Hanna Instruments HI 8733 User Manual

Instruction Manual
HI 8633
HI 8733 - HI 8734
Reliable and Waterproof
Multi-Range
Conductivity Meters
www.hannainst.com
Dear Customer, Thank you for choosing a Hanna Product. Please read this instruction
manual carefully before using the instrument. It will provide you with the necessary information for a correct use of the instrument, as well as a more precise idea of its versatility.
If you need additional technical information, do not hesitate to e-mail us at tech@hannainst.com.
These instruments are in compliance with the directives.
PRELIMINARY EXAMINATION
Remove the instrument from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any noticeable damage, notify your Dealer or the nearest Hanna office immediately.
Each meter is supplied with:
• Conductivity probe with DIN connector and 1 m (3.3') cable:
HI 76301D for HI 8633 and HI 8734
HI 76302W for HI 8733
• Calibration solution sachet
• Screwdriver, 1 x 9V battery and instruction manual
Note: Save all packing materials until you are sure that the
instrument functions correctly. Any damaged or defective item must be returned in its original packing materials together with the supplied accessories.
TABLE OF CONTENTS
PRELIMINARY EXAMINATION ...................................................... 3
GENERAL DESCRIPTION .............................................................. 3
FUNCTIONAL DESCRIPTION & SPECIFICATIONS OF HI 8633........ 4
FUNCTIONAL DESCRIPTION & SPECIFICATIONS OF HI 8733........ 5
FUNCTIONAL DESCRIPTION & SPECIFICATIONS OF HI 8734........ 6
OPERATIONAL GUIDE ................................................................. 7
CALIBRATION............................................................................. 8
CONDUCTIVITY VERSUS TEMPERATURE CHART ........................... 12
TDS VERSUS TEMPERATURE CHART ........................................... 13
DETERMINING THE TEMPERATURE COEFFICIENT OF A SOLUTION
(HI 8733) ............................................................................... 14
PROBE MAINTENANCE .............................................................. 15
BATTERY REPLACEMENT ............................................................ 16
ACCESSORIES ........................................................................... 17
WARRANTY .............................................................................. 18
CE DECLARATION OF CONFORMITY............................................ 19
GENERAL DESCRIPTION
32
FUNCTIONAL DESCRIPTION &
SPECIFICATIONS OF HI 8633
FUNCTIONAL DESCRIPTION &
SPECIFICATIONS OF HI 8733
1) Liquid Crystal Display
2) Conductivity/temperature selection key
3) Measurement range selection keys
4) Manual temperature compensation knob
5) ON/OFF key
Range 0.0 to 199.9 / 0 to 1999 µS/cm
0.00 to 19.99 / 0.0 to 199.9 mS/cm
Resolution 0.1 / 1 µS/cm
0.01 / 0.1 mS/cm
Accuracy ±1% Full Scale (@ 20°C/68°F) excluding probe error
Typical EMC ±2% Full Scale Deviation
Calibration Manual, 1 point, through trimmer Temperature Manual, 0 to 50°C (32 to 122°F)
Compensation with β = 2%/°C Probe (included) HI 76301D with 1m (3.3') cable Environment 0 to 50°C (32 to 122°F);
RH max 100%
Battery Type 1 x 9V, alkaline (IEC 6LR61) Life Approx. 100 hours of continuous use
Dimensions 164 x 76 x 45 mm (6.5 x 3.0 x1.8") Weight 250 g (8.8 oz.)
1) Liquid Crystal Display
2) Measurement range selection keys
3) Automatic Temperature Compensation coefficient knob
4) ON/OFF key
Range 0.0 to 199.9 / 0 to 1999 µS/cm
0.00 to 19.99 / 0.0 to 199.9 mS/cm
Resolution 0.1 / 1 µS/cm
0.01 / 0.1 mS/cm
Accuracy ±1% Full Scale (@ 20°C / 68°F) excluding probe error
Typical EMC ±2 % Full Scale Deviation
Calibration Manual, 1 point, through trimmer Temperature Automatic, 0 to 50°C (32 to 122°F) with
Compensation β adjustable from 0 to 2.5% per °C Probe (included) HI 76302W ATC with 1m (3.3') cable Environment 0 to 50°C (32 to 122°F);
RH max 100%
Battery Type 1 x 9V, alkaline (IEC 6LR61) Life Approx. 100 hours of continuous use
Dimensions 164 x 76 x 45 mm (6.5 x 3.0 x1.8") Weight 250 g (8.8 oz.)
54
FUNCTIONAL DESCRIPTION &
SPECIFICATIONS OF HI 8734
1) Liquid Crystal Display
2) Measurement range selection keys
3) Manual temperature compensation knob
4) TDS/temperature selection key
5) ON/OFF key
Range 0.0 to 199.9 / 0 to 1999 mg/L
0.00 to 19.99 g/L
Resolution 0.1 / 1 mg/L
0.01 g/L
Accuracy ±1% Full Scale (@ 20°C / 68°F) excluding probe error
Typical EMC ±2 % Full Scale Deviation
Calibration Manual, 1 point, through trimmer Temperature Manual, 0 to 50°C (32 to 122°F)
Compensation with β = 2%/°C TDS factor 0.5 Probe (included) HI 76301D with 1m (3.3') cable Environment 0 to 50°C (32 to 122°F); RH max 100% Battery Type 1 x 9V, alkaline (IEC 6LR61)
Life Approx. 100 hours of continuous use Dimensions 164 x 76 x 45 mm (6.5 x 3.0 x1.8") Weight 250 g (8.8 oz.)
OPERATIONAL GUIDE
• Each meter is supplied complete with a 9V battery. Remove the battery compartment cover on the back of the meter (see page 16). Install the battery while paying attention to its polarity.
• Connect the probe to the meter securely by aligning the pins with the socket and pushing the plug in.
• Make sure that the meter has been calibrated before taking any measurements (see "Calibration" section).
• Immerse the conductivity probe into the sample, with the holes on the shaft completely submerged.
If possible, use plastic beakers or con­tainers to minimize any EMC interference.
• Tap the probe lightly on the bottom of the beaker to remove any air bubbles which may be trapped inside the PVC sleeve.
• Turn the instrument on by pressing the ON/OFF key.
• For HI 8633 and HI 8734:
Take the temperature of the solution with a ChecktempC or another accurate thermometer.
Press the COND/TEMP key for HI 8633 or TDS/TEMP for HI 8734 to display the temperature and adjust the temperature knob to that of the solution e.g. 20°C.
COND. TEMP.
TDS
TEMP.
ºC
• For HI 8733:
Adjust the TEMPERATURE COEFFICIENT knob to 2% to compensate for the temperature effect of average solutions (to determine exact value for a particu-
TEMPERATURE COEFFICIENT
lar solution, see page 14).
°C
2.5
0
2
0.5
1.51
76
• Select the appropriate measurement range. Note: If the display shows only a "1" on the
far left hand side, the meter is out of range. Select the next (higher) range.
• Wait for a couple of minutes for the temperature sensor to reach thermal equilibrium with the sample before taking measure­ments.
• After the measurement has been completed, the instrument should be switched off and the probe should be cleaned and dried (see "Probe Maintenance" on page 15).
CALIBRATION
air bubbles remain trapped in the sleeve.
• Record the temperature of the buffer solution from the thermom­eter (e.g. 18°C).
• Switch the instrument on by pressing ON/OFF.
• Press COND/TEMP (HI 8633) or TDS/TEMP (HI 8734) to display
COND.
TEMP.
ON
OFF
TDS
TEMP.
the temperature.
• Adjust the TEMPERATURE knob to display 18°C.
Accessories needed:
• Use any calibration solution within the meter's range. The solution should ideally be close to the samples being mea­sured. Use for example HI 7030 or HI 8030, 12880 µS/cm (=12.88 mS/cm) conductivity solution, for HI 8633 and HI 8733, and HI 7032, 1382 mg/L (=2764 µS/cm) TDS solution, for HI 8734.
• ChecktempC or another accurate thermometer with 0.1°C resolution (not necessary for HI 8733).
• a small screwdriver.
PROCEDURE FOR HI 8633 AND HI 8734
• Pour sufficient quantity of a conductivity (HI 8633) or TDS (HI 8734) calibration solution (e.g. HI 7030 or HI 7032) into a beaker to cover the holes on the probe. If possible, use plastic beakers to mini­mize any EMC interference.
• Immerse the conductivity probe, making sure that holes are completely submerged, and the ChecktempC in the solution.
• Wait for a couple of minutes for thermal equilibrium to be reached.
• Tap the probe on the bottom, then shake it while rotating to make sure no
TEMPERATURE
• Press COND/TEMP (or TDS/TEMP) again to display conductivity mea-
COND.
TEMP.
TDS
TEMP.
surement.
• Select 19.99 mS/cm (HI 8633) or 1999 mg/L (HI 8734) range
19.99 mS
1999
mg/l
by pressing the appropriate range key.
• Remove the battery compartment cover and adjust the calibration trimmer located inside with the calibration screwdriver until the display shows for HI 8633 the conductivity reading at 25°C (see the conductivity vs. temperature table), e.g. @ 25°C, 12880 µS/ cm = 12.88 mS/cm, or for HI 8734 the TDS reading at 25°C
HI 7030
°C
(see the TDS vs. temperature chart), e.g. @25°C, 1382 mg/L.
98
• All subsequent measurements will be compensated to 25°C (77°F). If you prefer to standardize the temperature compensation to
20°C (68°F) rather than 25°C (77°F), leave the TEMPERATURE knob at 18°C (if the temperature of the solution is 18°C), adjust the trimmer to read "11.67 mS" (see the conductivity vs. tem­perature chart) or "1251 mg/L" (see the TDS vs. temperature chart). All subsequent measurements will be compensated to 20°C.
• The calibration is now complete and the instrument is ready for use.
The instrument should be recalibrated at least once a month, or when the probe is changed.
Note: For more accurate results, it is advisable to use a calibration
solution close to the measurement range. See the "Accessories" section for a wide selection of conductivity solutions.
PROCEDURE FOR HI 8733
• Pour sufficient quantity of a conductivity calibration solution (e.g. HI 7030/ HI 8030) into a beaker to cover the holes on the probe. If possible, use plastic beakers to minimize any EMC interfer­ence.
• Immerse the conductivity probe in the solution, making sure that holes are com­pletely submerged.
• Wait for a couple of minutes for thermal equilibrium to be reached.
• Tap the probe on the bottom, then shake it while rotating to make sure no air bubbles remain trapped in the sleeve.
• Switch the instrument on by pressing ON/OFF.
• Set the temperature coefficient knob to 2% to compensate for the temperature effect of average solutions (to determine exact value for a particular solution, see
0
0.5
TEMPERATURE COEFFICIENT
page 14).
• Select 19.99 mS/cm range by pressing the appropriate range key.
HI 7030
ON
OFF
2.5
2
1.51
19.99 mS
• Remove the battery compartment cover and adjust the calibration trimmer located inside with the calibration screwdriver until the display shows "12.88 mS" i.e. the conductivity reading @ 25°C.
• All subsequent measurements will be compensated to 25°C (77°F). If you prefer to standardize the temperature compensation to
20°C (68°F) rather than 25°C (77°F), adjust the trimmer to read "11.67 mS" (see the conductivity vs. temperature chart on page
18). All subsequent measurements will be compensated to 20°C.
• The calibration is now complete and the instrument is ready for use.
The instrument should be recalibrated at least once a month, or when the probe is changed.
Note: For more accurate results, it is advisable to use a calibration
solution close to the range to be measured. See the "Accesso­ries" section for a wide selection of conductivity solutions.
1110
CONDUCTIVITY VERSUS
TEMPERATURE CHART
TDS VERSUS
TEMPERATURE CHART
The conductivity of an aqueous solution is the measure of its ability to carry an electrical current by means of ionic motion.
The conductivity invariably increases with increasing temperature. It is affected by the type and number of ions in the solution and by
the viscosity of the solution itself. Both parameters are temperature dependent. The dependency of conductivity on temperature is ex­pressed as a relative change per degree Celsius at a particular temperature, commonly as percent per °C.
For manual temperature compensation, refer to the following chart:
°C °F HI 7030 HI 7031 HI 7033 HI 7034 HI 7035 HI 7039
HI 8030 HI 8031 HI 8033 HI 8034 HI 8035 HI 8039
(µS/cm) (µS/cm) (µS/cm) (µS/cm) (µS/cm) (µS/cm)
0 32 7150 776 64 48300 65400 2760
5 41 8220 896 65 53500 74100 3180 10 50 9330 1020 67 59600 83200 3615 15 59 10480 1147 68 65400 92500 4063 16 60.8 10720 1173 70 67200 94400 4155 17 62.6 10950 1199 71 68500 96300 4245 18 64.4 11190 1225 73 69800 98200 4337 19 66.2 11430 1251 74 71300 100200 4429 20 68 11670 1278 76 72400 102100 4523 21 69.8 11910 1305 78 74000 104000 4617 22 71.6 12150 1332 79 75200 105900 4711 23 73.4 12390 1359 81 76500 107900 4805 24 75.2 12640 1386 82 78300 109800 4902
25 77 12880 1413 84 80000 111800 5000
26 78.8 13130 1440 86 81300 113800 5096 27 80.6 13370 1467 87 83000 115700 5190 28 82.4 13620 1494 89 84900 117700 5286 29 84.2 13870 1521 90 86300 119700 5383 30 86 14120 1548 92 88200 121800 5479 31 87.8 14370 1575 94 90000 123900 5575
For instance, the conductivity values of the calibration solutions at 25°C are 12880 µS/cm, 1413 µS/cm or 5000 µS/cm when using HI 7030, HI 7031 or HI 7039, respectively.
At 20°C, the values are 11670 µS/cm, 1278 µS/cm or 4523 µS/cm, respectively.
With the solutions at 30°C, the values are 14120 µS/cm, 1548 µS/ cm or 5479 µS/cm, respectively.
The TDS value in aqueous solutions is directly proportional to conduc­tivity. The ratio between the two parameters depends on the solution and usually it is set to a factor of 0.5 (corresponding to a solution of CaCO3). This means that 1 µS/cm is equal to 0.5 mg/L (ppm) of TDS.
For manual temperature compensation, refer to the following chart:
° C ° F HI 7032 HI 7036
mg/L g/L
(ppm) (ppt)
0 32 758 6.82
5 41 876 7.88 10 50 999 8.99 15 59 1122 10.10 16 60.8 1148 10.33 17 62.6 1173 10.56 18 64.4 1200 10.78 19 66.2 1224 11.01 20 68 1251 11.24 21 69.8 1277 11.47 22 71.6 1303 11.71 23 73.4 1329 11.94 24 75.2 1358 12.18
25 77 1382 12.41
26 78.8 1408 12.65 27 80.6 1438 12.89 28 82.4 1461 13.13 29 84.2 1476 13.37 30 86 1515 13.61 31 87.8 1541 13.85
For instance, the TDS values of the calibration solutions at 25°C are 1382 mg/L or 12.41 g/L when using HI 7032 or HI 7036, respectively.
At 20°C, the values are 1251 mg/L or 11.24 g/L, respectively. With the solutions at 30°C, the values are 1515 mg/L or 13.61 g/L,
respectively.
1312
DETERMINING THE TEMPERATURE
COEFFICIENT OF A SOLUTION (HI 8733)
PROBE MAINTENANCE
Highly acidic, alkaline samples or solutions with high salt content might have a different coefficient than the customary 2% per degree °C.
In order to calculate this coefficient follow the procedure below:
• Immerse the probe of HI 8733 in the sample and adjust the TEMPERATURE COEFFICIENT knob to 0% (i.e. no compensation).
2.5
0
2
0.5
TEMPERATURE COEFFICIENT
1.51
• Condition the sample and probe to 25°C and note the conductiv­ity reading, C25.
• Condition the sample and probe to a different temperature t°C (approximately 10°C different from 25°C) and note the conduc­tivity reading Ct.
• The temperature coefficient β of the solution is calculated as given by the following formula:
β = 100 x
(Ct - C25)
(t - 25) x C
25
The above procedure is suitable for determining the temperature coefficient in a laboratory or where the temperature of the solution can be controlled.
If this is not possible (e.g. on-site measurements), the following procedure can be used providing the sample temperature varies by at least 5°C or preferably 10°C:
• Immerse the probe of HI 8733 in the test solution and turn the TEMPERATURE COEFFICIENT knob to 0% (no compensation).
• Check the conductivity reading and record the value. Make sure the reading is stable, i.e. no greater variations than ±0.2 mS/ cm within a minute.
• Repeat the procedure when the temperature of the test solution has changed by at least 5°C. Wait for the conductivity reading to stabilize.
• Adjust the TEMPERATURE COEFFICIENT knob until the display shows the same value as recorded earlier.
• The value indicated by the knob is the temperature coefficient of the solution.
Rinse the probe with tap wa­ter after every series of measurements. If a more thor­ough cleaning is required, remove the PVC sleeve and clean the probe with a cloth or a nonabrasive detergent. When reinserting the sleeve onto the probe, be sure that the sleeve is in the right direc­tion with the four holes towards the cable end.
After cleaning the probe, recalibrate the instrument.
The probe body is in PVC. For this reason it must never come into close contact with a heat source. If the probe is exposed to high temperatures (above 50°C/122°F), the rings might become loose or detached, re­sulting in a serious impairment of the probe. In such cases, the probe has to be replaced.
1514
BATTERY REPLACEMENT
ACCESSORIES
When the battery becomes weak the meters will display an additional blinking decimal point.
When the low battery indicator appears, the battery has only a few hours left. A low battery will result in unreliable measurements.
It is recommended to replace the battery immediately. Battery replacement must only take place in a nonhazardous area
using a 9V alkaline battery. Unscrew the three screws on the rear of the meter, remove the battery
compartment cover and replace the 9V battery with a new one.
CALIBRATION SOLUTIONS
HI 7030L 12880 µS/cm, 500 mL bottle HI 7030M 12880 µS/cm, 230 mL bottle HI 7031L 1413 µS/cm, 500 mL bottle HI 7031M 1413 µS/cm, 230 mL bottle HI 7033L 84 µS/cm, 500 mL bottle HI 7033M 84 µS/cm, 230 mL bottle HI 7034L 80000 µS/cm, 500 mL bottle HI 7034M 80000 µS/cm, 230 mL bottle HI 7035L 111800 µS/cm, 500 mL bottle HI 7035M 111800 µS/cm, 230 mL bottle HI 7039L 5000 µS/cm, 500 mL bottle HI 7039M 5000 µS/cm, 230 mL bottle HI 7032L 1382 ppm (mg/L), 500 mL bottle HI 7032M 1382 ppm (mg/L), 230 mL bottle HI 7036L 12.41 ppt (g/L), 500 mL bottle HI 7036M 12.41 ppt (g/L), 230 mL bottle
CONDUCTIVITY PROBES
HI 76301D Conductivity probe with 1m (3.3') cable and DIN
connector
HI 76302W Conductivity probe with built-in temperature sensor,
1m (3.3') cable and DIN connector
Make sure the battery contacts are tight and secure before replacing the cover.
OTHER ACCESSORIES
ChecktempC Electronic thermometer (range: -50.0 to 150.0°C)
HI 710015 Shockproof rubber boot, blue HI 710016 Shockproof rubber boot, orange HI 710022 Spare protective case
1716
WARRANTY
All Hanna Instruments meters are warranted for two years against defects in workmanship and materials when used for their intended purpose and maintained according to instructions. The probes are warranted for a period of six months. This warranty is limited to repair or replacement free of charge.
Damages due to accident, misuse, tampering or lack of prescribed maintenance are not covered.
If service is required, contact the dealer from whom you purchased the instrument. If under warranty, report the model number, date of purchase, serial number and the nature of the failure. If the repair is not covered by the warranty, you will be notified of the charges incurred. If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization number from the Cus­tomer Service department and then send it with shipping costs prepaid. When shipping any instrument, make sure it is properly packaged for complete protection.
All rights are reserved. Reproduction in whole or in part is prohibited without the written consent of the copyright owner.
CE DECLARATION OF CONFORMITY
Hanna Instruments reserves the right to modify the design, construction and
appearance of its products without advance notice.
Recommendations for Users
Before using these products, make sure that they are entirely suitable for the environment in which they are used. Operation of these instruments in residential area could cause unacceptable interference to radio and TV equipment, requiring the operator to take all necessary steps to correct interferences. The metal band at the end of the probe is sensitive to electrostatic discharges. Avoid touching this metal band at all times. Any variation introduced by the user to the supplied equipment may degrade the instruments' EMC performance. To avoid electrical shock, do not use these instruments when voltages at the measurement surface exceed 24 Vac or 60 Vdc. Use plastic beakers to minimize any EMC interferences. To avoid damage or burns, do not perform any measurement in microwave ovens.
1918
SALES AND TECHNICAL SERVICE CONTACTS
Australia:
Tel. (03) 9769.0666 • Fax (03) 9769.0699
China:
Tel. (10) 88570068 • Fax (10) 88570060
Egypt:
Tel. & Fax (02) 2758.683
Germany:
Tel. (07851) 9129-0 • Fax (07851) 9129-99
Greece:
Tel. (210) 823.5192 • Fax (210) 884.0210
Indonesia:
Tel. (21) 4584.2941 • Fax (21) 4584.2942
Japan:
Tel. (03) 3258.9565 • Fax (03) 3258.9567
Korea:
Tel. (02) 2278.5147 • Fax (02) 2264.1729
Malaysia:
Tel. (603) 5638.9940 • Fax (603) 5638.9829
Singapore:
Tel. 6296.7118 • Fax 6291.6906
South Africa:
Tel. (011) 615.6076 • Fax (011) 615.8582
Taiwan:
Tel. 886.2.2739.3014 • Fax 886.2.2739.2983
Thailand:
Tel. 66.2619.0708 • Fax 66.2619.0061
United Kingdom:
Tel. (01525) 850.855 • Fax (01525) 853.668
USA:
Tel. (401) 765.7500 • Fax (401) 765.7575
For e-mail contacts and complete list of Sales and Technical offices, please see www.hannainst.com
MAN33R2 06/05
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