Hanna Instruments HI 96747 User Manual
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INSTRUCTION MANUAL
HI 96747HI 96747
HI 96747
HI 96747HI 96747
Copper Low Range ISM
www.hannainst.com
Dear Customer,
Thank you for choosing a Hanna product. This manual will provide you
with the necessary information for the correct use of the instrument. Please
read it carefully before using the meter. If you need additional technical
information, do not hesitate to e-mail us at tech@hannainst.com.
Preliminary examination
Please examine this product carefully. Make sure that the instrument is
not damaged. If any damage occurred during shipment, please notify
your Dealer.
Each HI 96747 Ion Selective Meter is supplied complete with:
• Two Sample Cuvettes and Caps
• 9V Battery
• Instruction Manual
Note: Save all packing material until you are sure that the instrument
works correctly. Any defective item must be returned in its original
packing.
For more details about spare parts and
accessories see “Accessories”
Technical specifications:
Range 0.000 to 1.500 mg/L
Resolution 0.001 mg/L for
0.01 mg/L for
Accuracy ±0.010mg/L ±5% of reading
@ 25°C
Typical EMC Deviation ±0.001 mg/L
Light Source Tungsten lamp
Light Detector Silicon Photocell with narrow band
interference filter @ 560 nm
Method Adaptation of the USEPA approved
bicinchoninate method.
Environment 0 to 50°C (32 to 122°F);
max 95% RH non-condensing.
Battery Type 1 x 9 volt
Auto-Shut off After 10' of non-use in
after 1 hour of non-use in
with last reading reminder.
Dimensions 192 x 102 x 67 mm (7.6 x 4 x 2.6")
Weight 290 g (10 oz.).
measurement
calibration
measurement mode;
calibration mode;
and
validation
Functional description Errors and warnings
ON ZERO READING:
Light High: There is too much light to perform
a measurement. Please check the preparation of
the zero cuvette.
Light Low: There is not enough light to perform
a measurement. Please check the preparation of
the zero cuvette.
No Light:The instrument cannot adjust the
light level. Please check that the sample does
1. GLP/ key: press to enter
edit the date and time.
2. CAL CHECK key: press to perform the validation of the meter, or
press and hold for three seconds to enter
3. ZERO/CFM key: press to zero the meter prior to measurement, to
confirm edited values or to confirm factory calibration restore.
4. READ/ /TIMER key: In
measurement, or press and hold for three seconds to start a preprogrammed countdown prior to measurement. In
view the next screen.
5. ON/OFF : to turn the meter on and off.
6. Liquid Crystal Display (LCD)
7. Cuvette alignment indicator
8. Cuvette holder
DISPLAY ELEMENTS DESCRIPTION:
1. The measuring scheme (lamp, cuvette, detector), appears during
different phases of zero or reading measurement
2. Error messages and warnings
3. The battery icon shows the charging level of the battery
4. The hourglass appears when an interval checking is in progress
5. Status messages
6. The chronometer appears when the reaction timer is running
7. The month, day and date icons appear when a date is displayed
8. Four digit main display
9. Measuring units
10. Four digit secondary display
GLP mode
. In
calibration mode
calibration mode
measurement mode
press to
.
, press to make a
GLP mode
press to
ON SAMPLE READING:
DURING CALIBRATION PROCEDURE:
OTHER ERRORS AND WARNINGS:
not contain any debris.
Inverted cuvettes: The sample and the zero
cuvettes are inverted.
Zero: A zero reading was not taken. Follow the
instructions of the measurement procedure for
zeroing the meter.
Under range: A blinking “0.000” indicates
that the sample absorbs less light than the zero
reference. Check the procedure and make sure
you use the same cuvette for reference (zero)
and measurement.
Over Range: A flashing value of the maximum
concentration indicates an over range condition.
The concentration of the sample is beyond the
programmed range: dilute the sample and rerun the test.
Standard Low: The standard reading is less
than expected.
Standard High: The standard reading is higher
than expected.
Cap error: Appears when external light enters
in the analysis cell. Assure that the cuvette cap
is present.
Cooling lamp: The instrument waits for the
lamp to cool down.
Battery low: The battery must be replaced
soon.
Dead battery: This indicates that the battery
is dead and must be replaced. Once this
indication is displayed, the meter will lock up.
Change the battery and restart the meter.
Measurement procedure
Measurement
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1• Turn the meter on by pressing ON/OFF.
2• When the beeper sounds briefly and the
LCD displays dashes, the meter is ready.
The blinking “ZERO” indicates that the
instrument needs to be zeroed first.
3• Fill the cuvette with 10 mL of unreacted
sample, up to the mark, and replace the
cap.
4• Place the cuvette into the cuvette holder
and ensure that the notch on the cap is
positioned securely into the groove.
5• Press ZERO/CFM and the lamp, cuvette
and detector icons will appear on the display,
depending on the measurement phase.
6• After a few seconds the display will show
“-0.0-”. The meter is now zeroed and
ready for measurement.
7• Remove the cuvette.
8• Add the content of one packet of HI
95747-0 Copper Low Range reagent.
9• Replace the cap and shake gently for 15
seconds.
10•Replace the cuvette into the cuvette
holder and ensure that the notch on the
cap is positioned securely into the groove.
11•Press and hold
seconds. The display will show the
countdown prior to measurement. The
beeper is playing a beep at the end of
countdown period.
Alternatively, wait for 45 seconds and just
READ/READ/
press
READ/
READ/READ/
In both cases, the lamp, cuvette and
detector icons will appear on the display,
depending on the measurement phase.
12•The instrument directly displays concentration
in mg/L of copper on the LCD.
READ/READ/
READ/
READ/READ/
/TIMER/TIMER
/TIMER.
/TIMER/TIMER
/TIMER/TIMER
/TIMER
/TIMER/TIMER
for three
INTERFERENCES
• Cyanide
• Silver
• For strongly buffered alkaline or acidic samples,
pH should be adjusted between 6 and 8 before
addition of reagent.
• To avoid interferences due to fingerprints, oil
or dirt it is very important that the cuvette is
wiped clean prior to insertion in the cuvette
holder. Replacement of scratched cuvettes is
strongly recommended.
or
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Validation and Calibration procedures
Warning: Do not validate or calibrate the instrument with standard
solutions other than the Hanna CAL CHECK™ Standards, otherwise
erroneous results will be obtained.
For accurate validation and calibration results, please perform tests at
room temperature (18 to 25°C; 64.5 to 77.0°F).
Use the Hanna CAL CHECK™ cuvettes (see
“Accessories”) to validate or calibrate
instruments.
VALIDATION
1• Turn the meter on by pressing ON/OFF.
2• When the beeper sounds briefly and the
LCD displays dashes, the meter is ready.
3• Place the CAL CHECKTM Standard
HI 96747-11 Cuvette A into the cuvette
holder and ensure that the notch on the
cap is positioned securely into the groove.
4• Press ZERO/CFM and the lamp, cuvette
and detector icons will appear on the
display, depending on the measurement
phase.
5• After a few seconds, the display will
show “-0.0-”. The meter is now zeroed
and ready for validation.
6• Remove the cuvette.
7• Place the CAL CHECKTM Standard
HI 96747-11 Cuvette B into the cuvette
holder and ensure that the notch on the
cap is positioned securely into the groove.
8• Press CAL CHECK key and the lamp,
cuvette and detector icons together with
“CAL CHECK” will appear on the display,
depending on the measurement phase.
9• At the end of the measurement the display
will show the validation standard value.
The reading should be within specifications
as reported on the CAL CHECK™ Standard
Certificate. If the value is found out of
specifications, please check that the cuvettes
Validation
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4-5
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are free of fingerprints, oil or dirt and
repeat validation. If results are still found
out of specifications then recalibrate the
instrument.
CALIBRATION
Note: It is possible to interrupt the calibration
procedure at any time by pressing CAL
CHECK or ON/OFF keys.
1• Turn the meter on by pressing ON/OFF.
2• When the beeper sounds briefly and the
LCD displays dashes, the meter is ready.
3• Press and hold CAL CHECK for three
seconds to enter
display will show “CAL” during calibration
procedure. The blinking “ZERO” asks for
instrument zeroing.
4• Place the CAL CHECKTM Standard
HI 96747-11 Cuvette A into the cuvette
holder and ensure that the notch on the
cap is positioned securely into the groove.
5• Press ZERO/CFM and the lamp, cuvette
and detector icons will appear on the display,
depending on the measurement phase.
6• After a few seconds the display will
show “-0.0-”. The meter is now zeroed
and ready for calibration. The blinking
“READ” asks for reading calibration
standard.
7• Remove the cuvette.
8• Place the CAL CHECKTM Standard
HI 96747-11 Cuvette B into the cuvette
holder and ensure that the notch on the
cap is positioned securely into the groove.
9• Press READ/ /TIMER and the lamp,
cuvette and detector icons will appear on
the display, depending on the measurement
phase.
10•After measurement the instrument will show
for three seconds the Cal Check Standard
value.
Note: If the display shows “STD HIGH”, the
standard value was too high. If the display
shows “STD LOW”, the standard value
was too low. Verify that both CAL CHECK
Standards HI 96747-11 Cuvettes, A and B
are free from fingerprints or dirt and that
they are inserted correctly.
calibration mode
. The
Then the date of the last calibration
(e.g.: ”01.08.2005”) appears on the
display, or “01.01.2005” if the factory
calibration was selected before. In both
cases the year number is blinking, ready
for date input.
TM
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Calibration
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11•Press GLP/ to edit the desired year
(2000-2099). If the key is kept pressed,
the year number is automatically increased.
12•When the correct year has been set, press
ZERO/CFM or READ/ /TIMER to confirm.
Now the display will show the month blinking.
13•Press GLP/ to edit the desired month
(01-12). If the key is kept pressed, the
month number is automatically increased.
14•When the correct month has been set, press
ZERO/CFM or READ/ /TIMER to confirm.
Now the display will show the day blinking.
15•Press GLP/ to edit the desired day (01-
31). If the key is kept pressed, the day
number is automatically increased.
Note: It is possible to change the editing from
day to year and to month by pressing
READ/ /TIMER.
16•Press ZERO/CFM to save the calibration date.
17•The instrument displays “Stor” for one
second and the calibration is saved.
18•The instrument will return automatically
to
measurement mode
on the LCD.
by displaying dashes
GLP
In the
GLP mode
factory calibration can be restored.
LAST CALIBRATION DATE
1• Press GLP/ to enter
2• If no calibration was performed, the factory
FACTORY CALIBRATION RESTORE
It is possible to delete the calibration and restore
factory calibration.
1• Press GLP/ to enter
, the last calibration date can be consulted and the
GLP mode
GLP mode
. The
after three
.
calibration month and day will appear on
the main display and the year on the
secondary display.
calibration message, “F.CAL” will appear
on the main display and the instrument
returns to
measurement mode
seconds.
11-12
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1-2
2
or
or
Last
Calibration
Date
Factory
Calibration
Date
2• Press READ/ /TIMER to enter in the
factory calibration restore screen. The
instrument asks for confirmation of user
calibration delete.
3• Press ZERO/CFM to restore the factory
calibration or press GLP/ again to
abort factory calibration restore.
4• The instrument briefly notifies “done” when
restores factory calibration and returns to
measurement mode
.
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Battery management
To save battery, the instrument shuts down after 10 minutes of non-use
in
measurement mode
If a valid measurement was displayed before
auto shut off, the value is displayed when the
instrument is switched on. The blinking “ZERO”
means that a new zero has to be performed.
One fresh battery lasts for around 750 measurements, depending on the
light level.
The remaining battery capacity is evaluated at the instrument startup
and after each measurement.
The instrument displays a battery indicator with three levels as follows:
• 3 lines for 100 % capacity
• 2 lines for 66 % capacity
• 1 line for 33 % capacity
• Battery icon blinking if the capacity is under 10 %.
If the battery is empty and accurate measurements can’t be taken
anymore, the instrument shows “
To restart the instrument, the battery must be replaced with a fresh one.
To replace the instrument’s battery, follow the steps:
• Turn the instrument off by pressing ON/OFF.
• Turn the instrument upside down and remove the battery cover by
turning it counterclockwise.
• Extract the battery from its location and replace it with a fresh one.
• Insert back the battery cover and turn it clockwise to close.
and after 1 hour of non-use in
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dead batt” and turns off.
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calibration mode.
Accessories
REAGENT SETREAGENT SET
REAGENT SET
REAGENT SETREAGENT SET
HI 95747-01 Reagents for 100 tests
HI 95747-03 Reagents for 300 tests
OTHER ACCESORIESOTHER ACCESORIES
OTHER ACCESORIES
OTHER ACCESORIESOTHER ACCESORIES
HI 96747-11 CAL CHECK
TM
Standard Cuvettes (1 set)
HI 721310 9V battery (10 pcs.)
HI 731318 Cloth for wiping cuvettes (4 pcs.)
HI 731331 Glass cuvettes (4 pcs.)
HI 731335 Caps for cuvettes (4 pcs.)
HI 93703-50 Cuvette cleaning solution (230 mL)
Warranty
HI 96747 is warranted for two years against defects in workmanship and
materials when used for its intended purpose and maintained according
to the instructions.
This warranty is limited to repair or replacement free of charge.
Damages due to accident, misuse, tampering or lack of prescribed
maintenance are not covered.
If service is required, contact your dealer. If under warranty, report the
model number, date of purchase, serial number and the nature of the
failure. If the repair is not covered by the warranty, you will be notified
of the charges incurred.
If the instrument is to be returned to Hanna Instruments, first obtain a
Returned Goods Authorization Number from the Customer Service Department
and then send it with shipment costs prepaid. When shipping any
instrument, make sure it is properly packaged for complete protection.
To validate your warranty, fill out and return the enclosed warranty card
within 14 days from the date of purchase.
Recommendations for Users
Before using these products, make sure that they are entirely suitable for your specific application and for
the environment in which they are used.
Operation of these instruments may cause unacceptable interferences to other electronic equipments, this
requiring the operator to take all necessary steps to correct interferences.
Any variation introduced by the user to the supplied equipment may degrade the instrument’s EMC
performance.
To avoid damages or burns, do not put the instrument in microwave oven. For yours and the instrument
safety do not use or store the instrument in hazardous environments.
Hanna Instruments reserves the right to modify the
design, construction and appearance of its products
without advance notice.
For additional information, contact your
dealer or the nearest
Hanna Customer Service Center.
To find the Hanna Office in your area,
IST96747 07/11
www.hannainst.com
visit our web site
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