Hanna Instruments HI 98360 User Manual

Instruction Manual
HI 9835 HI 98360
Auto Ranging
EC/TDS/NaCl/
Temperature Meters
www.hannainst.com
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Dear Customer, Thank you for choosing a Hanna Instruments product. Please read this instruction manual carefully before using the instruments. This manual will provide you with the necessary information for correct
use of the instruments, as well as a precise idea of their versatility. If you need additional technical information, do not hesitate to e-mail us
at tech@hannainst.com.
WARRANTYWARRANTY
WARRANTYWARRANTY
HI 9835 and HI 98360 are guaranteed for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions. Electrodes and probes are guaranteed for six months. This warranty is limited to repair or replacement free of charge. Damage due to accidents, misuse, tampering or lack of prescribed maintenance is not covered. If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of purchase, serial number and the nature of the problem. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization number from the Technical Service department and then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packed for complete protection.
TABLE OF CONTENTSTABLE OF CONTENTS
TABLE OF CONTENTS
TABLE OF CONTENTSTABLE OF CONTENTS
WARRANTY ........................................................................................................... 2
PRELIMINARY EXAMINATION ................................................................................. 3
GENERAL DESCRIPTION ......................................................................................... 3
FUNCTIONAL DESCRIPTION .................................................................................... 4
SPECIFICATIONS ................................................................................................... 6
OPERATIONAL GUIDE ............................................................................................. 8
AUTO-RANGING ..................................................................................................... 9
AutoEnd ............................................................................................................. 10
TEMPERATURE COMPENSATION .......................................................................... 10
EC/TDS CALIBRATION ........................................................................................... 12
CONDUCTIVITY VERSUS TEMPERATURE CHART ...................................................... 14
NaCl CALIBRATION .............................................................................................. 15
GOOD LABORATORY PRACTICE (GLP) ..................................................................... 16
SETUP ................................................................................................................ 18
LOGGING (HI 98360 only) .................................................................................... 20
TEMPERATURE CALIBRATION (for technical personnel only) .................................. 21
PC INTERFACE (HI 98360 only) ........................................................................... 23
BATTERIES REPLACEMENT .................................................................................... 28
LCD MESSAGE GUIDE ........................................................................................... 30
PROBE MAINTENANCE ........................................................................................ 31
TROUBLESHOOTING GUIDE .................................................................................. 32
ACCESSORIES ..................................................................................................... 33
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PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
PRELIMINARY EXAMINATION
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer or the nearest Hanna Customer Service Center.
Each instrument is supplied with:
HI 76309 Conductivity probe with 1 m cable (HI 9835)
HI 76309/1.5 Conductivity probe with 1.5 m cable (HI 98360)
• 3 x 1.5V AAA Batteries
• Instruction Manual
• Rugged Carrying Case
Note: Save all packing material until you are sure that the instrument
functions correctly. All defective items must be returned in the original packing with the supplied accessories.
GENERAL DESCRIPTIONGENERAL DESCRIPTION
GENERAL DESCRIPTION
GENERAL DESCRIPTIONGENERAL DESCRIPTION
HI 9835 and HI 98360 are state-of-the-art, handheld conductivity meters, designed to provide laboratory results and accuracy under harsh industrial conditions. These instruments are provided with a series of new diagnostic features and messages on the LCD which add an entirely new dimension to the measurement of EC, TDS and NaCl, by allowing the user to dramatically improve the reliability of the measurement. The autoranging feature of the EC and TDS ranges automatically sets the meter to the scale with the highest possible resolution. The Auto Endpoint feature automatically freezes the display when a stable reading is reached. The measurements are automatically (ATC) or manually (MTC) compensated for temperature. The temperature coefficient value is user selectable. It is possible to disable the temperature compensation and measure the absolute (uncompensated) conductivity. The HI 98360 also has a logging feature (up to 500 records) and allows data transfer to computer through the USB port. The Battery Error Preventing System (BEPS) detects when the batteries become too weak to ensure reliable measurements. The backlight feature is automatically disabled when batteries are getting low and a clear indication is displayed to warn the user of this condition. However, the meter continues to measure correctly even when the low battery indication is displayed. The meter automatically switches itself off when the batteries are too weak to support proper function. In addition, the meters allow the user to enter an ID code to uniquely identify the instrument.
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FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
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7
HI 98360
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FUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
HI 9835
1) Liquid Crystal Display (LCD).
2) Range key, to select EC/TDS/NaCl range. Setup key, to enter/exit SETUP mode.
3) On/Off key, to turn the instrument ON and OFF.
4) CAL key, to enter/exit calibration mode. GLP key, to display Good Laboratory Practice information.
5) 2nd key, to select second key function.
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6) key, to manually increase temperature or other parameters. ATC key, to select temperature compensation mode.
7) USB connector (HI 98360 only).
8) Battery compartment cap.
9) DIN connector for EC probe.
10) key, to manually decrease temperature or other parameters. RCL key, to enter/exit view logged data mode (HI 98360 only).
11) Log key, to store measured data (HI 98360 only). CFM key, to confirm different values.
12) AutoEnd key, to freeze first stable reading on the LCD. CLR key, to delete logged data (HI 98360 only).
13) Light key, to toggle display backlighting. Lock to freeze/unfreeze the current displayed range.
14) Secondary LCD.
15) Primary LCD.
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SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
(*)
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OPERATIONAL GUIDEOPERATIONAL GUIDE
OPERATIONAL GUIDE
OPERATIONAL GUIDEOPERATIONAL GUIDE
INITIAL PREPARATION
The instrument is supplied complete with batteries. In order to place the batteries inside the instrument follow the instructions from page 28. To prepare the instrument for use, connect the EC probe to the input socket on the top of the instrument. Turn the instrument ON by pressing On/Off. At start-up the display will show all the used segments for a few seconds (or while the button is held), followed by the percentage indication of the remaining battery life. During instrument startup the “ ” and “WAIT” tags will blink.
The meter is now ready to operate.
Submerse the probe into the solution to be tested. The sleeve holes must be completely submersed. Tap the probe repeatedly to remove any air bubbles that may be trapped inside the sleeve. If needed, press the Range key repeatedly until the desired range (EC, TDS, NaCl) is selected on the LCD. Allow for the reading to stabilize. The upper LCD displays the measure in the selected range while the temperature is displayed on the lower LCD. The auto-off feature turns the instrument off after a set period (default 20 minutes) with no button pressed to save battery life. To set another period or to disable this feature, see SETUP menu on page 18. The auto-off backlight feature turns the backlight off after a set period (default 1 min) with no buttons pressed. To set another period or to disable this feature, see SETUP menu on page 18.
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Notes: • If the reading is out of range, the full scale value will be
displayed blinking.
• If the reading is not stable, the instability indicator “ ” will be on.
• Make sure the meter is calibrated before taking measurements.
• If measurements are taken successively in different samples, it is recommended to rinse the probe thoroughly with deionized water before immersion in the samples. If possible rinse with sample also.
• To maximize battery life, the meter is automatically switched off after a set period of non-use. To reactivate the instrument press the On/Off key. This feature can be disabled (see SETUP section for details).
• TDS reading is obtained multiplying the EC reading by the TDS factor, which has a default value of 0.50. It is possible to change the TDS factor in the 0.40 to 0.80 (see SETUP section). Always set the reference temperature to 25°C when measuring TDS.
• When the use of an alternate function is requested, press the 2nd key.
BACKLIGHT FEATURE
The instrument is provided with a Backlight feature to enhance display readability in low light conditions. It can be easily toggled on and off through the keypad by pressing Light.
Note: The backlight automatically shuts off after a set time period to
save battery life (see SETUP for details, page 18).
If battery percentage is less than 20% the backlight can not be ON.
AUTO-RANGINGAUTO-RANGING
AUTO-RANGING
AUTO-RANGINGAUTO-RANGING
The EC and TDS scales are auto-ranging. The meter automatically sets the scale with the highest possible resolution. By pressing 2nd then Lock, the auto-ranging feature is disabled and the current range is frozen on the LCD. The “MEASURE” tag is displayed blinking. To restore the auto-ranging option press 2nd then Lock again.
Note: Auto-ranging is automatically restored if the Range or 2nd then
Lock keys are pressed, if the setup or calibration modes are
entered and if the meter is turned off and back on again.
• If 2nd then Lock was pressed to freeze the LCD range and the
reading goes out of range, the full-scale value of the frozen range will be displayed blinking.
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AA
utoEndutoEnd
A
utoEnd
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utoEndutoEnd
To freeze the first stable reading on the LCD press AutoEnd while the instrument is in measurement mode.
The ”HOLD” tag will be displayed blinking on the LCD until the reading is stabilized.
When the reading is stable, the “HOLD” tag stops blinking and the reading is frozen on the LCD.
Press AutoEnd again to return to normal measurement mode. Note: • Pressing Range the instrument will skip to the displayed
range, without leaving AutoEnd mode. The Log key also holds AutoEnd mode.
• Pressing 2nd then Setup, GLP or RCL, the instrument leaves AutoEnd mode and performs the selected function.
TEMPERATURE COMPENSATIONTEMPERATURE COMPENSATION
TEMPERATURE COMPENSATION
TEMPERATURE COMPENSATIONTEMPERATURE COMPENSATION
The EC reading is affected by temperature and changes in ion concentration. To measure only one variable, conductivity measurements are normally
compensated to a fixed temperature. This reference temperature is configured in SETUP parameter rEF. See page 18.
Three options of temperature compensation are available: Automatic (Atc): The probe has a built-in temperature sensor; the
value of the temperature is used to automatically compensate the EC/TDS measurement to a reference temperature. This is the default option.
Manual (Mtc): The temperature value, shown on the lower LCD, can be manually set by the user with the up and down arrow keys to the solution temperature. The “ºC” or “ºF” symbol blinks when this option is active. The instrument compensates the conductivity measured at this temperature to the reference temperature.
No Compensation (NoTC): The temperature reading shown on the lower LCD is not taken into account. The reading displayed on the upper LCD is the absolute EC or TDS value without temperature compensation applied. The measurement changes due to temperature and ion concentration. The second “ºC” or “ºF” symbol blinks when this option is active.
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To select the desired option press the 2nd then ATC key. The option tag will blink for a few seconds then remain active on the LCD.
If temperature compensation is active, measurements are compensated using a default temperature coefficient of 1.90 %/°C to the 25°C reference temperature. This is a natural water tc value.
It is possible to view or select a different temperature coefficient (TC) in the
0.00 to 6.00 %/°C range by entering the setup mode and selecting the “tc” item (see SETUP section for details).
Notes: The default compensation mode is Atc.
If no temperature probe is detected, Atc mode can not be
selected and the instrument displays “----” on the secondary LCD.
• If the temperature reading is out of the -20.0 – 120.0 ºC range and Atc option is selected, the “ºC” tag will blink and the closest interval limit will be displayed.
• By pressing the ARROW keys the displayed temperature value is changed. This value is used to compensate the EC/TDS reading.
Temperature compensation is performed by means of the following formula:
Compensated conductivity =
where T is the measured temperature and T
Measured conductivity
1+TC25(T-T
)
ref
is the reference
ref
temperature (20 or 25°C). Note that if a solution has a temperature coefficient TC with T
=25°C,
ref
when changing the reference temperature to 20°C, the temperature coefficient must be manually adjusted by the user according to the following formula:
TC20=
TC
25
1-TC25/20
For example, TC20=2.10%/°C when TC25=1.90%/°C.
Always set reference temperature to 25°C when measuring TDS.
TDS MEASUREMENTS
Press the Range key while in EC range. The instrument will switch to TDS measuring range. The TDS reading will be displayed on the primary LCD and the temperature reading on the secondary LCD.
• If the reading is out of range, the full-scale value (100.0 for MTC/ATC
mode or 400.0 for uncompensated TDS) will be displayed blinking.
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