Julabo FPW55-SL, FPW90-SL, FPW52-SL, FP90-SL, FP52-SL Instruction Manual

...

English

Ultra-Low

www.julabo.com

Operating Manual

Refrigerated Circulators

air-cooled

FP52-SL FP55-SL FP90-SL

water-cooled

FPW52-SL FPW55-SL FPW90-SL FPW91-SL

• upgradable with supplementary pump - HSP

• upgradable with supplementary heater - HST

• special unit with bath opening for internal

temperature applications

19532830-V3.doc 09.02.16

JULABO USA, Inc. 884 Marcon Boulevard Allentown, PA 18109 Phone: +1(610) 231-0250 Fax: +1(610) 231-0260 info.us@julabo.com

Temperature control devices for research and industry are developed,

Congratulations!

You have made an excellent choice. JULABO thanks you for the trust you have placed in us. This operating manual has been designed to help you gain an understanding of the operation and possible applications of our circulators. For optimal utilization of all functions, we recommend that you thoroughly study this manual prior to beginning operation.

The JULABO Quality Management System

produced, and distributed according to the requirements of ISO 9001 and ISO 14001. Certificate Registration No. 01 100044846

Unpacking and inspecting

Unpack the circulator and accessories and inspect them for possible transport damage. Damage should be reported to the responsible carrier, railway, or postal authority, and a damage report should be requested. These instructions must be followed fully for us to guarantee our full support of your claim for protecting against loss from concealed damage. The form required for filing such a claim will be provided by the carrier.

Printed in Germany Changes without prior notification reserved

Important: keep operation manual for future use

1.953.2830-V3 02/16

TABLE OF CONTENTS

Operating manual ................................................................................................................ 5

1. Intended use ................................................................................................................. 5

1.1. Description ............................................................................................................... 5

2. Operator responsibility – Safety recommendations ....................................................... 6

2.1. Disposal ................................................................................................................... 8

2.2. Technical specifications ........................................................................................... 9

2.3. Mains power connections ....................................................................................... 15

2.4. Cooling water connection ....................................................................................... 17

Operating instructions ....................................................................................................... 18

3. Safety notes for the user ............................................................................................. 18

3.1. Explanation of safety notes .................................................................................... 18

3.2. Explanation of other notes ...................................................................................... 18

3.3. Safety recommendations ........................................................................................ 19

4. Operating controls and functional elements ................................................................ 21

5. Preparations ............................................................................................................... 25

5.1. Installation .............................................................................................................. 25

5.2. Bath fluids .............................................................................................................. 26

5.3. Temperature application to external systems ......................................................... 27

5.3.1. Tubing ............................................................................................................... 29

5.4. Filling / draining

...................................................................................................... 30

6. Operating procedures ................................................................................................. 31

6.1. Power connection ................................................................................................... 31

6.2. Switching on / Selecting the language .................................................................... 31

6.2.1. Switching on the circulator ................................................................................. 31

6.2.2. Switching on the cooling machine ...................................................................... 32

6.3. Start - Stop ............................................................................................................. 32

Setting of temperatures ................................................................................. 33

Safety installations, warning functions ........................................................... 33

8.0.1. Early warning system, low level protection ......................................................... 37

Menu functions .............................................................................................. 38

9.1. Start of a program .................................................................................................. 40

9.1.1. Status at the end of a program .......................................................................... 42

9.1.2. Indication after successful start .......................................................................... 42

9.1.3. Editing after Start ............................................................................................... 43

9.1.4. Interrupting a program ....................................................................................... 43

9.1.5. Interruption after a power failure ........................................................................ 44

9.1.6. Termination of a program................................................................................... 44

9.2. Program administration, creation ............................................................................ 45

9.3. Setting the pump pressure ..................................................................................... 49

9.4. Configuration .......................................................................................................... 50

9.4.1. Remote control via the serial interface ............................................................... 53

9.4.2. Keypad control or setpoint setting via the analog input ...................................... 53

9.4.3. Autostart ............................................................................................................ 54

9.4.4. Off-Mode ........................................................................................................... 54

9.4.5. ActVar - actuating variable ................................................................................. 55

9.4.6. Setting of clock and date .................................................................................... 56

9.4.7. Language ........................................................................................................... 56

9.4.8. Unit ..................................................................................................................... 56

9.4.9. Program type ...................................................................................................... 56

9.4.10. Reset ............................................................................................................. 56

9.5. Control .................................................................................................................... 57

9.5.1. Control internal / external ................................................................................... 59

9.5.2. Selftuning ........................................................................................................... 60

9.5.3. Dynamik intern ................................................................................................... 60

9.5.4. CoSpeed - extern ............................................................................................... 61

9.5.5. Control parameters – internal/external ................................................................ 61

9.6. Serial Interface ........................................................................................................ 63

9.7. ATC Absolute Temperature Calibration, 3-point calibration ..................................... 64

9.7.1. ATC Fühler - intern / extern ................................................................................ 67

9.7.2. ATC Status - yes / no ......................................................................................... 67

9.7.3. Type 1 -/ 2 -/ 3 point .......................................................................................... 67

9.7.4. Example: 3-point calibration for internal control ................................................. 68

9.8. Limits ...................................................................................................................... 70

9.8.1. Limits for internal control and external control.....................................................

9.8.2. Limits for external control.................................................................................... 72

9.9. Analog inputs/outputs ............................................................................................. 73

9.9.1. Control connector ............................................................................................... 77

9.9.2. Outputs of the connector - REG+E-PROG .......................................................... 77

9.9.3. Input of the connector - REG+E-PROG .............................................................. 78

9.9.4. External Stand-by input ...................................................................................... 80

9.9.5. Alarm-output ....................................................................................................... 81

10. Troubleshooting guide / Error messages ..................................................................... 82

11. Electrical connections .................................................................................................. 85

12. Remote control ............................................................................................................ 88

12.1. Setup for remote control .......................................................................................... 88

12.2. Communication with a PC or a superordinated data system ................................... 88

12.3. List of commands .................................................................................................... 89

12.4. Status messages .................................................................................................... 92

12.5. Error messages....................................................................................................... 92

13. JULABO Service – Online remote diagnosis ............................................................... 94

14. Installation of electronic module with analog connectors ............................................. 95

15. Cleaning / repairing the unit ......................................................................................... 95

Anhang: HST Zusatzheizer und HSP Zusatzpumpe .......................................................... 97

HST booster heater ..................................................................................................... 98

16.

16.1. Excess temperature protection on the HST booster heater ..................................... 99

16.2. Technical specifications - HST booster heater: ....................................................... 99

17. HSP booster pump .................................................................................................... 100

17.1. Pump connection with HSP booster pump ............................................................ 101

17.2. Technical specifications - HSP booster pump ....................................................... 101

18. WARRANTY PROVISIONS ....................................................................................... 102

Operating manual

JULABO circulators are not suitable for direct temperature control of foods, semi-

medium (bath fluid).

ICC

TCF

ATC

RS232 RS485

Pt100

PUMP

SMART

applications.

1. Intended use

JULABO circulators have been designed to control the temperature of specific fluids in a bath tank. The units feature pump connections for temperature control of external systems (loop circuit).

luxury foods and tobacco, or pharmaceutical and medical products. Direct temperature control means unprotected contact of the object with the bath

1.1. Description

 The circulators are operated via the splash-proof keypad. The implemented

microprocessor technology allows to set and to store different values that can be indicated on the VFD COMFORT-DISPLAY and LCD DIALOG-DISPLAY. Three menu keys facilitate adjusting setpoints, warning and safety functions and menu functions.

 The integrated programmer allows storing and running temperature and time-

dependent processes.

 The control electronics including “ICC - Intelligent Cascade Control“ automatically

adapts the heat supplied to the thermal requirements of the bath.

 The TCF - Temperature Control Features allow the user to have access to all

important temperature control parameters. This means: Full control on the control mode and the chance to manually adjust or adapt control to the specific application.

 Absolute Temperature Calibration (ATC3) provides high temperature stability in the

bath. With the 3-point calibration an offset is adjusted at three temperatures to ensure an accurate temperature pattern at the selected spot in the bath over the full temperature range.

 Electrical connections:

The serial interface, switchable from RS232 to RS485, allows modern process technology without additional interface. Connection for Pt100 external sensor for external temperature measurement and control. Alarm output for external alarm message or control of JULABO refrigerating baths or solenoid valve (cooling water). The electronic module (option) provides 3 further analog connections (alarm input, standby input, recorder output, programmer input).

 The excess temperature protection conforming to IEC 61010-2-010 is a safety

installation independent from the control circuit. This protection can be indicated and set on the LCD DIALOG-DISPLAY.

 The early warning system for low level signals that bath fluid needs to be refilled

before the low level protection conforming to IEC 61010-2-010 causes a complete shut-down of the main functional elements.

 Intelligent pump system: The pump capacity (electronically adjustable via the motor

speed) enables to adapt to varying conditions for internal and external temperature

Operator responsibility – Safety recommendations

2. Operator responsibility – Safety recommendations

The products of JULABO ensure safe operation when installed, operated, and maintained according to common safety regulations. This section explains the potential dangers that may arise when operating the circulator and also specifies the most important safety precautions to preclude these dangers as far as possible.

 The operator is responsible for the qualification of the personnel operating the units.  The personnel operating the units should be regularly instructed about the dangers involved with

their job activities as well as measures to avert these dangers.

 Make sure all persons tasked with operating, installing, and maintaining the unit have read and

understand the safety information and operating instructions.

 When using hazardous materials or materials that could become hazardous, the circulator may be

operated only by persons who are absolutely familiar with these materials and the circulator. These persons must be fully aware of possible risks.

If you have any questions concerning the operation of your unit or the information in this manual, please contact us!

Contact

Safety instructions for the operator:

 You have received a product designed for industrial use. Nevertheless, avoid strikes to the

housing, vibrations, damage to the operating-element panel (keypad, display), and contamination.

 Make sure the product is checked for proper condition regularly (depending on the conditions of

use). Regularly check (at least every 2 years) the proper condition of the mandatory, warning, prohibition and safety labels.

 Make sure that the mains power supply has low impedance to avoid any negative effects on

instruments being operated on the same mains.

 This unit is designed for operation in a controlled electromagnetic environment. This means that

transmitting devices (e.g., cellular phones) should not be used in the immediate vicinity. Magnetic radiation may affect other devices with components sensitive to magnetic fields (e.g., monitors). We recommend maintaining a minimum distance of 1 m.

 Permissible ambient temperature: max. 40 °C, min. 5 °C.  Permissible relative humidity: 50% (40 °C).  Do not store the unit in an aggressive atmosphere.  Protect the unit from contamination.  Do not expose the unit to sunlight.

JULABO USA, Inc. 884 Marcon Boulevard Allentown, PA 18109

Phone: +1(610) 231-0250 Fax: +1(610) 231-0260 info.us@julabo.com www.julabo.com

Appropriate operation

Only qualified personnel is authorized to perform configuration, installation, maintenance and repairs of the circulator. Routine operation can also be carried out by untrained personnel who should however be instructed by trained personnel.

Use:

The bath can be filled with flammable materials. Fire hazard! There might be chemical dangers depending on the bath medium used. Observe all warnings for the used materials (bath fluids) and the respective instructions (safety data sheets). Insufficient ventilation may result in the formation of explosive mixtures. Only use the unit in well ventilated areas.

Only use recommended materials (bath fluids). Only use non-acid and non corroding materials.

When using hazardous materials or materials that could become hazardous, the operator must affix the enclosed safety labels to the front of the unit so they are highly

visible:

If this unit is intended for use within the United States of America, all 3 warning labels must be affixed to the housing of the unit prior to use. Directions for the positioning of the individual warning labels are enclosed with the warning labels included in the delivery. Warning labels must be easily visible to users.

Warning label W00: Colors: yellow, black Danger area. Attention! Observe instructions. (operating manual, safety data sheet)

Mandatory label M018: Colors: blue, white Carefully read the user information prior to beginning operation.

Scope: EU

Semi S1-0701 Table A1-2 #9 Carefully read the user information prior to beginning operation.

Scope: USA, NAFTA

Warning label Proposition 65

Particular care and attention is necessary because of the wide operating range. There are thermal dangers: Burn, scald, hot steam, hot parts and surfaces that can be touched.

Warning label W26: Colors: yellow, black

Hot surface warning. (The label is put on by JULABO)

Observe the instructions in the manuals for instruments of a different make that you connect to the circulator, particularly the respective safety recommendations. Also observe the pin assignment of plugs and technical specifications of the products.

Operator responsibility – Safety recommendations

Contact an authorized waste management company in your country.

2.1. Disposal

The circulator contains a back-up battery that supplies voltage to memory chips when the unit is switched off. Do not dispose of the battery with household waste! Depending on battery regulations in your country, you might be obliged to give back used or defect batteries to gathering places. The product may be used with oil as bath fluid. These oils fully or partially consist of mineral oil or synthetic oil. For disposal, observe the instructions in the safety data sheets.

This unit contains refrigerants, which at this time are not considered harmful to the ozone layer. However, over the long operating period of the unit, disposal rules may change. Therefore, only qualified personnel should handle the disposal.

Disposal with household waste (unsorted waste) or similar collections of municipal waste is not permitted!

air-cooled

water-cooled

working temperature range

Medium ethanol

3.0 2.8 1.6 0.65 0.1

(WxL)

2.2. Technical specifications

Ultra-Low Refrigerated Circulator

Working temperature range °C -60 ... 100

Special unit with extended

Temperature stability °C ±0.05

Cooling capacity

Cooling compressor 1-stage

Refrigerant R404A

Cooling water flow rate at 20 °C l/h approx. 300

Overall dimensions (WxDxH) cm 59x76x116

Filling port dia. cm 7

Special unit with bath opening

FP52-SL

°C -60 ... 150

°C

cm 28x23

+20 0 -20 -40 -60

FPW52-SL

Bath depth cm 22

Filling volume liters 24

Weight kg 156 153

Ambient temperature °C 5 ... 40

Cooling water connection ------ G3/4“ male thread

Mains power connection V/ Hz 400 V/3PNPE/ 50 Hz 400 V/3PNPE/ 50 Hz

Current draw (at 400 V) A 21 20

Mains power connection V/ Hz 208 V/3PPE/ 60 Hz 208 V/3PPE/ 60 Hz

Current draw (at 208 V) A 25 24

Mains power connection V/ Hz 230 V/3PPE/ 50 Hz

Current draw (at 230 V) A 25 --

 Current draw: Refer to notice page 15

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.

Operator responsibility – Safety recommendations

air-cooled

water-cooled

working temperature range

Medium ethanol

5.2 4.1 2.2 0.7 0.13

(WxL)

Ultra-Low Refrigerated Circulator

Working temperature range °C -60 ... 100

Special unit with extended

Temperature stability °C ±0.05

Cooling capacity

Cooling compressor 1-stage

Refrigerant R404A

Cooling water flow rate at 20 °C l/h approx. 400

FP55-SL

°C -60 ... 150

°C

+20 0 -20 -40 -60

FPW55-SL

Overall dimensions (WxDxH) cm 85x76x116

Filling port dia. cm 7

Special unit with bath opening

Bath depth cm 23

Filling volume liters 27

Weight kg 180 146

Ambient temperature °C 5 ... 40

Cooling water connection ------ G3/4“ male thread

Mains power connection V/ Hz 400 V/3PNPE/ 50 Hz 400 V/3PNPE/ 50 Hz

Current draw (at 400 V) A 20 20

Mains power connection V/ Hz 208 -230V/3PPE/ 60 Hz 208-230 V/3PPE/ 60 Hz

Current draw (at 208 V / 230 V) A 28 28

cm 28x23

59x76x116

 Current draw: Refer to notice page 15

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.

air-cooled

water-cooled

working temperature range

Medium ethanol

1.8 1.7 1.6 1.35 0.75 0.15

(WxL)

Ultra-Low Refrigerated Circulator

Working temperature range °C -90 ... 100

Special unit with extended

Temperature stability °C ±0.05

Cooling capacity

Cooling compressor 2-stage

Refrigerant R404A / R23

Cooling water flow rate at 20 °C l/h ----- approx. 250

Overall dimensions (WxDxH) cm 59x76x116

Filling port dia. cm 7

Special unit with bath opening

FP90-SL

°C -90 ... 150

°C

cm 28x23

+20 0 -20 -40 -60 -80

FPW90-SL

Bath depth cm 20

Filling volume liters 22

Weight kg 195 195

Ambient temperature °C 5 ... 40

Cooling water connection ------ G3/4“ male thread

Mains power connection V/ Hz 400 V/3PNPE/ 50 Hz 400 V/3PNPE/ 50 Hz

Current draw (at 400 V) A 22 19

Mains power connection V/ Hz 208-230 V/3PPE/ 60 Hz 208-230 V/3PPE/ 60 Hz

Current draw (at 208 V / 230 V) A 29 26

Mains power connection V/ Hz 230 V/3PPE/ 50 Hz 230 V/3PPE/ 50 Hz

Current draw (at 230 V) A 29 26

 Current draw: Refer to notice page 15

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.

Operator responsibility – Safety recommendations

water-cooled

Medium ethanol

4.5 4.1 3.7 3.1 2.0 0.75

(WxL)

Ultra-Low Refrigerated Circulator

Working temperature range °C -91 ... 100

Temperature stability °C ±0.2

FPW91-SL

Cooling capacity

Cooling compressor 2-stage

Refrigerant R404A / R23

Cooling water flow rate at 20 °C l/h approx. 450

Overall dimensions (WxDxH) cm 85x76x116

Filling port dia. cm 7

Special unit with bath opening

Bath depth cm 20

Filling volume liters 22

Weight kg 216

Ambient temperature °C 5 ... 40

Cooling water connection G3/4“ male thread

Mains power connection V/ Hz 400 V/3PNPE/ 50 Hz

°C

cm 28x23

+20 0 -20 -40 -60 -80

Current draw (at 400 V) A 32

Mains power connection V/ Hz 230 V/3PPE/ 60 Hz

Current draw (at 230 V) A 32

 Current draw: Refer to notice page 15

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.

Temperature selection digital

via keypad indication on LCD DIALOG-DISPLAY (°C/°F)

remote control via PC indication on monitor

Temperature indication VFD COMFORT-DISPLAY (°C/°F)

Resolution °C 0.01

ATC3 INT / EXT °C ±3 / ±9

Temperature control ICC - Intelligent Cascade Control

Heater wattage (at 230 V) 3.0

Electronically adj. pump capacity stages 1 ... 4

Flow rate at 0 bar l/min 22 ... 26

Max. pressure at 0 liters bar 0.7

Max. suction at 0 liters bar 0.4

Pump connections, male mm M16x1

Electrical connections: See page 14

Ambient temperature °C 5 ... 40

Mains power connection V/ Hz 208 V - 230 V/ 50/60 Hz

Current draw (at 208 V / 230 V) A 13 / 14

All measurements have been carried out at: rated voltage and frequency ambient temperature: 20 °C Technical changes without prior notification reserved.

Operator responsibility – Safety recommendations

Caution:

Electrical connections:

External alarm device 24-0 V DC / max. 25 mA Computer interface RS232 or RS485 External Pt100 sensor

Optional for HL, SL (Order No. 8900100 Electronic module with analog connections) Programmer input -100 °C to 400 °C = 0 - 10 V or 0 - 20 mA or 4 - 20 mA Input for the signal of a flow meter or external manipulated variable Temperature recorder outputs 0 - 10 V (0 V = -100 °C, 10 V = 400 °C) 0 - 20 mA (0 mA = -100 °C, 20 mA = 400 °C) 4 - 20 mA (4 mA = -100 °C, 20 mA = 400 °C) Standby input for external emergency switch-off Alarm output for external alarm signal

Safety installations according to IEC 61010-2-010: Excess temperature protection adjustable from 0 °C ... 320 °C Low liquid level protection float switch Classification according to DIN 12876-1 class III

Supplementary safety installations Early warning system for low level float switch High temperature warning function optical + audible (in intervals) Low temperature warning function optical + audible (in intervals) Supervision of working sensor plausibility control Reciprocal sensor monitoring between working and safety sensors difference >35 K Alarm message optical + audible (permanent) Warning message optical + audible (in intervals)

Environmental conditions according to IEC 61 010-1: Use indoors only. Altitude up to 2000 m - normal zero. Ambient temperature: see Technical specifications Humidity: Max. relative humidity 80% for temperatures up to +31 °C, linear decrease down to 50% relative humidity at a temperature of +40 °C Max. mains voltage fluctuations of ±10% are permissible. Protection class according to IEC 60 529 IP21 The unit corresponds to Class I Overvoltage category II Pollution degree 2

The unit is not suitable for use in explosive environment

EMC requirements according to EN 61326-1 This unit is an ISM device classified in Group 1 (using high frequency for internal purposes), Class A (industrial and commercial range).



Note concerning current consumption: Mains power connection 3PNPE and 3PPE

shares (2x3 kW) on the two other phases..

Model Mains power connection 3PNPE

2.3. Mains power connections

The indicated value of current consumption is the maximum useful current of the phase, which also feeds the SL circulator with a 3 kW heater. If the ultra-low refrigerated circulator is operated with the HST additional heater, the 6 kW heating capacity is divided in equal

FP52-SL 400 V/3PNPE/50 Hz FPW52-SL 400 V/3PNPE/50 Hz

FP55-SL 400 V/3PNPE/50 Hz FPW55-SL 400 V/3PNPE/50 Hz

FP90-SL 400 V/3PNPE/50 Hz FPW90-SL 400 V/3PNPE/50 Hz

FPW91-SL 400 V/3PNPE/50 Hz

Operator responsibility – Safety recommendations

Model Mains power connection 3PPE

FP52-SL 230 V/3PPE/50 Hz

FP52-SL 208 V/3PPE/60 Hz FPW52-SL 208 V/3PPE/60 Hz

FP55-SL 208 V/3PPE/60 Hz FPW55-SL 208 V/3PPE/60 Hz

FP90-SL 230 V/3PPE/50 Hz FPW90-SL 230 V/3PPE/50 Hz

FP90-SL 230 V/3PPE/60 Hz FPW90-SL 230 V/3PPE/60 Hz

Model Mains power connection 3PPE

FPW91-SL 230 V/3PPE/60 Hz

Attention:

Pay attention to the rotary field direction of the compressor engines! The rotating field direction is to the right.

Note concerning current consumption:

Each, the SL circulator, the additional HST heater and the cooling unit FPW91 have their own supply mains.

Notice: Cooling water circuit

location where the unit is operated.

• Avoid putrid water.

7.5 to 9.0

Sulfate [SO4 2- ]

< 100 ppm

Hydrocarbonate [HCO 3-]/sulfate [SO4 2-]

> 1 ppm

Hardness [Ca 2+, Mg 2+]/[HCO 3-]

> 0.5 °dH

Alkalinity

60 ppm < [HCO 3-] < 300 ppm

Conductivity

< 500 μS/cm

Chloride (Cl -)

< 50 ppm

Phosphate (PO4 3-)

< 2 ppm

Ammonia (NH3)

< 0.5 ppm

Free chlorine

< 0.5 ppm

Trivalent iron ions (Fe 3+)

< 0.5 ppm

Manganese ions (Mn 2+)

< 0.05 ppm

Carbon dioxide (CO2)

< 10 ppm

Hydrogen sulfide (H2S)

< 50 ppm

Content of oxygen

< 0.1 ppm

Algae growth

impermissible

Suspended solids

impermissible

2.4. Cooling water connection

Cooling water pressure (IN/OUT) max. 6 bar Pressure difference (IN - OUT) 3.5 to 6 bar Cooling water temperature < 20 °C

Risk of oil leaking from the refrigeration system (compressor) of the recirculating cooler into the cooling water in case of a fault in the cooling water circuit!

Observe the laws and regulations of the water distribution company valid in the

Notice:

Danger of corrosion of heat exchanger due to unsuitable quality of cooling water.

• Due to its high content of lime, hard water is not suitable for cooling and causes scale in the heat exchanger.

• Ferrous water or water containing ferrous particles will cause formation of rust even in heat exchangers made of stainless steel.

• Chlorinated water will cause pitting corrosion in heat exchangers made of stainless steel.

• Due to their corrosive characteristics, distilled water and deionized water are unsuitable and will cause corrosion of the bath.

• Due to its corrosive characteristics, sea water is not suitable.

• Due to its microbiological (bacterial) components, which settle in the heat

exchanger, untreated and unpurified river water and water from cooling towers is unsuitable.

• Avoid particulate matter in cooling water.

Recommended quality of cooling water:

Operating instructions

In addition to the safety warnings listed, warnings are posted throughout the operating

Warning:

Caution:

Notice:

in its surroundings can be damaged.

Note! Draws attention to something special.

Important! Indicates usage tips and other useful information.

This icon is used in the operating instructions to indicate which have to be set or confirmed.

Operating instructions

3. Safety notes for the user

3.1. Explanation of safety notes

manual. These warnings are designated by an exclamation mark inside an equilateral triangle. “Warning of a dangerous situation (Attention! Please follow the documentation).” The danger is classified using a signal word. Read and follow these important instructions for averting dangers.

Describes a possibly highly dangerous situation. If these instructions are not followed, serious injury and danger to life could result.

Describes a possibly dangerous situation. If this is not avoided, slight or minor injuries could result. A warning of possible property damage may also be contained in the text.

Describes a possibly harmful situation. If this is not avoided, the product or anything

3.2. Explanation of other notes

flashing values or parameters

these parts.

3.3. Safety recommendations

Follow the safety instructions to avoid personal injury and property damage. Also, the valid safety instructions for workplaces must be followed.

• Only connect the unit to a power socket with an earthing contact (PE – protective

earth)!

• The power supply plug serves as a safe disconnecting device from the line and

must always be easily accessible.

• Place the unit on an even surface on a base made of non-flammable material.

• Do not stay in the area below the unit.

• Make sure you read and understand all instructions and safety precautions listed in

this manual before installing or operating your unit.

• Set the excess temperature safety installation at least 25 °C below the fire point of

the bath fluid.

• Observe the limited working temperature range when using plastic bath tanks.

• Never operate the unit without bath fluid in the bath.

• Pay attention to the thermal expansion of bath oil during heating to avoid

overflowing of the fluid.

• Prevent water from entering the hot bath oil.

• Do not drain the bath fluid while it is hot!

Check the temperature of the bath fluid prior to draining (e.g., by switching the unit on for a short moment).

• Use suitable connecting tubing.

• Avoid sharp bends in the tubing, and maintain a sufficient distance from

surrounding walls.

• Make sure that the tubing is securely attached.

• Regularly check the tubing for material defects (e.g., for cracks).

• Never operate damaged or leaking units.

• Always turn off the unit and disconnect the mains cable from the power source

before performing any service or maintenance procedures, or before moving the unit.

• Always turn off the unit and disconnect the mains cable from the power source

before cleaning the unit.

• Always empty the bath before moving the unit.

• Transport the unit with care.

• Sudden jolts or drops may cause damage in the interior of the unit.

• Observe all warning labels.

• Never remove warning labels.

• Never operate units with damaged mains power cables.

• Repairs are to be carried out only by qualified service personnel.

 Some parts of the bath tank and the pump connections may become extremely hot

during continuous operation. Therefore, exercise particular caution when touching

Safety notes for the user

Caution:

determine the method of decontamination.

example.

defects or other reproductive harm.

The temperature controlling i.e. of fluids in a reactor constitutes normal circulator practice.

We do not know which substances are contained within these vessels. Many substances are:

• inflammable, easily ignited or explosive

• hazardous to health

• environmentally unsafe

i.e.: dangerous

The user alone is responsible for the handling of these substances!

The following questions shall help to recognize possible dangers and to reduce the risks to a minimum.

• Are all tubes and electrical cables connected and installed? Note: sharp edges, hot surfaces in operation, moving machine parts, etc.

• Do dangerous steams or gases arise when heating? Is an exhaust needed when working?

• What to do when a dangerous substance was spilled on or in the unit? Before starting to work, obtain information concerning the substance and

Notice: Check the safety installations at least twice a year!

• Excess temperature protection according to IEC 61010-2-010. With a screwdriver turn back the adjustable excess temperature protection until the shut-down point (actual temperature).

• Low level protection according to IEC 61010-2-010. To check the function of the float, it can be manually lowered with a screwdriver for

WARNING

This product contains chemicals known to the state of California to cause cancer, birth

4. Operating controls and functional elements

Mains power switch, illuminated for circulator

PS Capacity in % - with manipulated variable set to >serial<* or

Front view Rear view

Mains power switch, illuminated for cooling machine

VFD COMFORT-DISPLAY

Header: Control indicators Line 1: Actual value internal or external

The display is depending on the selected control mode in the menu > Control < (internal or external).

Line 2: Working temp. setpoint, constantly S xxx.xx

Line 3: Actual value (E = external or I = internal)

Alternating with the display in line 1

Use the keys PI Capacity in % - with manipulated variable set to >control<*

to indicate further values in line 3

Operating controls and functional elements

2.1

2.2

LCD DIALOG-DISPLAY

Navigation aid in MENU - Window

>eprog<* H Heater capacity in Watts U Mains voltage Volts F Flow rate in liters/minute (providing EPROG input set to >Flow rate<)

2.3

*refer to >MENU / CONFIGIGURATIO> page 40

Control indicators in the header: Heating / Cooling / Alarm /

emote control

Control indicators in the header: Temperature indication Internal or External actual value Temperature indication in °C or °F

Display for the adjusted pump pressure stage in the -OFF- mode. Display for the effective pump pressure stage (rotation speed) after start. Four stages, adjustable via the

Line 1: Setpoint and origin of setpoint programming

(Key / RS232 or RS485 / ext. Pt100 / EProg)

Line 2: Actual value - internal or external,

identical to line 1 of the VFD-COMFORT-DISPLAY

Line 3: Heating capacity in %.

Line 4: Control type: internal / external

button, in the menu >PUMP<.

Keys / : Selection of menu items / parameters

- Setting in line 3:

Actual value / parameter

Orientation aid in MENU - Window

Line 1 - name with allocation to key

2 Submenu Level 2 Example: CONFIGURATION

3 Submenu Level 3

Safety values

T – Setpoint

1 Main menu Level 1

A beep signals the end of setting

The above graph “front side” shows an example for standard display.

Keypad 2

Numeric keypad: numerals 0 to 9

Keypad 1 Navigation keys

4.1

4.2

4.3

1. Key: >OK< Start / Stop (pump / heater )

2. >OK< in the menu Menu item / select submenu for setting Save set value Save selected parameter

After the actions Start, Stop and change from VFD Display to standard display the key

is locked for a short time.

1. Key: >Return< Stop (pump / heater) Special display on VFD Display leave line 3.

2. >Return< in the menu one menu level down Correction function for parameters or values (prior to OK)

immediately back to standard display

- icon for „keep key pressed down“.

1. Key: >Up / Down <temperature – increase/decrease setpoint Push key quickly for single steps, Keep key pressed for fast change.

2. >Up/Down< in the menu selection of menu items / parameters

4.4

4.5

4.6

Menu keys

Key: start the menu > warning and safety values<

Key: start the menu >temperature setpoints<

Key: display of MENU structure

minus / decimal point

Backspace key on LCD DIALOG-DISPLAY.

Adjustable excess temperature protection according to IEC 61010-2-010

Operating controls and functional elements

ext Pt100

Socket for external measurement and control sensor 8

9 9a

Control cable of JULABO refrigerated circulator Socket: output for alarm messages

The circulator automatically recognizes the connected electronic module.

ALARM

Alarm output (for external alarm signal)

STAND-BY

REG+E-PROG

Connector for supplementary pump or solenoid valve

No control voltage in the -OFF- condition

14 Connector solenoid valve

2. Configurable for controlled counter cooling via solenoid valve

Fuses (for connectors 13, 14), T1.25A

16 17a

Mains power cable with plug for circulator Mains power cable with plug cooling machine

Built-in mains outlet for connection of circulator (230 V / 16 A) Not on - FPW91-SL - 230 V/3PPE/60 Hz

Drain screw with drain connection

21 22

23 Castor without brake (at the back)

and Special units with bath opening

or external setpoint programming

Interface RS232 / RS485: remote control via personal computer

SERIAL

Socket:

Option: Electronic module Order No. 8 900 100

Standby input (for external emergency switch-off)

Programmer input and temperature recorder output

17b

230 V / max. 1.25 A

1. No control voltage in the -OFF- condition

Mains fuses, T16A

Venting grid, removable

Pump connections suction pump pressure pump

Castor with brake (at the front)

Only water cooled models. Cooling water connectors. G 3/4"

25 Built-in mains outlet for connection of HST booster heater

Not on - FPW91-SL - 230 V/3PPE/60 Hz

5. Preparations

HST

HSP

19a

19b

SL Circulator

Bath opening 28x23

Important: For cooling water, see page 17

5.1. Installation

Top view:

Special unit

• Place the unit on an even surface on a pad made of non-flammable material. Using the castors move the unit to the intended location. For better stability, apply the holding breaks on the front casters.

Upgradable with supplementary pump - HSP see page 100

Upgradable with supplementary heater - HST see page 98

• Cooling machine, pump motor and electronics produce intrinsic heat that is dissipated via the venting openings! Never cover these openings!

• Keep at least 20 cm of open space on the front and rear venting grids.

• The place of installation should be large enough and provide sufficient

air ventilation to ensure the room does not warm up excessively because of the heat the instrument rejects to the environment. (Max. permissible ambient temperature: 40 °C). For a fault (leakage) in the refrigeration system, the standard EN 378 prescribes a certain room space to be available for each kg of refrigerant. The refrigerant quantity is specified on the type plate.

> For 0.52 kg of refrigerant R404A, 1 m > For 0.68 kg of refrigerant R23, 1 m

of space is required.

• Do not set up the unit in the immediate vicinity of heat sources and do not expose to sun light

• Before operating the unit after transport, wait about one hour after setting it up. This will allow any oil that has accumulated laterally during transport to flow back down thus ensuring maximum cooling performance of the compressor.

Only for water-cooled models: Ensure circulation of cooling water by connecting the tubing to the cooling water inlet and outlet at the rear of the refrigerated circulator.

G 3/4"

Cooling water connections: G 3/4"

Preparations

Caution:

corrosion in the bath, even in stainless steel.

Bath fluid

Temperature range

soft/decalcified water

5 °C to 80 °C

mixture water/glycol, mixture 1:1

-20°C to 50°C

Description

Order Number

10 liters

8 940 124

8 940 104

8 940 106

5 liters

8 940 125

8 940 105

8 940 107

Temperature range

°C

-30 ... 80

-80 ... 55

-50 ...105

Flash point

°C

124

Fire point

°C

142

Color

light yellow

clear

Description

H10

H20S

Order Number

10 liters

8 940 114

8 940 108

5 liters

8 940 115

8 940 109

Temperature range

°C

-20 ... 180

0 ... 220

Flash point

°C

190

230

Fire point

°C

216

274

Color

clear

light brown

5.2. Bath fluids

Carefully read the safety data sheet of the bath fluid used, particularly with regard to the fire point! If a bath fluid with a fire point of ≤65 °C is used, only supervised operation is possible.

Water: The quality of water depends on local conditions.

• Due to the high concentration of lime, hard water is not suitable for temperature control because it leads to calcification in the bath.

• Ferrous water can cause corrosion - even on stainless steel.

• Chloric water can cause pitting corrosion.

• Distilled and deionized water is unsuitable. Their special properties cause

Recommended bath fluids:

JULABO bath fluids

JULABO

Thermal

ATTENTION: The maximum permissible viscosity is 70 mm

See website for list of recommended bath fluids.

/s.

• No liability for use of other bath fluids!

with the cap nut.

T16A

T1.25A

ext

Pt100

SERIAL

ALARM

REG+ E-PROG

STAND-BY

Caution:

Fire or other dangers when using bath fluids that are not recommended:

Use only nonacidic and noncorrosive bath fluids.

JULABO assumes no liability for damage caused by the selection of an unsuitable bath liquid. Unsuitable bath fluids are fluids which, e.g.,

• are highly viscous (much higher than recommended at the respective working temperature)

• have a low viscosity and have creep characteristics

• have corrosive characteristics or

• tend to crack.

5.3. Temperature application to external systems

Caution: Securely attach all tubing to prevent slipping.

If the circulator is operated without external system, close the pump connector (22)

Temperature application to external, closed systems

The circulator is used for temperature application to external, closed systems (loop circuit) with simultaneous temperature application in the circulator bath.

Model combination without HSP booster pump

Pump connection:

• Unscrew the M16x1 collar nuts on the pump connectors with a 19 mm (3/4“) wrench and remove the sealing disks. Using the collar nuts, screw on the tubing connection fittings (for tubing 8 mm or 12 mm in diameter) delivered with the unit and tighten firmly. (Pressure pump: 22, suction pump: 21)

• Push on the tubing, and secure with tube clamps.

• Attach the tubing to the connectors of the external closed

system, e.g., an instrument with a pressure-resistant temperature jacket or a temperature coil, and fasten with tube clamps to prevent slipping.

Preparations

H = Height adjustment

T16A

T1.25A

ext

Pt100

SERIAL

ALARM

REG+ E-PROG

STAND-BY

Temperature application to external, open systems

The circulator is equipped with both a pressure and suction pump for external temperature application in open systems.

Differing flow rates of the pressure and suction pumps should be compensated. To maintain a constant liquid level, the JULABO „D+S“ Level Adapter is recommended for the external bath tank. The flow rate of the pressure pump will be then regulated by a built-in float device. The liquid level may be changed by a height adjustment on the „D+S“ Level Adapter.

Accessory: „D+S“ Level Adapter Order No. 8 970 410

Important:

 The liquid level should be equal in the internal and external

S = Suction pump connection D = Pressure pump connection K = Float

baths (absolute height).

 If you take out samples (for example Erlenmeyer flasks) from

the external bath, turn the circulator off with the Start/Stop key.

Backflow safety device

(see page 73)

If the liquid levels in the circulator bath and the external system are at different heights, overflowing must be prevented after the power has been turned off.

Flood hazard!

For this reason, solenoid valves for loop circuit or shut-off valves can be integrated in the loop circuit.

 Connect the valve to the connector (13).  If socket (14) is used:

In menu >Inputs/Outputs< set the menu item >SV-Out< to >Backflow<.

Order No. Description 8 980 701 Set of solenoid valves for loop circuit up to +100 °C

8 970 456 Shut-off valve (suitable up to +90 °C) 8 970 457 Shut-off valve (suitable up to +200 °C)

Order No. Length

Temperature range

8930008 1 m

CR® tubing 8 mm inner dia.

-20 °C to 120 °C

8930012 1 m

CR® tubing 12 mm inner dia.

-20 °C to 120 °C

8930108 1 m

Viton tubing 8 mm inner dia.

-50 °C to 200 °C

8930112 1 m

Viton tubing 12 mm inner dia.

-50 °C to 200 °C

8930410 1 m

Insulation for tubing 8 mm inner dia.

-50 °C to 100 °C

8930412 1 m

Insulation for tubing 12 mm inner dia.

-50 °C to 100 °C

8 930 209 0.5 m

8 930 214 3.0 m

Metal tubing, triple insulated, M16x1

-100 °C to +350 °C

8 930 220 0.5 m

8 930 223 3.0 m

Metal tubing, insulated, M16x1

-50 °C to +200 °C

Warning: Tubing:

• Preventive maintenance: Replace the tubing from time to time.

5.3.1. Tubing

Recommended tubing:

8 930 210 1.0 m 8 930 211 1.5 m

8 930 221 1.0 m 8 930 222 1.5 m

At high working temperatures the tubing used for temperature application and cooling water supply represents a danger source. A damaged tubing line may cause hot bath fluid to be pumped out within a short time. This may result in:

• Burning of skin

• Difficulties in breathing due to hot atmosphere

Safety recommendations

• Employ suitable connecting tubing.

• Make sure that the tubing is securely attached.

• Avoid sharp bends in the tubing, and maintain a sufficient distance from

surrounding walls.

• Regularly check the tubing for material defects (e.g. for cracks).

Preparations

protection.

Wait for a while and open the drain tap to drain the water.

5.4. Filling / draining

Notice:

• Pay attention to the thermal expansion of bath oil during heating to avoid overflowing of the liquid.

• Do not drain the bath fluid while it is hot! Recommendation: Temperature range 5 °C to 40 °C Check the temperature of the bath fluid prior to draining (by switching the unit on for a short moment, for example).

• Store and dispose the used bath fluid according to the laws for environmental

Filling

Take care that no liquid enters the interior of the circulator. Remove the bath cover and, if necessary, use a funnel.

Observe the level indication (19b).

• Recommended maximum filling level with water as bath fluid: 30 mm below the tank rim

• Recommended maximum filling level with bath oils: 40 mm below the tank rim

Special unit with bath opening 28x23 cm

 After filling, immerse the samples in the bath, or place the

lid on the bath if the opening is not to be used.

 The circulator has an early warning system for low level

(see description on page 37) that may be triggered when changing samples in the bath.

Draining:

• The drain tap is located behind the venting grid on the front of the unit, which can be taken off by removing 4 screws.

• Slide a short piece of tube onto the drain connection and hold it into a container.

• Loosen the drain screw a few turns and drain the unit completely.

• Tighten the drain tap.

Penetration of ice flakes/water into bath oil

At working temperatures below 0 °C humidity from the atmosphere may penetrate into bath oil through condensation. This may subsequently result in the formation of ice flakes, preventing the pump from proper operation. For this reason, the bottom of the bath tank provides a groove sloping down towards the drain tap. Thus water having penetrated into the bath

oil gathers in the groove immediately behind the drain tap. Shut down the refrigerated circulator at a bath temperature of +10 °C.

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