Hanna Instruments HI 93102 User Manual

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Instruction Manual
HI 93102
Multiparameter
Turbidity &
Ion Specific Meter
www.hannainst.com
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Dear Customer, Thank you for choosing a Hanna Product. Please read this instruction manual carefully
before using the instrument. This manual will provide you with the necessary
information for correct use of the instrument, as well as a precise idea of its versatility. If you need more technical information, do not hesi­tate to e-mail us at tech@hannainst.com.
This instrument is in compliance with direc­tives.
TABLE OF CONTENTS
General Description .................................... 4
Principle of Operation .................................. 6
Functional Description................................. 9
PRELIMINARY EXAMINATION
HI 93102 is supplied complete with:
Glass cuvet with cap
Batteries (4 x 1.5V AA)
Instruction manual
The HI 731327 complete maintenance kit is also available, including:
2 glass cuvets
Primary calibration standards: HI 93102-0 AMCO-AEPA-1 0 NTU* cali-
bration solution, 30 mL HI 93102-20 AMCO-AEPA-1 20 NTU* cali-
bration solution, 30 mL
• HI 93703-50 cleaning solution, 230 mL
Tissue for wiping cuvets
Rugged carrying case
Specifications ........................................... 13
Operational Guide ..................................... 14
Cali bra tio n................................................. 22
Diagnostic Mode ....................................... 3 0
Logging with C 102.................................... 31
User-selectable Auto-off ............................ 33
Battery Replacement ................................ 34
Diagnostic Codes...................................... 35
Accessories.............................................. 36
Warranty ................................................... 38
CE Declaration of Conformity .................... 39
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Note: Save all packing material until you are
sure that the instrument functions cor­rectly. Any defective item must be re­turned in its original packaging with the supplied accessories.
* 1 NTU (Nephelometric Turbidity Unit) = 1 FTU (For-
mazine Turbidity Unit)
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GENERAL DESCRIPTION
The Hanna HI 93102 is a portable micropro­cessor driven, multiparameter, turbidity and ion specific meter. It measures Free & Total Chlorine, Cyanuric Acid, pH, Iodine, Bromine, Low Range Iron and Turbidity.
In the colorimetric mode, the user can select either factory preprogrammed calibration set­tings or calibrate the meter using customized calibration values based on the concentration or relative absorbance of the sample. Calibra­tion data is also stored in a non-volatile EEPROM.
In the turbidity mode, periodic recalibration of the meter with primary standards according to regulatory requirements or personal experi­ence is suggested. Turbidity ranges are 0.00-
9.99 NTU and 10.0-50.0 NTU. HI 93102 complies with G.L.P. Standards
(Good Laboratory Practice), that is:
• When switched on, the LCD displays all segments (display check).
• Battery status is monitored during every measurement cycle warning the user if the batteries become weak.
In addition, HI 93102 will turn itself off before low voltage causes erroneous read­ings.
• It utilizes a real time clock and recalls calibration data such as date, time and calibration values.
There are eight keys for the different operationals modes. The large Liquid Crystal Display is dual-level: the upper level has four digits and can display the measured param­eter in hundredths. The lower level has three characters and indicates current mode (e.g. F CL for free chlorine or TR for turbidity). Different LCD segments indicate low battery, logging mode, date, time, etc.
A pure green LED has been utilized as a light source for both turbidimetric and colorimetric measurements. A silicon photocell is used to receive transmitted light from colorimetric chan­nel while another photocell receives scattered light from the turbidimetric (nephelometric) channel.
In order to measure colorimetric parameters, all the operator has to do is zero the blank sample and then add 1 packet of reagent (for Bromine, Chlorine, Cyanuric Acid, Iodine and Low Range Iron) or 0.2 mL of Phenol Red (for pH). After placing the cuvet back in the meter and pressing READ, the measurements are shown directly on the LCD.
The instrument operates with four AA batter­ies and may be operator-programmed to turn itself off automatically after 10, 20, 30, 40, 50 or 60 minutes of inactivity.
HI 93102 and all accessories such as sample vials, reagent pillows, primary standards, can be easily stored in the optional carrying case.
To facilitate field tests, the meter provides a logging mode. In this mode, the user can store up to twenty five time-tagged measure­ments in RAM and scroll the memory at any time.
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PRINCIPLE OF OPERATION
Turbidity Mode
surements according to the USEPA’s 180.1 method and the Standard Method 2130B.
The instrument functions by passing a beam of light through a vial containing the sample being measured.
The light source is a Pure Green LED to ensure that any interference caused by a colored samples is minimized.
A sensor, positioned at 90° with respect to the direction of light, detects the amount of light scattered by the undissolved particles present in the sample. The microprocessor converts such readings into NTU* values.
Colorimetric Mode
The color of every object we see is deter­mined by a process of absorption and emis­sion of the electromagnetic radiation (light) of its molecules.
Colorimetric analysis is based on the principle that specific compounds react with others to form a color, the intensity of which is proportional to the concentration of the substance being measured.
LED
EMITTED LIGHT
CUVET MICROPROCESSOR
Block diagram of an ion specific measurement
LIGHT
DETECTOR
When a substance is exposed to a beam of light intensity Io, a portion of the radiation is absorbed by the substance's molecules and a radiation of intensity I, lower than Io, is emitted.
The quantity of radiation absorbed is given by the Lambert-Beer Law:
log Io/I = ελ c d
NTU units are equal to FTU units. However, there are other known measurement units for turbidity, namely the Jackson Turbidity Unit (JTU) based on the old method of Jackson's candle, and Silica Unit (mg / L of SiO2). The conversion table between these measurement units is shown below:
JTU NTU/FTU SiO2 (mg/L)
JTU 1 19 2.5
NTU/FTU 0.053 1 0.13
SiO2 (mg/L) 0.4 7.5 1
6
* 1 NTU = 1 FTU
Where log Io/I = Absorbance (A)
ελ= molar extinction coefficient of the
substance at wavelength λ
c = molar concentration of the
substance
d = optical distance light travels
through the sample
Since other factors are known, the concen­tration "c" can be calculated from the color intensity of the substance determined by the emitted radiation I.
An LED (Light Emitting Diode) emits radiation at a relatively narrow spectrum, supplying the system with the intensity Io.
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A substance absorbs a color complimentary to the color it emits. For example, a substance appears yellow because it absorbs blue light. As a result, the Hanna meters use LED’s with specific wavelengths to measure samples.
The optical distance (d) is measured by the internal diameter of the cuvet containing the sample.
The photoelectric cell collects the radiation I that is not absorbed by the sample and converts it into an electric current.
The microprocessor converts the value into the desired measuring unit and displays it on the LCD.
The measurement process is done in two phases: setting the meter to zero and actual measurement.
The cuvet is an optical element and hence has an important role in the measurement process. Both the measurement and the calibration cuvets must be optically identical to provide the same measurement conditions.
It is also important that the surface of the cuvet is clean and free from scratches or dents, in order to avoid measurement interference due to unwanted reflection and absorption of light.
It is recommended that wherever possible the cuvet walls are not touched by the operator.
Furthermore, in order to maintain the same conditions during the zeroing and the measuring phases, it is necessary to close the cuvets to prevent any contamination.
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FUNCTIONAL DESCRIPTION
1) Primary LCD: The four-digit LCD shows
all segments for several seconds when the meter is switched on. It then dis­plays four dashes to indi­cate “ready to measure”. It is also the area where the date, time and value of last calibration are shown. In “Read” and “Zero” mode, “SIP” is shown to indicate “Sample
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In Progress”. The upper level also indicates the concentration or turbidity of the sample, as well as different diagnostic modes, such as “-BA-” for low bat­tery.
2) Secondary LCD: The three-digit LCD shows
the current mode of mea­surement that is “F CL”, “tCL”, “CY”, “PH”, “Id”, “Br”, “L FE”, “tr”, and di­agnostic or calibration modes, such as “d11”, “2 Fn”, “5c1”.
3) DATE: Indicates that the upper
level of LCD is showing the current date, the date of last calibration or the date of logged measure­ment in memory.
4) TIME: Indicates that the upper
level of LCD is showing the current time, the time of last calibration or the time of logged measure­ment in memory.
5) LOBAT: Blinking segment warns
user of low battery volt­age.
6) LOG: If intermittent, it indicates
that the user is in the scroll mode viewing the logged measurements. If fixed, it indicates that the meter is in the log mode and every reading taken will be stored in memory.
7) ON/OFF key: Turns the meter on and off.
8) ZERO / key: In ion specific (colorimet­ric) mode, it zeros the sample. In calibration and diagnostic modes, it func­tions as ENTER (not used in turbidity mode).
9) READ/ key: Takes the measuremnt of concentration/turbidity of the sample which is shown on the LCD. In diagnostic or calibration mode, shifts the flashing digit to the right.
10) CAL key: If pressed during calibra- tion, the calibration proce­dure will be aborted and the last calibration data will be reinstated. If pressed together with the ALT key for less then 3 seconds, the diagnostic mode will be entered. If pressed to­gether with the ALT key again, the meter will quit diagnostic mode. If pressed for more then 3 seconds, an intermittent “CAL” prompt will appear on the upper LCD level and the calibration proce­dure is entered.
11) GLP/Abs key: In ion specific mode, it will toggle concentration/ab­sorbance readings on the upper LCD. In turbidity mode, date, time and the two calibration values of the current mode will be
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shown. If pressed in time/date setup mode, the meter will quit current mode without making any changes to current time/ date.
12) key Scrolls upwards through the parameters to be mea­sured. In calibration/diag­nostic mode, increments the blinking digit by one. If pressed together with ALT while the meter is in logging mode, the upper LCD will show the data (date/time/value) in the memory.
13) ALT key: Alternative functions.
14) key: Scrolls downwards through the parameters to be mea­sured. In calibration/diag­nostic mode, decreases the blinking digit by one. If pressed together with ALT while the meter is in logging mode, the upper LCD will show the current lot number.
SPECIFICATIONS
HI 93102
Range Turbidity 0.00 to 50.0 NTU*
Bromine 0.00 to 8.00 mg/L
Free Cl
2
Total Cl
2
CYS 0 to 80 mg/L
Iodine 0.0 to 12.5 mg/L
LR Iron 0.00 to 1.00 mg/L
pH 5.9 to 8.5
Resolution
Turbidity 0.01 and 0.1 NTU*
Bromine 0.01 mg/L
Free Cl
2
Total Cl
2
CYS 1 mg/L
Iodine 0.1 mg/L
LR Iron 0.01 mg/L
pH 0.1
Accuracy
Turbidity ±0.5 NTU* or ±5% (whichever greater)
Bromine ±0.08 mg/L; ±3%
Free Cl
2
Total Cl
2
CYS ±1 mg/L; ±15%
Iodine ±0.1 mg/L; ±5%
LR Iron ±0.02 mg/L; ±3%
pH 0.1 pH Light Source Pure Green LED Light Source Life Life of the instrument Light Detector Two Silicon Photocells Power Source 4 x 1.5V AA alkaline batteries Battery Life 60 hours or 1000 measurements Auto-off Selectable after 10, 20, 30,
Environment 0 to 50°C (32 to 122°F)
Dimensions 220 x 82 x 66 mm
Weight 510 g (1.1 lb.)
0.00 to 2.50 mg/L
0.00 to 3.50 mg/L
0.01 mg/L
0.01 mg/L
±0.03 mg/L; ±3% ±0.03 mg/L; ±3%
40, 50 or 60 min. of non-use
RH max 95% (non-condensing)
(8.7 x 3.2 x 2.6")
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* 1 NTU = 1 FTU
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OPERATIONAL GUIDE
SET CURRENT TIME/DATE
To set or change the current time, turn on the meter. After initialization routine, the LCD will show:
CURRENT TIME/DATE RECALL
To recall current TIME/DATE press and hold the ALTand READ keys together. The current time and an intermittent “TIME” will be dis­played.
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Release the keys.
Press and hold the ALT and GLP keys to­gether. Display will show the current date in MM.DD format (e.g. August 28 is shown as
08.28).
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Release the keys. The month digits will blink. Make the necessary adjustments with the and keys. To skip to the day digits, press the key.
After the adjustments, press the key. The unit will store the newly set month-day data in its EEPROM and will show the current time by a 24 hour clock HH.MM format, e.g. 2:28 pm is:
Press and hold the ALT and READ keys again and the meter will show the current date together with an intermittent “DATE”.
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TURBIDITY MEASUREMENTS
Fill the vial with the sample. The surface of the vial should be clean and scratch free.
Turn the meter on. After the initialization rou­tine, the LCD will show:
Use the and keys to set the lower level of the LCD to turbidity (tr).
Similarly, make the necessary adjustments as described above and press . The newly set up “month - day - hour - minute” data will be stored in memory.
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Insert the sample into the cuvet holder and ensure that the notch on the cap is positioned securely into the groove.
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Press READ. The meter will intermittently display “SIP” on the upper level of the LCD.
The meter will show “SIP” for a few seconds and then a zero indication:
After a few seconds the display will show the turbidity value, e.g. 5.34 NTU:
COLORIMETRIC MEASUREMENTS
Turn the meter on. After the initialization rou­tine, the LCD will display:
Use the and keys to choose the desired param­eter:
F CL Free Chlorine t CL Total Chlorine CY Cyanuric Acid PH pH Id Iodine Br Bromine L FE Iron
Measuring Chlorine, Cyanuric Acid, pH, Iodine, Bromine
Fill the vial with the sample (blank). The surface of the vial should be clean and scratch free.
Insert the blank sample into the cuvet holder and ensure that the notch on the cap is posi­tioned securely into the groove. Press ZERO.
For pH, add 0.2 mL of HI 93710-01:
For Chlorine, Iodine and Bromine, add the content of their re­spective packet:
1 x
For Cianuric Acid only, add the con­tent of one packet of HI 93722 re­agent to a beaker filled up to the 25mL mark with unreacted sample up to the 25 mL mark. Stir gently to mix and then fill the cuvet up to
1.5 cm
1.5 cm (¾“) below the rim with 10 mL of the reacted sample.
Replace the cap, shake the cuvet and allow a few seconds for color to develop. For best results, wait 2½ mins. for Total Chlorine, Bro­mine, Iodine, and 45 secs. for Cyanuric Acid. Insert the reacted sample into the cuvet holder and ensure that the notch on the cap is posi­tioned securely into the groove. Press READ.
The meter will show “SIP” for a few seconds and then the concentration:
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Measuring Iron
Fill one graduated mixing cylin­der up to the 25 mL mark with deionized water.
Add the content of one packet of HI 93746 TPTZ reagent, close the cylinder and agitate for 30 seconds. This is the blank.
30"
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9
3
6
Fill a cuvet with 10 mL of
1.5 cm
the blank up to 1.5 cm (¾") below the rim and replace the cap.
Insert the blank into the cuvet holder and make sure that the notch on the cap is positioned securely into the groove. Press ZERO.
Add the content of one packet of HI 93746 TPTZ reagent, close the cylinder and agitate for 30 seconds.
30"
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9
3
6
Fill a cuvet with 10 mL of the reacted sample up to 1.5 cm
1.5 cm
(¾") below the rim and re­place the cap. This is the sample.
Insert the reacted sample into the cuvet holder and make sure that the notch on the cap is positioned securely into the groove. Wait 30” and then press READ.
The meter will show “SIP” for a few seconds and then a zero indication:
Fill one graduated mixing cyl­inder up to the 25 mL mark with the sample.
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The meter will show “SIP” for about a few seconds and then the concentration:
Note: To review the relative absorbance of
the sample, wait until the concentra­tion measurement is completed, and then press GLP/Abs. The display will show the absorbance in milliunits to-
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gether with the “Ab” indicator, e.g.: 533 Ab = 533 milliabs. units
Note: Absorbance readings may have a nega-
tive sign if the transmittance of the “ZERO” sample is less then that of the reacted sample.
Note: For better accuracy wash glassware
with HCl 6N.
Measurements in user-customized mode
Note: The meter must be calibrated for this
purpose. Follow the two-point custom­ized calibration on page 26 before proceeding.
Turn the meter on and by momentarily press­ing both ALT and CAL.
+
The LCD will show four dashes on the upper and “d 00” on the lower part of the LCD with the second “0” flashing:
Using the , and keys change the lower row of the display to show “d 11”:
Press the key. This key is also used as a toggle between (FCT) programmed functions. Select the USER mode (if necessary by pressing the key more than once):
USER
(USR) and
FACTORY
Press ALT and CAL until four dashes are displayed on the upper display and “# fn” are shown in the lower part of the LCD.
Using the and keys select the number from 0 to 7 where the appropriate calibration data have been stored. Add the appropriate reagent into the blank sample cuvet. Shake and allow a few sec­onds for color to develop.
Insert the reacted sample into the cuvet holder and make sure that the notch on the cap is positioned securely into the groove. Press READ.
The meter will first show “SIP” for a few seconds and afterwards the sample concen­tration:
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CALIBRATION
TURBIDITY CALIBRATION
The meter should be properly calibrated with a standard prepared as described in USEPA method 180.1.
Span calibration
To calibrate the span of the meter, fill the cuvet with the primary turbid­ity formazine standard of 50NTU.
Inspect and clean thoroughly the sur­face of the vial.
Shake the standard vigorously for a few seconds and wait a few minutes for the bubbles to disappear.
Turn the meter on and press both ALT and CAL momentarily.
The display will blink “-Lt-” for several sec­onds, indicating that the LED is being adjusted for the turbidimetric channel.
Afterwards, a sequence of numbers between
-511 to 512 will appear on the upper part of the LCD indicating different levels of LED light intensity.
In approximately one minute, the adjustment will be made and the calibration data stored in the non-volatile memory.
The display will show four dashes again indicating the end of the span cali­bration procedure.
Press the ALT and CAL keys together again to leave the diagnostic mode.
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The LCD will show four dashes on the upper and “d 00” on the lower part of the LCD with the second “0” blinking.
Using the , and keys change the lower row of the display to show “d 21”.
Insert the previously prepared 50 NTU stan­dard into the cuvet holder and make sure that the notch on the cap is positioned securely into the groove. Press .
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Two-point customized calibration
To enter the turbidity calibration mode, the meter should be in “turbidity” mode.
Use the and keys to set the lower level of the LCD to “tr”.
To enter the calibration mode, press and hold the ALT and CAL keys together for at least three seconds. The upper display will start flashing “CAL” for approximately three sec­onds.
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To confirm entry into the calibration mode, press the CAL key again while “CAL” is blinking.
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If the CAL key is not pressed, the upper dis­play will show “----”, in­dicating that calibration mode was not entered. In which case, hold down the ALT and CAL keys together for 3 seconds to restart the procedure.
After entering the cali­bration mode, the dis­play will show the first point of the previous calibration. The most significant digit will also be blinking.
Using the , , keys, set the turbidity of first calibration standard (from 0.00 to 50.0 NTU).
Insert the standard vial into the cuvet holder and ensure that the notch is positioned se­curely into the groove. Press the key. The display will indicate Sample In Progress (SIP).
After the first calibra­tion point is memo­rized, the LCD will indi­cate the second point of the previous calibration with the most sig­nificant digit blinking.
Using the , , keys, set the turbidity of the second calibration standard (from 0.00 to 50.0 NTU). Insert the standard into the cuvet holder and make sure that the notch is positioned securely into the groove. Press the key. The display will indicate “SIP” again.
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After the second calibration point is memo­rized, the unit will store the calibration data together with time and date in the EEPROM while intermittently indicating “CAL” and “Stor” for several seconds.
Subsequently, the up­per display will show “----”, indicating that the meter is calibrated and ready to measure turbidity of an unknown sample.
By pressing CAL during calibration, user can quit the calibration mode at any time without changing the previously stored calibration data.
COLORIMETRIC CALIBRATION
Zero calibration
To calibrate the span of the meter, fill the cuvet with a clean deionized water sample. Inspect and thoroughly clean the surface of the vial.
Turn the meter on and press both ALT and CAL momentarily.
+
The display will show four dashes and “d 00”. The second “0” will blink to allow the user to make a selection.
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Using , , keys set the lower part to “d 31”.
Insert the previously prepared deionized wa­ter standard into the cuvet holder and make sure that the notch on the cap is positioned securely into the groove. Press the key.
The display will blink “-Lc-” for several sec­onds, indicating that adjustment of the LED for the colorimetric measurements is in progress.
After this, a sequence of numbers between
-511 to 512 will appear on the upper LCD indicating the different levels of LED light intensity. In approximately one minute, the adjustment will be made and the calibration data will be stored in the non-volatile memory.
Display will show four dashes again indicating the end of the zero cali­bration procedure.
Press the ALT and CAL keys again to leave the diagnostic mode.
Two-point customized calibration
To enter the colorimetric calibration mode, press momentarily both the ALT and CAL keys. The LCD will show four dashes and “d00”.
+
+
Using the and keys, set the lower part of the LCD to “d 11” and then press the key.
The key is used as a toggle function in this mode and allows the user to select be­tween
USER
(USR) or
grammed functions.
Select the USER mode and press ALT and CAL keys together to leave the diagnostic mode. The display of the meter will indicate four dashes together with a number from 0 to 7 on the lower part of the LCD.
FACTORY
(FCT) pro-
+
Press and hold the ALT and CAL keys to­gether for at least three seconds. The upper display will start flashing “CAL” for approxi­mately three seconds.
+
To confirm entry into the calibration mode, press the CAL key again while “CAL” is still blinking.
If the CAL key is not pressed, the upper row of the display will show “----”, indicating that the calibration mode was not entered. In which case, hold down the ALT and CAL keys together for 3 seconds to restart the procedure.
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After entering the cali­bration mode, the dis­play will show the first point of the previous calibration with the most significant digit blinking.
Using the , and keys, choose the concentration of the first calibration standard.
Insert the known standard into the cuvet holder and make sure that the notch is positioned securely into the groove. Press the key. The display will indicate sample in progress.
After the first calibra­tion point is memo­rized, the LCD will indi­cate the second point of the previous calibration with the most sig­nificant digit blinking.
Using the , , keys, choose the known concentration of the second calibration stan­dard.
Insert the standard into the cuvet holder and make sure that the notch is positioned se­curely into the groove. Press the key. The display will blink “SIP” again.
Subsequently, the up­per display will show “----”, indicating that the meter is calibrated and ready to measure the concentration of an unknown sample.
By pressing the CAL key during calibration, user can leave the cali­bration mode at any time without changing the previously stored calibration data.
After the second calibration point is memo­rized, the unit will store the calibration data, time and date in the EEPROM while intermit­tently indicating “CAL” and “Stor” for several seconds.
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DIAGNOSTIC MODE
HI 93102 facilitates operations by providing a
diagnostic mode. In this mode, user can set or verify different parameters necessary to ensure optimum performance of the meter. To enter the diagnostic mode, turn the meter on and momentarily press ALT and CAL to­gether. The display will show four dashes to­gether with “d 00”:
+
Using the , and keys, select the re­quired diagnostic mode and press the key. The meter will execute one of the following user-diagnostic functions:
10 Customizes automatic shutdown 11 Selects User or Factory functions 12 Turns logging mode on or off 21 Calibrates span in turbidimetric mode 31 Calibrates span in colorimetric mode 40 Clears the logged memory
To quit diagnostic mode, press the ALT and CAL keys together again.
LOGGING WITH C 102
HI 93102 allows user to log 25 time/day-tagged
measurements. User can easily turn the log­ging mode on and off, review the logged memory, review the current lot number and clean the buffer (memory). C 102 also re­minds user if its memory is full.
TURNING THE LOG MODE ON OR OFF
Enter the diagnostic mode by pressing ALT and CAL together.
Select mode 12 and press the key.
The display will show the current (vacant) lot together with “LOG” if the log mode is on. Otherwise it will show “----” if the log mode is off.
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The following diagnostic modes are reserved for authorized service technicians:
00 Shows the 01 Shows the 02 Shows the 05 Shows the 06 Shows 5V on-board level 07 Shows battery voltage level 08 Shows 1.23V reference voltage level 09 Shows -5V on-board level 99 Shows software version number
Blank
level in colorimetric mode
Sample
level in colorimetric mode
Dark
level in colorimetric mode
Ground
voltage
30
By pressing the key, the meter toggles between the Log on and off positions. If the log on mode is selected, every time a mea­surement is taken (READ pressed) the rel­evant values will be stored in the current (vacant) lot number.
To quit diagnostic mode, press the ALT and CAL keys together again.
The LCD will then show “diAG” and “Stor” for a few seconds. If the log on mode was selected “LOG” will appear on the bottom left hand side
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of the display to remind the user that every time a measurement is taken, the value is stored in the next available lot number.
REVIEWING THE LOGGED BUFFER
To review the memo­rized values, press to-
gether ALT and .
+
To clear the buffer, press the ALT and CAL keys.
Select mode 40. Press the key. The dis­play will show the “Cln” message, indicating that memory is being cleaned.
+
The meter will scroll all the data in the buffer showing the lot number, value, date and time.
e.g. The first recorded reading in the buffer is
lot # 0, 0.35 mg/L of Iron, memorized on 23rd August at 3:34 pm;
The second logged data relates to lot # 1, 1.35 mg/L of the customized param­eter, logged on 23rd August at 3:55 pm.
First lot Second lot
The lot number will be reset to 00 automatically.
REVIEWING THE CURRENT LOT NUMBER
To check the current (vacant) lot number, while in log mode, press ALT and to­gether.
USER-SELECTABLE AUTO-OFF
With HI 93102, the users can customize the shutdown time to save power.
To change the shutdown time, enter the diagnos­tic mode by momentarily pressing the ALT and CAL keys together.
Select mode 10 and press the key repeat­edly to set the desired shutdown time from 10 to 60 minutes with 10 minute increments, or disable the shutdown mode by choosing the OFF selection.
+
CLEARING THE MEMORY
After all the buffer (memory) is taken up, the LCD will blink “Full”.
32
After the selection is com­pleted, exit the diagnos­tic mode by pressing ALT+CAL together.
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The meter will store new settings in its non­volatile memory and the display will flash “diAG” and “Stor” alternatively for several sec­onds.
BATTERY REPLACEMENT
A “LOBAT” indication appears on the lower right hand side of the display when the bat­teries are weak and require replacement. At this point the instrument is still able to per­form approximately 50 additional measure­ments.
A “-BA-” indication will appear on the display when the batteries are too weak to perform accurate measurements. This message ap­pears for a few seconds and then the meter will completely switch itself off. At this point the batteries must be replaced.
Batteries should only be replaced in a safe area using 1.5V AA al­kaline type.
In order to replace the batteries, simply re­move the two screws on the rear cover of the instrument and replace all four 1.5V AA batter­ies with new ones, while paying attention to their polarity.
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DIAGNOSTIC CODES
LOBAT Weak batteries. Change all batter-
ies as soon as possible.
-BA- Exhausted batteries. Change all batteries immediately.
-LO- Low level of light is received during the zeroing procedure. Check for scratches on the cuvet and ensure that sample is not ex­cessively turbid. Repeat the read­ings. If the problem persists, recalibrate the meter using deion­ized water in the diagnostic mode “31” (see Calibration).
-CAP- Light intensity is high during last measurement. Make sure the cuvet is capped and placed properly in the holder, and that ambient light does not reach the photodetector. Repeat the measurement. If the problem persists, contact your dealer or the nearest Hanna Office.
Er 1 Hardware error. Repeat the mea-
surement. If the error message ap­pears again, contact your dealer or the nearest Hanna Office.
rnG Out of range. Check the measuring
procedure and verify the concentration of the sample to ensure that is not too high.
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ACCESSORIES
HI 731327 Maintenance kit: rugged
carrying case including HI93102-0 and HI93102-20 calibration solutions, HI 93703-50 cuvet cleaning solution, one tissue for wiping cuvets and two cuvets
HI 93102-0 AMCO-AEPA-1 @ 0 NTU*
calibration solution, 30 mL
HI 93102-20 AMCO-AEPA-1 @ 20 NTU*
calibration solution, 30 mL
HI 93701-01 Reagents for 100 Free Chlo-
rine tests
HI 93701-03 Reagents for 300 Free Chlo-
rine tests
HI 93703-50 Cuvet cleaning solution, 230
mL bottle
HI 93710-01 Reagents for 100 pH tests HI 93710-03 Reagents for 300 pH tests HI 93711-01 Reagents for 100 Total Chlo-
rine tests
HI 93711-03 Reagents for 300 Total Chlo-
rine tests
HI 93716-01 Reagents for 100 Bromine
tests
HI 93716-03 Reagents for 300 Bromine
tests
HI 93718-01 Reagents for 100 Iodine tests HI 93718-03 Reagents for 300 Iodine tests HI 93722-01 Reagents for 100 Cyanuric
Acid tests
HI 93722-03 Reagents for 300 Cyanuric
Acid tests
HI 93746-01 Reagents for 100 Low Range
Iron tests
HI 93746-03 Reagents for 300 Low Range
Iron tests
HI 731318 Tissue for wiping cuvets
(4 pcs)
36
* 1 NTU = 1 FTU.
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Page 20
WARRANTY
Hanna Instruments meters are guaranteed for two years against defects in workman-
ship and materials when used for their in­tended purpose and maintained according to instructions.
This warranty is limited to repair or replace­ment free of charge. Damages due to acci­dents, misuse, tampering or lack of prescribed maintenance are not covered.
If service is required, contact the dealer from whom the instrument was purchased. If under warranty, report the model number, date of purchase, serial number and the nature of the failure. First obtain a Returned Goods Autho­rization number from the Customer Service department and then return the instrument indicating the Authorization # with shipment costs prepaid.
If the repair is not covered by the warranty, you will be notified of the charges.
When shipping any instrument, make sure it is properly packaged for complete protection.
CE DECLARATION OF CONFORMITY
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
Hanna Instruments reserves the right to modify the design, construction and appear­ance of its products without advance notice.
38
Recommendations for Users
Before using this product, make sure that it is entirely suitable for the environment in which it is used.
Operation of this instrument in residential areas could cause unacceptable interfer­ence to radio and TV equipment, requiring the operator to take all necessary steps to correct the interference.
Any variation introduced by the user to the supplied equipment, may degrade the instrument's EMC performance.
To avoid electrical shocks, do not use this instrument when voltage at the measure­ment surface exceeds 24 Vac or 60 Vdc.
To avoid damage or burns, do not perform any measurement in microwave ovens.
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Page 21
SALES AND TECHNICAL SERVICE CONTACTS
Australia:
Tel. (03) 9769.0666 • Fax (03) 9769.0699
China:
Tel. (10) 88570068 • Fax (10) 88570060
Egypt:
Tel. & Fax (02) 2758.683
Germany:
Tel. (07851) 9129-0 • Fax (07851) 9129-99
Greece:
Tel. (210) 823.5192 • Fax (210) 884.0210
Indonesia:
Tel. (21) 4584.2941 • Fax (21) 4584.2942
Japan:
Tel. (03) 3258.9565 • Fax (03) 3258.9567
Korea:
Tel. (02) 2278.5147 • Fax (02) 2264.1729
Malaysia:
Tel. (603) 5638.9940 • Fax (603) 5638.9829
Singapore:
Tel. 6296.7118 • Fax 6291.6906
South Africa:
Tel. (011) 615.6076 • Fax (011) 615.8582
Taiwan:
Tel. 886.2.2739.3014 • Fax 886.2.2739.2983
Thailand:
Tel. 66.2619.0708 • Fax 66.2619.0061
United Kingdom:
Tel. (01525) 850.855 • Fax (01525) 853.668
USA:
Tel. (401) 765.7500 • Fax (401) 765.7575
For e-mail contacts and complete list of Sales and Technical offices, please see www.hannainst.com
MANC102R4 07/05
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