Hanna Instruments HI 38082 User Manual

Instruction Manual
HI 38082
Potassium
Test Kit for
Soil
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Dear Customer, Thank you for choosing a Hanna Product. Please read the instruction sheet carefully before using the
test kit. It will provide you with the necessary information for correct use of the kit. If you need additional information, do not hesitate to e-mail us at tech@hannainst.com.
Remove the chemical test kit from the packing material and examine it carefully to make sure that no damage has occurred during shipping. If there is any noticeable dam­age, notify your Dealer or the nearest Hanna office immediately.
Each kit is supplied with:
Formaldehyde Solution, 4 bottles with dropper (4 x 25 mL);
• HI 38082A-0 Alkaline Solution, 3 bottles (3 x 100 mL);
• HI 38082B-0 Potassium Reagent, packets (100 pcs);
• 1 long glass test tube (50 mL);
•1 calibrated plastic vessel (50 mL);
•1 long plastic pipette (1 mL);
• 1 plastic pipette (3 mL);
•1 syringe (1 mL) with tip;
• 1 spoon; 1 graduated card;
• 1 point card.
Note: Any damaged or defective item must be returned in
its original packing materials.
SPECIFICATIONSSPECIFICATIONS
SPECIFICATIONS
SPECIFICATIONSSPECIFICATIONS
Range 0 to 50 mg/L (ppm) as K
50 to 250 mg/L (ppm) as K
Smallest Increment 5 mg/L [in the 0-50 mg/L range]
25 mg/L [in the 50-250 mg/L range] Analysis Method Turbidimetric Sample Size 3 mL and 0.6 mL Number of Tests 100 Case Dimensions 235x175x115 mm (9.2x6.9x4.5") Shipping Weight 889.0 g (31.3 oz.)
SIGNIFICANCE AND USESIGNIFICANCE AND USE
SIGNIFICANCE AND USE
SIGNIFICANCE AND USESIGNIFICANCE AND USE
Potassium is present in tissues responsible for the growth of plants (primary and secondary meristems). It plays an important role in how much water is absorbed by the roots and in the regulation of cellular activity. In addition, potassium makes plants more resistant to diseases and yields a positive effect on the color and fragrance in flowers.
The problem of lack of potassium is quite frequent in calcareous soils.
Note: mg/L is equivalent to ppm (parts per million).
CHEMICAL REACTIONCHEMICAL REACTION
CHEMICAL REACTION
CHEMICAL REACTIONCHEMICAL REACTION
The Hanna Test Kit determines Potassium in soil via a turbidimetric method. Potassium is precipitated in a basic environment with sodium tetraphenylborate. The developed turbidity is proportional to potassium concentration.
INSTRUCTIONSINSTRUCTIONS
INSTRUCTIONS
INSTRUCTIONSINSTRUCTIONS
READ THE ENTIRE INSTRUCTIONS BEFORE USING THE KIT 1- Obtain a Mehlich extract
from the soil sample by performing the Mehlich
extraction.
2- Using the syringe, add
3 mL of soil extract to the plastic vessel (a full syringe contains 1 mL of
ISTR38082 10/00 PRINTED IN ITALY
solution, hence repeat 3
3 mL
times). Add deionized water up to the 25 mL mark.
3- Add 18 drops of Formaldehyde
Solution and swirl to mix.
x18
4- Using the short plastic pipette, add 3 mL of HI 38082A-0
Alkaline Solution and swirl to mix.
3 mL
5- Add 1 packet of HI 38082B-0
reagent and mix by means of the spoon.
6- Wait for 5 min-
utes to allow reaction to com­plete. If Potassium is present, the solution will become tur­bid.
7- Place the test tube on the
Point card and look from the top of the tube at the black spot on the Point card. Use the long pipette to fill the tube with the reacted sample until the black spot completely disappears.
25 mL
8- Hold the tube close to the Graduated
card as shown in the figure.
9- Read directly from the Graduated card
the concentration in mg/L (ppm) of po­tassium that corresponds to the level of the liquid in the test tube.
10-In case the black spot on the Point
card disappears when the liquid level is under the 50 ppm mark, the potassium concentration is higher than 50 ppm. Dilute the original sample and perform the test as follows.
11 -Using the syringe, add to the plastic
vessel 0.6 mL of soil extract.
Note: To measure exactly 0.6 mL, take
the syringe and push the plunger completely down into the syringe. Insert tip into the extract and pull the plunger out until the lower edge of the seal is on the
0.0 mL mark of the syringe. Insert the syringe into the vessel and push the sample out until the lower edge of the seal is on the 0.6 mL mark.
0.6 mL
12- Add demineralized water up to
the 25 mL mark.
13-Follow the instructions from step
3 to step 8.
14- Read from the Graduated card the value corresponding
to the level of the liquid in the test tube and multiply it by 5 to obtain the concentration in mg/L (ppm) of potassium.
15- Rinse all labware with demineralized water after each
analysis and shake dry.
POTASSIUM CONVERSION TABLE mg/L lbs/A Kg/A meq/100g
10 20 22 0.026 15 30 33 0.038 20 40 45 0.051 25 50 56 0.064 30 60 67 0.076 35 70 78 0.090 40 80 89 0.100 45 90 100 0.120 50 100 112 0.130 75 150 167 0.190 100 200 223 0.260 125 250 279 0.320 150 300 334 0.380 175 350 390 0.450 200 400 446 0.510 225 450 502 0.580 250 500 558 0.640
Note: meq/100 g is milliequivalent per 100 grams.
REFERENCESREFERENCES
REFERENCES
REFERENCESREFERENCES
Adaptation of the Turbidimetric Tetraphenylborate Method.
HEALTH AND SAFETYHEALTH AND SAFETY
HEALTH AND SAFETY
HEALTH AND SAFETYHEALTH AND SAFETY
The chemicals contained in this kit may be hazardous if improperly handled. Read the relevant Health and Safety Data Sheet before performing this test.
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