Hanna Instruments HI 98230 User Manual

Instruction Manual
HI 98230 - HI 98240
Portable
Microprocessor
Printing and Logging
pH / ORP Meters
http://www.hannainst.com
These Instruments are in
Dear Customer, Thank you for choosing a Hanna Instruments Product. Please read this instruction manual carefully before using the
instrument. This manual will provide you with all the necessary information for
the correct use of the instrument, as well as a precise idea of its versatility in a wide range of applications.
These instruments are in compliance with directives.
TABLE OF CONTENTSTABLE OF CONTENTS
TABLE OF CONTENTS
TABLE OF CONTENTSTABLE OF CONTENTS
PRELIMINARY EXAMINATION ................................................................. 3
GENERAL DESCRIPTION ....................................................................... 3
FUNCTIONAL DESCRIPTION ...................................................................5
SPECIFICATIONS .............................................................................6
INITIAL PREPARATION ..........................................................................7
SETUP MODE ............................................................................. 8
TAKING pH MEASUREMENTS ...............................................................15
TAKING ORP MEASUREMENTS ............................................................. 16
TAKING TEMPERATURE MEASUREMENTS .............................................. 16
pH CALIBRATION PROCEDURE ............................................................. 17
mV CALIBRATION PROCEDURE ........................................................... 20
TEMPERATURE CALIBRATION PROCEDURE ............................................ 21
PRINTING / LOGGING FUNCTION ......................................................... 22
OTHER FEATURES ........................................................................... 24
GOOD LABORATORY PRACTICE (GLP) ................................................... 25
FAULT CONDITIONS .......................................................................... 26
DATA TRANSFER TO PC ......................................................................27
MEMORY ORGANIZATION ................................................................... 28
PRINTER MAINTENANCE .................................................................... 29
BATTERY REPLACEMENT .................................................................... 30
TEMPERATURE-RESISTANCE CORRELATION
FOR HANNA PH SENSITIVE GLASS ........................................................ 31
ELECTRODE CONDITIONING AND MAINTENANCE ..................................... 32
ACCESSORIES .................................................................................. 35
OTHER PRODUCTS FROM HANNA ........................................................ 37
WARRANTY..................................................................................... 38
CE DECLARATION OF CONFORMITY ...................................................... 39
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
PRELIMINARY EXAMINATION
PRELIMINARY EXAMINATIONPRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any damage, notify your Dealer.
Each printing/logging pH meter is supplied complete with:
Amplified pH electrode with built-in temperature sensor and EEPROM for GLP data and DIN connector
AA size Alkaline Batteries (4 pcs)
HI70004 pH 4.01 sachet (1 pc)
HI70007 pH 7.01 sachet (1 pc)
Instruction Manual
• Paper rolls (5 pcs)
Rugged Carrying Case.
Note: Save all packing material until you are sure that the
instrument functions correctly. All defective items must be returned in their original packaging together with the sup­plied accessories.
GENERAL DESCRIPTIONGENERAL DESCRIPTION
GENERAL DESCRIPTION
GENERAL DESCRIPTIONGENERAL DESCRIPTION
HI98240 is a portable printing and logging microprocessor-based pH/ ORP/temperature meter.
HI98230 is a portable printing and logging microprocessor-based pH/ temperature meter.
HI98230 and HI98240 are supplied with an exclusive HANNA (smart) amplified pH/temperature electrode with DIN connector. The electrode has an internal memory for storing calibration data.
All pH measurements are automatically compensated for temperature (ATC). The instrument housing is made of rugged, lightweight material, making it truly portable.
Five memorized buffers (4.01, 6.86, 7.01, 9.18 and 10.01pH) and wrong buffer recognition technology make calibration simple and error free. One or two-point calibration is possible.
The meters are also equipped with a stability indicator and backlight feature for comfortable reading even in excessively dark environments.
A user friendly interface provides clear messages regarding errors, functions and more.
The GLP features provide a guarantee of data consistency. Measurements can be performed with lab-grade precision in the field as
well as in the laboratory.
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An alarm time-out is available to alert the user if too much time has elapsed since the last pH calibration and that re-calibration may be required.
The meters provide a controlled access to calibration and GLP settings through a password protection method.
The Battery Error Preventing System (BEPS) recognizes batteries levels as they become weaker.
To prolong battery life, the backlight and printing features are disabled when the batteries are getting low; "LOBAT" indication is displayed on LCD to warn the user of this condition. However, the meter continues to measure correctly even when the low battery indication is displayed. The meter automatically switches itself off when the batteries are too weak to support proper function.
The meters are equipped with an internal lithium battery that powers the clock circuit even in the absence of power supplies.
For long term field and lab applications, these meters can be connected to a 12VDC adapter.
When in logging mode, the meter stores the measurements in memory at a user selectable interval from 1 to 180 minutes. This information can be retrieved at a later time and also printed.
HI98230 and HI98240 also allow the transfer of stored data to a computer via the HI9200 infrared transmitter connected to the computer RS232 port.
In addition, the meters allow the user to enter an ID code to uniquely identify the instruments.
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTION
FUNCTIONAL DESCRIPTIONFUNCTIONAL DESCRIPTION
1) Power adapter plug
2) Electrode Connector
3) LCD Display
4) PAPER key, to move the paper up
5) ON/OFF key, to turn the meter on or off
6) ALT key, to alternate key function
7) RANGE/LIGHT key, to select measurement ranges, to display time and to enable/disable backlight (with ALT)
8) LOG key, to store measurements
9) ÈCAL key, to move down or enter calibration (with ALT)
10) ÆCFM key, to move right or confirm values (with ALT)
11) ÇFNC key, to move up or select function codes (with ALT)
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SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
INITIAL PREPARATIONINITIAL PREPARATION
INITIAL PREPARATION
INITIAL PREPARATIONINITIAL PREPARATION
Range pH -4.00 to 19.99 pH
mV ±400.0 mV (HI98240 only)
±2000 mV autoranging (HI98240 only)
Temp. -10.0 to 120.0 C (14.0 to 248.0 F)
Resolution pH 0.01 pH
mV 0.1 mV between ±400mV (HI98240 only)
1 mV outside (HI98240 only)
Temp. 0.1 C (0.1F)
Accuracy pH ±0.01 pH @25ºC
(@20C/68F) mV ±0.5mV between ±400mV (HI98240 only)
±2mV outside (HI98240 only)
Temp. ±0.5 C (1F) from 0 to 70C (32 to 158F)
±1C (1.8F) outside
Typical EMC pH ±0.03 pH Deviation mV ±1mV between ±400mV (HI98240 only)
±2 mV outside (HI98240 only)
Temp. ±0.8C (1.4F)
pH Calibration Automatic, at 1 or 2 points with 5 memorized
buffers (4.01, 6.86, 7.01, 9.18 and 10.01 pH) mV Calibration Automatic, 2 points at 0 and 350 mV or (HI98240 only) 3 points at 0, 350 and 1900 mV
Temperature Compensation Automatic from -10 to 120C (14 to 248F) pH Electrode Amplified pH electrode with built-in tempera-
ture sensor and EEPROM for GLP data and
DIN connector (see accessories) ORP Electrode Amplifed ORP electrode with DIN connector (HI98240 only) (see accessories)
Input Impedance 10 Printer Low power impact type-belt, 14 characters
Printing/Logging 1, 2, 5,10, 15, 30, 60, 120 and 180 minutes Interval Power supply 4x1.5V AA alkaline type/350 hours typical life
Environment 0 to 50C (32 to 122F);
Dimensions 220 x 82 x 66 mm (8.7 x 3.2 x 2.6") Weight 500 g (18 oz)
12
Ohm
per line; 38 mm plain paper (HI 710034)
(with 2700mA/h batteries, without printing
and backlight).
12 VDC adapter (HI710005 or HI710006)
0-95% RH non-condensing
Each meter is supplied complete with batteries. Remove the back cover, unwrap the batteries and install them while paying attention to the polarity. Alternatively, connect the HI 710005 or HI 710006 voltage adapter to the power adapter plug.
To prepare the instrument for use, connect the pH or ORP (HI98240 only) electrode to the connector located on the top of the instrument.
To switch the meter on, press the ON/OFF key. The batteries charge status or "LINE" message (if external power adapter is connected) will be displayed on the LCD for a few seconds.
The meter is now ready to operate.
To maximize battery life, the meter is automatically switched off after a user selectable period of non-use (default is 5 minutes). If in logging mode, after the period of non-use, the meter will continue to monitor pH or mV (HI98240 only) and temperature periodically at the end of every logging interval. Only the "LOG" indication will be visible on LCD. While storing data in memory, during the sleep mode, the reading will appear briefly on the LCD.
Before proceeding with pH measurements follow the calibration proce­dure.
Note: When the use of an alternate function (FNC, CFM and CAL) is
requested, press and hold the ALT key first and then the second listed key.
Note: To prevent damage to the electrode, remove the pH electrode
from the sample before turning the meter off. If the meter is OFF, detach the electrode from the meter before
immersing the electrode in the storage solution.
ON/OFF
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SETUP MODESETUP MODE
SETUP MODE
SETUP MODESETUP MODE
Setup can be used to view data regarding instrument status (e.g. battery charge) or GLP data (e.g. calibration date) or to view or print the logged data. It also allows the user to change the meter parameters (e.g. time) and to have access to stored data.
• To enter this mode ensure the meter is
not logging and then press the ALT and FNC keys.
PASSWORD PROTECTION
Setting of the GLP parameters (calibration alarm time-out, instru­ment ID code, time and date) can be password protected. If password is set to a value different from 0000 (factory setting), the user will be asked to enter the password.
• Select the desired GLP parameter code.
• Enter the password by the arrow keys.
• The scrolling message "Insert the function code or press ALT - FNC
to escape" in the upper LCD and the indication "F 00" with the first digit blinking in the lower LCD will be displayed.
• Enter the first digit of the code of the parameter you want to set
using the Ç or È key and pass to the next digit with Æ. The second digit will start blinking.
• Enter the second digit using the Ç or
È key.
• Press ALT and CFM to confirm the code.
• If the entered code doesn't exist the "Err"
message will be displayed for a few seconds and then the message "Insert the function code or press ALT - FNC to escape" will recommence scrolling in the upper LCD.
• Press the ALT and CFM keys to confirm.
• If password is wrong the meter will return to the function selection mode without any warning message.
• If password is correct, the meter provides access to the parameter.
PARAMETER SETTINGS
• Once the parameter code has been entered, the appropriate message will scroll across the LCD for a few seconds.
• The current value of the selected parameter on the upper LCD and the parameter code on the lower LCD will be displayed. The first digit will blink if the parameter can assume continuous values. All the digits will blink if the parameter can assume only a fixed set of values.
• Enter the new value using the arrow keys.
• Press ALT and CFM to confirm the value.
The following table lists the setup codes along with the description of the specific setup items, their valid values and the factory settings (default):
Code Valid values Default
00 Lot data printing/scrolling 0016 00 01 Print lots data summary 02 Printer enable On(enabled); Off(disabled) On 03 Logging interval 1,2,5,10,15,30,60,120,180 1 05 Log on demand delete 06 Timed data delete
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Code Valid values Default
10 Show pH GLP data 11 Show ORP GLP data (HI98240 only) 12 Print GLP data 13 Calibration alarm time-out 0099 days 00
00 means option disabled 14 Instrument ID code 00009999 0000 30 Current time 31 Current day 32 Current month 33 Current year
1
1
1
1
hh:mm 00:00
dd 01
MM 01
YYYY 1998 40 Auto-Off/Power down time-out 5,10,15,30,45,60 5 41 Battery level test 50 RS232 baud rate 1200, 2400, 4800 4800 60 Firmware version 70 Celsius/Fahrenheit selection C ; F C 99 Password
2
00009999 0000 Note: If a wrong code is entered the "Err" message is displayed on
LCD for a few seconds.
1
The meter automatically checks for entered time/date accuracy as follows:
0hh23; 0mm59; 01dd28/29/30/31; 1MM 12; 1998YYYY2097.
2
To change the password, the correct code must be entered first. If the password has been forgotten, the password protected features are no longer accessible; in this case contact your nearest Hanna Service Center.
SETUP MESSAGES LIST
cod. 00: Lot data Printing cod. 01: Lot table Printing cod. 02: Printer enable cod. 03: Log Interval cod. 05: Press "ALT CFM" to delete Lot 00 or "ALT FNC" to escape cod. 06: Press "ALT CFM" to delete Lot 01-16 or "ALT FNC" to escape cod. 10: pH GLP cod. 11: Volt GLP (HI98240 only) cod. 12: GLP data printing cod. 13: Calibration alarm time-out cod. 14: Instrument ID Code cod. 30: Hour - Minute cod. 31: Day cod. 32: Month cod. 33: Year
cod. 40: Auto OFF cod. 41: Battery test cod. 50: Baud rate cod. 60: Release code cod. 70: Celsius or Fahrenheit cod. 99: Pass Code
Some of the most important functions are explained below in a step by step sequence.
TO SCAN LOGGED DATA
COD. 00 - Lot data Printing / Scrolling
• Select the code 00.
• The message "Lot data Printing" will scroll twice on LCD.
• The upper LCD will then display L 00 with the 00 blinking.
• Set the desired lot by the arrow keys. L00 is the lot of data of the "log on demand" and L01 to L16 are the lots of the "timed log".
• Press the ALT and CFM keys to confirm the lot number.
• If the lot doesn't contain data, the "no data" message will scroll across the LCD twice and the meter will return to setup mode.
• If the lot contains one or more data the LCD will display the sample number in its upper part and Sn in the lower part.
Note: In the L00 lot (log on demand) the sample number will be
displayed with 3 digits (001).
• Select the sample number to scan by the arrow keys.
Printing logged data
• Press ALT and CFM to print logged data.
• If the selected sample number is invalid (equal to 0 or bigger than the number of samples), the "Err" message will be displayed for a few seconds.
• If the sample number is correct, the samples starting from the selected one to the last sample of the lot will be printed. To stop printing before the last sample is reached, press and hold the ALT and PAPER keys until the printer stops.
• During printout the LCD will display the sample number being
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printed at that moment. If printout is stopped the LCD will show the last printed sample number. It is then possible to select another sample.
• Press the ALT and FNC keys to return to setup mode. Viewing logged data
• Press RANGE to view data of the selected sample. Data will be displayed in the following order:
pH or mV (mV reading available in HI98240 only) temperature date time
• If RANGE is pressed when the time is displayed, the LCD will pass to the next Sample number.
• It is then possible to scroll the data of the next sample by pressing RANGE or select a different sample by the arrow keys.
• to return to setup mode, press ALT and FNC when the meter displays the sample number.
Cod. 01 - Lot summary printout
• Select the code 01.
• The message "Lot table Printing" will scroll twice on LCD.
• The meter will then print a complete set of information based on the data stored in memory:
a - lot number b - logging interval c - starting date d - number of samples e - starting time f - number and measure unit of
the logged channels.
Note: For lot 00 the number of samples only will be printed.
DELETE SET DATA
• Select code 05 to delete the Log on Demand data or code 06 to delete the Timed Log Data.
• A scrolling message will be displayed.
• Press the ALT and CFM keys to confirm deletion.
• It is also possible to escape without data deletion pressing the ALT and FNC keys.
TO SCAN GLP DATA
Cod. 10 - viewing pH GLP
• Select the code 10
• The " pH GLP" message will scroll twice on LCD.
• Electrode calibration data are verified to be within acceptable values. If not the message "Old probe" or "Dead probe" will scroll once on LCD, depending on calibration data.
• The LCD will then display the instrument identification (ID) code.
• Press Ç to scan remaining data, in the following order:
last calibration date (DD.MM) last calibration year last calibration time (hh.mm) electrode offset value in mV ("OF" appears in the lower LCD) electrode slope in mV/pH ("SL" appears in the lower LCD) first point calibration buffer second point calibration buffer (only if a 2-point calibration has
been performed).
Note: Data can be viewed in reverse order pressing the È key.
• Press ALT and FNC to return to function selection mode.
Code 11 - Viewing mV GLP (HI98240 only)
• Select code 11. The message "Volt GLP" will scroll twice across LCD.
• The LCD will then display the instrument identification (ID) code.
• Press Ç to scan remaining data, in the following order:
last calibration date (DD.MM) last calibration year last calibration time (hh.mm) first calibration point second calibration point third calibration point (if present).
• Press ALT and FNC to return to setup mode.
Code 12 - printing GLP data
• Select code 12. The message "GLP data printing" will scroll across LCD.
• The meter will then print a complete set of the following GLP data:
a - Instrument identification (ID) code
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