KERN & SOHN DLB 160-3A User Manual

KERN & Sohn GmbH
Ziegelei 1
E-Mail: info@kern-sohn.com
Internet: www.kern-sohn.com
Operating instructions Electronic Moisture Analyzer
KERN DLB_A
Version 1.1
02/2015
GB
D-72336 Balingen
Fax: +49-[0]7433-9933-149
DLB_A-BA-e-1511
KERN DLB_A
Electronic Moisture Analyser
GB
Version 1.1 02/2015
Operating instructions
Contents
1 Technical data .................................................................................................... 4
2 Appliance overview ............................................................................................ 6
2.1 Keyboard and display overview ................................................................................................... 9
3 B as ic Information (General) ............................................................................ 10
3.1 Proper use .................................................................................................................................... 10
3.2 Improper Use ................................................................................................................................ 10
3.3 Warranty ....................................................................................................................................... 10
3.4 Monitoring of Test Resources .................................................................................................... 10
3.5 Danger Information ...................................................................................................................... 11
4 B asic S afety Precautions ................................................................................ 12
4.1 Pay attention to the instructions in the Operati o n Manual ..................................................... 12
4.2 Personnel trainin g ....................................................................................................................... 12
5 Transport and storage ..................................................................................... 12
5.1 Testing upon acceptance ........................................................................................................... 12
5.2 Packaging / retur n transport ....................................................................................................... 12
6 Unpacking, S etup and C ommis s ioning.......................................................... 12
6.1 Installation Site, Lo cation of Use ............................................................................................... 12
6.2 Unpacking and erection .............................................................................................................. 14
6.2.1 Scope of delivery ........................................................................................................................... 15
6.3 Mains connection ........................................................................................................................ 15
6.4 Connection of peripheral devices .............................................................................................. 16
6.5 Initial Commissioning ................................................................................................................. 16
7 Weighing ........................................................................................................... 17
8 Adjus tment ....................................................................................................... 18
8.1 Adjust balance ............................................................................................................................. 18
8.2 Calibrate / adjust temperature .................................................................................................... 19
8.2.1 Calibration of temperature value .................................................................................................... 21
8.2.2 Adjustment of temperature value ................................................................................................... 22
9 Appliance configuration .................................................................................. 23
9.1 Baud rate ...................................................................................................................................... 25
9.2 Auto Zero ...................................................................................................................................... 26
9.3 Filter .............................................................................................................................................. 28
9.4 Standstill control display ............................................................................................................ 29
9.5 Display background illumination ............................................................................................... 30
10 Operator menu – moisture analysis ............................................................... 31
2 DLB_A-BA-e-1511
10.1 How to implement drying .............................................................................................................32
10.1.1 Moisture analysis with drying program PrG1 – PrG5 .................................................................33
10.1.2 Moisture analysis with drying program PrG time ........................................................................37
10.1.3 Moisture analysis with drying program PrG Auto Mode .............................................................40
10.2 Save the drying programs PrG1, PrG2, PrG3, PrG4, PrG5 .......................................................44
11 R S 232C interface ............................................................................................. 46
11.1 Technical data ...............................................................................................................................46
11.2 Pin allocation of the output plug ................................................................................................46
11.3 Menu settings „Serial“ .................................................................................................................47
11.3.1 Printout examples (YKB-01N) ....................................................................................................48
12 General information concerning mois ture analysis ...................................... 49
12.1 Application ....................................................................................................................................49
12.2 Basics ............................................................................................................................................49
12.3 Adjustment to existing measuring method ................................................................................49
12.4 Preparing a sample.......................................................................................................................50
12.5 Sample material ............................................................................................................................51
12.6 Sample size / origi n ally weighted in quantity ............................................................................51
12.7 Drying temperature.......................................................................................................................52
12.8 Recommendations / Guidelines ..................................................................................................52
13 E rror mess ages ................................................................................................. 56
14 S ervice, maintenance, dispos al ....................................................................... 57
14.1 Cleaning.........................................................................................................................................57
14.2 Service, maintenance ...................................................................................................................57
14.3 Disposal .........................................................................................................................................57
15 Ins tant help ........................................................................................................ 58
16 Declaration of conformity ................................................................................ 59
DLB_A-BA-e-1511 3

1 Technical data

Weighed in quantity
5°C….+40°C ambient temperature
45% - 75% air humidity non-condensing
Data DLB 160-3A
Radiator Halogen (1 x 400 W)
Temperature range
Maximum load (Max) 160 g Warm-up time 120 min Minimum for drying 0.5 g
Weighing mode 0.001g
Readability (d)
Moisture analysis mode 0.01 % Weighing mode 0.001g
Reproducibility
Moisture analysis mode
Linearity ± 0.003 g Stabilization time (typical) 4 sec. Recommended adjustment
weight, not added (class)
35°C - 160°C
Choice of steps at 1°C
100g (E2)
10 g: 0.03 %
Environmental conditions
4 DLB_A-BA-e-1511
Housing 210 x 340 x 225 mm
drying room
Net weight
4.2 kg
Electric Supply
230V AC 50Hz
Mains adapter
9V AC, 1000mA
Shutoff criterion
Sample dishes included Ø 100 mm Result display [g] residual weight
Internal memory 5 memory locations for drying programs
1. Time mode
Drying is finished after the set time, adjustable 1 – 99 minutes.
2. Auto mode
Drying is completed, when the set weight value per time unit is lower than the nominal value,
0.1 – 9.9 % loss of weight adjustable.
[%] moisture [%] dry mass: ATRO [%] = Start weight : Residual weight x 100%
Interface RS232 Dimensions
Available
Ø 100 mm, 20 mm high
DLB_A-BA-e-1511 5

2 Appliance overview

Pos. Description
1 Foldable hood 2 Temperature sensor 3 Sample dish 4 Heating top 5 Balance 6 Display 7 Keyboard 8 Levelling screw
6 DLB_A-BA-e-1511
3
6
4
5 2 7
1
1. Plug-in connection cable „Balance / Heating top“
2. Connection net adapter „Balance“.
3. Current supply „Heating top“.
4. RS 232 interface
5. Plug-in connection cable „Balance / Heating top“
6. Main switch „Heating top“
7. Adjustable foot screws
DLB_A-BA-e-1511 7
9 8 11
10
8. Housing screws
9. Housing screws (for access remove the foot screws)
10. Adjustable foot screws
11. Rigid foot screw
8 DLB_A-BA-e-1511

2.1 Keyboard and display overview

Zero indicator
]
Stability display
%
Display of percentage
Status „Weighted in quantity sample“
H
Drying process active
g
Gram display
Long time pressed button gets mute
Invoke user menu
Invoke / exit
Display Description
Key Description Description
Short key pressing
MENU button/
Switch over display of result
Navigation button
STOP
ON/OFF button
Select menu items – scroll fo rward
Complete drying
Turn on/off
Exit user menu
CAL button/
Adjustment
START
Navigation button
PRINT button
Select menu items – scroll backward
Start drying
Calculate weighing data via interface
until the acoustic signal
configuration menu
Navigation button
TARE button
DLB_A-BA-e-1511 9
Confirm / store settings
Taring
Zeroing

3 Basic Information (General)

3.1 Proper use

The device purchased by you is designed for a fast and reliable determination of material moisture in liquid, porous and solid materials by applying the method of thermogravimetrics.

3.2 Improper Use

Impacts and overloading exceeding the stated maximum load (max) of the device, minus a possibly existing tare load, must be strictly avoided. This could damage the instrument. Never operate device in explosive environment. The serial version is not explosion protected. Changes to the unit's design are not permitted. This may lead to incorrect weighing results, safety-related faults and destruction of the appliance. The unit may only be operated in accordance with the described default settings. Other areas of use must be released by KERN in writing.

3.3 Warranty

Loss of warranty due to
Our conditions in the operation manual are ignored
The appliance is used outside the described uses
The appliance is modified or opened
mechanical damage and damage caused by media, liquids
natural wear and tear
The appliance is improperly set up or incorrectly electrically connected
The measuring system is overloaded

3.4 Monitoring of Test Resources

In the framework of quality assurance the measuring-related properties of the moisture analyser and, if applicable, the testing weight, must be checked regularly. The responsible user must define a suitable interval as well as type and scope of this test. Information is available on KERN’s home page (www.kern-sohn.com) with regard to the monitoring of balance test substances and the test weights required for this. In KERN's accredited DKD calibration laboratory test weights and balances may be calibrated (return to the national standard) fast and at moderate cost.
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3.5 Danger Information

Individual parts of the case (e. g. the ventilation grids) may heat up considerably during operation. For this reason, please touch the device only at the designated handles. Sample materials developing aggressive vapours (e. g. acids) may cause corrosion problems on some parts of the device. The moisture meters should mainly be used for drying aqueous substances. Explosion prone, flammable samples must not be analysed using the moisture meter.
Do not open or touch drying chambers during the drying
process as the device develops very high temperatures. Even after finishing the measurement the appliance remains hot.
Careful when removing the sample. The sample itself, the sample dish and the heating unit may be very hot.
Do not use the moisture meter for analysing explosion prone, easily flammable samples.
Do not operate the humidity analyser in areas with hazard of explosion
Sample materials emitting toxic substances must be dried with a special extraction system in place. Create an environment that prevents the inhalation of vapours hazardous to health.
Do not place combustible materials on, under or next to the device.
Ensure that there is sufficient empty space around the device in order to prevent heat accumulation (distance to device 20 cm, above it 1m).
Make sure that liquids do not get in contact with the interior of the device or the connections at the rear of the device. If you spill liquid on the device, disconnect it immediately. Afterwards do not operate the appliance and have it checked by a competent KERN stockist before any further use.
DLB_A-BA-e-1511 11

4 Basic Safety Precautions

4.1 Pay attention to the instructions in the Operation Manual

Carefully read this operation manual before setup and commissioning, even if you are already familiar with KERN

4.2 Personnel training

The appliance may only be operated and maintained by trained personnel.
appliances.

5 Transport and stora ge

5.1 Testing upon acceptance

When receiving the appliance, please check packaging immediately, and the appliance itself when unpacking for possible visible damage.

5.2 Packaging / return transport

Keep all parts of the original packaging for a possibly
required return.
Only use original packaging for returning. Prior to dispatch disconnect all cables and remove
loose/mobile parts.
Reattach possibly supplied transport securing devices. Secure all parts such as the glass wind screen, the
weighing platform, power unit etc. against shifting and damage.

6 Unpacking, Setup and Commissioning

6.1 Installation Site, Location of Use

The unit is designed to achieve reliable weighing results under normal conditions of use. You will work accurately and fast, if you select the right location for the appliance.
12 DLB_A-BA-e-1511
On the installation site observe the following:
4. Major display deviations (incorrect weighing results) may
weighing container and windshield
7. Protect the appliance against high humidity, vapours and
appliance for ca. 2 hours at room temperature.
1. Avoid extreme heat as well as temperature fluctuation caused by installing next to a radiator or in the direct sunlight;
2. Remove explosion prone, easily flammable material in the immediate vicinity. Emerging vapours, sample dish and all parts of the sample chamber are hot!
3. Place the device on a firm, level surface.
be experienced should electromagnetic fields (e.g. due to mobile phones or radio equipment), static electricity accumulations or instable power supply occur. Change location or remove source of interference.
5. Avoid static charging of the material to be weighed,
6. Avoid jarring during weighing.
dust,
8. Do not expose the device to extreme dampness for longer periods of time. Non-permitted condensation (condensation of air humidity on the appliance) may occur if a cold appliance is taken to a considerably warmer environment. In this case, acclimatize the disconnected
9. Protect the device against direct draughts due to open windows and doors.
DLB_A-BA-e-1511 13

6.2 Unpacking and erection

Take the appliance carefully out of its packaging, remove the plastic jacket and install it at the designated work space.
The appliance is supplied part-assembled. Immediately after unpacking check if the delivered items are complete. Assemble the separate component parts according to their sequence.
1.
2.
3.
4.
1. Put cover into the weighing chamber.
2. Put on the dish retainer carefully.
3. Position removal aid in a way that the handle fits under the groove of the cover.
4. Put sample dish on the dish holder.
5. Level the appliance with the help of the foot screws until it is standing evenly.
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6.2.1 Scope of delivery

2
1
Serial accessories:
Moisture analyzer, see chap. 2
10 sample dishes
Power cable
Mains adapter
Connection cable „Balance / Heating top“
Operating instructions

6.3 Mains connection

1. Power is supplied to the balance via the external power unit. The stated voltage value must be the same as the local voltage. Only use original KERN mains adapters. Using other makes requires consent by KERN. After connection to the power supply the balance will carry out a self-test. The balance changes into stand-by mode.
To switch on press the ON/OFF button. As soon as the weight display appears, the balance is ready for weighing.
DLB_A-BA-e-1511 15
3
2. Power supply to the heating top is provided via the supplied mains cable. Do not connect the appliance to the power grid unless the information on the appliance (sticker) matches the local mains voltage. To switch on, press the main switch on the rear side of the appliance.
3. Attach the connection cable balance / heating top.
The appliance must be connected to a standard socket with earth terminal. Do not eliminate the protective effect by using an extension lead without earth terminal. For power supplies from power grids without earth terminals call a specialist to establish equivalent protection according to the relevant installation regulations.

6.4 Connection of peripheral devices

Before connecting or disconnecting of additional devices (printer, PC) to the data interface, always disconnect the moisture analyser from the power supply. Only use accessories and peripheral devices by KERN, as they are ideally tuned to the appliance.

6.5 Initial Commissioning

In order to obtain exact results with the electronic balances, your balance must have reached the operating temperature (see warming up time chap. During this warming up time the balance must be connected to the power supply (mains, accumulator or battery).
The accuracy of the balance depends on the local acceleration of gravity. Strictly observe hints in chapter Adjustment.
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7 Weighing

Start-up
Switching Off
Simple weighing
1. In stand-by mode (see chap. 6.3) press ON/OFF button. As soon as the weight display appears, the balance is ready for weighing.
2. Press the ON/OFF button, the balance returns into stand­by mode.
3. Place goods to be weighed on balance.
4. Wait until the stability display appears []
5. Read weighing result.
Taring
6. Place the weighing box and press the TARE button. „0-t“ is displayed.
7. After standstill control the zero display appears.
The weight of the container is now internally saved.
8. Weigh the material, the net weight will be indicated. After removing the weighing container, the weight of the
weighing container appears as negative display. The tare weight is saved until it is deleted. Remove the load
from the balance and press the TARE button. „0-t“ is displayed, wait until the zero display appears.
The tare procedure can be repeated as many times as necessary, for example with initial weighing of several components for a mix (add-on weighing). The limit is reached when the total weighing range capacity is full.
DLB_A-BA-e-1511 17

8 Adjustment

8.1 Adjust balance

As the acceleration value due to gravity is not the same at every location on earth, each balance must be coordinated - in compliance with the underlying physical weighing principle - to the existing acceleration due to gravity at its place of location (only if the balance has not already been adjusted to the location in the factory). This adjustment process must be carried out for the first commissioning, after each change of location as well as in case of fluctuating environment temperature. To receive accurate measuring values it is also recommended to adjust the balance periodically in weighing operation.
Observe stable environmental conditions. A warming up time (see chapter 1) is required for stabilization.
Carry out adjustment with placed sample dish. Ensure that no objects are within the sample dish.
Weight value of the required adjustment weight see chpt. 1 “Technical specifications“:
In weighing mode press the CAL button.
Wait until the weighed value for the required adjustment weight appears
flashing.
Example 100 g
During the flashing display put the required adjustment weight carefully in the
centre of the sample dish. The flashing display disappears. After successful adjustment the balance automatically returns to weighing mode.
Take away adjustment weight
In case of an adjustment error (e.g. objects on the weighing plate) the display will show an error message, repeat adjustment.
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