Hanna Instruments HI 9828 User Manual

Instruction Manual
HI 9828
Multiparameter
www.hannainst.com
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Dear CustomerDear Customer
Dear CustomerDear Customer
Thank you for choosing a Hanna Instruments product. Please read this instruction manual carefully before using the instrument. It will provide you with the necessary information for correct use of the instrument, as well as a precise idea of its versatility. If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.comtech@hannainst.com
tech@hannainst.com or see the back cover for our worldwide contact list.
tech@hannainst.comtech@hannainst.com This instrument is in compliance with the
directives.
Hanna Instruments reserves the right to modify the design,
construction and appearance of its products without advance notice.
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TABLE OF CONTENTS
CHAPTER 1- INTRODUCTION
1.1 Preliminary examination .............................................................................. 7
1.2 Model identification .................................................................................... 7
1.3 General description .................................................................................... 8
1.4 Power supply.............................................................................................. 9
1.4.1 Batteries installation .............................................................................. 9
1.4.2 Recharging batteries ............................................................................. 9
1.5 Probe description & installation .................................................................. 10
1.5.1 Sensors description ............................................................................. 10
1.5.2 Sensors specifications ......................................................................... 11
1.5.3 D.O. sensor activation ........................................................................ 12
1.5.4 Installation ......................................................................................... 12
1.6 Specifications ........................................................................................... 13
1.7 Display & keyboard description .................................................................. 17
1.8 Help function ........................................................................................... 18
CHAPTER 2 - MEASUREMENT MODE
2.1 Procedure ................................................................................................ 19
CHAPTER 3 - SYSTEM SETUP
3.1 Measurement setup .................................................................................. 20
3.2 System setup ............................................................................................ 22
3.3 Table of measurement & setup items .......................................................... 26
CHAPTER 4 - CALIBRATION MODE
4.1 Quick calibration ..................................................................................... 28
4.2 pH calibration .......................................................................................... 30
4.2.1 Preparation ........................................................................................ 30
4.2.2 Procedure .......................................................................................... 30
4.2.3 Error list ............................................................................................ 32
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4.3 Dissolved oxygen calibration ..................................................................... 33
4.3.1 Procedure .......................................................................................... 33
4.4 Conductivity calibration ............................................................................ 34
4.4.1 Procedure .......................................................................................... 35
4.5 Atmospheric pressure ................................................................................ 37
4.5.1 Procedure ............................................................................................. 37
4.6 ORP calibration ....................................................................................... 37
4.6.1 Procedure .......................................................................................... 37
4.7 Temperature calibration ........................................................................... 38
4.7.1 Procedure .......................................................................................... 38
CHAPTER 5 - LOGGING MODE
5.1 Logging ................................................................................................... 39
5.1.1 Logging options ................................................................................. 39
5.2 Log data setup ......................................................................................... 40
5.2.1 Lots ................................................................................................... 41
5.2.2 Delete all lots ..................................................................................... 42
5.2.3 Remarks ............................................................................................ 42
5.2.4 Delete all remarks .............................................................................. 43
5.2.5 Tags .................................................................................................. 43
CHAPTER 6 - GLP
6.1 Probe information..................................................................................... 45
6.2 pH .......................................................................................................... 46
6.3 Dissolved oxygen...................................................................................... 46
6.4 Conductivity............................................................................................. 47
6.5 Atmospheric pressure ................................................................................ 47
6.6 ORP........................................................................................................ 48
6.7 Temperature............................................................................................. 48
CHAPTER 7 - PC CONNECTION
7.1 Software installation ................................................................................. 49
7.2 PC connection ......................................................................................... 49
CHAPTER 8 - ERROR MESSAGES................................................................ 51
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APPENDIX
A - PROBE MAINTENANCE ............................................................................ 53
B - ACCESSORIES.......................................................................................... 55
C - WARRANTY.............................................................................................. 57
USER NOTES ............................................................................................ 58
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Chapter 1 - INTRODUCTION
1.1 PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any notice­able damage, notify your Dealer or the nearest Hanna Customer Service Center immediately.
HI9828HI9828
HI9828 is supplied complete with:
HI9828HI9828
- Multisensor probe (pH/ORP, Conductivity, D.O.) HI9828-25HI9828-25
-
HI9828-25 quick calibration standard solution, 500 mL
HI9828-25HI9828-25
- Calibration beaker
- Probe maintenance kit
- 4 rechargeable C size, Ni-MH batteries
- Power adaptor and cable
- Cigarette lighter cable
- 5 i-Button HI7698281HI7698281
-
HI7698281 USB interface cable
HI7698281HI7698281 HI92000HI92000
-
HI92000 Windows® compatible software
HI92000HI92000
- Instruction manual
- Rugged carrying case
©
with holder
NONO
TETE
NO
TE Save all packing materials until you are sure that the instrument func-
NONO
TETE
tions correctly. Any damaged or defective items must be returned in their original packing materials together with the supplied accessories.
1.2 MODEL IDENTIFICATION
Based on probe cable length, 3 different models are available according to the following scheme:
Windows® is a registered Trademark of “Microsoft Co.”
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1.3 GENERAL DESCRIPTION
HI 9828HI 9828
HI 9828 is a multiparameter system that benefits from years of experience of
HI 9828HI 9828 Hanna Instruments as a manufacturer of analytical instruments. Waterproof, resistant and easy to use, it is the ideal solution for field measurements of lakes, rivers and sea. Thanks to the microprocessor based multisensor probe, it is pos­sible to measure all the parameters necessary to evaluate the water quality, as dissolved oxygen saturation percentage, conductivity, seawater specific gravity and other parameters that ensure life in water as pH and temperature. It is also possible to use the same probe with different meters without the need to recalibrate the system.
Up to 12 parameters can be enabled and seen on the large graphic display with backlight. All readings can be memorized and associated to a precise sampling area thanks to the i-Button
©
system and the remarks that the operator can insert before or during measurements. The same data can be plotted on the meter and also downloaded to a PC by means of USB connector and
HI92000HI92000
HI92000 Windows
HI92000HI92000
compatible application for successive elaborations.
The setting menu can be protected by password to avoid not authorized modifi­cations and the help function is always available to explain the selected function, operation or message.
®
The main features of
HI9828HI9828
HI9828 series include:
HI9828HI9828
• Measurement of dissolved oxygen, pH, ORP, conductivity and related param-
eters, temperature, atmospheric pressure and seawater specific gravity
• Field replaceable sensor modules for DO, EC and pH/ORP
• 5 interface languages: English, Spanish, French, Portuguese, Italian
• Graphical display with backlight
• GLP features
• i-Button
©
system to remark the sampling area
• Up to 60,000 samples stored in 100 different lots
• Four C size Ni-MH rechargeable batteries
• Batteries recharged from mains power supply and from cigarette lighter
• Password protection
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1.4 POWER SUPPLY
HI9828HI9828
HI9828 runs with 4 rechargeable C size, Ni-MH batteries.
HI9828HI9828 On the display the battery symbol visualizes the remaining battery charge. When
this symbol starts blinking, it is necessary to recharge or replace them with new ones. When the batteries are completely rundown the meter automatically shuts off to avoid wrong readings.
1.4.1 Batteries installation
Battery replacement must only take place in a nonhazardous area.
Remove the 4 screws on the rear cover of the instrument and insert the batteries while paying attention to the correct polarity.
Move the switch down toward the probe con­nector if using rechargeable batteries. Move the switch up for alkaline batteries.
Alkaline batteries can explode or leak when attempting to recharge them with the switch set to down position.
1.4.2 Recharging batteries
HI9828HI9828
HI9828 is supplied with two cables for recharging batteries:
HI9828HI9828 HI710046HI710046
HI710046.
HI710046HI710046
HI710045HI710045
HI710045 and
HI710045HI710045
Mains power supply In order to recharge batteries from the mains power supply, use
combined with the 12 Vdc adapter.
• With the meter OFF, disconnect the probe.
• Connect
HI710045HI710045
HI710045 to the meter and to the power adapter; connect the
HI710045HI710045
adapter to the mains power supply.
• The message “Battery charging in progress” ap-
pears and then the battery symbol.
• A complete batteries recharging will last about
14 hours.
HI710045HI710045
HI710045
HI710045HI710045
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Cigarette lighter supply
To recharge
HI9828HI9828
HI9828 from a vehicle cigarette lighter supply, use
HI9828HI9828
HI710046HI710046
HI710046.
HI710046HI710046
• Simply connect the cable to the meter and to the car’s cigarette lighter.
• The message “Battery charging in progress” appears on the display, followed
by the battery symbol.
• A complete batteries recharging will last about 14 hours.
NONO
TETE
NO
TE Batteries can also be recharged with the meter ON; if the auto-off
NONO
TETE
feature is enabled, the meter turns off automatically after the set time.
1.5 PROBE DESCRIPTION & INSTALLATION
HI9828HI9828
HI9828 is supplied with the multisensor probe for dissolved oxygen, tempera-
HI9828HI9828 ture, conductivity, pH and redox measurements.
1.5.1 Sensors description
The galvanic D.O. sensor allows to have stable readings in a few seconds. The thin permeable membrane isolates the sensor elements from the testing solution, but allows oxygen to enter. Oxygen that passes through the membrane causes a current flow, from which the oxygen concentration is de­termined. Before installing the probe, it is necessary to acti­vate the D.O. sensor; see paragraph 1.5.3 for details.
The conductivity sensor uses the 4-ring technology that al­lows stable and linear readings without any interference in the whole range.
The pH/ORP sensor features a glass membrane for pH read­ings and a Pt sensor for redox measurements. To avoid clogging problems and ensure a fast response, the pH bulb must be kept moist at any time. Store the electrode with few drops of
HI70300HI70300
HI70300 storage solution in the protec-
HI70300HI70300
tive cap.
The EC sensor also works as matching pin and must be always mounted to have cor­rect pH readings.
For correct redox measurements, the surface of the elec­trode must be clean and smooth, and a pretreatment pro­cedure should be performed to ensure quick responses.
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Since the Pt/PtO system depends on the pH, the pretreatment of the electrode may be determined by the pH and the redox potential values of the solution to be measured.
As a general rule, if the ORP (mV) reading corresponding to the solution pH value is higher than the values in the table below, an oxidizing pretreatment is necessary; otherwise perform a reducing pretreatment.
pHpH
mVmV
pHpH
mVmV
pHpH
mVmV
pHpH
mVmV
pH pH
pH
pHpH
mV
mVmV
pH
pHpH
mV
mVmV
pH
pHpH
mV
mVmV
pH
pHpH
mV
mVmV
pH
pH pH
mV mV
mV
mV mV
pHpH
pH
pHpH
mVmV
mV
mVmV
0 990 1 920 2 860 3 800 4 740 5 680
6 640 7 580 8 520 9 460 10 400 11 340
12 280 13 220 14 160
For reducing pretreatment: immerse the electrode for a few minutes in HI 7091L.
For oxidizing pretreatment: immerse the electrode for a few minutes in HI 7092L.
1.5.2 Specifications of sensors
HI769828-0 HI769828-1 HI769828-2 HI769828-3
Sensor Type pH pH/ORP DO EC
Measure Type pH; mV (pH) pH; mV (pH); mV DO% sat; DO conc. EC; TDS;
resistivity; salinity
Measure Range 0.00 to 14.00 0.00 to 14.00 0.0 to 500.0 % 0.000-200.000 mS/cm
±600.0 mV (pH) ±600.0 mV (pH) 0.00 to 50.00 mg/L 0-400000 mg/L
Color Code Red Red White Blue
Materials Tip: glass (pH) Tip: glass (pH); Pt (ORP) Cat/An: Ag/Zn Stainless steel
Junction: cloth Junction: cloth Membrane: PTFE AISI 316
Body: PEI Body: PEI Body: PVC Body: PVC
Electrolyte: gel Electrolyte: gel
Reference: double Reference: double
Maintenance HI 70300 HI 70300 HI 7042S - Solution (storage) (storage) (refilling)
Dimensions 100 x 14 Ø mm 100 x 14 Ø mm 101 x 16.5 Ø mm 111 x 14 Ø mm
±2000.0 mV 0 to 1.0000 MΩ/cm
0.00 to 70.00 PSU
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1.5.3 D.O. sensor activation
The D.O. probe is shipped dry. To hydrate the probe and prepare it for use pro­ceed as follows:
• Remove the black & red plastic cap. This cap is used for shipping purposes only
and can be thrown away.
• Insert the supplied O-ring in the membrane.
• Rinse the supplied membrane with electrolyte while shaking it gently. Refill with
clean electrolyte. Gently tap the membrane over a surface to ensure that no air bubbles remain trapped. To avoid damaging the membrane, do not touch it with your fingers.
• With the sensor facing down screw the cap clockwise to the end of the threads.
Some electrolyte will overflow.
1.5.4 Installation
The multisensor probe can support 3 different electrodes, DO, EC, pH/ORP. To make easier the installation, the 3 sensors have 3 proper color codes.
For correct sensor installation, proceed as follow:
• Grease the O-ring gaskets.
• Insert the sensor while paying attention to the correct alignment with the corre-
sponding colored connector; fix the sensor by screwing the locking nut with the supplied tool.
• When all sensors are mounted, screw the protection sleeve for taking mea-
surements or the transparent beaker for calibration.
• With the meter off, connect the probe to the DIN socket on
the bottom of the meter by aligning the pins and pushing in the plug. Tighten the nut to ensure a good connection.
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1.6 SPECIFICATIONS
TEMPERATURE
RR
angeange
R
ange -5.00 to 55.00 °C;
RR
angeange
23.00 to 131.00 °F; 268.15 to 328.15 K
RR
esolutionesolution
R
esolution 0.01 °C; 0.01 °F; 0.01 K
RR
esolutionesolution
AccuracyAccuracy
Accuracy ± 0.15 °C; ± 0.27 °F; ±0.15 K
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 custom point
CalibrationCalibration
pHpH
pH
pHpH RR
angeange
R
ange 0.00 to 14.00 pH; ± 600.0 mV
RR
angeange
RR
esolutionesolution
R
esolution 0.01 pH; 0.1 mV
RR
esolutionesolution
AccuracyAccuracy
Accuracy ± 0.02 pH; ± 0.5 mV
AccuracyAccuracy CalibrationCalibration
Calibration Automatic 1, 2 or 3 points with 5 memorized
CalibrationCalibration
standard buffers (pH 4.01, 6.86, 7.01, 9.18, 10.01)
or 1 custom buffer
ORP
RR
angeange
R
ange ± 2000.0 mV
RR
angeange
RR
esolutionesolution
R
esolution 0.1 mV
RR
esolutionesolution
AccuracyAccuracy
Accuracy ± 1.0 mV
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 custom point
CalibrationCalibration
DISSOLVED OXYGEN
RR
angeange
R
ange 0.0 to 500.0 %
RR
angeange
0.00 to 50.00 mg/L
RR
esolutionesolution
R
esolution 0.1 %
RR
esolutionesolution
0.01 mg/L
AccuracyAccuracy
Accuracy 0.0 to 300.0 %: ± 1.5 % of reading
AccuracyAccuracy
or ± 1.0% whichever is greater;
300.0 to 500.0 %: ± 3% of reading
0.00 to 30.00 mg/L: ± 1.5 % of reading or 0.10 mg/L whichever is greater;
30.00 mg/L to 50.00 mg/L: ± 3% of reading
CalibrationCalibration
Calibration Automatic 1 or 2 points at 0, 100 % or 1 custom point
CalibrationCalibration
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CONDUCTIVITY
RR
angeange
R
ange 0.000 to 200.000 mS/cm
RR
angeange
(actual EC up to 400 mS/cm)
RR
esolutionesolution
R
esolution
RR
esolutionesolution
Manual 1 µS/cm; 0.001 mS/cm; 0.01 mS/cm; 0.1 mS/cm; 1 mS/cm Automatic 1 µS/cm from 0 to 9999 µS/cm
0.01 mS/cm from 10.00 to 99.99 mS/cm
0.1 mS/cm from 100.0 to 400.0 mS/cm
Automatic mS/cm 0.001 mS/cm from 0.000 to 9.999 mS/cm
0.01 mS/cm from 10.00 to 99.99 mS/cm
0.1 mS/cm from 100.0 to 400.0 mS/cm
AccuracyAccuracy
Accuracy ±1 % of reading or ±1 µS/cm whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration Automatic at 1 point with 6 memorized standards
CalibrationCalibration
(84 µS/cm, 1413 µS/cm, 5.00 mS/cm, 12.88 mS/cm,
80.0 mS/cm, 111.8 mS/cm) or custom point
RESISTIVITY
RR
angeange
R
ange 0 to 999999 Ω·cm;
RR
angeange
(depending on measurement setup) 0 to 1000.0 kΩ·cm;
0 to 1.0000 MΩ·cm
RR
esolutionesolution
R
esolution Depending on resistivity reading
RR
esolutionesolution
CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
TDS
RR
angeange
R
ange 0 to 400000 mg/L or ppm;
RR
angeange
(the maximum value depends on the TDS factor)
RR
esolutionesolution
R
esolution
RR
esolutionesolution
Manual 1 mg/L (ppm); 0.001 g/L (ppt);
0.01 g/L (ppt); 0.1 g/L (ppt); 1 g/L (ppt)
Automatic 1 mg/L (ppm) from 0 to 9999 mg/L (ppm)
0.01 g/L (ppt) from 10.00 to 99.99 g/L (ppt)
0.1 g/L (ppt) from 100.0 to 400.0 g/L (ppt)
Automatic g/L (ppt) 0.001 g/L (ppt) from 0.000 to 9.999 g/L (ppt)
0.01 g/L (ppt) from 10.00 to 99.99 g/L (ppt)
0.1 g/L (ppt) from 100.0 to 400.0 g/L (ppt)
AccuracyAccuracy
Accuracy ±1 % of reading or ±1 mg/L (ppm) whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
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SALINITY
RR
angeange
R
ange 0.00 to 70.00 PSU (extended Practical Salinity Scale)
RR
angeange
RR
esolutionesolution
R
esolution 0.01 PSU
RR
esolutionesolution
AccuracyAccuracy
Accuracy ±2% of reading or ±0.01 PSU whichever is greater
AccuracyAccuracy CalibrationCalibration
Calibration 1 custom point
CalibrationCalibration
SEAWATER SPECIFIC GRAVITY
RR
angeange
R
ange 0.0 to 50.0 σt, σ0, σ
RR
angeange
RR
esolutionesolution
R
esolution 0.1 σt, σ0, σ
RR
esolutionesolution
AccuracyAccuracy
Accuracy ± 1σt, σ0, σ
AccuracyAccuracy CalibrationCalibration
Calibration Based on conductivity or salinity calibration
CalibrationCalibration
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ATMOSPHERIC PRESSURE
RR
angeange
R
ange 450 to 850 mmHg;
RR
angeange
17.72 to 33.46 inHg;
600.0 to 1133.2 mbar;
8.702 to 16.436 psi;
0.5921 to 1.1184 atm;
60.00 to 113.32 kPa
RR
esolutionesolution
R
esolution 0.1 mmHg; 0.01 inHg; 0.1 mbar
RR
esolutionesolution
0.001 psi; 0.0001 atm; 0.01 kPa
AccuracyAccuracy
Accuracy ± 3 mmHg within ± 15 °C
AccuracyAccuracy
from the temperature during calibration
CalibrationCalibration
Calibration Automatic at 1 custom point
CalibrationCalibration
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GENERAL CHARACTERISTICS
TT
emperature Compensationemperature Compensation
T
emperature Compensation automatic from -5 to 55 °C (23 to 131 °F)
TT
emperature Compensationemperature Compensation
LL
ogging Memoryogging Memory
L
ogging Memory Up to 60,000 samples with 13 measurements each*
LL
ogging Memoryogging Memory
LL
ogging Intervalogging Interval
L
ogging Interval From 1 second to 3 hours
LL
ogging Intervalogging Interval
PC InterfacePC Interface
PC Interface USB (with HI 92000 software)
PC InterfacePC Interface WW
aterproof Paterproof P
W
aterproof P
WW
aterproof Paterproof P
EnvironmentEnvironment
Environment 0 to 50 °C (32 to 122 °F); RH 100 %
EnvironmentEnvironment PP
ower Supplyower Supply
P
ower Supply 4 x 1.5 V alkaline C cells (approximately 150
PP
ower Supplyower Supply
rotectionrotection
rotection Meter IP67, Probe IP68
rotectionrotection
hours of continuous use, without backlight) or
4 x 1.2 V rechargeable C cells (approximately 70 hours
of continuous use, without backlight)
DimensionsDimensions
Dimensions
DimensionsDimensions Meter 221 x 115 x 55 mm (8.7 x 4.5 x 2.2”) Probe L = 270 (10.6”), dia = 46 mm (1.8”)
WW
eighteight
W
eight
WW
eighteight Meter 750 g (26.5 oz.) Probe 750 g (26.5 oz.)
* Without remarks. When using remarks the maximum number of samples decreases but in practical cases
it will never be less than 50,000.
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1.7 DISPLAY & KEYBOARD DESCRIPTION
1. Display
2. Battery level indicator
3. Softkey functions
4. Left softkey: function defined on display
5. On/Off key: to turn on and off the meter
6. Backlight: to activate the backlight
7. Alphanumeric keyboard: to insert alphanumeric codes
8. HELP key: to have information about the shown screen
9. Arrow keys: to scroll between options
10. ESC key: to go back to the previous screen
11. Right softkey: function defined on display
12. Tag reader
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1.8 HELP FUNCTION
HI9828HI9828
HI9828 is provided with the HELP function, useful to have short information
HI9828HI9828 regarding the displayed screen. Simply press the HELP key and an information window will appear.
For longer messages press the arrow keys to scroll.
To escape from the help window press again the HELP key or ESC.
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