Hanna Instruments HI 9829 User Manual

Instruction Manual
HI 9829
Multiparameter Meter
With available GPS,
logging probe, turbidity
and ion measurements
www.hannainst.com
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Dear CustomerDear Customer
Dear Customer,
Dear CustomerDear Customer
Thank you for choosing a HANNA instruments
®
product. Please read this instruction manual carefully before using the instrument. It will provide you with the necessary information for correct use of the instrument, as well as it’s versatility. If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.comtech@hannainst.com
tech@hannainst.com or visit our website www.hannainst.com for our
tech@hannainst.comtech@hannainst.com worldwide contact list. This instrument is in compliance with the
directives.
HANNA instruments® reserves the right to modify the design,
construction and appearance of its products without advance notice.
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TABLE OF CONTENTS
CHAPTER 1- INTRODUCTION
1.1 Preliminary Examination ................................................................................. 6
1.2 Model Identification ....................................................................................... 6
1.3 General Description....................................................................................... 6
1.4 Display and Keypad Description ...................................................................... 8
CHAPTER 2 - QUICK START
2.1 Sensor and Probe Installation .......................................................................... 9
2.2 Basic Operation ........................................................................................... 10
2.3 Help Function ..............................................................................................11
CHAPTER 3 - SPECIFICATIONS
3.1 System Specifications ..................................................................................... 12
3.2 Probe Specifications ...................................................................................... 17
3.3 Sensor Specifications ..................................................................................... 18
CHAPTER 4 - PROBE INSTALLATION
4.1 Sensor Descriptions....................................................................................... 19
4.2 Sensor Preparation/Activation ........................................................................ 21
4.3 Sensor Installation ........................................................................................23
CHAPTER 5 - INITIALIZATION AND MEASUREMENT
5.1 Battery Installation ........................................................................................25
5.2 Meter Initialization ........................................................................................ 28
5.3 Measurement Mode ...................................................................................... 29
5.4 Setup Menu Structure .................................................................................... 30
CHAPTER 6 - PARAMETER SETUP MENU
6.1 Select Parameters.......................................................................................... 31
6.2 Parameter Units ............................................................................................ 31
6.3 Parameter Coefficients ................................................................................... 33
6.4 Averaging ................................................................................................... 34
6.5 Turbidity Averaging ....................................................................................... 34
CHAPTER 7 - CALIBRATION MODE................................................................ 35
7.1 Quick Calibration ........................................................................................36
7.2 pH Calibration ............................................................................................. 38
7.3 ISE Calibration ............................................................................................. 41
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7.4 ORP Calibration .......................................................................................... 42
7.5 Dissolved Oxygen Calibration ........................................................................ 43
7.6 Conductivity Calibration ................................................................................ 45
7.7 Turbidity Calibration ...................................................................................... 49
7.8 Temperature Calibration ................................................................................ 51
7.9 Atmospheric Pressure Calibration ................................................................... 52
CHAPTER 8 - SYSTEM SETUP
8.1 Meter Setup ................................................................................................. 53
8.2 Probe Setup ................................................................................................. 56
CHAPTER 9 - GPS MENU (optional) ............................................................... 57
CHAPTER 10 - STATUS
10.1 Meter Status ............................................................................................... 59
10.2 Probe Status ...............................................................................................59
10.3 GLP Data .................................................................................................. 60
CHAPTER 11 - LOGGING MODE ................................................................... 64
11.1 Logging menu structure ............................................................................... 66
11.2 Logging on Meter ....................................................................................... 66
11.3 Probe Log ..................................................................................................68
11.4 Log Recall ................................................................................................. 69
11.5 Log Notes ..................................................................................................71
CHAPTER 12 - PC CONNECTION
12.1 Software Installation .................................................................................... 74
12.2 Meter to PC Connection .............................................................................. 74
12.3 Probe to PC Connection .............................................................................. 76
CHAPTER 13 - TROUBLESHOOTING / ERROR MESSAGES ............................... 78
APPENDIX
A - PROBE MAINTENANCE ................................................................................ 81
B - PROBE DEPLOYMENT .................................................................................. 84
C - ISE INFORMATION ...................................................................................... 89
D - ACCESSORIES ............................................................................................. 95
E - WARRANTY ............................................................................................... 101
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Chapter 1 - INTRODUCTION
1.1 PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any dam­age, notify your Dealer or the nearest HANNA Customer Service Center immedi­ately.
NoteNote
Note Save all packing materials until you are sure that the instrument
NoteNote
functions correctly. Any damaged or defective items must be returned in their original packing material with the supplied accessories.
1.2 MODEL IDENTIFICATION
Meter: There are two models for the meter:
HI 9829: Portable multiparameter meter HI 98290: Portable multiparameter meter with GPS
Probe: There are two base models of multiparameter probes:
HI 7609829: Standard multiparameter probe HI 7629829: Multiparameter probe with autonomous logging
capability
All meters and probes are fully compatible with each other, and all available measurement sensors can be used on both probe models.
Different combinations of meters, probes, sensors and accessories can be or­dered either in predefined configurations or individually. See Appendix D for ordering configurations.
For example, ordering codes of probes follow: HI 7609829/X is a HI 7609829 probe with X meter cable for pH/pH+ORP/
ISE, D.O., EC, temperature sensors with a short probe shield HI 7619829/X is a HI 7609829 probe with X meter cable for pH/pH+ORP/
ISE, D.O., EC+turbidity, temperature sensors with a long probe shield HI 7629829/X is a HI 7629829 logging probe with X meter cable for pH/
pH+ORP/ISE, D.O., EC, temperature sensors with a short probe shield HI 7639829/X is a HI 7629829 logging probe with X meter cable for pH/
pH+ORP/ISE, D.O., EC+turbidity, temperature sensors with a long probe shield
1.3 GENERAL DESCRIPTION HI 9829 is a portable logging multiparameter system that monitors up to 14
different water quality parameters (7 measured, 7 calculated). The microprocessor-based intelligent multisensor probe allows measurement of
many water quality parameters such as pH, ORP, turbidity, dissolved oxygen,
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conductivity, chloride, nitrate, ammonium and temperature with data logging. The system is easy to setup and easy to use.
The HI 98290 with GPS option has a built-in 12 channel GPS receiver and antenna that guarantees a position accuracy of 10 m (30 ft). Measurements from specific locations are tracked with detailed coordinate information that can be viewed immediately on the display. GPS information can be transferred to a PC using HANNA’s HI 929829 software. GPS information can also be viewed using a GPS mapping software such as Google™ Maps. Clicking on visited locations using a mapping software displays the measurement information.
All HI 9829 are equipped with Fast Tracker™ an invaluable tool for associating measurements with their locations. HANNA’s exclusive Fast Tracker™—T.I.S. (Tag ID System) uses
iButton®s that can be installed at any number of sampling sites.
The HI 9829 features a graphic, backlit display that automatically sizes the digits to fit the screen with on-screen graphing capability. Each parameter is fully configurable.
HI 9829 was designed to withstand harsh environments and is the ideal solu­tion for field measurements of lakes, rivers and sea. The meter meets IP67 standards (30 minute immersion at a depth of 1 m) and the multisensor probe meets IP68 standards (continuous immersion in water). Settings and logged data can be protected with a passcode to avoid unautho­rized modifications and context-sensitive help is always available.
Main features of the HI 9829 system:
• Rugged meter and probe
• Easy to use
• Measure up to 16 parameters and display of up to 12 parameters
• Tracking of measurement locations with GPS (optional)
• Waterproof protection (IP67 for the meter and IP68 for the probe)
• Exclusive Fast Tracker™—T.I.S. (Tag ID System)
• Graphic LCD with backlight
• Built-in barometer for D.O. concentration compensation
• Quick calibration feature
• Measurement check to eliminate any erroneous readings
• Autorecognition of probe and sensors
• Log-on-demand and automatic logging (up to 45,000 samples) on meter for all parameters
• Graphical display of logged data
GOOGLE™ is a registered trademark of Google, Inc. HANNA instruments® has no affiliation with Google™, Inc. iButton® is a registered trademark of Maxim/Dallas Semiconductor Corp.
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• USB interface for PC communication
• Auto-ranging for EC, ISE and turbidity readings
• Good Laboratory Practice feature, the last 5 calibrations are automatically stored
• Field-replaceable sensors with color coded caps
• Meter can be powered with either alkaline or rechargeable batteries
• Fast charging capability
1.4 DISPLAY & KEYBOARD DESCRIPTION
1. Graphic LCD
2. Battery level indicator
3. Softkey functions
4. Left softkey: function defined on display
5. On/Off key: turn the meter on and off
6. Lamp key: turn the backlight on and off
7. Alphanumeric keyboard: insert alphanumeric codes
8. HELP key: obtain information about the displayed screen
9. Arrow keys: scroll the displayed options/message
10. ESC key: return to the previous screen
11. Right softkey: function defined on display
12. GPS signal strength indicator (optional)
13. Tag reader
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Chapter 2 - QUICK START
Before you begin using the included rechargeable C batteries for at least 6 hours or replace the rechargeable batteries with non-rechargeable alkaline batteries.
2.1 SENSOR AND PROBE INSTALLATION
Sensor o-rings must be lubricated with the supplied grease prior to
installation.
HI 76x9829 probes have 3 sensor connectors identified with color­coded triangles:
• Connector 1 (red): For either pH/ORP, pH, ammonium, chloride or nitrate sensor
• Connector 2 (white): For dissolved oxygen sensor
• Connector 3: (blue): For either EC or EC/turbidity sensor
• Position the connector key towards the center of the probe, make sure the connector is seated correctly (the sensor will no longer move freely) before tightening the locking threads.
• To protect the sensors, screw the protective shield onto the probe body.
• Unscrew the battery cover of the HI 7629829 logging probe and install 4 AA batteries for autonomous logging before connecting to the meter.
• With the meter off, connect the probe to the DIN socket on the bottom of the meter. Align the pins and key then push the plug into the socket and tighten the thread.
• Turn the meter on by pressing the ON/OFF key. The meter will automatically recognize the probe and the installed sensors and identify them on the probe status screen.
• Press <Measure> to view the measurement screen.
HI 9829HI 9829
HI 9829 multiparameter system, either charge the
HI 9829HI 9829
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2.2 BASIC OPERATION
The main operating modes for HI 9829 are measurement, logging and setup. The measurement screen can be configured to display a single measurement or
up to 12 simultaneous measurements by using the numbers 1-7 on the keypad. Use the arrow keys to scroll through the measurements not being displayed. See section 5.3 for more details.
The measurement units will blink if the system has not been calibrated and the measurement number will blink when the reading is out of range.
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Press <Log> to display the logging menu. You can either log a single sample on the meter, start an interval log on the meter, or start an interval log on a logging probe (HI 7629829). See chapter 11 for more details.
Press <Menu> to enter setup mode. You can configure which parameters you want to measure, calibrate the sensors, change system settings, access the GPS menu and view the meter and probe status.
2.3 HELP FUNCTION
HI 9829 features context sensitive HELP, which provides useful information re-
garding the displayed screen. Simply press the HELP key to access this function, then use the arrow keys to
scroll through the message. To escape from the HELP window, press the HELP key again or ESC.
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Chapter 3 - SPECIFICATIONS
3.1 SYSTEM SPECIFICATIONS
TEMPERATURE
RangeRange
Range -5.00 to 55.00 °C;
RangeRange
23.00 to 131.00 °F;
268.15 to 328.15 K
ResolutionResolution
Resolution 0.01 °C; 0.01 °F; 0.01 K
ResolutionResolution AccuracyAccuracy
Accuracy ± 0.15 °C; ± 0.27 °F; ±0.15 K
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 custom point
CalibrationCalibration
pH/mVpH/mV
pH/mV
pH/mVpH/mV RangeRange
Range 0.00 to 14.00 pH; ± 600.0 mV
RangeRange ResolutionResolution
Resolution 0.01 pH; 0.1 mV
ResolutionResolution AccuracyAccuracy
Accuracy ± 0.02 pH; ± 0.5 mV
AccuracyAccuracy CalibrationCalibration
Calibration Automatic 1, 2 or 3 points with automatic recognition
CalibrationCalibration
of 5 standard buffers (pH 4.01, 6.86, 7.01, 9.18, 10.01)
and 1 custom buffer
ORP
RangeRange
Range ± 2000.0 mV
RangeRange ResolutionResolution
Resolution 0.1 mV
ResolutionResolution AccuracyAccuracy
Accuracy ± 1.0 mV
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 custom point (relative mV)
CalibrationCalibration
DISSOLVED OXYGEN
RangeRange
Range 0.0 to 500.0 %
RangeRange
0.00 to 50.00 ppm (mg/L)
ResolutionResolution
Resolution 0.1 %
ResolutionResolution
0.01 ppm (mg/L)
AccuracyAccuracy
Accuracy 0.0 to 300.0 %: ± 1.5 % of reading
AccuracyAccuracy
or ± 1.0 % whichever is greater;
300.0 to 500.0 %: ± 3 % of reading
0.00 to 30.00 ppm (mg/L): ± 1.5 % of reading or ±0.10 ppm (mg/L) whichever is greater;
30.00 ppm (mg/L) to 50.00 ppm (mg/L): ± 3 % of reading
CalibrationCalibration
Calibration Automatic 1 or 2 points at 0, 100 % or 1 custom point
CalibrationCalibration
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CONDUCTIVITY
RangeRange
Range 0 to 200 mS/cm
RangeRange
(absolute EC up to 400 mS/cm)
ResolutionResolution
Resolution
ResolutionResolution
Manual 1 µS/cm; 0.001 mS/cm; 0.01 mS/cm; 0.1 mS/cm; 1 mS/cm Automatic 1 µS/cm from 0 to 9999 µS/cm
0.01 mS/cm from 10.00 to 99.99 mS/cm
0.1 mS/cm from 100.0 to 400.0 mS/cm
Automatic (mS/cm) 0.001 mS/cm from 0.000 to 9.999 mS/cm
0.01 mS/cm from 10.00 to 99.99 mS/cm
0.1 mS/cm from 100.0 to 400.0 mS/cm
AccuracyAccuracy
Accuracy ±1 % of reading or ±1 µS/cm whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration Automatic single point, with 6 standard solutions
CalibrationCalibration
(84 µS/cm, 1413 µS/cm, 5.00 mS/cm, 12.88 mS/cm,
80.0 mS/cm, 111.8 mS/cm) or custom point
RESISTIVITY
RangeRange
Range 0 to 999999 ·cm;
RangeRange
(depending on measurement setup) 0 to 1000.0 kΩ·cm;
0 to 1.0000 MΩ·cm
ResolutionResolution
Resolution Depending on resistivity reading
ResolutionResolution CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
TDS (Total Dissolved Solids)
RangeRange
Range 0 to 400000 ppm (mg/L);
RangeRange
(the maximum value depends on the TDS factor)
ResolutionResolution
Resolution
ResolutionResolution Manual 1 ppm (mg/L); 0.001 ppt (g/L);
0.01 ppt (g/L); 0.1 ppt (g/L); 1 ppt (g/L)
Automatic 1 ppm (mg/L) from 0 to 9999 ppm (mg/L)
0.01 ppt (g/L) from 10.00 to 99.99 ppt (g/L)
0.1 ppt (g/L) from 100.0 to 400.0 ppt (g/L)
Automatic ppt (g/L) 0.001 ppt (g/L) from 0.000 to 9.999 ppt (g/L)
0.01 ppt (g/L) from 10.00 to 99.99 ppt (g/L)
0.1 ppt (g/L) from 100.0 to 400.0 ppt (g/L)
AccuracyAccuracy
Accuracy ±1 % of reading or ±1 ppm (mg/L) whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
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SALINITY
RangeRange
Range 0.00 to 70.00 PSU
RangeRange ResolutionResolution
Resolution 0.01 PSU
ResolutionResolution AccuracyAccuracy
Accuracy ±2% of reading or ±0.01 PSU whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration Based on conductivity calibration
CalibrationCalibration
SEAWATER SIGMA
RangeRange
Range 0.0 to 50.0 σt, σ0, σ
RangeRange ResolutionResolution
Resolution 0.1 σt, σ0, σ
ResolutionResolution AccuracyAccuracy
Accuracy ± 1σt, σ0, σ
AccuracyAccuracy CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
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TURBIDITY
RangeRange
Range 0.0 to 99.9 FNU;
RangeRange
100 to 1000 FNU
ResolutionResolution
Resolution 0.1 FNU from 0.0 to 99.9 FNU
ResolutionResolution
1 FNU from 100 to 1000 FNU
AccuracyAccuracy
Accuracy ±0.3 FNU or ±2 % of reading,
AccuracyAccuracy
whichever is greater
CalibrationCalibration
Calibration Automatic 1, 2 or 3 points at 0, 20 and 200 FNU, or custom
CalibrationCalibration
ISE
Ammonium-Nitrogen
RangeRange
Range 0.02 to 200.0 ppm Am (as NH
RangeRange ResolutionResolution
Resolution 0.01 ppm to 1 ppm
ResolutionResolution
+
-N)
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0.1 ppm to 200.0 ppm
AccuracyAccuracy
Accuracy ±5 % of reading or 2 ppm
AccuracyAccuracy CalibrationCalibration
Calibration 1 or 2 point, 10 ppm and 100 ppm
CalibrationCalibration
Chloride
RangeRange
Range 0.6 to 200.0 ppm Cl (as Cl-)
RangeRange ResolutionResolution
Resolution 0.01 ppm to 1 ppm
ResolutionResolution
0.1 ppm to 200.0 ppm
AccuracyAccuracy
Accuracy ±5 % of reading or 2 ppm
AccuracyAccuracy CalibrationCalibration
Calibration 1 or 2 point, 10 ppm and 100 ppm
CalibrationCalibration
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Nitrate-Nitrogen
RangeRange
Range 0.62 to 200.0 ppm Ni (as NO
RangeRange ResolutionResolution
Resolution 0.01 ppm to 1 ppm
ResolutionResolution
3
-
-N)
0.1 ppm to 200 ppm
AccuracyAccuracy
Accuracy ±5 % of reading or 2 ppm
AccuracyAccuracy CalibrationCalibration
Calibration 1 or 2 point, 10 ppm and 100 ppm
CalibrationCalibration
ATMOSPHERIC PRESSURE
RangeRange
Range 450 to 850 mm Hg; 17.72 to 33.46 in Hg;
RangeRange
600.0 to 1133.2 mbar; 8.702 to 16.436 psi;
0.5921 to 1.1184 atm; 60.00 to 113.32 kPa
ResolutionResolution
Resolution 0.1 mm Hg; 0.01 in Hg; 0.1 mbar
ResolutionResolution
0.001 psi; 0.0001 atm; 0.01 kPa
AccuracyAccuracy
Accuracy ±3 mm Hg within ±15°C from calibration temperature
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 custom point
CalibrationCalibration
METER SPECIFICATIONS
TT
emperature Compensationemperature Compensation
T
emperature Compensation Automatic from -5 to 55 °C (23 to 131 °F)
TT
emperature Compensationemperature Compensation
Logging MemoryLogging Memory
Logging Memory 44,000 records
Logging MemoryLogging Memory
(continuous logging or log-on-demand of all parameters)
Logging IntervalLogging Interval
Logging Interval 1 second to 3 hours
Logging IntervalLogging Interval PC InterfacePC Interface
PC Interface USB (with HI 929829 software)
PC InterfacePC Interface WW
aterproof Paterproof P
W
aterproof P
WW
aterproof Paterproof P
EnvironmentEnvironment
Environment 0 to 50 °C (32 to 122 °F); RH 100 %
EnvironmentEnvironment Battery TBattery T
Battery T
Battery TBattery T
rotectionrotection
rotection IP67
rotectionrotection
ypeype
ype 4 x 1.2 V, NiMH, rechargeable batteries, size C
ypeype
or 4 x 1.5 V alkaline, C size batteries
Battery LifeBattery Life
Battery Life See below
Battery LifeBattery Life Dimensions/WDimensions/W
Dimensions/W
Dimensions/WDimensions/W
eighteight
eight
eighteight
221 x 115 x 55 mm (8.7 x 4.5 x 2.2”) / 750 g (26.5 oz.)
GPSGPS
GP S 12 channel receiver
GPSGPS 10 m (30 ft) accuracy
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METER BATTERY LIFE
The power consumption of the HI 9829 multiparameter system is dependent on three things:
1. The measurement system configuration (probe type, sensor configuration)
2. The meter configuration (logging interval, GPS and backlight use)
3. The battery type (alkaline or rechargeable). Note: Alkaline batteries have two times the expected life.
The following table estimates the meter’s battery life connected to a HI 76X9829 probe with backlight off. The logging interval only affects meter
battery life when GPS Powersave mode is used (units with GPS). (Note: GPS and backlighting use consume the most power). The table variables are GPS, battery selection and parameter selection. Note: When a HI 7629829 logging probe is connected to a meter, it uses the meter’s power.
pH, ORP, DO, EC enabled pH, ORP, DO, EC and
Turbidity disabled Turbidity enabled
Alkaline batteries 280 hours 190 hours without GPS
Rechargeable batteries 140 hours 95 hours without GPS
Alkaline batteries 90 hours 70 hours with GPS
Rechargeable batteries 45 hours 35 hours with GPS
Alkaline batteries with 110 hours 100 hours GPS powersave on, 4 min log
Rechargeable batteries with 55 hours 50 hours GPS powersave on 4, min log
Alkaline batteries with 180 hours 160 hours GPS powersave on, 10 min log
Rechargeable batteries with 90 hours 80 hours GPS powersave on 10, min log
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3.2 PROBE SPECIFICATIONS
Non-logging Probe Logging Probe
Sample Environment Fresh, brackish, seawater
Waterproof protection IP68
Computer Interface NA USB PC (HI 76982910)
Internal Battery Type NA 4 X 1.5V Size AA Alkaline
Typical Battery Life NA See below
Memory NA 140,000 measurements
Operating Temperature -5 to 55° C *
Storage Temperature -20 to 70° C
Maximum Depth 20 m (66 ft.) *
Dimensions
HI 7609829HI 7609829
HI 7609829 342mm (13.5”),
HI 7609829HI 7609829
(without cable) dia=46 mm (1.8”) dia=46 mm (1.8")
HI 7619829HI 7619829
HI 7619829 382 mm (15.1”),
HI 7619829HI 7619829
dia=46 mm (1.8”) dia=46 mm (1.8")
Weight (with batteries and sensors)
HI 7609829HI 7609829
HI 7609829 570g (20.1 oz.)
HI 7609829HI 7609829 HI 7619829HI 7619829
HI 7619829 650g (22.9 oz.)
HI 7619829HI 7619829
Cable Specification Multistrand-multiconductor shielded cable with internal strength
member rated for 68 kg (150 lb) intermittent use
Wetted Materials Body: ABS
Threads: Nylon Shield: ABS/ 316 SS Temp probe: 316 SS
O-rings: EPDM
(single parameter logged)
35,000 measurements (all parameters logged)
HI 7629829HI 7629829
HI 7629829 442mm (17.4"),
HI 7629829HI 7629829
HI 7639829HI 7639829
HI 7639829 482 mm (19.0"),
HI 7639829HI 7639829
HI 7629829HI 7629829
HI 7629829 775g (27.3 oz.)
HI 7629829HI 7629829
HI 7639829HI 7639829
HI 7639829 819g (28.9oz.)
HI 7639829HI 7639829
* Reduced for ISE sensors
LOGGING PROBE BATTERY LIFE*
Interval All channels logging All channels logging
(no averaging) (10 sample averaging)
1 - 5 sec 72 hours 72 hours
1 min 22 days 11 days
10 min 70 days 65 days
* Continuous logging is contingent on availability of log memory
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3.3 SENSOR SPECIFICATIONS
HI 7609829-0 HI 7609829-1 HI 7609829-2 HI 7609829-3
Description pH pH/ORP Dissolved Oxygen EC
Measure Type Primary Unit pH, mV (pH) pH, mV (pH/ORP) D.O. (% sat. & conc.) EC
Measure Range 0.00 to 13.00 pH 0.00 to 13.00 pH 0.0 to 500.0 % 0.0 to 200.0 mS/cm
±600.0 mV ±600.0 mV 0.00 to 50.00 mg/L 0.0 to 400 mS/cm
±2000.0 mV (absolute)
Temperature Range -5 to 55°C -5 to 55°C -5 to 55°C -5 to 55°C
Color Code Red Red White Blue
Materials Tip: glass (pH) Tip: glass (pH); Pt (ORP) Cat/An: Ag/Zn Stainless steel electrodes
Maintenance HI 70300 HI 70300 HI 7042S none Solution (storage solution) (storage solution) (D.O. electrolyte)
Dimensions 118 x 15 mm 118 x 15 mm 99 x 17 mm 111 x 17 mm
Depth 20 m (65’) 20 m (65’) 20 m (65’) 20 m (65’)
Description EC/Turbidity Ammonium ISE Chloride ISE Nitrate ISE
Measure Type EC ppm ppm ppm Primary Unit FTU
Measure Range 0 to 200.0 mS/cm 0.02 to 200.0 ppm 0.6 to 200.0 ppm 0.6 to 200.0 ppm
0.0 to 1000 FNU
Temperature Range-5 to 55°C 0 to 40°C 0 to 40°C 0 to 40°C
Color Code Red Red Red
Materials Body: ABS/EPOXY Tip: Polymeric Tip: Solid State Tip: Polymeric
Maintenance none none none none Solution
Dimensions 135 x 35 mm 118 x 15 mm 118 x 15 mm 118 x 15 mm Depth 20 m (65’) 5 m ( 16‘) 5 m ( 16‘) 5 m ( 16‘)
Junction: ceramic Junction: ceramic Membrane: HDPE AISI 316
Body: PEI Body: PEI Body: white top ABS Body: ABS/EPOXY
Electrolyte: gel Electrolyte: gel CAP
Reference: double Reference: double
HI 7609829-4 HI 7609829-10 HI 7609829-11 HI 7609829-12
0.0 to 400 mS/cm (abs) as NH
PMMA Liquid Membrane AgCl Pellet Liquid Membrane
Reference: double Reference: double Reference: double
+
-N Cl
4
Body: PEI Body: PEI Body: PEI
Electrolyte: gel Electrolyte: gel Electrolyte: gel
-
as NO
-
-N
3
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Chapter 4 - PROBE INSTALLATION
HI 7609829 and HI 7629829 multisensor probes are used for the measure­ments of pH, ORP, conductivity, turbidity, dissolved oxygen, chloride, nitrate­nitrogen, ammonium-nitrogen and temperature. Each probe can utilize 3 sensors. A description of each sensor follows.
4.1 SENSOR DESCRIPTIONS
HI 7609829-0
pH sensitive bulb and a silver/silver chloride double junc­tion reference with gelled electrolyte.
HI 7609829-1
glass sensitive bulb for pH readings, a platinum sensor for redox measurements and a silver/silver chloride double junc­tion reference with gelled electrolyte.
NoteNote
Note See section 4.2.1 for pH preparation.
NoteNote
See section 4.2.2 for ORP activation.
HI 7609829-2 Galvanic dissolved oxygen (D.O.) sensor. The thin gas permeable membrane isolates the sensor elements from the testing solution but allows oxygen to pass through. The oxygen that passes through the mem­brane is reduced at the cathode and causes a current, from which the oxygen concentration is determined. The D.O. sen­sor conforms to Standard Methods 4500-AG, EPA 360.1.
NoteNote
Note The D.O. sensor needs to be activated before
NoteNote
installation. See section 4.2.3 for details.
HI 7609829-3
is immune to polarization or surface coatings.
Combination pH sensor features a glass
Combination pH/ORP sensor features a
4-electrode conductivity sensor. The sensor
The HI 7609829-4 includes a 4-electrode conductivity sensor and a turbidity sensor that conforms to ISO 7027 standards in a single sensor body. The turbidity sensor uses an optical technique to measure suspended particles in water.
Combination EC/Turbidity sensor. It
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HI 7609829-10: Ammonium selective electrode (ISE) is a
combination liquid membrane sensor used for the detec­tion of free ammonium-nitrogen in freshwater samples. The sensor utilizes a polymeric membrane made with ammo­nium ionophore in a PVC head and silver/silver chloride double junction gel filled reference electrode. This sensor is used in place of the pH sensor in the probe.
HI 7609829-11
: :
: The Chloride ISE is a combination solid state sensor used for
: : the detection of free chloride ions in freshwater samples. The sensor utilizes a silver chloride pellet housed in a PEI head and a silver/silver chloride double junction gel filled reference electrode. This sensor is used in place of the pH sensor in the probe.
HI 7609829-12
: :
: The Nitrate ISE is a combination liquid membrane sensor
: : used for the detection of nitrate nitrogen in freshwater samples. The sensor uti­lizes a polymeric membrane made with nitrate ionophore in a PVC head and a silver/silver chloride double junction gel filled reference electrode. This sensor is used in place of the pH sensor in the probe.
See Appendix C for details regarding the ISE sensors.
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4.2 SENSOR PREPARATION / ACTIVATION
4.2.1 pH Preparation
Remove the shipping cap from the pH sensor. If the shipping cap does not contain any liquid, pour HI 70300 into shipping cap, place it back on the sensor and soak for at least 1/2 hour before use. If HI 70300 is not available, pH 4.01 buffer may be substituted.
4.2.2 ORP Activation
For improved redox measurements, the surface of the sensor must be clean and smooth. A pretreatment procedure should be performed to ensure quick re­sponse.
The pretreatment of the sensor is determined by the pH and the ORP potential values of the sample. Use the table below to determine the treatment required.
First locate the typical sample pH. If the corresponding ORP value (mV) is higher than the values in the table below, an oxidizing pretreatment is necessary. If the value is lower, a reducing pretreatment is necessary.
pHpH
pH
pHpH
mVmV
mV
mVmV
pHpH
pH
pHpH
mVmV
mV
mVmV
pHpH
pH
pHpH
mVmV
mV
mVmV
pHpH
pH
pHpH
mVmV
mV
mVmV
pH pH
pH
pH pH
mV mV
mV
mV mV
0 990 1 920 2 860 3 800 4 740
5 680 6 640 7 580 8 520 9 460
10 400 11 340 12 280 13 220 14 160
For reducing pretreatment: immerse the electrode for at least five minutes in HI 7091.
For oxidizing pretreatment: immerse the electrode for at least five minutes in HI 7092.
4.2.3 D.O. Sensor Activation
The D.O. probe is shipped dry. To prepare the sensor for use:
• Remove the black & red plastic shipping cap and discard.
• Insert the supplied O-ring in to the membrane cap.
• Rinse the membrane with some electrolyte solution. Refill with clean electrolyte.
Gently tap the black membrane cap to dislodge air bubbles. To avoid damag­ing the membrane, do not touch it with your fingers or directly tap the mem­brane.
21
• With the sensor facing down screw the membrane cap counterclockwise to the
end of the threads. Some electrolyte will overflow.
• Rinse outside of sensor with deionized water.
• Invert sensor and inspect. There should be no bubbles or debris between the
membrane and sensor body.
4.2.4 EC and EC/Turbidity Sensor Preparation
The EC and EC/Turbidity sensors do not need to be soaked or hydrated before use. Use the small brush included in the probe maintenance kit to clean and loosen any debris before using.
4.2.5 Ammonium Sensor Preparation
Remove the shipping cap and inspect sensor. Verify no air pockets have devel­oped near the ceramic junction during shipping. Hold the sensor at the connec­tor and shake it down (like a mercury thermometer). Condition the sensor by soaking it in a small amount of
HI 9829-10HI 9829-10
HI 9829-10, 10 ppm NH
HI 9829-10HI 9829-10
+
-N standard for at
4
least a 1/2 hour.
4.2.6 Chloride Sensor Preparation
Remove the shipping cap and inspect sensor. Verify no air pockets have devel­oped near the ceramic junction during shipping. Hold the sensor at the connec­tor and shake it down (like a mercury thermometer). Condition the sensor by soaking it in a small amount of
HI 9829-12HI 9829-12
HI 9829-12, 10 ppm Cl
HI 9829-12HI 9829-12
-
standard for at least
a 1/2 hour.
4.2.7 Nitrate Sensor Preparation
Remove the shipping cap and inspect sensor. Verify no air pockets have devel­oped near the ceramic junction during shipping. Hold the sensor at the connec­tor and shake it down (like a mercury thermometer). Condition the sensor by soaking it in a small amount of
HI 9829-14HI 9829-14
HI 9829-14, 10 ppm NO
HI 9829-14HI 9829-14
-
-N standard for at
3
least a 1/2 hour.
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4.3 SENSOR INSTALLATION
The HI 76x9829 can support 3 different sensors: Connector 1: pH, pH/ORP or ISE (Ammonium, Chloride, Nitrate), Connector 2: D.O., Connector 3: EC or EC/Turbidity.
To make installation easier, the sensors have color-coded caps and the sockets are identified with colored triangles.
NoteNote
Note The EC/Turbidity sensor with 9 pin connector does not have a
NoteNote
color-coded cap. It is always installed into the socket with three blue triangles.
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For a correct installation:
• Grease the sensor O-ring with the lubricant found in the probe maintenance
kit. DO NOT SUBSTITUTE other grease/lubricants as it may cause the O-ring to swell.
• Insert the sensor into the correctly color coded opening while positioning the
connector key toward the center of the probe. Make sure the connector is seated correctly (the sensor will no longer move freely) before tightening the locking threads with your fingers.
• Continue to tighten the locking threads with the tool supplied in the mainte
nance kit until the sensor is secured tightly against the probe body.
• To protect the sensors, screw the protective shield onto the probe body.
• With the meter off, connect the probe to the DIN socket on the bottom of the
meter. Align the pins and key then push the plug into the socket. Tighten the knurled, threaded shell.
• Turn on the meter by pressing the ON/OFF key. The meter
should automatically recognize the installed sensors and identify them on the probe status screen. If you have an error message or the sensor is not recognized, reconnect the sensor(s) or probe and try again.
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Chapter 5 - INITIALIZATION AND MEASUREMENT
5.1 BATTERY INSTALLATION
HI 9829 is supplied with 4 rechargeable, size C NiMH (Nickel-metal hydride)
batteries. The battery symbol on the LCD indicates the remaining battery charge. The meter
has a low battery warning, and when the symbol starts blinking, batteries should be charged or replaced with new ones. When the batteries are discharged the meter will automatically shut off to avoid erroneous readings.
5.1.1 Meter Battery Installation
Replace batteries in nonhazard­ous areas only.
Remove the 4 screws on the rear of the instrument and in­sert the batteries observing po­larity.
If you wish to replace the sup­plied rechargeable batteries with nonrechargeble alkaline batter­ies, move the switch in the bat­tery compartment upward.
A warning message is displayed if you connect the charging cable to a meter with alkaline batteries.
Nonrechargeable alkaline batteries can explode or leak if you try to charge them. Verify that the switch is in the up position when using
alkaline batteries to prevent recharging.
Note: Do not mix old and new alkaline batteries.Note: Do not mix old and new alkaline batteries.
Note: Do not mix old and new alkaline batteries.
Note: Do not mix old and new alkaline batteries.Note: Do not mix old and new alkaline batteries.
5.1.2 Charging Meter Batteries
Two cables are available for HI 710046.
AC power supply In order to charge the rechargeable batteries, use the HI 710045 cable and the
12 Vdc power adapter.
• With the meter OFF, disconnect the probe.
charging the HI 9829 batteries: HI 710045 and
25
• Connect the HI 710045 cable to the probe connector on the meter and
power adapter, then connect the adapter to an AC power outlet.
• The battery charging animation will be displayed.
It takes about 6 hours to completely charge fully discharged batteries.
NoteNote
Note The meter log, GPS information, system setup and status can be viewed
NoteNote
during battery charging. The battery charging status is indicated by a small animated battery icon found in the lower left corner.
During charging the meter may feel quite warm. This is normal. “Battery temp” (under “Meter Status”) may display values approaching 50 °C.
Automotive auxiliary power outlet (Cigarette lighter receptacle) To charge batteries from a automotive auxiliary power outlet, use HI 710046
cable.
• Connect the HI 710046 cable to the probe connector on the meter and to
the auxiliary plug.
• The battery charging animation will be displayed.
A complete battery charging will take about 6 hours if they are completely discharged.
26
5.1.3 Probe Battery Installation (for logging probes only)
To install probe batteries: Replace batteries in a nonhazardous area only. Remove the battery cover by
turning it counterclockwise. Insert the batteries observing polarity.
Note:Note:
Note:
Note:Note:
Do not mix old and new batteries.Do not mix old and new batteries.
Do not mix old and new batteries.
Do not mix old and new batteries.Do not mix old and new batteries.
Replace the battery cover by engaging the threads and turning it clockwise. Continue turning until it is flush with probe body.
27
5.2 METER INITIALIZATION
After connecting the desired sensors to the probe and connecting the probe to the meter (see previous chapter), turn the meter on by pressing ON/OFF.
After the initialization has been completed, the meter displays the PROBE STA­TUS SCREEN.
The probe status screen identifies the probe and attached sensors. Non-logging probes are identified as HI 7609829 and logging probes are identified as HI 7629829.
Two active soft keys are found at the bottom of the status screen.
Press <Measure> to access the measurement mode.
Press <Param> to access the “Select Parameter” menu. (This screen can also
be accessed from the main menu, see Chapter 6 for a detailed description.).
Press the DOWN arrow to view additional information about the probe.
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5.3 MEASUREMENT MODE
Measurement mode is one of the three main operating modes of HI 9829 (along with logging mode and setup mode).
During measurement mode
HI 9829 will simultaneously measure data for all
enabled parameters.
• Use the numbers on the keyboard to select the number of parameters that are
shown on the screen at one time. The display will automatically resize the font.
• Press the [up] and [down] arrows to scroll through the enabled parameters if
they do not fit on one screen.
NoteNote
Note A flashing measurement value indicates that the measurement is out of
NoteNote
range. A flashing measurement unit indicates that the user calibration has not
been done and is needed for accurate readings.
• Press <Log> to enter the log menu. See Chapter 11 for details.
• Press <Menu> to enter the main setup menu. The main menu accesses the
parameter setup, calibration, system setup, GPS and status options. See the following chapters for details.
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5.4 SETUP MENU STRUCTURE
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