process value, Temperature)

• Start-up Yes, No

• System forecast On, Off

Each: Medium, Displaced volume, Residual volume, Monitoring of medium (Off / Process value / Temperature)

Pg 68

Pg 69

Pg 70

Pg 81

Pg 82

Pg 87

Pg 88

Page 68

Cal preset values

Time control

Menu Display Unical 9000 parameter setting

7.05 pH

Menu selection

Select:

Return to meas

Parameter setting (Administrator)

System control Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Return

Probe control (Administrator)

Control

Cal preset values

Time control

Week program Program flow Installation

Return

Cal preset values (Administrator)

Measuring module

Knick 2.00 4.01

Cal Buffer 1 Cal Buffer 2

Cal mode

Return

Module PHU 3400-110

25.6 °C

[enter]

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Unical 9000

Week program

Block

7.05 pH

25.6 °C

Module PH 3400-032

Adjustment

Calibration

Open parameter setting

From the measuring mode: Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm.

Lingua

Select “Probe control / Unical 9000”. Icons to assign the measured values displayed:

specifies module slot I specifies module slot II

Cal Preset Values Unical 9000

Select pH module: (only if equipped with more than 1 pH module).

Select cal mode

• Adjustment: The values determined by a calibration are taken over.

• Calibration: The values determined by a calibration are logged but not taken over.

Cal timer program

Starts the selected program after caltimer expiry.

Probe control (Administrator)

Control Measuring Module

Cal mode

Time control

Program flow

Installation

Return

Unical 9000

Fixed interval

Week program

Block

7.05 pH

25.6 °C

Time Control

• Fixed interval (3): Specify times (000.0 h ... xxx.x h) (Please note: 000.1 h = 6 min)

• Week program: Specify weekday

Page 69

Time control (fixed interval / week program)

Menu Display Time control configuration

Fixed interval (Administrator)

Program

Interval

Program

Interval

Program

Interval

Abort

Week program (Administrator)

Monday

Tuesday Wednesday (Today) Thursday Friday Saturday

Return

Monday (Administrator)

User 3 User 2 Parking

Cal 1point

Cal 2point Clean

0:00 6:00 12:00 18:00 24:00

Return

Monday (Administrator)

01: Program

Start 06:00 End 18:00 Int. 002.0 h 02: Program

Time of start 08:00

03: Program

Return

Off

Clean Cal 2point Cal 1point User 1 User 2

User 3

Clean

Cal 1point

--- End ---

7.05 pH

25.6 °C

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Weekday

7.05 pH

25.6 °C

Time control: Fixed interval

The “Fixed interval” menu allows selection of up to three programs. An individual time interval an be assigned to each program.

Time control: Week program

In this menu you can View, Edit, and Copy.

View shows the configured program sequences over the day

Edit allows selection of up to 10 programs per day and you can choose between “Individual start” or “Interval” (the program is executed within a start and an end time at a specified interval).

Copy day (Administrator)

Copy Monday to “Weekday” Old day is overwritten!

Weekday

Return

7.05 pH

25.6 °C

Copy allows taking over a configured program for another weekday. (Further editing is possible.)

Page 70

Parameter setting: Program flows Cleaning program

Parameter Setting: Program Flows

Cleaning (Continuous), Media Monitoring Off

Display text Time [s]

01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Probe in MEASURE 0005 s 06: Program end

Cleaning (continuous) can also be started via a DCS input signal at input BIN1

of the Unical 9000 probe controller.

Program step

Message (display)

Probe: Measure Probe: Service

Rinse water

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

01 02

Stroke 1

Stroke 2

03 04 05 06

Exposure time

[t] s

Page 71

Calibration program

Parameter Setting: Program Flows

Cal 2point (Continuous), Media Monitoring Off

Display text Time [s]

01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Buffer I 0000 s 06: Cal Buffer 1 07: Rinse water ON 0010 s 08: Rinse water OFF 0002 s 09: Buffer II 0000 s 10: Cal Buffer 2 11: Rinse water ON 0010 s 12: Rinse water OFF 0002 s 13: Probe in MEASURE 0005 s 14: Program end

Cal 2point (continuous) can also be started via a DCS input signal at input BIN2

of the Unical 9000 probe controller.

Program step

Message (display)

Probe: Measure Probe: Service

Rinse water

Buffer 4.01 (Pump I)

Buffer 7.00 (Pump II)

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

01 02

Stroke 1

Stroke 2

03 04 05 06 07

Exposure time

Calibration with 1st buffer

08 09 10

Calibration with 2nd buffer

11 12 13 14

[t] s

Page 72

Parameter Setting: Program Flows

Cal 1point (Continuous), Media Monitoring Off

Display text Time [s]

01: Probe in SERVICE 02: Cleaning agent 0003 s 03: Rinse water 0010 s 04: Rinse water 0002 s 05: Buffer I 0000 s 06: Cal buffer 1 (pH 4.01) 07: Rinse water 0010 s 08: Rinse water 0002 s 09: Probe in MEASURE 10: Program end

Program step

Message (display)

Probe: Measure Probe: Service

Rinse water

Buffer 4.01 (Pump I)

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

01 02

Stroke 1

Stroke 2

03 04 05 06 07

Exposure time

Calibration with 1st buffer

08 09 10

[t] s

Page 73

Park program

Park Program: Wait Position

The park program includes the programming step “Wait position”. When the program is started via the DCS inputs BIN 1 ... BIN 3 on the Unical 9000, the program will be executed until the “Wait position” is reached. There it remains until the signal status at the DCS inputs changes.

• The program is started via the DCS inputs and remains in “Wait position” until the assignment of the DCS inputs changes:

DCS inputs BIN 1 ... BIN 3 of Unical 9000

Program until

wait position

Program after

wait position

• The program is started by a short signal at the DCS inputs: Wait position is skipped.

DCS inputs BIN 1 ... BIN 3 of Unical 9000

Program is executed completely.

Wait position is skipped.

Notice:

If the programs are started by the Protos 3400(X) from the Calibration or Maintenance menu, the wait position will be skipped.

Page 74

Parameter Setting: Program Flows

Parking

Display text Time [s]

01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Purge air ON 0010 s 06: Purge air OFF 0002 s 07: Cal buffer 1 (pH 4.01) 08: Wait position > Position will be held until next command (e.g., DCS) 09: Rinse water ON 0010 s 10: Rinse water OFF 0002 s 11: Probe in MEASURE 0005 s 12: Program end

Parking is started via a DCS input signal at input BIN3

of the Unical 9000 probe controller.

Program step

01 02

03 04 05 06 07

08 09 10

Message (display)

Probe: Measure Probe: Service

Rinse water

Buffer 4.01 (Pump I)

Purge air (AUX1 valve)

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

Stroke 1

Stroke 2

Exposure time

Wait

Wait position

[t] s

Page 75

Parameter Setting: Program Flows

Measurement (Short-Time), Media Monitoring Off

Display text Time [s]

01: Rinse water ON 0010 s 02: Rinse water OFF 0002 s 03: Probe in MEASURE 0005 s 04: Meas duration 0030 s 05: Probe in SERVICE 06: Cleaning agent 0020 s 07: Rinse water ON 0060 s 08: Rinse water OFF 0002 s 09: Program end

Measurement (short-time) can also be started via a DCS input signal at input BIN1

of the Unical 9000 probe controller.

Program step

01 02

03 04 05 06

07 08

Message (display)

Probe: Measure Probe: Service

Rinse water

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

Probe in MEASURE (short-time)

Stroke 1

Stroke 2

Exposure time

[t] s

Page 76

Parameter Setting: Program Flows

Cal 2point (Short-Time), Media Monitoring Off

Display text Time [s]

01: Rinse water ON 0010 s 02: Rinse water OFF 0002 s 03: Buffer I 0000 s 04: Cal Buffer 1 05: Rinse water ON 0010 s 06: Rinse water OFF 0002 s 07: Buffer II 0000 s 08: Cal Buffer 2 09: Rinse water ON 0010 s 10: Rinse water OFF 0002 s 11: Program end

Cal 2point (short-time) can also be started via a DCS input signal at input BIN2

of the Unical 9000 probe controller.

Program step

01 02

03 04 05 06

08 09

Message (display)

Probe: Measure Probe: Service

Rinse water

Buffer 4.01 (Pump I)

Buffer 7.00 (Pump II)

HOLD

Calibration with 1st buffer

Calibration with 2nd buffer

[t] s

Page 77

Parameter Setting: Program Flows

Cal 1point (Short-Time), Media Monitoring Off

Display text Time [s]

01: Rinse water ON 0010 s

02: Rinse water OFF 0002 s

03: Buffer I 0000 s

04: Cal buffer 1 (pH 4.01)

05: Rinse water ON 0010 s

06: Rinse water OFF 0002 s

07: Program end

Cal 1point (short-time)

Program step

Message (display)

Probe: Measure Probe: Service

Rinse water

Buffer 4.01 (Pump I)

HOLD

DCS ML3 (Program running)

01 02

03 04 05 06

Calibration with 1st buffer

[t] s

Page 78

Service program

Parameter Setting: Program Flows

Service

Display text Time [s]

Service can also be is started via a DCS input signal at input M/S

of the Unical 9000 probe controller.

Program step

Message (display)

Probe: Measure Probe: Service

Rinse water

Purge air (AUX1 valve)

Cleaning agent (Pump III)

HOLD

DCS ML3 (Program running)

01 02

Stroke 2

Stroke 1

Part 1: Measure —> SERVICE

03 04

Exposure time

08 09 10 11

Wait position

Part 2: SERVICE —> Measure

Page 79

Menu Display

Parameter setting Program flow

Program flow (Administrator) Clean Cal 2point

Cal 1point

Service

Parking

User 2

Abort

User 2 (Administrator)

Program name

01: Probe in SERVICE

02: Cleaning agent

03: Rinse water ON 04: Rinse water OFF 05: Buffer I

Abort

Example (Administrator)

Program name 01: Probe in SERVICE

02:

03: Rinse water ON 04: Rinse water OFF 05: Cleaning agent

Abort

approx. 2:02 min approx. 2:50 min approx. 2:26 min

approx. 2:40 min

Edit:

Copy

0020 s 0060 s 0002 s 0000 s

Example

Edit:

Insert Delete 0020 s

7.05 pH

25.6 °C

7.05 pH

25.6 °C

ser-2-----------

7.05 pH

25.6 °C

Configuring the Program Flow

Parameter setting / Probe control / Program flow / User 2: Select “Edit” using arrow keys, confirm with enter

Entering a Program Name

A new program name can be entered using the arrow keys. Confirm the name with enter

Editing a Program Step

Select the program step you want to edit using the arrow keys. Press enter: Now you can choose between “Edit, Insert, Delete”.

• Edit:

Allows selecting a function

• Insert:

Inserts an empty step above the selected program step and then allows selecting a function by “editing” the empty step. Allows selecting a function

• Delete:

The program step is deleted.

Page 80

Menu Display

• Configure function

• Activate monitoring

7.05 pH

Program flow (Administrator)

Function

Abort

For valve functions the run time must be specified, for pumps the exposure time.

Example (Administrator)

Function Run-time Monitoring

Return

Example (Administrator)

Program name

01: Probe in SERVICE

02: Cleaning agent 0020 s Chk

03: Rinse water ON 04: Rinse water OFF 05: Pump

Return

Media adapter (Administrator)

Port III

Medium Monitoring

Setpoint

Adm. deviation

25.6 °C

Cal Buffer 1 Cal Buffer 2 Purge air On Purge air Off Aux medium On Aux medium Off

Blank step

7.05 pH

25.6 °C

Cleaner On 0020 s

Off

7.05 pH

25.6 °C

Example 1

0060 s 0002 s 0000 s

7.05 pH

25.6 °C

Cleaning valve Mr Proper Process value

09.20 pH

01.00 pH

Configuring a Function

Select a function using arrow keys, confirm with enter

Program end Probe in SERVICE Probe in MEASURE Rinse water On Rinse water Off Wait time Buffer I - - - Text can be edited during installation Buffer II - - Text can be edited Cleaning agent - Text can be edited Cal Buffer 1 Cal Buffer 2 Purge air On - Text can be edited Purge air Off - Text can be edited Aux medium On - Text can be edited Aux medium Off - Text can be edited Wait position Goto line ORP check

Activating Monitoring

(see “Media monitoring”)

With several functions you can monitor the media used in the calibration chamber (“Monitoring: On”) (e.g. cleaning agent, buffers, rinse water, ...).

The respective program step is then marked with “Chk”. In any case it is necessary that you select the monitoring function for the respective medium in the “Installation” menu and specify valid tolerance limits for temperature or process value, otherwise the respective line is not displayed.

Return

Page 81

Parameter setting: Installation

Parameter Setting: Installation

Configuration of Unical 9000 Functions

Installation Default setting Adjustable parameters

• Measurement procedures Continuous (Short-time)

• Ext. control (DCS) (Polarity / Output settings)

- Signal level of inputs DCS (36 ... 39) M/S (42, 43) A/M (40, 41)

- DCS output (34) Measure Alarm

- Signal level of outputs DCS (31 ... 34)

• Sensor detection Off On

• Immersion lock Off Sensocheck Glass el

• Access manual control Access code for manual

• Probe

- Probe type Ceramat (SensoGate, InTrac, Other)

- Max. move time 0015 s

- Safety valve No (Yes)

- Sealing water Off (On)

- Cavity rinsing Off (Off, Interval, Continuous:

- Check interval Off On (Check after travels)

- Maintenance interval Off On (Maintenance after travels)

• Rinse water

- Monitoring Off (Process value/Temperature)

- Setpoint +07.00 pH

- Adm. deviation 01.00 pH

• Media adapter

- Port I ... III Off* “Pump” or “Off”

- Medium: --- (e.g. “Buffer I”)

- Displaced volume 25 ml (50 / 75 / 100 ml)

- Residual volume 250 ml (0 / 250 / 500 ml)

- Monitoring Off (Process value/Temperature)

- Setpoint 07.00 pH (Process medium or temp)

- Adm. deviation 0.50 pH

• Additional media

- Additional medium 1 Off (On - with monitoring)

- Additional medium 2 Off (On - with monitoring)

• Start-up No Yes/No

• System forecast Off Off / On: Monitors the probe travels for

Active: 10 ... 30 V (Active: 10 ... 30 V / active < 2V)

N/O (N/O / N/C)

control (Maintenance menu) Default: 2598

Default for interval: 0001.0 h, Rinse duration: 05 s)

predictive maintenance of Ceramat und SensoGate

*Automatic adjustment by “Plug & Play” in: System control / Factory setting Probe control

Page 82

Menu Display

• Meas. procedure

• External control via DCS

Installation (Administrator)

Meas. procedure

Ext. control (DCS) Sensor detection

Access manual control Probe

Rinse water

Return

Ext. Control (DCS) (Administrator)

Control

DCS inputs (36...39)

M/S input (42/43) A/M input (40/41)

DCS output (34)

DCS outputs (31…34)

Return

Continuous

Short-time

active 10...30V

active < 2 V active 10...30 V

Measure

N/O

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Off

Alarm

Selecting the Measurement Procedure

• Continuous measurement: With continuous measurement the pH electrode is located in the process medium and is retracted for calibration or cleaning.

• Short-time measurement: (interval measurement, sampling, sample mode ...) The pH electrode is only momentarily moved into the process medium. This method is applied when measuring aggressive or thermally demanding process media which require short measurement times with long rest periods.

External Control via DCS

• DCS inputs: Inputs for selecting the control programs. Here, the active signal level is specified. ( < 2 V or 10 ... 30 V).

• M/S input: Control of probe movement

• A/M input: Intervals automatic / blocked

• DCS output (34): Specify output signal for terminal 34:

- Measuring or

- Alarm

• DCS outputs (31 … 34): Specify contact type (N/O, N/C)

Page 83

Control via process control system

Control via Process Control Cystem (DCS)

Inputs/Outputs of Unical 9000(X)

Designation I / O FunctionNo.

Measuring/ Service

Auto / Manual

Bin 3

Bin 2

Bin 1

Measuring*** (user-defined: “Alarm”)

Service

Program runs

Level

Probe moves to measure position

Probe moves to service position43

Automat. interval control from Unical

Automat. intervals locked41

I Program selection and start, manual / DCS

(Program 1 ... 6 - see next page)

O34

O33

O32

Probe in “MEASURE” position

Probe in “SERVICE” position

Program running

* Passive contacts, 24 V must be supplied externally or via DCS

* **

** Signal duration at least 2 s (passing contacts)

*** As delivered, the signal output DCS 34 serves for probe position feedback – as shown. However, you can also program this output as “Alarm”. Then it sends a signal to the DCS in the event of calibration errors or faulty probe movement.

Page 84

Control Programs and Meas. Procedures

Factory Settings

Control Programs of Unical 9000(X)

6 programs and one service program can be started. 5 program flows are preset. 2 further programs can be entered by the user (User 1, User 2). The programs are started ...

• for manual operation via Protos 3400(X)

• remotely via DCS or switch with passive inputs Bin 1 ... 3 (24 V must be externally supplied, see Specifications)

Program Description Bin 3 Bin 2 Bin 1

1 Cleaning 0 0 1 2 Two-point calibration (Cal 2point) 0 1 0 3 One-point calibration (Cal 1point) 0 1 1 4 Park position 1 0 0 5 User-programmable (User 1) 1 0 1 6 User-programmable (User 2) 1 1 0 7 Service program Request via M/S

The service program (7) stops all other running programs (1 - 6) immediately and erases stored requests. For programs 1-6 the following applies: When you start a new program, the remaining steps of a currently running program are executed first. Further requests are stored and executed subsequently. When you control the Unical 9000(X) via Protos 3400(X), you can block the Bin 1, Bin 2, Bin 3 signal lines as well as M/S and A/M to prevent conflicts (Parameter setting / Probe control / Installation / Ext. control (DCS): Off)

Measurement Procedures

• Continuous measurement: After cleaning / calibration the probe moves into the process for measurement

• Short-time measurement (interval measurement, sampling, sample mode ...): After cleaning / calibration the probe remains in the calibration chamber and only moves into the process for measurement upon request.

Page 85

Menu Display

• Sensor detection

• Probe

Installation (Administrator)

Meas. procedure Ext. control (DCS)

Sensor detection

Immersion lock Access manual control

Probe

Return

Probe (Administrator)

Probe type

Move time max. Sealing water

Cavity rinsing Check interval

Check after travels

Return

7.05 pH

25.6 °C

Continuous

Off

7.05 pH

25.6 °C

Ceramat 006 s

Off Off

Off

20000

Sensor Detection

Sensor detection “On” prevents accidental probe movement when the electrode has been removed. This is done by checking whether the temperature detector integrated in the sensor is connected.

Probe

Selecting the retractable fitting. Here, the max. move time is automatically adjusted (depending on model).

Sealing Water

Sealing water is switched on shortly before the probe movement is started to keep the rinsing chamber free from medium. This is important for processes containing fibrous or adhering media. The sealing water pressure must be higher than the medium pressure. Intrusion of medium is prevented by the counter-pressure in the rinsing chamber which is caused by the sealing water.

Check Interval, Maintenance Interval

Permits specifying the max. admissible number of move cycles until a message is generated, factory setting: Check after travels: 20000 Maintenance after travels: 100000

Page 86

Configuring media monitoring

Configuring Media Monitoring

Parameter setting / Unical 9000 / Installation

Media Monitoring

For perfect system control, the pH value (or temperature) of the media used (buffer solutions, cleaning solution, rinsing water ...) can be checked against a specified value in the calibration chamber. This ensures that only correct media are used in the calibration chamber of the probe. Exchanged or contaminated media or media with a wrong temperature are recognized. In that case a message will be released. If faulty media are recognized before a calibration step, that step will not be performed.

NOTICE!

When monitoring the pH value of a medium, the zero and slope deviations of the electrode must be taken into account. Therefore the value specified for “adm. deviation” must not be too low!

Menu Display

Rinse water (Administrator)

Monitoring

Setpoint Adm. deviation

Return

7.05 pH

25.6 °C

Off

Process value

Temperature

Configuring the media monitoring

Media monitoring can be configured in the “Parameter setting / Probe control / Installation” menu for:

• Rinse water

• Media at media adapter (... in the “Media adapter” menu)

• Additional media The process value or temperature of the media can be monitored. Please note that the value specified for “Adm. deviation” should not be too low. The minimum response time is automatically taken into account when configuring the user programs.

Page 87

Menu Display

• Media adapter, Additional media

• Start-up

Media adapter (Administrator)

Port I

Medium Displacement volume

Residual volume

Monitoring Setpoint

Return

Additional media (Administrator)

Additional medium 1

Medium Monitoring Setpoint

Adm. deviation

Additional medium 2

Return

Installation (Administrator)

Access manual control Probe Rinse water Media adapter

Additional media

Start-up

Return

Metering pump

Buffer - I -------

25 ml 250 ml Process value

+07.00 pH

Purge air-----

Process value

+07.00 pH

00.20 pH

Yes

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Off

7.05 pH

25.6 °C

Media Adapter

• Specifying the equipment (Metering pump, Off, or Cleaner)

• Designation of medium

• Specifying the displaced volume depending on model, e.g.: Ceramat 25 ml InTrac 77Xe 50 ml InTrac 797e 75 ml InTrac 798e 100 ml)

• Residual volume

• Monitoring (Process value/Temp)

• Setpoint

Additional Media (2)

• Specifying the equipment (On, Off)

• Designation of medium,

• Monitoring (Process value/Temp)

• Setpoint

Start-Up

At the end of the parameter-setting procedure, a “Start-up” line appears in the “Installation” menu. When you are sure to have set all parameters, select “Yes” to confirm. Now the pumps perform the number of stroke movements required for filling the media tubes completely. The necessary rinsing cycles are automatically started.

Page 88

System forecast

System Forecast (Ceramat, SensoGate)

Monitoring the probe travel behavior of retractable fittings (with Unical 9000(X) software version 4.3 or higher)

The "System Forecast" function enables monitoring of the probe travel behavior of the Ceramat or SensoGate retractable fittings. Possible signs of wear are detected in good time to prevent failure or downtimes ("predictive maintenance").

Fittings frequently display signs of wear as a change in their travel behavior. The travel time can increase significantly, for example, if aggressive media or critical processes cause

monitored probe travel

SensoGate in Service position...

... and in Process position

the retractable fitting to become sticky or seals to swell. The switching behavior of control elements such as piezo valves also changes in the course of time, particularly with long dwell times in one position.

The opening and closing times as well as the passing capacity of these valves can then be significantly changed. Over time, pneumatically-controlled valves are also subject to changed switching times as a result of increasing friction, fatty deposits or other influences. The "System Forecast" determines whether the probe movement is continuous or jerky, which, for example, would indicate resinified fat. These changes can be recorded in a probe travel profile.

By comparing with reference times, an expert can draw conclusions on the status of the separate components, and the system itself can

Message list

U172

Warn SP probe sluggish

UNICAL active

1 messg.

generate appropriate messages, see example (menu "Diagnostics / Message list").

Return

Page 89

System Forecast: Probe Travel Profiles

Reference / Probe Travel Profiles

Following installation of a system or after a repair, several cycles are run by calling the "System forecast / Edit reference profile" function. The travel behavior (probe travel profile) detected is saved as a "reference profile" with time and date. A distinction is made here between retraction behavior S (service) and insertion behavior P (process).

Creation of a Probe Travel Profile and Presentation in Protos

Menu: Parameter setting / Probe control / Installation / System forecast

07.00 pH

System forecast (Administrator)

Active reference profile

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Auto - New record Edit reference profile Tolerances

Return

25.6 °C

Auto

Yes

The active reference profile contains the following parameters:

12/21/16 12:37 S a06 b17 c25 d33 e02 CM

CM/SG probe type CM: Ceramat, SG: SensoGate

aXX … eXX Records of separate travel times

aXX: Time [1/10 s] from run command to response of air sensor. bXX: Time [1/10 s] from run command until drop-out of the exit limit position. cXX: Time [1/10 s] from run command to response of desired limit position. dXX: Time [1/10 s] from run command to drop-out of air sensor. eXX: Counter: number of air current interruptions during a travel cycle.

S/P: Direction of travel

S: Service position P: Process position

Date and time of profile creation

Page 90

Setting the system forecast parameters

Setting the System Forecast Parameters

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display System forecast

07.00 pH

Yes

25.6 °C

7.00 pH

25.6 °C

WA150

System control (Administrator)

Probe

Rinse water Media adapter

Additional media

System forecast

Start-up

Return

Note:

Clicking on "System forecast" brings up the following message: “Please wait! Function is executed". Protos initially reads the data for the reference profile saved in the Unical. This can take some time.

System forecast (Administrator)

Active reference profile

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Edit reference profile Tolerances Messages

Return

Setting the system forecast parameters

(only Ceramat and SensoGate types) Select a Ceramat or SensoGate retractable fitting from within the "Probe" menu item. Further parameters can then be set under "System forecast".

Active reference profile

Reference profiles are preinstalled by default for the following probes: Ceramat WA150 Ceramat WA160 SensoGate WA130S (short) SensoGate WA130L (long) These profiles can be selected under "Active reference profile".

They are based on the following process conditions:

Process pressure: 3 bar Compressed air: 5 bar Unical hose length: 5 m Temperature: 20 °C

In the event of greater deviations in the process conditions, you should create an individual “User” reference profile.

Page 91

System Forecast: Reference Profile

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display

System forecast

Active reference profile

12/21/16 12:37 S a06 b17 c2 12/21/16 12:37 P a09 b16 c2

Auto - New record

Edit reference profile

Tolerances

Return

System forecast

Active reference profile

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Auto - New record

Edit reference profile

Tolerances

Return

System forecast

01/01/00 00:00 S a00 b00 c00 d00 e00 X Auto 01/01/00 00:00 P a00 b00 c00 d00 e00 X Auto

............................................................................................

12/21/16 12:37 S a06 b17 c25 d33 e02 12/21/16 12:37 P a09 b16 c26 d34 e02

7.00 pH

25.6 °C

Auto

User WA 150 WA 153 WA 154 WA 160

7.00 pH

25.6 °C

Auto

Yes

7.00 pH

25.6 °C

System forecast: Active reference profile

Active reference profile “Auto”

A reference profile is recorded in the background during the first probe movements (at least 20probe movements).

Auto - New record

The old reference profile is deleted and and a new one is recorded.

While recording is in progress, all values are set to “0” and the “Auto” remark is active.

Return

7.00 pH

System forecast

12/21/16 12:37 S a06 b17 c25 d33 e02 CM Auto 12/21/16 12:37 P a09 b16 c26 d34 e02 CM Auto

............................................................................................

12/21/16 12:37 S a06 b17 c25 d33 e02 12/21/16 12:37 P a09 b16 c26 d34 e02 12/21/16 12:37 S a06 b17 c25 d33 e02

Return

25.6 °C

“Auto” reference profile created

After 20 probe movements the reference values are created. They are followed by the probe identifier (CM=Ceramat, SG=SensoGate) and "Auto" for the reference profile.

Page 92

System forecast: create reference profile

System Forecast: Creating a Reference Profile

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display

System forecast

Active reference profile

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Edit reference profile

Tolerances

Messages

Return

Edit reference profile (Administrator)

Record new profile with "Start" softkey

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Reference profile

Return

Start

7.00 pH

25.6 °C

User

7.00 pH

25.6 °C

User

System forecast: Active reference profile: “User”

Creating a “User” reference profile

By selecting "Edit reference profile", you can create an individual “User” reference profile. Use the Start soft- key to record a reference profile. For this purpose, six probe movements are executed. The reference profile is the average of the recorded values.

Auto, User reference profiles: Setting tolerances

For monitoring during operation, permissible deviations in the separate travel times can be set in the "Tolerances" menu. The tolerances a...e are permissible deviations from the active reference profile. – See next page

The name "User" cannot be modified by the user. The new profile is identifiable by the date and time of its recording.

Page 93

System forecast: Tolerance specifications

System Forecast: Tolerance Specifications

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display System forecast: Tolerances

7.00 pH

Off

25.6 °C

WA150

System control (Administrator)

Active reference profile

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Monitoring Edit reference profile

Tolerances

Return

Tolerance specifications

For monitoring during operation, permissible deviations in the separate travel times can be set in the "Tolerances" menu. The tolerances "a...e" are permissible deviations from the active reference profile.

If monitoring is set to "on", the icon is displayed in measuring mode if a tolerance limit is exceeded – the corresponding message text can be viewed under "Diagnostics / Messages".

Tolerances (tol.) Input range

a Probe valve switching time (tol.+) 00 ... 99 [1/10 s] b Exit of limit position (tol.+) 00 ... 99 [1/10 s] c Achievement of limit position (tol.+) 00 ... 99 [1/10 s] d Air sensor deactivated (tol.+) 00 ... 99 [1/10 s]

Air sensor deactivated (tol.–) 00 ... 99 [1/10 s]

e Air current interruptions (tol.+) 01 ... 09 [number]

Reference profile tolerance 00 ... 99 %

Page 94

System Forecast: Reference Profiles, Messages

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display System forecast

Messages

Monitoring

U160 Pressure loss/Air sensor U161 Probe valve not functioning U162 Air sensor not functioning U163 Probe valve sluggish

U164 Air sensor sluggish

Return

7.00 pH

25.6 °C

Maintenance

Active Active

Active

Reference profiles, messages

Monitoring allows forecast messages to be switched off (“Off”) or to be output as maintenance message (“Maintenance”) or as failure message (“Failure”). The corresponding message text can be viewed under "Diagnostics / Messages".

The individual messages can be set to “active” or “inactive” (switched off ).

With “Maintenance” selected, the icon is shown in measuring mode when a tolerance is exceeded.

With “Failure” selected, the

icon is shown in measuring mode when a tolerance is exceeded.

Page 95

System Forecast: Diagnostic Messages

Menu: Diagnostics / System forecast

Menu Display System forecast: Diagnostics

UNICAL active

S >>>

1 messg.

7.00 pH

25.6 °C

7.00 pH

25.6 °C

Message list

U168

SP SERVICE position not functioning

Return

System forecast

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM User

Load probe travel profile

Return

System forecast

Return

For better comparability, the travel cycles can be displayed using the right softkey:

- in Service “S“ and Process “P“ directions

- in Service "S" direction only

- in Process "P" direction only

Message list

When you have activated "Monitoring On" in the System forecast menu, a violation of a preset tolerance will generate a message text. These texts can be viewed in the message list.

System forecast

In operation, travel times are saved for every cycle (max. 200) and are compared with the active reference profile. If "System forecast" is selected in the diagnostics menu, the active reference profile and probe profiles already recorded are displayed (this may take some time). If tolerance limits are exceeded in the probe travel profile, the error number is displayed after the probe profile.

NOTICE

In the Protos/Unical system, the last 200 travel cycles are recorded in volatile memory, i.e. the data is lost when the supply voltage is switched off. Recording on a SmartMedia card is therefore recommended – see following page.

Page 96

System forecast: Record on SmartMedia card

System Forecast: RecordingonSmartMediaCard

Menu: Parameter setting / Probe control / Installation / System forecast

Menu Display System forecast: SmartMedia card

7.00 pH

Off

25.6 °C

System control (Administrator)

12/21/16 12:37 S a06 b17 c25 d33 e02 CM 12/21/16 12:37 P a09 b16 c26 d34 e02 CM

Monitoring Edit reference profile Tolerances

Record on card Off

Return

Record on SmartMedia card

If a SmartMedia card is installed, probe travel times can be saved on it (ASCII). The recording capacity is limited only by the amount of memory on the card. For this function, use the final menu item in the system forecast – "Record on card".

Page 97

System forecast: Messages

System Forecast: Messages

No. "System forecast" message Cause

U160 SP Pressure loss/Air sensor Air leaking uncontrolled – air sensor defective

U161 SP Probe valve not functioning Pilot valve does not switch; probe valve possibly

U162 SP Air sensor not functioning Air sensor does not switch

U163 SP Probe valve sluggish Pilot valve switches late; probe valve possibly

U164 SP Air sensor sluggish Air sensor switches late

U165 SP Limit positions interrupted Both limit positions do not switch

U166 SP Limit positions short-circuited Both limit switches are actuated (short-circuited)

U170 SP Probe stopped between end positions Probe is stuck between the limit positions

U171 SP PROCESS position sluggish Limit switch (PROCESS) reacts too late after start of

U172 SP Probe sluggish Probe sluggish (limit position is reached)

U173 SP Probe is stuck during probe travel Probe is stuck during probe travel (limit position is

U174 SP SERVICE position not functioning Limit switch (SERVICE) does not react after end of

U175 SP PROCESS position not functioning Limit switch (PROCESS) does not react after end of

U176 SP SERVICE position sluggish Limit switch (SERVICE) reacts too late after end of

U177 SP SERVICE position not functioning Limit switch (SERVICE) not functioning

U178 SP PROCESS position not functioning Limit switch (PROCESS) not functioning

U179 SP Probe instantly got stuck Probe is stuck in limit position

U188 SP General error Error not clearly assignable

does not switch

switches late

(e.g. GND missing)

probe travel

not reached)

probe travel

Messages are automatically reset after two correct probe movements.

Page 98

Setting the Uniclean 900(X) parameters

Uniclean 900(X) Parameter Setting

Functional Capabilities

Setting Adjustable parameters Page

• Control Off, Unical 9000, Uniclean 900

• Time control Fixed interval, Week program:

Fixed interval: Select program, interval Week program: Configuration of program flows

• Program flow Individual adaptation of program steps for: Rinsing, Cleaning, Parking, Service

• Installation

Meas. procedures Continuous / Short-time External control (DCS) Off, On

• Sensor detection On, Off

• Immersion lock Off, Sensocheck Glass el

• Access manual control Access code required. All valves can be actuated separately.

• Probe Probe type (SensoGate, Ceramat, others)

Move time max. Adjustable; default setting 0015 s Sealing water On, Off Cavity rinsing Off, Interval, Continuous Check interval On, Off (On: Entry: Check after x travels) Maintenance interval On, Off (On: Entry: Maintenance after x travels)

Pg 99

Pg 100

Pg 108

• Media adapter (I ... III)

(up to 3 metering pumps)

• Add. media (1 ... 2) Monitoring of medium (On, Off, Medium)

• Start-up Yes, No

• System forecast On, Off

Each: Pump (On, Off), Medium, Displaced volume, Residual volume

Pg 113

Pg 88

Page 99

Time control (fixed interval / week program)

Menu Display

Menu selection

Return to meas

Parameter setting (Administrator)

System control Module FRONT 3400-011 Module BASE 3400-021

Module PHU 3400-110

Probe control

Return

Probe control (Administrator)

Control

Meas. module

Time control

Week program Program flow Installation

Return

Select:

Uniclean 900

Module PHU 3400-110

Week program

[enter]

Block

7.05 pH

25.6 °C

Lingua

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Uniclean 900 parameter setting

Open parameter setting

From the measuring mode: Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm.

Select “Probe control / Uniclean 900”. Icons to assign the measured values displayed:

specifies module slot I specifies module slot II

Measuring Module

Select measuring module: Select the pH module for evaluation with the Uniclean 900 controller (only if equipped with more than 1 pH module).

Probe control (Administrator)

Control Measuring module

Cal mode

Time control

Program flow

Installation

Return

Uniclean 900

Fixed interval

Week program

Block

7.05 pH

25.6 °C

Time Control

• Fixed interval: Specify times (000.0 h ... xxx.x h) (Please note: 000.1 h = 6 min)

• Week program: Specify weekday

Page 100

Week program

Menu Display Time control configuration

Fixed interval (Administrator)

Program

Interval

Abort

Week program (Administrator)

Monday

Tuesday Wednesday (Today) Thursday Friday Saturday

Return

Monday (Administrator)

User 2

User 1 Parking Parking Clean Rinse

0:00 6:00 12:00 18:00 24:00

Return

Monday (Administrator)

01: Program

Start 06:00 End 18:00 Int. 002.0 h 02: Program Time of start 08:00 03: Program

Return

Off

Rinse Clean Parking

Clean

Cal 1point

--- End ---

Weekday

7.05 pH

25.6 °C

7.05 pH

25.6 °C

7.05 pH

25.6 °C

7.05 pH

25.6 °C

Time control: Fixed interval

The “Fixed interval” menu allows selection of up to three programs. An individual time interval an be assigned to each program.

Time control: Week program

In this menu you can View, Edit, and Copy.

View shows the configured program sequences over the day.

100

Copy day (Administrator)

Copy Monday to “Weekday” Old day is overwritten!

Weekday

Return

7.05 pH

25.6 °C

Copy allows taking over a configured program for another weekday. (Further editing is possible.)